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Impact Resistance of Concrete Containing Waste Rubber Fiber and Silica Fume
Impact Resistance of Concrete Containing Waste Rubber Fiber and Silica Fume
a r t i c l e i n f o a b s t r a c t
Article history: High impact resistance and greater energy absorption capacity are desirable properties for concrete.
Received 11 February 2015 Innovative and sustainable materials may be used to improve these properties. In the present study, the
Received in revised form effect of replacement of fine aggregates by waste rubber fibers on the impact resistance of concrete has
29 April 2015
been assessed. Silica fume has also been considered as replacement of cement. Six replacement levels of
Accepted 2 May 2015
Available online 12 May 2015
rubber fiber (0%, 5%, 10%, 15%, 20% and 25%) and three replacement levels of silica fume (0%, 5% and 10%)
have been considered for three different water cement ratios. Impact tests on concrete have been con-
ducted by three different techniques; drop weight test, flexural loading test and rebound test. Re-
Keywords:
Waste rubber fiber concrete
lationships between impact test results of drop weight test, flexural loading test and rebound test have
Silica fume also been established. In view of large variation of impact values, a two-parameter Weibull distribution is
Impact resistance adopted to analyze the experimental data of drop weight test. The study demonstrates that the waste
Energy absorption capacity rubber fiber can be used as a sustainable material to improve the impact resistance and ductility of
Weibull distribution concrete. The study also demonstrates that the silica fume improves the impact resistance and reduces
the ductility of rubber fiber concrete.
© 2015 Elsevier Ltd. All rights reserved.
1. Introduction Studies have also been carried out for the impact resistance or
energy absorption capacity of fibrous concrete containing silica
Concrete is a brittle material with high rigidity. High impact fume [15e17]. Nili et al. [15] reported that the impact energy in-
resistance and more energy absorption capacity are required in creases on partial replacement of cement by silica fume and addi-
many applications such as shock absorbers, foundation pads of tion of steel fibers. Yan et al. [16] reported that the addition of steel
machinery, railway buffers etc. Additional ingredients are required fibers and partial replacement of cement by silica fume in concrete
to improve the properties of concrete in some situations where effectively reduces the number and size of cracks, and enhances the
these requirements are not fulfilled. performance of high strength concrete under impact and fatigue
Many studies have been carried out for evaluating the impact loads. Nili et al. [17] reported that the silica fume improves the
resistance and energy absorption capacity on fibrous concrete impact resistance of concrete containing polypropylene fibers by
[1e14]. The impact resistance of concrete has been found to in- facilitating dispersion of fibers.
crease up to fifteen times on using steel fibers [5e10] and up to ten Accumulation of discarded rubber tyres is a major problem as its
times on using polypropylene fibers [11,12]. The addition of natural degradation is very difficult because of the highly complex
fibers in the form of coir, sisal, jute, and hibiscus cannabinus has configuration of ingredient materials. The available studies
also been found to increase the impact resistance of concrete by up regarding utilization of waste rubber tyres in concrete provide a
to eighteen times [13]. Rao et al. [14] studied the behavior of slurry- strong recommendation for the use of this waste as a partial
infiltrated concrete slabs, containing steel fibers, under impact replacement of fine aggregate in concrete production [18]. This
loading and reported an increase in energy absorption of concrete would facilitate effective use of the solid waste, minimize its
with the increase of fiber volume. accumulation and help in reducing the consumption of natural
resources.
Some studies have been carried out on the impact resistance of
* Corresponding author. Tel.: þ91 94144 75375. concrete. Topcu [19] reported a decrease in elastic energy capacity
E-mail address: sandeep.nitjaipur@gmail.com (S. Chaudhary).
http://dx.doi.org/10.1016/j.ijimpeng.2015.05.002
0734-743X/© 2015 Elsevier Ltd. All rights reserved.
T. Gupta et al. / International Journal of Impact Engineering 83 (2015) 76e87 77
Table 1
Chemical composition of cement and silica fume.
