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    10 views6 pages

    Astm D 4239 - 2014 - S

    Uploaded by

    Menna Moustafa

    Copyright:

    © All Rights Reserved
    Download as PDF or read online from Scribd
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    of 6
    Designation: D4a39 14 ‘Standard Test Method for ‘Sulfur in the Analysis Sample of Coal and Coke Using High- ‘Temperature Tube Furnace Combustion’ ‘su se we et gin De tml sing be eign in yao iat secures egret hun pe acre a A SS eto cae egret aml a ope rat br ac of US. gare of 1. Scope LL Tis tet method cover he deteminston of suf in samples of coal or coke by aighsemperatre tbe Trace combustion. TEL Two analysis methods ae described. 12 When stoma equpaent i sed, ether meth can te clad wa isrumeta method 12 The vals stdin Sule ar 10 be regarded standard, No other ants of earemen ar nla ois nda 1A Al percentages are percet mas factions unless oe 1S This standard doesnot purport i aires all of the safey concer, fay. ssoted with fs we. It the expos of the wer of ths standard establish appro Dre softy and heath pacer and determine he apple: ‘iy f regulatory lion ior to se 2 Referenced Documents 21 ASTM Sundae? ‘BuéPracice for Colleton and Preparation of Coke Supls fr Laborry Anaya 'DBOI3 Pate for Preping Coal Samples for Analysis 'DBI7} Tew Metod for Msi the Acyl Sample of ‘Coal and Coke 'D3176Pracce for Utimate Analysis of Cal and Coke RIO Pesce for Caeulaing Cos! as Coke Analyses Thom At Deemine to Diferent Bases DTA Prati for Enablishing te Competence of Late Toes Using ASTM Procedures in te Sampling and “Ct elie ppd Mach 1 204, Paed Mach 2214 gn agen res pn ous at Cece irene Re Be Analysis of Coal and Coke DIN en Mos for Primate Ansys of Conlon ‘Coke by Maro Themogravinaic Alyse oa Practice for Conducting an Inteitraory Stay co ‘Demin the Pein of Test Mth 122 150 Sundand> {80 11722 Said Moral Fuels Hard Coa - Deteminaton 1 Mitr in the gener nay ears ying ‘awogen 4 Summary of Tit Method 31 Combusion Methd &(1350°C}—A weighed tet por- Yon of sample bumed in tae frac a 4 le ‘ombuston tbe opening temperate of 135 ina steam ‘tonyen: During cobain st iemperature above 1350°C, the rlfer and uf compounds contained nthe mpl re ