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IS : 147 - 1950

(Reaffirmed 1999)
Edition 1.2
(1988-10)

Indian Standard
SPECIFICATION FOR READY MIXED PAINT,
SLUSHING, PETROL RESISTING, STOVING,
FOR INTERIOR PAINTING OF TANKS
AND CONTAINERS, RED OXIDE
(COLOUR UNSPECIFIED)
(Incorporating Amendment Nos. 1 & 2)

UDC 667.624.69 : 621.798.148 (083.75) (54)

Paints and Allied Products Sectional Committee, CDC 8


Chairman Representing
MR P. C. CHANDA Indian Paint Manufacturers’ Association, Calcutta
Members
MR R. G. BHATAWADEKAR Central Standards Office for Railways, New Delhi
MR S. RAMANUJAM Alternative
MR B. B. CHAUDHURI Inspectorate of Military Explosives, Kirkee
THE DIRECTOR Government Test House, Calcutta
MR C. J. FIELDER Shalimar Paint, Colour & Varnish Co Ltd, Calcutta
MR EMIL FJERMEROS Ganges Printing Ink Factory Ltd, Calcutta
MR MAGNE HJELDE Alternative
MR B. N. GANGULI Technical Development Establishment Laboratory
(Stores), Kanpur
MR A. N. KAPOOR Indian Red Lead Factory Ltd, Calcutta
MR K. C. MUKHERJEE Paint Federation, Calcutta
MR S. V. SATHAYE Alternative
MR P. W. PARISH D. Waldie & Co Ltd, Calcutta
MR R. B. SEYMOUR Alternative
MR N. SRINIVASAN Directorate General of Industries and Supplies, New Delhi
MR F. W. VIOL Imperial Chemical Industries (India) Ltd, Bombay
Staff
DR K. L. MOUDGILL Indian Standards Institution, Delhi
Drafting Subcommittee for Paints and Allied Products, CDC 8 : 1
Convener
DR K. L. MOUDGILL Indian Standards Institution, Delhi
Members
THE DIRECTOR Government Test House, Calcutta
MR B. N. GANGULI Technical Development Establishment Laboratory
(Stores), Kanpur
DR A. KARIM Solar Paint & Varnish Manufacturing Co, Calcutta
MR S. V. SATHAYE Goodlass Wall Ltd, Bombay

© BIS 2002

BUREAU OF INDIAN STANDARDS


MANAK BHAVAN , 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI 110002

Price Group 2
IS : 147 - 1950

Indian Standard
SPECIFICATION FOR READY MIXED PAINT,
SLUSHING, PETROL RESISTING, STOVING,
FOR INTERIOR PAINTING OF TANKS
AND CONTAINERS, RED OXIDE
(COLOUR UNSPECIFIED)
FOREWORD
This Indian Standard was adopted by the Ordnance Branch, which was set up in 1942
Indian Standards Institution on and continued to function till 1947. In drafting
7 September 1950 on the endorsement by the this standard, British standards and the
Chemical Division Council of the draft finalized standards of the American Society for Testing
on 8 June 1950 by the Paints and Allied Materials on the subject have been drawn upon
Products Sectional Committee. It is based freely, and the assistance so derived is
largely on the interim co-ordinated draft acknowledged.
produced with the assistance of the
representatives of manufacturers and of The Indian Standard Methods of Test for Ready
various departments and authorities of the Mixed Paints and Enamels (IS : 101-1950) is a
necessary adjunct to this standard.
Government of India, by the Co-ordinating
Subcommittee of the No. 5 Standing Committee This edition 1.2 incorporates Amendment No. 2
on Specifications for Paints and Allied Stores of (October 1988). Side bar indicates modification
the General Headquarters, India (now Army of the text as the result of incorporation of the
Headquarters), Master General of the amendment.