Element/Material CaO (%) SiO2 (%) Al2O3 (%) Fe2O3 (%) SO3 (%) MgO (%) K2O (%) LOI (%)
and increase in plastic energy capacity of the concrete on replace- Rubber fibers, obtained from mechanical grinding of waste
ment of coarse aggregates and fine aggregate by coarse rubber rubber tyres, were used as partial replacement of fine aggregates.
chips and fine rubber chips respectively. Khaloo et al. [20] carried These rubber fibers were of 2e5 mm in width and up to 20 mm in
out a study on concrete containing high volume chip rubber as length (aspect ratio 4e10) with a specific gravity of 1.07. As the
partial replacement of coarse aggregate and crumb rubber as par- rubber fibers are obtained from a waste product of used rubber
tial replacement of fine aggregate. The toughness was reported to tyres, detailed microstructural characteristics are necessary to be
be highest for 25% concentration of both the types of rubber par- ascertained to ensure the compatibility of this material with the
ticles as a part of the total aggregate volume. Sukontasukkul et al. concrete. Scanning electron microscope (SEM) was used for this
[21] carried out flexural test and reported an increase in toughness purpose.
of concrete blocks on partial replacement of 10% of fine aggregate SEM images of a rubber fiber are shown in Fig. 1(a) and (b). A
and 20% of coarse aggregate by crumb rubber. Aiello and Leuzzi [22] large cavity was observed in the rubber fiber which acts as large
also carried out flexural tests and reported a significant increase in pore in the concrete and influences its properties. Micro cracks
the energy absorption for up to 75% replacements of coarse/fine within the rubber fibers were also visible (Fig. 1(a) and (b)) and
aggregate by rubber shreds. Ozbay et al. [23] carried out rebound these cracks indicate a weak interfacial bonding between the rub-
tests and reported about 25% increase in energy absorption ca- ber fibers and cement paste which affected the strength of rubber
pacity of concrete on 25% replacement of fine aggregate by crumb fiber concrete.
rubber. Al-Tayeb et al. [24] substituted up to 25% of fine aggregate
by waste crumb rubber and tested the concrete under impact three 2.2. Mix proportions
point bending load. They reported an improvement in impact load
behaviour with the increase in replacement level of fine aggregates. Concrete mixes were prepared using water/cement ratios of
It is evident from the work reported above that although a 0.35, 0.45 and 0.55 with a partial replacement of fine aggregate (FA)
number of studies have been undertaken for the impact resistance by rubber fibers ranging from 0% to 25%. Concrete mixes were also
of rubberised concrete; none of the studies has considered waste cast by replacing cement with silica fume, ranging from 0% to 10% in
rubber in the form of fibers. Therefore, there is a need to carry out the control concrete as well as rubber fiber concrete. Concrete
systematic experimental studies to evaluate the impact resistance mixes were first dry-mixed for 2e3 min in the mixer. To maintain
of concrete incorporating rubber fibers (with and without silica the workability and the uniformity of the mixes, the proportion of
fume), as partial replacement of fine aggregate, for varying w/c super-plasticizer (SP) with that of cement by weight was varied.
ratios. When the concrete mix showed the desired workability and uni-
In the present work, detailed experimental studies have been form rubber fiber distribution, it was placed in a mould and
carried out to determine the impact resistance of concrete con- vibrated on a table vibrator. The specimen were covered with
taining waste rubber fibers. The studies have been undertaken for plastic sheets and stored at room temperature for 24 h prior to de-
varying percentage of waste rubber fibers (0%, 5%, 10%, 15%, 20% and moulding. The details of concrete mix with the observed work-
25%) as partial replacement of fine aggregates at three different w/c ability in terms of compaction factor (C.F.) are shown in Table 2.
ratios (0.35, 0.45 and 0.55). Three replacement levels of silica fume
(0%, 5% and 10%) have been considered for partial replacement of 3. Testing program
cement in the rubber fiber concrete. Impact resistance has been
evaluated by carrying out drop weight test (concrete cylinder In this experimental study, following properties of hardened
subjected to impact), flexural loading test (concrete beam subjected concrete were evaluated as per the relevant standards.
to impact) and rebound test (concrete cube subjected to impact).
Relationships between results of drop weight test, flexural loading
3.1. Compressive strength
test and rebound test have also been established. The experimental
results obtained from various techniques have been analyzed by
The mechanical strength of rubber fiber concrete with and
statistical approaches to account for the variability in the properties
without silica fume was measured by conducting compression
of concrete.
strength test. This test was performed on 100 mm concrete cubes
(three for each mix) at 28 days as per BIS Committee BDC 2 [25].
2. Experimental studies Load was applied gradually with the rate of travel of machine
equivalent to 240 ± 35 kN/m2/s [25].
