Bring Down Costs Through,
Rice acco
GL eeeConrents.
Three Essential Phase
Separation Steps
Pall Liquid/Gas Coatescers
Comparison of Liquid/Gas
Separation Equipment
Pall Liquid/Liquid Coalescers
Comparison of Liquid Liquid
Separation Equipment...
Pal! Coalescer Configuration
Liquid/Gas & Liquid/Liquid
Application Tables
Pall Corporation
Customer Support
Pall Offices Worldwide
10-13,
4
Back
Cover
Pall Phase Separation Technology
For Control And Protection Of Your Plant
very year, refineries, gas processing plants and
petrochemical plants around the world spend millions
of dollars needlessly without realizing it. Maintenance
cycles are shorter than they should be; operating costs
are higher than ne
sary; and unscheduled shutdowns
causing lost production are all 10 common.
Fortunately, solutions are readily available from one
source: Pall Corpora
n, the world's leading filtration
and separations company.
Pall SepraSol” liquid/ga
coalescers, as well as AquaSep® Plus
and PhaseSep® liquid/liquid coalescers, give you far greater
coalescing efficiency, capacity and contaminant removal
than traditional coalescers or other conventional
separation techniques.
Pall Corporation is unique resource in phase separation
technology. Only Pall can help you achieve a higher
degree of product control and equipment protection
through teamworkThree Essential Phase Separation Steps to
Reduce Operating and Maintenance Costs
Our customers ben
ned in developing
filtration and separations
technology that has reduced costs
in hundreds of installations around
the world, There are three
essential steps to achieving cost
reductions in your plant.
from what
1. Preconditioning of the Fluid
Pall recommends a prefilter to
minimize solids in the coalescer
influent that can plug the
coalescer, reducing the overall life
and efficiency. The prefilter
provicles peak performance of the
coalescing system and a lower
total cost of ownership.
2. Coalescence of
the Dispersed Phase
Pall high-efficiency coalescers
menge small droplets of liquid into
langer ones as the fluid stream
passes through several layers of
filter media, each with progressively
larger pores. As droplets compete
for the open pores, they coalesce
forming larger droplets. These larger
droplets are easier to separate
from the continuous phase fluid.
‘The coalescer size and type are
«letermined by numerous factors
physical properties of the fluid,
flow rate, process conditions
and chemical compatibility with
process fluids and additives,
Pall has the expertise and
capability to determine the correct
ccoalescer size and type for y
specific process parameters.
ar
3. Separation of the
Dispersed Phase from
the Continuous Phase
Once large droplets are formed,
they have to be separated. In gas
systems, Pall spaces the cartridges to
control the exit velocity of the gas
so that coalesced droplets are not
entrained in this stream,
removed trom the fud stream are merged into larger Separation —
bythe ter mecium, ‘ones as they pass through
severe layers of iter ‘Separation: savy
fakes ofect, tho large
dioplets ae separates
fro the proc uid
In liquie/liquid systems, depending steam
on the liquid to be separated,
Pall will provide a separator
cartridge which has “repelling”
properties toward the coalesced
liquids. Alternatively, the assembly
can be designed to allow time for
the coalesced liquid to settle
When Pall works with you in all
three phase separation steps, you
see the difference in process
efficiency and reduced operating
and maintenance costs.a
0
Ofna
Pall SepraSol Coalescers For Separating
Liquids and Solids From Gases
Pall can eliminate a common
problem — poor liquid separation.
Is a problem that eats away at
profit margins,
quid aerosols,
which are dispersed in gases,
attack several critical areas of
your process: compressors and
turho-equipment, amine-glycol
contactors, burner and combustion
equipment, and desiccant
telltale symptoms are:
+ Compressor valves that
need changing out more
than once every two years
+ Turbo-equipment servicing
+ Plugging of reboiler heat exchang.
+ Frequent replacement
of amines and glycols
+ Frequent foaming
incidents
+ Loss of efficiency in
bumer and combustion
equipment
+ Frequent desiccant
regeneration or
‘The Efficient Way
to Remove Liquids
Liquid aerosols are formed by three
atomization and reentrainment from
upstream separation equipment
Condensation and atomization
almost always form very stable, fine
aerosols usually smaller than one
micron in diameter
Such aeros
removed by “knock-out drums,” mist
eliminators, vane packs or
conventional coalescers. If not
removed, these aerosols can damage
downstream equipme!
The solution is Pall’s patented
SepmiSol coalescers. They are rated
Up to 99.99% removal efficiency fc
solid particles 0,3 micron and larger
and reduce liquid content i
streams down fo 0.003 ppmw
No othComparison of Liquid/Gas
Separation Equipment
This chart compares the various equipment availabe for removing
aerosols. You can see that only Pall SepraSol coalescers effectively
remove aerosols smaller than one micron.
