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International Journal of Impact Engineering 83 (2015) 76e87

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International Journal of Impact Engineering


journal homepage: www.elsevier.com/locate/ijimpeng

Impact resistance of concrete containing waste rubber fiber and silica


fume
Trilok Gupta a, Ravi K. Sharma a, Sandeep Chaudhary b, *
a
Department of Civil Engineering, College of Technology and Engineering, MPUAT, Udaipur, India
b
Department of Civil Engineering, Malaviya National Institute of Technology Jaipur, Jaipur 302017, India

a r t i c l e i n f o a b s t r a c t

Article history: High impact resistance and greater energy absorption capacity are desirable properties for concrete.
Received 11 February 2015 Innovative and sustainable materials may be used to improve these properties. In the present study, the
Received in revised form effect of replacement of fine aggregates by waste rubber fibers on the impact resistance of concrete has
29 April 2015
been assessed. Silica fume has also been considered as replacement of cement. Six replacement levels of
Accepted 2 May 2015
Available online 12 May 2015
rubber fiber (0%, 5%, 10%, 15%, 20% and 25%) and three replacement levels of silica fume (0%, 5% and 10%)
have been considered for three different water cement ratios. Impact tests on concrete have been con-
ducted by three different techniques; drop weight test, flexural loading test and rebound test. Re-
Keywords:
Waste rubber fiber concrete
lationships between impact test results of drop weight test, flexural loading test and rebound test have
Silica fume also been established. In view of large variation of impact values, a two-parameter Weibull distribution is
Impact resistance adopted to analyze the experimental data of drop weight test. The study demonstrates that the waste
Energy absorption capacity rubber fiber can be used as a sustainable material to improve the impact resistance and ductility of
Weibull distribution concrete. The study also demonstrates that the silica fume improves the impact resistance and reduces
the ductility of rubber fiber concrete.
© 2015 Elsevier Ltd. All rights reserved.

1. Introduction Studies have also been carried out for the impact resistance or
energy absorption capacity of fibrous concrete containing silica
Concrete is a brittle material with high rigidity. High impact fume [15e17]. Nili et al. [15] reported that the impact energy in-
resistance and more energy absorption capacity are required in creases on partial replacement of cement by silica fume and addi-
many applications such as shock absorbers, foundation pads of tion of steel fibers. Yan et al. [16] reported that the addition of steel
machinery, railway buffers etc. Additional ingredients are required fibers and partial replacement of cement by silica fume in concrete
to improve the properties of concrete in some situations where effectively reduces the number and size of cracks, and enhances the
these requirements are not fulfilled. performance of high strength concrete under impact and fatigue
Many studies have been carried out for evaluating the impact loads. Nili et al. [17] reported that the silica fume improves the
resistance and energy absorption capacity on fibrous concrete impact resistance of concrete containing polypropylene fibers by
[1e14]. The impact resistance of concrete has been found to in- facilitating dispersion of fibers.
crease up to fifteen times on using steel fibers [5e10] and up to ten Accumulation of discarded rubber tyres is a major problem as its
times on using polypropylene fibers [11,12]. The addition of natural degradation is very difficult because of the highly complex
fibers in the form of coir, sisal, jute, and hibiscus cannabinus has configuration of ingredient materials. The available studies
also been found to increase the impact resistance of concrete by up regarding utilization of waste rubber tyres in concrete provide a
to eighteen times [13]. Rao et al. [14] studied the behavior of slurry- strong recommendation for the use of this waste as a partial
infiltrated concrete slabs, containing steel fibers, under impact replacement of fine aggregate in concrete production [18]. This
loading and reported an increase in energy absorption of concrete would facilitate effective use of the solid waste, minimize its
with the increase of fiber volume. accumulation and help in reducing the consumption of natural
resources.
Some studies have been carried out on the impact resistance of
* Corresponding author. Tel.: þ91 94144 75375. concrete. Topcu [19] reported a decrease in elastic energy capacity
E-mail address: sandeep.nitjaipur@gmail.com (S. Chaudhary).

http://dx.doi.org/10.1016/j.ijimpeng.2015.05.002
0734-743X/© 2015 Elsevier Ltd. All rights reserved.
T. Gupta et al. / International Journal of Impact Engineering 83 (2015) 76e87 77

Table 1
Chemical composition of cement and silica fume.

Element/Material CaO (%) SiO2 (%) Al2O3 (%) Fe2O3 (%) SO3 (%) MgO (%) K2O (%) LOI (%)