2.1. Material
3.2. Impact resistance under drop weight test
Ordinary Portland cement of specific gravity 3.12 and silica fume
of specific gravity 2.18 were used for the concrete mixes in this Drop weight test was performed on cylindrical specimens
study. The chemical compositions of cement and silica fume are (150 mm in diameter and 65 mm in height, three specimens for
shown in Table 1. Fine aggregate (natural sand) of specific gravity each mix) as per ACI Committee 544 [26] to estimate the energy
2.56 and coarse aggregate (crushed gravel) of maximum size of absorption capacity of concrete specimens. In this test, repeated
12 mm and of specific gravity 2.59 were used in the concrete mixes. loading was applied on the specimen from a height. The number of
Super plasticizer (SP) “Glanium Sky 777” from BASF was used as an blows was obtained for the prescribed level of distress (occurrence
admixture to obtain the desired workability. of first crack and failure cracks).
78 T. Gupta et al. / International Journal of Impact Engineering 83 (2015) 76e87
Fig. 1. SEM image of rubber fiber at (a) 40x magnification; and (b) 150x magnification.
Table 2
Concrete mix proportions of rubber fiber concrete with and without silica fume.
Mix Cement (kg) Silica fume (kg) Fine aggregates (kg) Coarse aggregates Rubber fibers (kg) Water (kg) Super plasticizer (%) C.F.
(kg)
10 mm 20 mm
R1-R6 364 0 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64,80 127.4 2.1% 0.91
R7-R12 364 0 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64,80 163.8 0.5% 0.92
R13-18 364 0 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64,80 200.2 0% 0.92
U1eU6 345.8 18.2 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64, 80 127.4 2.1% 0.92
U7eU12 345.8 18.2 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64, 80 163.8 0.5% 0.92
U13eU18 345.8 18.2 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64, 80 200.2 0% 0.92
V1eV6 327.6 36.4 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64, 80 127.4 2.1% 0.92
V7eV12 327.6 36.4 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64, 80 163.8 0.5% 0.92
V13eV18 327.6 36.4 764, 726, 688, 650, 611, 573 562 562 0, 16, 32, 48, 64, 80 200.2 0% 0.92
Specimens of 28 days age were tested by the drop weight impact Similarly, the impact energy at ultimate crack, Ep,dwu was
testing machine fabricated in the laboratory as per guidelines of ACI calculated by the equation given below:
committee 544 [26]. The machine consists of a 4.5 kg hammer ball
dropping from 450 mm height on a hardened steel ball of 65 mm Ep;dwu ¼ N2 mgh (2)
diameter (Fig. 2(a)). The steel ball was placed at the centre of
specimen and this specimen was placed on the base plate within where, N1 and N2 are the number of blows at initial and ultimate
the positioning lugs as shown in Fig. 2(a). The hammer ball was crack level, m is the mass of drop hammer (4.5 kg), g is acceleration
dropped repeatedly and the number of blows (N1) required to cause due to gravity (9.81 m/s2) and h is the releasing height of drop
the first visible crack on the top was recorded. Number of blows hammer (450 mm).
(N2) which caused opening of cracks in such a way that the concrete
pieces started touching side lugs was also recorded. The values of 3.3. Impact resistance under flexural loading
N1 and N2 were designated as initial crack resistance factor and
ultimate crack resistance factor respectively. Impact test on the beams was performed to determine the po-
The impact energy at initial crack, Ep,dwi (where first subscript p tential energy of rubber fiber concrete (Fig. 2(b)). In this test, beams
denotes the type of energy absorbed i.e. potential energy and sec- of 100 mm 100 mm 500 mm size (three specimens for each
ond subscript dw denotes the type of test i.e. drop weight) was mix) were tested with a center to center span of 400 mm. A
calculated by the equation given below: hammer of 1.0 kg weight was dropped on the mid span of the beam
from a height of 450 mm. Number of drops up to failure, Nf was
Ep;dwi ¼ N1 mgh (1) measured and energy absorbed by the specimen, Ep,fl (subscript fl
denotes flexural loading) was calculated by the following equation:
Fig. 2. (a) Drop weight test; (b) Flexural loading test; and (c) Rebound test.
T. Gupta et al. / International Journal of Impact Engineering 83 (2015) 76e87 79
X
Nf
Ep;fl ¼ mi ghi (3)
i¼1
where, mi is the mass of drop hammer (1.0 kg) and hi is the drop
height (450 mm).
where m is mass of steel ball (0.5 kg), hi is the initial height of steel
ball (1.0 m) and hf is height recorded after rebound (varies for
different mixes).
The energy absorption capacity of concrete specimen, Ep,r was
calculated as the difference of the final and initial potential energy
(Ep,r¼Ep,riEp,rf). Loss due to air resistance was ignored.
Table 3
28 days compressive strength of rubber fiber concrete.
Mix Mean (N/mm2) SD COV (%) Mix Mean (N/mm2) SD COV (%) Mix Mean (N/mm2) SD COV (%)
Table 4
Impact resistance results for rubber fiber concrete without silica fume.
Mean SD COV (%) Mean SD COV (%) First crack Ultimate failure
waste rubber fiber concrete for w/c ratios of 0.35, 0.45 and 0.55 at Table 4 for concrete without silica fume. The values of N1 and N2 for
28 days, is shown in Fig. 3(a), (b) and (c) respectively. It can be seen all three water cement ratios, increase by about five times on
that the compressive strength decreases with an increase in the incorporation of 25% rubber fiber for both 5% silica fume concrete
replacement level of rubber fibers for all three w/c ratios. The and 10% silica fume concrete.
compressive strength of control concrete (without rubber fiber and In general, it can be concluded that the impact resistance, for
silica fume) decreases from 58.97 N/mm2 to 28.43 N/mm2, 50.43 N/ first crack as well as for ultimate failure, increases with the increase
mm2 to 23.60 N/mm2 and 33.70 N/mm2 to 15.30 N/mm2 for w/c in rubber fiber content. Similar observations were made by
ratios of 0.35, 0.45 and 0.55 respectively, on 25% replacement of Mohammadi et al. [12] for steel fibers and the increase in impact
sand by rubber fiber. energy was attributed to long fibers which are expected to arrest
It is also observed from Fig. 3(a), (b) and (c) that on replacement the cracks due to their superior bond resistance. As the replace-
of cement by silica fume, the compressive strength increases for ment level of rubber fibers will increase, rubber-cement composite
control concrete as well as for the rubber fiber concrete. will have higher flexibility and this increase in flexibility level will
Compressive strength of control concrete (without rubber fiber and lead to more energy absorption as compared to the control mix.
silica fume) increases from 58.97 N/mm2 to 75.20 N/mm2, 50.43 N/ Tables 4e6 reveal that although the impact energy is enhanced
mm2 to 62.70 N/mm2 and 33.70 N/mm2 to 39.70 N/mm2 for w/c by silica fume, however, no definite pattern is observed for effect of
ratios of 0.35, 0.45 and 0.55 respectively on 10% replacement of silica fume on N2eN1.
cement by silica fume. Compressive strength of rubber fiber con- The number of blows required for the first crack in concrete, for
crete (25% rubber fiber) increases from 28.43 N/mm2 to 37.90 N/ three different w/c ratios, is shown in Fig. 4. It can be observed that
mm2, 23.60 N/mm2 to 29.90 N/mm2 and 15.30 N/mm2 to 19.10 N/ the number of blows is more for the rubberized concrete as
mm2 for w/c ratios of 0.35, 0.45 and 0.55 respectively, on 10% compared to the corresponding case of non rubberized concrete.
replacement of cement by silica fume. The fracture pattern of cylindrical specimen for control concrete
and rubber fiber concrete (25% rubber fibers) without silica fume is
4.2. Impact resistance under drop weight test shown in Fig. 5(a) and (b) respectively. It may be noted that there
may be some deviation in the results as the surfaces of the spec-
The impact resistance of rubber fiber concrete for three different imen were not polished.
w/c ratios (0.35, 045 and 0.55) was recorded in terms of numbers of
blows required for producing first visible crack (N1) and ultimate 4.3. Regression analysis for drop weight test
failure (N2) of the specimen.