1. SCOPE 3.2 The purchaser may select, as approved


sample, the sample submitted by the vendor, or
1.1 This standard prescribes the requirements any other agreed sample. He shall return to the
and the methods of test for the material vendor one suitably sealed container of the
commercially known as Ready Mixed Paint, approved sample.
Slushing, Petrol Resisting, Stoving, for Interior
Painting of Tanks and Containers, Red Oxide 3.3 Representative samples of the material
(colour unspecified). The material is used for shall be drawn as prescribed under 3 of
the interior protection of small petrol tanks and IS : 101-1950.
containers and is such that on stoving it gives a
4. REQUIREMENTS
film which is petrol resisting and does not
increase “gumming” of petrol. 4.1 Composition — The material shall be of
such a composition as to satisfy the
1.2 This standard is intended chiefly to cover
the technical provisions relating to the requirements of this standard.
purchase of the material, but it does not include 4.1.1 Clause deleted
all the necessary provisions of a contract.
4.2 Freedom from Copper — The material
2. TERMINOLOGY shall be free from copper and compounds of
copper.
2.1 For the purposes of this standard, the
definitions given under 2 of IS : 101-1950 shall 4.3 Resistance to Fuel for Aeroengines and
apply. Effect on Fuel
4.3.1 When the test drum treated with the
3. SAMPLE material is tested as described in Appendix A,
3.1 The vendor shall submit a tender sample the paint film shall show no surface defects.
packed in three different containers, each 4.3.2 The fuel for aeroengines, stored as described
containing not less than 500 g of the material. in Appendix A and tested as described in
2
IS : 147 - 1950

Appendix B, shall not show an increase in


TABLE I REQUIREMENTS FOR READY MIXED
existent gum by more than 10 mg per 100 ml of PAINT, SLUSHING, PETROL RESISTING,
fuel. STOVING, FOR INTERIOR PAINTING OF
TANKS AND CONTAINERS, RED OXIDE
4.4 The material shall also conform to the (COLOUR UNSPECIFIED) — Contd
requirements in Table I. ( Clause 4.4 )
5. TESTS SERIAL CHARACTERISTIC REQUIREMENT REFERENCE
NUMBER TO
5.1 Unless specified otherwise, tests shall be IS:101-1950
conducted as prescribed in IS : 101-1950. (1) (2) (3) (4)
References to the relevant clauses of that
standard are given in column (4) in Table I. iii) *Finish Smooth 7.5
iv) Covering power Not less than 90 2.1.11 & 8
5.2 The tests marked with an asterisk shall be percent of the
carried out on stoved films after keeping for 24 approved
hours at room temperature. sample
v) Opacity Not less than 90 2.1.13 &
5.2.1 Unless otherwise agreed between the percent of the 10
purchaser and the vendor, the stoving approved
temperature and time shall be 150°C and 30 sample
minutes for dark colours, and 93°C and 1 hour vi) Colour Close match to 11
for pale and light colours. the approved
sample
TABLE I REQUIREMENTS FOR READY MIXED vii) Residue on Not more than 13
PAINT, SLUSHING, PETROL RESISTING, sieve 0.3 percent
STOVING, FOR INTERIOR PAINTING OF viii) *Scratch No such scratch 15.1
TANKS AND CONTAINERS, RED OXIDE hardness as to show the
(COLOUR UNSPECIFIED) bare metal
( Clause 4.4 ) ix) *Flexibility and No visible 16
SERIAL CHARACTERISTIC REQUIREMENT REFERENCE adhesion damage or
NUMBER TO detachment of
IS:101-1950 film
x) Protection No signs of 18
(1) (2) (3) (4) against break-down or
corrosion corrosion
i) Consistency Smooth and 7.4
uniform xi) Weight in kg/10 Within 3 percent 2.1.14 &
litres of the approved 25
ii) *Drying time: sample
Hard dry Dark colours 2.1.9, 7.1, xii) Keeping Not less than one 31
stoved at 7.2 & properties year from the
150°C, not 7.3.2 date of
more than ½ manufacture
hour; light and xiii) Marking and As agreed with 32
pale colours delivery the purchaser
stoved at 93°C,
not more than *These tests shall be carried out on stoved films after
1 hour keeping for 24 hours at room temperature.