Cement 62.34 20.14 4.65 3.29 2.42 2.23 0.72 1.96


Silica Fume 0.87 90.12 0.94 1.62 0.29 e 1.21 2.87

and increase in plastic energy capacity of the concrete on replace- Rubber fibers, obtained from mechanical grinding of waste
ment of coarse aggregates and fine aggregate by coarse rubber rubber tyres, were used as partial replacement of fine aggregates.
chips and fine rubber chips respectively. Khaloo et al. [20] carried These rubber fibers were of 2e5 mm in width and up to 20 mm in
out a study on concrete containing high volume chip rubber as length (aspect ratio 4e10) with a specific gravity of 1.07. As the
partial replacement of coarse aggregate and crumb rubber as par- rubber fibers are obtained from a waste product of used rubber
tial replacement of fine aggregate. The toughness was reported to tyres, detailed microstructural characteristics are necessary to be
be highest for 25% concentration of both the types of rubber par- ascertained to ensure the compatibility of this material with the
ticles as a part of the total aggregate volume. Sukontasukkul et al. concrete. Scanning electron microscope (SEM) was used for this
[21] carried out flexural test and reported an increase in toughness purpose.
of concrete blocks on partial replacement of 10% of fine aggregate SEM images of a rubber fiber are shown in Fig. 1(a) and (b). A
and 20% of coarse aggregate by crumb rubber. Aiello and Leuzzi [22] large cavity was observed in the rubber fiber which acts as large
also carried out flexural tests and reported a significant increase in pore in the concrete and influences its properties. Micro cracks
the energy absorption for up to 75% replacements of coarse/fine within the rubber fibers were also visible (Fig. 1(a) and (b)) and
aggregate by rubber shreds. Ozbay et al. [23] carried out rebound these cracks indicate a weak interfacial bonding between the rub-
tests and reported about 25% increase in energy absorption ca- ber fibers and cement paste which affected the strength of rubber
pacity of concrete on 25% replacement of fine aggregate by crumb fiber concrete.
rubber. Al-Tayeb et al. [24] substituted up to 25% of fine aggregate
by waste crumb rubber and tested the concrete under impact three 2.2. Mix proportions
point bending load. They reported an improvement in impact load
behaviour with the increase in replacement level of fine aggregates. Concrete mixes were prepared using water/cement ratios of
It is evident from the work reported above that although a 0.35, 0.45 and 0.55 with a partial replacement of fine aggregate (FA)
number of studies have been undertaken for the impact resistance by rubber fibers ranging from 0% to 25%. Concrete mixes were also
of rubberised concrete; none of the studies has considered waste cast by replacing cement with silica fume, ranging from 0% to 10% in
rubber in the form of fibers. Therefore, there is a need to carry out the control concrete as well as rubber fiber concrete. Concrete
systematic experimental studies to evaluate the impact resistance mixes were first dry-mixed for 2e3 min in the mixer. To maintain
of concrete incorporating rubber fibers (with and without silica the workability and the uniformity of the mixes, the proportion of
fume), as partial replacement of fine aggregate, for varying w/c super-plasticizer (SP) with that of cement by weight was varied.
ratios. When the concrete mix showed the desired workability and uni-
In the present work, detailed experimental studies have been form rubber fiber distribution, it was placed in a mould and
carried out to determine the impact resistance of concrete con- vibrated on a table vibrator. The specimen were covered with
taining waste rubber fibers. The studies have been undertaken for plastic sheets and stored at room temperature for 24 h prior to de-
varying percentage of waste rubber fibers (0%, 5%, 10%, 15%, 20% and moulding. The details of concrete mix with the observed work-
25%) as partial replacement of fine aggregates at three different w/c ability in terms of compaction factor (C.F.) are shown in Table 2.
ratios (0.35, 0.45 and 0.55). Three replacement levels of silica fume
(0%, 5% and 10%) have been considered for partial replacement of 3. Testing program
cement in the rubber fiber concrete. Impact resistance has been
evaluated by carrying out drop weight test (concrete cylinder In this experimental study, following properties of hardened
subjected to impact), flexural loading test (concrete beam subjected concrete were evaluated as per the relevant standards.
to impact) and rebound test (concrete cube subjected to impact).
Relationships between results of drop weight test, flexural loading
3.1. Compressive strength
test and rebound test have also been established. The experimental
results obtained from various techniques have been analyzed by
The mechanical strength of rubber fiber concrete with and
statistical approaches to account for the variability in the properties
without silica fume was measured by conducting compression
of concrete.
strength test. This test was performed on 100 mm concrete cubes
(three for each mix) at 28 days as per BIS Committee BDC 2 [25].
2. Experimental studies Load was applied gradually with the rate of travel of machine
equivalent to 240 ± 35 kN/m2/s [25].
2.1. Material
3.2. Impact resistance under drop weight test
Ordinary Portland cement of specific gravity 3.12 and silica fume
of specific gravity 2.18 were used for the concrete mixes in this Drop weight test was performed on cylindrical specimens
study. The chemical compositions of cement and silica fume are (150 mm in diameter and 65 mm in height, three specimens for
shown in Table 1. Fine aggregate (natural sand) of specific gravity each mix) as per ACI Committee 544 [26] to estimate the energy
2.56 and coarse aggregate (crushed gravel) of maximum size of absorption capacity of concrete specimens. In this test, repeated
12 mm and of specific gravity 2.59 were used in the concrete mixes. loading was applied on the specimen from a height. The number of
Super plasticizer (SP) “Glanium Sky 777” from BASF was used as an blows was obtained for the prescribed level of distress (occurrence
admixture to obtain the desired workability. of first crack and failure cracks).
78 T. Gupta et al. / International Journal of Impact Engineering 83 (2015) 76e87

Fig. 1. SEM image of rubber fiber at (a) 40x magnification; and (b) 150x magnification.

Table 2
Concrete mix proportions of rubber fiber concrete with and without silica fume.