The numbers of blows for 0%e25% replacement of fine aggregate Linear relationship between number of blows for first crack and
by rubber fiber, without any replacement of cement by silica fume, ultimate failure crack for rubber fiber concrete, with and without
at three selected w/c ratios are listed in Table 4. It can be seen from silica fume, was established. The prediction equations developed
the Table that the number of blows, required for causing the first for the ultimate failure are expressed as below:
crack and ultimate failure, increase significantly with the increase
in replacement level of rubber content for all three w/c ratios. The N2 ¼ 1:145 N1
difference between number of blows for ultimate failure and first þ 1:037 for rubber fiber concrete without silica fume
crack (N2eN1) is also found to increase significantly with the in-
(6)
crease of replacement level of rubber fibers for all three w/c ratios.
Typically, for w/c ratio of 0.45, the difference increases from 6 to 32
on 25% replacement of fine aggregate by rubber fibers. N2 ¼ 1:155 N1
The number of blows for rubber fiber concrete, with 5% and 10% þ 1:108 for rubber fiber concrete with 5% silica fume
replacement of cement by silica fume, are shown in Tables 5 and 6
(7)
respectively. An increase in number of blows is observed with the
increase in replacement level of rubber fiber as observed earlier in
T. Gupta et al. / International Journal of Impact Engineering 83 (2015) 76e87 81
Table 5
Impact resistance results for rubber fiber concrete with 5% silica fume.
Mean SD COV (%) Mean SD COV (%) First crack Ultimate failure
Table 6
Impact resistance results for rubber fiber concrete with 10% silica fume.
Mean SD COV (%) Mean SD COV (%) First crack Ultimate failure
Fig. 5. Fracture pattern of concrete with different rubber fiber volume: (a) control concrete; and (b) rubber fiber concrete (25% rubber fibers).
Fig. 6. Impact energy under flexural loading of rubber fiber concrete containing (a) 0%
silica fume; (b) 5% silica fume; and (c) 10% silica fume.
Fig. 7. Impact energy absorbed under rebound test by rubber fiber concrete containing
(a) 0% silica fume; (b) 5% silica fume; and (c) 10% silica fume.
84 T. Gupta et al. / International Journal of Impact Engineering 83 (2015) 76e87
Table 7
Relationship between Impact Energy under drop weight test Ep,dwi and flexural loading Ep,fl.
FN ðnÞ ¼ 1 e
u
(10) has been made earlier by Xiang-yu et al. [4] for the concrete con-
taining steel fibers.
The probability of survivorship function is given by Ref. [4].
a 4.8. Micro structural analysis
n
LN ðnÞ ¼ 1 FN ðnÞ ¼ e
u
(11)
SEM images of the concrete containing 15% rubber fiber for 0.45
Following relation is obtained by taking natural logarithms of w/c ratio specimens are shown in Fig. 10(a), (b) and (c). A number of
both sides of equation (11). micro cavities are observed in the cement matrix as shown in
Table 8
Relationship between Impact Energy under drop weight test Ep,dwi and rebound test Ep,r.
Fig. 9. Weibull distribution of N2 for rubber fiber concrete containing (a) 0% silica
fume; (b) 5% silica fume; and (c) 10% silica fume.
Fig. 8. Weibull distribution of N1 for rubber fiber concrete containing (a) 0% silica
fume; (b) 5% silica fume; and (c) 10% silica fume.
Table 9
Linear regression coefficients of impact resistance in Weibull distribution.
Failure crack blow Silica fume (%) w/c ratio Regression coefficient (a) Regression coefficient (a ln u) Correlation coefficient (R2)
Fig. 10(a), which reduce the strength of concrete. Gaps are observed 5. Conclusions
in the interface of rubber fibers and cement matrix in Fig. 10(b) and
(c) reflecting a weak bond between rubber fibers and cement In the present study, the impact resistance of concrete con-
mortar. The SEM images further show that the rubber fiber particles taining waste rubber fibers and silica fume was evaluated by
have irregular shapes. It indicates that the interfacial bonding be- carrying out experimental studies. Waste rubber tyres converted
tween the rubber fiber and cement paste is weak, resulting in the to the form of rubber fibers were used to partially replace the
cracking at the interface. The cracking results in the reduction of the fine aggregate whereas silica fume was used to partially replace
strength of rubber fiber concrete. the cement. Six replacement levels of rubber fibers (0%, 5%, 10%,
15%, 20% and 25%) and three replacement levels of silica fume
(0%, 5% and 10%) were considered. Drop weight test, flexural
loading test and rebound test were carried out as per relevant
standards for three different w/c ratios (0.35, 0.45 and 0.55).
Based on the test results and discussions, following conclusions
are drawn:
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