Pall Soprasol Mist Vane Cyclonic ———Knock-out
Liquid/Gas Eliminator Separator Separator. Drum
Coalescor
‘Smallest Liquid <04 c 300
Droplet Efficiently
Removed (Micron)
Relative Operating Medi Medium i
Pressure Drop
Sensitivity to Increased insenstive Very Ser Medium Mediu Medium
Liquid Loading
Sensitivity to Increased Some to None Very Sensitive Medium Medium Mec
Flow Rate
Sensitivity to Sensitve Sensi Medium Medium
‘Turn-Down'
3. Higher Liquid Capa 4. No Reentrainment of Liquids
By handling several times more The spacing of the cartridgy
liquid volume without liquid enables Pall SepraSol liquid/gas
entrainment in effluent gas, voallescets to control the exit
Pall coalescers reduce equipment velocity of the gas, allowing the
problems downstream, Fewer and coalesced drops to drain effectivelyPall AquaSep Plus and PhaseSep Coalescers
for Separating Liquids From Liquids
Tough beter usu Also, ol becomes dispersed
eee Separating these liquids can be
be diicuk,depending onthe
o-razy prot uot brig pial properties ofeach —
and clear) One of the most important peer eeeeee eee
abone pa Pe png oueaeln
of lagki“eg exvacion unis can bine a broad ange
gasoline, LPG or kerosene 0
* Camyover of amine in LPG The lower the interfacial tension, No-auttotant eit
* Oil and hydrocarbon in water and the more stable the emulsion
other aqueous streams and the more difficult the liquids
are to separate, Frequently, the
problem is the presence of a
surfactant which lowers interfacial
tension, Conventional coalescers
Degin to lose efficiency when
he interfacial tension is below 4
20 dyne/em. In addition, a small
amount of surfactant can
disarm conventional
Defining the Problems coalescers, rendering them
Liquid/liquiid dispersions or ineffective, Surfactants are
emulsions are often formed by everywhere: in corrosion
process operations such as liquid inhibitors, organic acids,
iquid extraction and water washing. well treating chemicals,
As liquid mixtures cool, the sulfur compounds and
solubility decreases numerous chemical
In the case of steam stripped additives, Pall AquaSep
nydrocarbons, for example Plus and PhaseSep
as the temperature decreases, coalescers separate
‘water comes out of solution liquids with interfacial
to form a second distinct liquid tensions as low as
phase, resulting in hazy product 0.5 dyne/em.Comparison of Liquid/Liquid
Separation Equipment
You can see from this table that Pall coalescers
separate liquids with interfacial tensions far lower
than any other means of separation.
Pall Salt and Conventional Mesh Pack Electrostatic Tank Setting Vacuum
‘AquaSep Plus/ Desiccant Goalescors Precipitator Dehydration
PhaseSep Tower Tower
System
Lowest AquaSep: <2 dynam >20 dyne/em >20 dyne/om >10 dynafcm >20 dyne/om <2 ay
Interfacial Tension 3 dyne/em
Efficiently PhaseSep:
Separated 05 dynefem
Relative Operating Low High Medum Low High Low High
‘and Maintenance
Costs
Effect of Additional Low High Low Low High low Medium
Dispersed Liquid
(on Operating Cost
Effect of Surface None None Reduces Reduces “Reduces. «Reduces. ~—=—«None
‘Active Chemicals ficiency Efciency —Efcioncy —_Eficienoy
on Efficiency
Effect of Additional Low Medium Low Medum = Medum Medium
Dispersed Liquid
on Etfciency
‘Sensitivity to Low Medum Low Low High Low Low
Temperature
Changes
Relative Low High Medium Low Hoh Low Medium
Maintenance
a's AquaSen Pius and PhaseSap
Auidnquic coalescers separate water
from hazy diesel et)
and ol from wastewater and
produced water, providing
Contaminant -Fee product.
dering Inform:
Open here for a Complete Selection Guide for Coalescer Part Number‘wo Configurations
for Optimum
Separation Efficiency
Pall Aquasep Plus and
PhaseSep system
available in a horizontal and a
vertical configuration, The
right one for you depends on
the liquids in your process
Both configurations begin with
a prefitration stage to remove
solid contaminants, This
signi
life, improves the fluid quality
and decres
liquieViquid emulsions,
making coalescing easier
are
santly extends service
the stability of
all's Patented Vertical
Coalescer/Separator Stack
This is the most efficient
technique for separating wo
liquids when the dispersed
fluid is water and the inter-
facial tension is greater than
3 dyne/em. The coalescer
clements are stacked on
top of a separator element
to ensure uniform flow
distribution from the
coalescer to the separator.
Loyewiouy Buvapic/SseqUN Led JeOS=ECD J0} BIND UOITES BieIAUED #10} 2164 UBIO
Pal AquaSep Pls and PhaseSap Stack Assembly
The assembly is smaller and
has a longer service life than
conventional coalescers. After
water droplets are coalesced
in Pall's proprietary media,
water-free liquid and large
droplets of water flow toward
the separator. The hydrophobic
separator medium repels the
aqueous pha
se, so only the
waterfiee bulk fluid passes
through the separator, The
two liquids are removed by
separate drain connections,
‘The Pall Horizontal
Coalescer
If the dispersed liquid phase
is not water, an AquaSep Plus
or PhaseSep coalescer without
a separator is placed in a
horizontal housing, It should
be used to separate oil from
fer, fWO NoN-aqueous
liquids or when the interfacial
tension of two liquids is less
than 3 dyne/em.