Mix Cement (kg) Silica fume (kg) Fine aggregates (kg) Coarse aggregates Rubber fibers (kg) Water (kg) Super plasticizer (%) C.F.
(kg)

10 mm 20 mm

R1-R6 364 0 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64,80 127.4 2.1% 0.91
R7-R12 364 0 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64,80 163.8 0.5% 0.92
R13-18 364 0 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64,80 200.2 0% 0.92
U1eU6 345.8 18.2 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64, 80 127.4 2.1% 0.92
U7eU12 345.8 18.2 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64, 80 163.8 0.5% 0.92
U13eU18 345.8 18.2 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64, 80 200.2 0% 0.92
V1eV6 327.6 36.4 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64, 80 127.4 2.1% 0.92
V7eV12 327.6 36.4 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64, 80 163.8 0.5% 0.92
V13eV18 327.6 36.4 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64, 80 200.2 0% 0.92

Specimens of 28 days age were tested by the drop weight impact Similarly, the impact energy at ultimate crack, Ep,dwu was
testing machine fabricated in the laboratory as per guidelines of ACI calculated by the equation given below:
committee 544 [26]. The machine consists of a 4.5 kg hammer ball
dropping from 450 mm height on a hardened steel ball of 65 mm Ep;dwu ¼ N2 mgh (2)
diameter (Fig. 2(a)). The steel ball was placed at the centre of
specimen and this specimen was placed on the base plate within where, N1 and N2 are the number of blows at initial and ultimate
the positioning lugs as shown in Fig. 2(a). The hammer ball was crack level, m is the mass of drop hammer (4.5 kg), g is acceleration
dropped repeatedly and the number of blows (N1) required to cause due to gravity (9.81 m/s2) and h is the releasing height of drop
the first visible crack on the top was recorded. Number of blows hammer (450 mm).
(N2) which caused opening of cracks in such a way that the concrete
pieces started touching side lugs was also recorded. The values of 3.3. Impact resistance under flexural loading
N1 and N2 were designated as initial crack resistance factor and
ultimate crack resistance factor respectively. Impact test on the beams was performed to determine the po-
The impact energy at initial crack, Ep,dwi (where first subscript p tential energy of rubber fiber concrete (Fig. 2(b)). In this test, beams
denotes the type of energy absorbed i.e. potential energy and sec- of 100 mm  100 mm  500 mm size (three specimens for each
ond subscript dw denotes the type of test i.e. drop weight) was mix) were tested with a center to center span of 400 mm. A
calculated by the equation given below: hammer of 1.0 kg weight was dropped on the mid span of the beam
from a height of 450 mm. Number of drops up to failure, Nf was
Ep;dwi ¼ N1 mgh (1) measured and energy absorbed by the specimen, Ep,fl (subscript fl
denotes flexural loading) was calculated by the following equation:

Fig. 2. (a) Drop weight test; (b) Flexural loading test; and (c) Rebound test.
T. Gupta et al. / International Journal of Impact Engineering 83 (2015) 76e87 79

X
Nf
Ep;fl ¼ mi ghi (3)
i¼1

where, mi is the mass of drop hammer (1.0 kg) and hi is the drop
height (450 mm).

3.4. Impact resistance under rebound test

Rebound test was performed on cubes of 150 mm size to


determine the impact resistance of waste rubber fiber concrete (Fig
2(c)). A steel ball of 0.5 kg weight was dropped on to the specimens
(three for each mix) from a standard height of 1.0 m. The rebound
height of steel ball was recorded by a sensitive camera. Initial po-
tential energy before rebound, Ep,ri and final potential energy after
rebound,Ep,rf were calculated using following equations:

Ep;ri ¼ mghi (4)

Ep;rf ¼ mghf (5)

where m is mass of steel ball (0.5 kg), hi is the initial height of steel
ball (1.0 m) and hf is height recorded after rebound (varies for
different mixes).
The energy absorption capacity of concrete specimen, Ep,r was
calculated as the difference of the final and initial potential energy
(Ep,r¼Ep,riEp,rf). Loss due to air resistance was ignored.

3.5. Micro-structural analysis

The microstructure of the specimen was analyzed using Scan-


ning Electron Microscope (ZEISS make) at EHT 20 kV. Testing was
performed on 1 cm  1 cm pieces cut from concrete samples. A gold
coating was applied to the surface before carrying out the analysis.

4. Results and discussion


Fig. 3. 28 days compressive strength of rubber fiber concrete for (a) 0.35 w/c ratio; (b)
4.1. Compressive strength 0.45 w/c ratio; and (c) 0.55 w/c ratio.

Three specimens were tested for compressive strength for each


type of mix [25]. The results presented in the study are the average
of these three values in Table 3. The compressive strength of the

Table 3
28 days compressive strength of rubber fiber concrete.