APPENDIX A
( Clause 4.3.1 )

DETERMINATION OF RESISTANCE TO AEROENGINE FUEL AND EFFECT ON FUEL

1. PREPARATION OF THE CONTAINER 2. PROCEDURE


1.1 Flush with the paint a cylindrical, pickled, 2.1 Store 200 ml of fuel for aeroengines in the
cold-rolled, close annealed, mild steel plate container and keep the container at room
container, 2.5 in. (or 60 mm) diameter and 3 in. temperature. After one month, examine the
(or 75 mm) high, provided with a well fitting lid paint film for blistering, cracking or any other
and allow the excess to drain off. Allow the surface defect.
container to dry for a period of seven days at 2.1.1 Reserve the aeroengine fuel for test as
room temperature. described in Appendix B.
3
IS : 147 - 1950
APPENDIX B
( Clause 4.3.2 )

DETERMINATION OF THE EXISTENT GUM

1. APPARATUS 2.2 Disconnect the flask from the distillation


head and pour the contents into one of the
1.1 The following apparatus is required: dishes which has been heated previously in
a) Flask — round-bottomed, of about 250 ml steam oven, cooled in dust-free atmosphere
total capacity with ground joint. for 15 to 20 minutes and weighed to an
Alternatively, a distillation flask may be accuracy of ± 0.2 mg on a balance shielded from
used, direct sunlight. Allow the flask to drain into the
b) Distillation head — with a ground joint to dish in an inverted vertical position
fit the flask, for 15 seconds. Place the dish at once on a
c) Condenser — Liebig type, with a bent end vigorously boiling water bath and allow it to
which does not hold water when remain supported in a hole having a diameter
assembled, of 64 ± 1 mm and protected from dust, for one
and a half hours.
d) Graduated receiver — of 100 ml capacity,
e) Dishes — hemispherical in shape, without 2.2.1 In the case of fuels distilling less than 50
lip, 66.5 ± 2 mm in external diameter, percent at 100°C and less than 95 percent
and 18 ± 3 g in weight. at 145°C, continue the evaporation on the
water bath, if necessary, for a longer period
1.2 The flask, distillation head, condenser, than one and a half hours, and until
receiver and dishes shall be made entirely of evaporation is complete.
Pyrex or Hysil or Monax or Geraote-20 glass.
2.3 After evaporating on the water bath
2. PROCEDURE transfer the dish to a water or steam oven and
2.1 Measure 100 ml of the aeroengine fuel, allow it to remain at a temperature
stored as described in Appendix A, into the of 100° ± 2°C for one hour. Allow the dish to
flask and connect it to the distillation head. cool for 15 to 20 minutes in a dust-free
Place the flask on an asbestos sheet, 150 mm in atmosphere and weigh to an accuracy
diameter and having a central hole 40 mm in of ± 0.2 mg.
diameter. Pass the delivery end of the 2.4 Repeat the test with aeroengine fuel
condenser through a two-hole cork inserted in without storing it in the prepared container
the 100 ml graduated receiver. Provide the cork and treat the result as a blank.
with another tube through which the gases and
uncondensed vapours evolved during the
distillation can be led away from any source of 3. CALCULATION
ignition. Bring the contents of the flask
cautiously to boiling over a boiling water bath 3.1 Express the residue on evaporation as
or a hot plate or a Bunsen flame, avoiding any milligrams of residue per 100 ml of the fuel.
sudden evolution of vapour. Distil at the rate
3.2 The prescribed limit for increase in existent
of 4 to 5 ml per minute or about two drops per
gum shall be taken as not having been
second until 75 ml of distillate are collected in
exceeded if the difference in weight, if any, of
the graduated receiver.
the residue on evaporation in the test and the
2.1.1 For referee tests a Bunsen flame shall be blank is not more than 10 mg per 100 ml of the
used. fuel.

4
Bureau of Indian Standards
BIS is a statutory institution established under the Bureau of Indian Standards Act, 1986 to promote
harmonious development of the activities of standardization, marking and quality certification of goods and
attending to connected matters in the country.

Copyright
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without the prior permission in writing of BIS. This does not preclude the free use, in the course of
implementing the standard, of necessary details, such as symbols and sizes, type or grade designations.
Enquiries relating to copyright be addressed to the Director (Publications), BIS.

Review of Indian Standards


Amendments are issued to standards as the need arises on the basis of comments. Standards are also
reviewed periodically; a standard along with amendments is reaffirmed when such review indicates that no
changes are needed; if the review indicates that changes are needed, it is taken up for revision. Users of
Indian Standards should ascertain that they are in possession of the latest amendments or edition by
referring to the latest issue of ‘BIS Catalogue’ and ‘Standards : Monthly Additions’.
This Indian Standard has been developed from Doc : No. CDC 8

Amendments Issued Since Publication


Amend No. Date of Issue
Amd. No. 1 Incorporated earlier
Amd. No. 2 October 1988

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