In this configuration, the
liquid/Liquid mixture enters
the coalescing element and
flows inside to out, Small
liquid contaminant droplets
coalesce into larger droplets
which are separated by
gravity and are removed,
Pall vertical iquidliquid coalescer
Configuration with prefiter onthe let
and fquaSep Plus/PhaseSep coalescer shown
fer night Mater exts bottom et, water-ree
procsct bottom grt.
Pall horizontal iquid/iquid coalescer
Conguration with proitr far ft
and AquaSep Plus/PhaseSep coalesce right.
Contaminant-ree contewous phase
‘ex top night, squid contamnant,
bottom nigh
SeparatorFortunately, For Each Problem, There Is A Solution:
Pall Seprasol Liquid/Gas Coalescers.
ad Se eC
eel en eR meg Teen et Lad
cio re eg
Cie
‘SepraSol Cree o o d ey
ra a eg eesti
Cec
ee
a
hi ee ccc ice ME gE et mee eres Cee ee rt
i ats ear en ee ea
fel 5% aromatics in liquid
Sone fee A tied ee ems
cas Ca ee
cece od ec
panos
rT}Equipment service life between maintenance shutdowns and plant
tumarounds is often shorter than it could be. And the causes of increased
maintenance and operating costs are not always obvious. These tables will
eee eet nn eae ae omc neta
applications, followed by brief summaries of the Pall liquid/gas and
Pretec nee eee eed Coreen eos
Inadequate Liquid Removal Can Create Costly Maintenance
ee ones
‘Application ‘Symptom Problem
Gas transmission compressors. Tin less than 2 years Gas throughput below design: fouling
and salting of compressor internal
Reciprocating hydrogen than 2 yi Gas throughput below design; fouling
compressors and salting of compressor internals,
|Amine or glycol contactors
foaming in contac
efciency; fouling of exchanger ar
1 the ine
urface tension of the
nd initiate foaming episod
Fuel gas burners an 1 year bet Burner nozzles plugged and frequently
(or flame patterns.
Desiccant or absorbent bed 3-year c ft n problems
[Compressor lube oil in refinery, 1p; fouling
}gas and chemical plants. sm equioment with lube oll
product (e.9.
JAmine from contactors i igher than design amine Ic
fouling of downstream equipment.
Gas separation membranes e memibrane seperation efficien
ice iteThe Solution is Advanced Technology:
Pall AquaSep Plus and PhaseSep Liquid/Liqt
| Poor Separation Can Damage Equipment and Reduce Product Quality
‘Symptom - Measured Problem
Interfacial Tension
[Separation of water from: 3-25 dy f-spec product. Presence
‘gasoline, jet fuel and diesel ant sting in the feedstack or added
on, increasing
[Separation of caustic from: 05-18 dyne/em
Jgasoline, jet fuel and diesel
| Separation of water from light 2 te isting in the fee
hydrocarbons (G, and below) educe interfacial tension,
and petrochemicals. a
Separation of amine from LPG N/A
28, Sufur compounds
on, making separation n
‘Separation of hydrogen peroxide
from working solution
‘Separation of acids from
[petrochemicals and hydrocarbons
to separate.
[Separation of oil fro Oil wil foul steam system and incr
* water vater treatment plant.
+ anhydrous ammoni Off-spec anhydrous ammonia.
Palll Liquid/Liquid Coalscer
Perereaketit
Tete Ream eet mee gC
the Correct Product and Configuration for Your Process.
Recommended Product
[Contaminating uid is aque
IFT >3 dyne/cm
[Contaminating fluid is aqueous, Aa alescer
jousing)
Both fluids are non-aqueo ‘AquaSep Pius or PhaseSep cosiescer
ithout separator (Horizontal Housing)
yntaminating fluid is ol AguaSep Plus or Phast
vthout separator (Hi
7Coalescers.
Ce ed Sey Peed
Pence eer nM a ee
oe 1 A Rr ue
a ee
Integral Prefiter
CR en ue
Coalescer iro OC ee eu ees
Bee a
peroxide from working,
ete
er See eae
foe et OAT ee Coes
ee a
Ee) Ca me esd Separation of water
3.75°795 mm diam, medium does not Cen ieee
peoa
Cay
13Pall Corporation
A Powerful Resource for Control,
Protection and TeamworkPall Corporation
£2200 Northern Boulevard
East Hils, New York 11548-1269
888.873.7255 toll ree
‘516.484 5400 phone
516.<84, 0964 fax
Fitration. Separation. Solution.
Visit us on the Web at www.pall.com
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