0% silica fume 5% silica fume 10% silica fume

Mix Mean (N/mm2) SD COV (%) Mix Mean (N/mm2) SD COV (%) Mix Mean (N/mm2) SD COV (%)

R1 58.97 1.13 2.06 U1 67.2 0.56 0.82 V1 75.2 0.67 0.87


R2 48.37 1.05 2.3 U2 56.1 0.21 0.38 V2 64.5 1.00 1.56
R3 45.50 1.00 2.27 U3 52.3 0.50 0.95 V3 59.6 1.01 1.71
R4 38.47 1.05 2.36 U4 45.4 1.01 2.21 V4 53.1 1.00 1.89
R5 34.73 1.00 2.85 U5 40.3 0.66 1.58 V5 46.7 0.52 1.1
R6 28.43 0.56 1.75 U6 33.3 0.55 1.61 V6 37.9 0.59 1.51
R7 50.43 1.01 2.1 U7 56.5 0.54 0.94 V7 62.7 1.52 2.46
R8 39.03 0.5 1.33 U8 44.5 1.11 2.4 V8 50.7 1.05 2.12
R9 35.87 1.61 4.41 U9 40.8 0.52 1.26 V9 45.7 1.54 3.28
R10 30.73 0.25 0.8 U10 35.3 0.79 2.11 V10 39.2 1.52 3.79
R11 26.93 1.01 3.45 U11 30.4 1.01 3.28 V11 33.1 0.82 2.32
R12 23.60 0.53 1.91 U12 26.9 0.51 1.87 V12 29.9 0.71 2.24
R13 33.70 0.51 1.51 U13 37.1 0.51 1.36 V13 39.7 0.61 1.49
R14 27.23 0.5 1.33 U14 30.5 0.50 1.64 V14 33.6 0.75 2.11
R15 24.97 0.07 0.23 U15 27.7 0.52 1.84 V15 29.4 1.05 3.45
R16 20.13 1.00 3.58 U16 22.5 0.54 2.33 V16 24.5 0.63 2.44
R17 17.10 0.12 0.55 U17 19.1 0.51 2.63 V17 20.1 0.57 2.71
R18 15.30 0.50 2.34 U18 17.4 0.79 4.32 V18 19.1 0.57 2.85

SD ¼ Standard deviation; COV ¼ coefficient of variation.


80 T. Gupta et al. / International Journal of Impact Engineering 83 (2015) 76e87

Table 4
Impact resistance results for rubber fiber concrete without silica fume.

Mix N1 N2 N2eN1 Impact energy (J) N2/N1

Mean SD COV (%) Mean SD COV (%) First crack Ultimate failure

R1 58 5.29 10.17 65 3.61 5.23 7 1152 1291 1.12


R2 82 9.64 13.58 95 2.65 2.82 13 1629 1887 1.16
R3 106 6.93 6.79 124 7.00 5.88 18 2106 2463 1.17
R4 198 9.64 5.16 219 23.39 9.51 21 3933 4350 1.11
R5 242 6.08 2.47 278 7.81 2.90 36 4807 5523 1.15
R6 302 24.33 8.88 349 4.00 1.13 47 5999 6933 1.16
R7 47 1.73 3.53 53 2.00 3.64 6 934 1053 1.13
R8 69 6.08 9.81 78 5.29 7.35 9 1371 1549 1.13
R9 87 9.54 12.55 102 7.81 8.40 15 1728 2026 1.17
R10 145 11.53 8.73 167 10.82 6.98 22 2880 3317 1.15
R11 197 8.66 4.63 221 16.64 6.93 24 3913 4390 1.12
R12 214 4.36 2.09 246 2.65 1.09 32 4251 4887 1.15
R13 39 3.61 9.03 44 2.65 6.46 5 775 874 1.13
R14 48 3.61 7.68 56 5.29 10.17 8 954 1112 1.17
R15 65 1.73 2.75 76 2.65 3.63 11 1291 1510 1.17
R16 89 9.64 12.36 106 7.94 8.19 17 1768 2106 1.19
R17 118 4.58 3.75 144 6.24 4.55 26 2344 2861 1.22
R18 189 3.61 1.95 224 2.65 1.20 35 3755 4450 1.19

SD ¼ Standard deviation; COV ¼ coefficient of variation.

