MASS 1B i 100 By a ISL 1 232 = Sear t"] l 957 1105 2403] fel ull tl al eee 50 100 180 200 IR é & 4000 3000 2000 1000 Wavenumber (cm-1) "HNMR 600 MHz - 200 My ~~«SSO 1300 1250 «1200 +1150 1160 1080 100 980 900-850 Hs f a a 45 40 35 30 25 20 i} ppm “C/DEPT NMR 150.9 MHz T T T T T +r 200 180 160 140120 ~—100_—=BD 60 40 20 ppm4540 35 30 25 20 13 19 ppm COSY SOOMILZ 20 . as 30 3s 40 . - So a3 ub 0a ao aS de TS FO apm a INADEQUATE 150.9 MHz ie 20000 150004 100004 FL 5000-4 -5000 o4 0 5000-4 5000 ' . so 6 ano men sn 1 | ss 24000 2400 23000 i | ‘ | 23000 00 i | 00 mt 2100 -21000 -20000- | 1 -20000 -1900 tt -19000 13000 -18000 Po o4itae £19000 re peencperer errr rrr 700 © ss 50 45 40 35,30 25 20 15 10 5 ppm