waste rubber fiber concrete for w/c ratios of 0.35, 0.45 and 0.55 at Table 4 for concrete without silica fume. The values of N1 and N2 for
28 days, is shown in Fig. 3(a), (b) and (c) respectively. It can be seen all three water cement ratios, increase by about five times on
that the compressive strength decreases with an increase in the incorporation of 25% rubber fiber for both 5% silica fume concrete
replacement level of rubber fibers for all three w/c ratios. The and 10% silica fume concrete.
compressive strength of control concrete (without rubber fiber and In general, it can be concluded that the impact resistance, for
silica fume) decreases from 58.97 N/mm2 to 28.43 N/mm2, 50.43 N/ first crack as well as for ultimate failure, increases with the increase
mm2 to 23.60 N/mm2 and 33.70 N/mm2 to 15.30 N/mm2 for w/c in rubber fiber content. Similar observations were made by
ratios of 0.35, 0.45 and 0.55 respectively, on 25% replacement of Mohammadi et al. [12] for steel fibers and the increase in impact
sand by rubber fiber. energy was attributed to long fibers which are expected to arrest
It is also observed from Fig. 3(a), (b) and (c) that on replacement the cracks due to their superior bond resistance. As the replace-
of cement by silica fume, the compressive strength increases for ment level of rubber fibers will increase, rubber-cement composite
control concrete as well as for the rubber fiber concrete. will have higher flexibility and this increase in flexibility level will
Compressive strength of control concrete (without rubber fiber and lead to more energy absorption as compared to the control mix.
silica fume) increases from 58.97 N/mm2 to 75.20 N/mm2, 50.43 N/ Tables 4e6 reveal that although the impact energy is enhanced
mm2 to 62.70 N/mm2 and 33.70 N/mm2 to 39.70 N/mm2 for w/c by silica fume, however, no definite pattern is observed for effect of
ratios of 0.35, 0.45 and 0.55 respectively on 10% replacement of silica fume on N2eN1.
cement by silica fume. Compressive strength of rubber fiber con- The number of blows required for the first crack in concrete, for
crete (25% rubber fiber) increases from 28.43 N/mm2 to 37.90 N/ three different w/c ratios, is shown in Fig. 4. It can be observed that
mm2, 23.60 N/mm2 to 29.90 N/mm2 and 15.30 N/mm2 to 19.10 N/ the number of blows is more for the rubberized concrete as
mm2 for w/c ratios of 0.35, 0.45 and 0.55 respectively, on 10% compared to the corresponding case of non rubberized concrete.
replacement of cement by silica fume. The fracture pattern of cylindrical specimen for control concrete
and rubber fiber concrete (25% rubber fibers) without silica fume is
4.2. Impact resistance under drop weight test shown in Fig. 5(a) and (b) respectively. It may be noted that there
may be some deviation in the results as the surfaces of the spec-
The impact resistance of rubber fiber concrete for three different imen were not polished.
w/c ratios (0.35, 045 and 0.55) was recorded in terms of numbers of
blows required for producing first visible crack (N1) and ultimate 4.3. Regression analysis for drop weight test
failure (N2) of the specimen.
The numbers of blows for 0%e25% replacement of fine aggregate Linear relationship between number of blows for first crack and
by rubber fiber, without any replacement of cement by silica fume, ultimate failure crack for rubber fiber concrete, with and without
at three selected w/c ratios are listed in Table 4. It can be seen from silica fume, was established. The prediction equations developed
the Table that the number of blows, required for causing the first for the ultimate failure are expressed as below:
crack and ultimate failure, increase significantly with the increase
in replacement level of rubber content for all three w/c ratios. The N2 ¼ 1:145 N1
difference between number of blows for ultimate failure and first þ 1:037 for rubber fiber concrete without silica fume
crack (N2eN1) is also found to increase significantly with the in-
(6)
crease of replacement level of rubber fibers for all three w/c ratios.
Typically, for w/c ratio of 0.45, the difference increases from 6 to 32
on 25% replacement of fine aggregate by rubber fibers. N2 ¼ 1:155 N1
The number of blows for rubber fiber concrete, with 5% and 10% þ 1:108 for rubber fiber concrete with 5% silica fume
replacement of cement by silica fume, are shown in Tables 5 and 6
(7)
respectively. An increase in number of blows is observed with the
increase in replacement level of rubber fiber as observed earlier in
T. Gupta et al. / International Journal of Impact Engineering 83 (2015) 76e87 81

Table 5
Impact resistance results for rubber fiber concrete with 5% silica fume.

Mix N1 N2 N2eN1 Impact energy (J) N2/N1

Mean SD COV (%) Mean SD COV (%) First crack Ultimate failure

U1 61 2.65 4.14 67 2.65 3.79 6 1212 1331 1.10


U2 84 2.00 2.38 96 4.36 4.32 12 1669 1907 1.14
U3 115 1.73 1.52 135 1.73 1.29 20 2285 2682 1.17
U4 209 7.94 3.97 233 7.94 3.54 24 4152 4629 1.11
U5 245 13.23 5.51 279 9.64 3.60 34 4867 5542 1.14
U6 309 2.65 0.86 355 8.54 2.35 46 6138 7052 1.15
U7 49 3.00 6.12 56 3.61 6.94 7 973 1112 1.14
U8 75 1.73 2.37 83 3.61 4.57 8 1490 1649 1.11
U9 89 1.73 1.99 108 6.56 6.50 19 1768 2145 1.21
U10 153 3.61 2.42 178 4.36 2.41 25 3039 3536 1.16
U11 214 10.54 5.19 251 13.11 5.53 37 4251 4986 1.17
U12 221 1.73 0.79 261 3.46 1.32 40 4390 5185 1.18
U13 43 2.65 6.46 49 3.61 8.02 6 854 973 1.14
U14 52 1.73 3.46 62 2.65 4.49 10 1033 1232 1.19
U15 71 6.24 9.75 83 4.36 5.59 12 1410 1649 1.17
U16 97 1.73 1.75 112 2.65 2.43 15 1927 2225 1.15
U17 128 7.00 5.60 162 6.56 4.23 34 2543 3218 1.27
U18 197 11.36 6.17 236 2.65 1.13 39 3913 4688 1.20

SD ¼ Standard deviation; COV ¼ coefficient of variation.

Table 6
Impact resistance results for rubber fiber concrete with 10% silica fume.

Mix N1 N2 N2eN1 Impact energy (J) N2/N1

Mean SD COV (%) Mean SD COV (%) First crack Ultimate failure

V1 64 3.61 6.02 72 6.08 9.35 8 1271 1430 1.13


V2 89 1.73 1.92 101 6.08 6.47 12 1768 2006 1.13
V3 124 1.00 0.81 143 3.00 2.14 19 2463 2841 1.15
V4 214 2.00 0.94 240 3.61 1.53 26 4251 4768 1.12
V5 251 8.19 3.38 289 6.08 2.13 38 4986 5741 1.15
V6 322 6.08 1.93 372 6.08 1.67 50 6397 7390 1.16
V7 54 4.58 9.35 59 4.36 8.07 5 1073 1172 1.09
V8 84 3.46 4.33 91 6.24 7.43 7 1669 1808 1.08
V9 94 3.00 3.30 112 4.36 4.07 18 1867 2225 1.19
V10 158 6.00 3.66 184 3.46 1.92 26 3139 3655 1.16
V11 223 2.65 1.20 265 12.49 4.98 42 4430 5264 1.19
V12 229 8.89 4.06 274 5.57 2.08 45 4549 5443 1.20
V13 49 4.36 9.91 54 6.56 10.75 5 973 1073 1.10
V14 58 2.65 4.82 67 5.57 9.13 9 1152 1331 1.16
V15 74 4.36 6.32 89 6.08 7.41 15 1470 1768 1.20
V16 101 7.00 7.53 121 6.24 5.47 20 2006 2404 1.20
V17 132 6.08 4.86 164 15.13 10.29 32 2622 3258 1.24
V18 204 11.14 5.80 244 5.57 2.34 40 4053 4847 1.20

SD ¼ Standard deviation; COV ¼ coefficient of variation.

Fig. 4. Number of blows for first crack (N1).


82 T. Gupta et al. / International Journal of Impact Engineering 83 (2015) 76e87

Fig. 5. Fracture pattern of concrete with different rubber fiber volume: (a) control concrete; and (b) rubber fiber concrete (25% rubber fibers).

experimental error [29,30]. It may be noted that this behavior was


N2 ¼ 1:171 N1 not observed in drop weight test (Table 6) where the height of
þ 0:884 for rubber fiber concrete with 10% silica fume dropping the weight is maintained by the equipment.
(8)
2
Coefficient of determination (R ) for rubber fiber concrete 4.5. Impact resistance under rebound test
without silica fume, with 5% silica fume and with 10% silica fume
are 0.998, 0.996 and 0.997 respectively. According to Rahmani et al. Fig. 7(a) shows the impact energy absorbed in rebound test for
[27], a coefficient of determination of 0.7 or higher is sufficient for a rubber concrete without silica fume. It can be seen that the increase
reasonable model, hence above equations can be successfully used in the replacement level of rubber fibers significantly improves the
to represent the relationship between the number of blows for first impact energy absorbed for all three w/c ratios of 0.35, 0.45 and
crack and ultimate failure strength for rubber fiber concrete, 0.55. It is also observed that on 25% replacement of fine aggregates
without and with silica fume. by rubber fibers, the impact energy absorbed by concrete increases
from 1.79 J to 1.99 J, 1.77 J to 1.96 J and 1.74 J to 1.94 J for w/c ratios
0.35, 0.45 and 0.55 respectively. Fig. 7(b) and (c) show the impact
4.4. Impact resistance under flexural loading energy absorbed under rebound test for rubber fiber concrete with
5% and 10% silica fume respectively. It is again observed that the
Fig. 6(a) shows the impact energy at failure, under flexural impact energy absorbed increases with the increase of replacement
loading, for rubber fiber concrete without silica fume. It can be seen level of rubber fiber. Similar observations were made by Obzay et al.
that increase in the replacement level of rubber fibers significantly [24] for the crumb rubber concrete.
improves the impact energy for all three w/c ratios. It is observed It can be observed from Fig. 7(a), (b) and (c), that there is a minor
that on 25% replacement with rubber fibers in fine aggregates, the effect of replacement of cement by silica fume on the impact energy
impact energy of control concrete increases from 36.0 J to 108.0 J, absorbed. It is also observed that on 10% replacement of cement by
27.0 Je90.0 J and 22.5 Je81.0 J for w/c ratios 0.35, 0.45 and 0.55 silica fume, the impact energy absorbed by control concrete in-
respectively. Fig. 6(b) and (c) show the impact energy at failure creases marginally from 1.79 J to 1.80 J, 1.77 J to 1.79 J and 1.74 J to
under flexural loading for rubber fiber concrete with 5% and 10% 1.76 J for w/c ratios 0.35, 0.45 and 0.55 respectively. Similarly,
silica fume respectively. It is again observed that the impact energy impact energy absorbed by rubber fiber concrete (25% rubber fiber)
increases with the increase of replacement level of fine aggregate increases marginally from 1.99 J to 2.01 J, 1.96 J to 1.98 J and 1.94 J to
by rubber fiber. According to RedaTaha et al. [28], the low stiffness 1.97 J for w/c ratios 0.35, 0.45 and 0.55 respectively on 10%
of the rubber particles leads to higher flexibility of rubberized replacement of cement by silica fume.
concrete and absorption of considerable amount of impact energy.
It can be observed from Fig. 6(a), (b) and (c) that the impact
energy increases with the increase of silica fume in concrete. It is 4.6. Relationship between impact energy under drop weight and
also observed that on 10% replacement of cement by silica fume, the flexural loading
impact energy of control concrete increases from 36.0 J to 50.0 J,
27.0 J to 41.0 J and 22.5 J to 32.0 J for w/c ratios 0.35, 0.45 and 0.55 A relationship was developed in form of an equation for evalu-
respectively. Similarly, the impact energy of rubber fiber concrete ating the impact energy under drop weight test from the impact
(25% rubber fiber) increases from 108.0 J to 131.0 J, 90.0 J to 117.0 J energy under flexural loading or the impact energy under rebound
and 81.0 J to 113.0 J for w/c ratios 0.35, 0.45 and 0.55 respectively, test and vice-versa. Table 7 shows the logarithmic relationship
on 10% replacement of cement by silica fume. For 10% silica fume between impact energy under drop weight, Ep,dwi and impact en-
with 10% rubber fiber, a lower value of impact resistance is ergy under flexural loading, Ep,fl. Correlation coefficient (R2) values
observed at w/c ratio 0.45 in comparison to w/c ratio 0.55 show good relationship between Ep,dwi and Ep,fl. Similarly, Table 8
(Fig. 6(c)). This may be due to error in manually maintaining the shows the logarithmic relationship between impact energy under
height of dropping the weight (450 mm) or some unidentified drop weight, Ep,dwi and impact energy under rebound test, Ep,r.
T. Gupta et al. / International Journal of Impact Engineering 83 (2015) 76e87 83

Fig. 6. Impact energy under flexural loading of rubber fiber concrete containing (a) 0%
silica fume; (b) 5% silica fume; and (c) 10% silica fume.
Fig. 7. Impact energy absorbed under rebound test by rubber fiber concrete containing
(a) 0% silica fume; (b) 5% silica fume; and (c) 10% silica fume.
84 T. Gupta et al. / International Journal of Impact Engineering 83 (2015) 76e87

Table 7
Relationship between Impact Energy under drop weight test Ep,dwi and flexural loading Ep,fl.

Silica fume (%) w/c ratio Equation Correlation coefficient (R2)

0 0.35 Ep,dwi ¼ 4589.lnEp,fl  15621 0.988


0.45 Ep,dwi ¼ 2954.lnEp,fl  8886 0.972
0.55 Ep,dwi ¼ 2374.lnEp,fl  7098 0.930
5 0.35 Ep,dwi ¼ 4783.lnEp,fl  17318 0.972
0.45 Ep,dwi ¼ 3165.lnEp,fl 10208 0.938
0.55 Ep,dwi ¼ 2291.lnEp,fl  7122 0.856
10 0.35 Ep,dwi ¼ 4967.lnEp,fl  18478 0.949
0.45 Ep,dwi ¼ 3666.lnEp,fl  12768 0.969
0.55 Ep,dwi ¼ 2240.lnEp,fl  7255 0.801

Ep,dwi and Ep,fl are in J.

Correlation coefficient (R2) values show good relationship between   


Ep,dwi and Ep,r. 1
ln ln ¼ a lnðnÞ  a lnðuÞ (12)
LN
The relation expressed in Equation (12) is used to verify the
4.7. Weibull distribution analysis of drop weight test number of blows for first crack resistance and failure resistance.
The data of impact resistance (N1 and N2) is arranged in ascending
The statistical analysis of impact test data of concrete has been order and the empirical survivorship functions for N1 and N2 are
described in literature by different mathematical probability obtained as [4].
models [4,31e33]. In the present study, a number of blows were
required in drop weight test making the mechanism similar to the j
LN ¼ 1  (13)
fatigue test. Thus, Weibull distribution function [4] has been sþ1
adopted as a method for statistical analysis of impact test data since
this function has been widely used for statistical description of where, j ¼ failure order number and s ¼ total number of specimen.
fatigue test data [34,35]. The relationship between ln[ln[1/LN]] and lnn should be linear
Weibull distribution function is characterized by a probability for the application of two parameter Weibull distribution to sta-
distribution function f(n) and is given below [4]: tistical data of impact resistance [4]. The variation of ln[ln[1/LN]]
with lnN1 for rubber fiber concrete without silica fume, with 5%
 a
a na1  n silica fume and with 10% silica fume is shown in Fig. 8(a), (b) and (c)
f ðnÞ ¼
u
e (9) respectively. Similarly, the variation of ln[ln[1/LN]] with lnN2 for
u u
rubber fiber concrete without silica fume, with 5% silica fume and
where, a is Weibull slope or shape parameter; u is scale parameter; with 10% silica fume is shown in Fig. 9(a), (b) and (c) respectively.
and n is specific value of random variable N (¼N1 and N2 for the The regression coefficients of a, alnu and the correlation coef-
present study). ficient R2 corresponding to all the concrete samples for linear
Cumulative density function is obtained by integration of regression are shown in Table 9. The correlation coefficient R2 is
probability distribution function and expressed as more than 0.95 in all the cases. Therefore, a two parameter Weibull
distribution can be assumed to apply to statistical distribution of N1
 a
and N2 for concrete containing rubber fibers. Similar observation
 n

FN ðnÞ ¼ 1  e
u
(10) has been made earlier by Xiang-yu et al. [4] for the concrete con-
taining steel fibers.
The probability of survivorship function is given by Ref. [4].
 a 4.8. Micro structural analysis
 n

LN ðnÞ ¼ 1  FN ðnÞ ¼ e
u
(11)
SEM images of the concrete containing 15% rubber fiber for 0.45
Following relation is obtained by taking natural logarithms of w/c ratio specimens are shown in Fig. 10(a), (b) and (c). A number of
both sides of equation (11). micro cavities are observed in the cement matrix as shown in

Table 8
Relationship between Impact Energy under drop weight test Ep,dwi and rebound test Ep,r.

Silica fume (%) w/c ratio Equation Correlation coefficient (R2)

0 0.35 Ep,dwi ¼ 43444.lnEp,r  24441 0.937


0.45 Ep,dwi ¼ 33013.lnEp,r  18223 0.915
0.55 Ep,dwi ¼ 25782.lnEp,r  13956 0.832
5 0.35 Ep,dwi ¼ 44957.lnEp,r  25558 0.921
0.45 Ep,dwi ¼ 35073.lnEp,r  19607 0.914
0.55 Ep,dwi ¼ 26567.lnEp,r  14485 0.854
10 0.35 Ep,dwi ¼ 46458.lnEp,r  26798 0.900
0.45 Ep,dwi ¼ 34887.lnEp,r  19578 0.923
0.55 Ep,dwi ¼ 25809.lnEp,r  14143 0.809

Ep,dwi and Ep,r are in J.


T. Gupta et al. / International Journal of Impact Engineering 83 (2015) 76e87 85

Fig. 9. Weibull distribution of N2 for rubber fiber concrete containing (a) 0% silica
fume; (b) 5% silica fume; and (c) 10% silica fume.
Fig. 8. Weibull distribution of N1 for rubber fiber concrete containing (a) 0% silica
fume; (b) 5% silica fume; and (c) 10% silica fume.

Table 9
Linear regression coefficients of impact resistance in Weibull distribution.

Failure crack blow Silica fume (%) w/c ratio Regression coefficient (a) Regression coefficient (a ln u) Correlation coefficient (R2)

N1 0 0.35 1.373 7.293 0.961


0.45 1.483 7.477 0.966
0.55 1.525 7.172 0.948
5 0.35 1.397 7.469 0.963
0.45 1.469 7.49 0.956
0.55 1.569 7.492 0.95
10 0.35 1.429 7.692 0.971
0.45 1.539 7.92 0.953
0.55 1.661 8.013 0.935
N2 0 0.35 1.378 7.501 0.972
0.45 1.483 7.675 0.972
0.55 1.482 7.227 0.957
5 0.35 1.39 7.613 0.975
0.45 1.442 7.581 0.964
0.55 1.516 7.516 0.955
10 0.35 1.417 7.82 0.976
0.45 1.457 7.734 0.963
0.55 1.588 7.95 0.955
86 T. Gupta et al. / International Journal of Impact Engineering 83 (2015) 76e87

Fig. 10(a), which reduce the strength of concrete. Gaps are observed 5. Conclusions
in the interface of rubber fibers and cement matrix in Fig. 10(b) and
(c) reflecting a weak bond between rubber fibers and cement In the present study, the impact resistance of concrete con-
mortar. The SEM images further show that the rubber fiber particles taining waste rubber fibers and silica fume was evaluated by
have irregular shapes. It indicates that the interfacial bonding be- carrying out experimental studies. Waste rubber tyres converted
tween the rubber fiber and cement paste is weak, resulting in the to the form of rubber fibers were used to partially replace the
cracking at the interface. The cracking results in the reduction of the fine aggregate whereas silica fume was used to partially replace
strength of rubber fiber concrete. the cement. Six replacement levels of rubber fibers (0%, 5%, 10%,
15%, 20% and 25%) and three replacement levels of silica fume
(0%, 5% and 10%) were considered. Drop weight test, flexural
loading test and rebound test were carried out as per relevant
standards for three different w/c ratios (0.35, 0.45 and 0.55).
Based on the test results and discussions, following conclusions
are drawn:

1. The impact resistance of concrete improves on replacement of


fine aggregate by rubber fibers and on replacement of cement by
silica fume.
2. The difference between number of blows for ultimate failure
and first crack increases significantly with the increase in
replacement level of rubber fibers, which indicate the reduction
in brittleness of concrete or increase in ductility of waste rubber
fiber concrete.
3. Linear relationship exists between number of blows for first
crack and ultimate failure cracks for rubber fiber concrete.
4. A good correlation exists between the results of drop weight
test, flexural loading and rebound test.
5. The impact resistance data for drop weight test follows the two-
parameter Weibull distribution function.

Further studies can be carried out for higher replacement levels


of rubber fibers and silica fumes. Studies can also be carried out in
future using the bigger impactors and higher heights along with the
measurement of impact force and acceleration of the sample/
impactor.

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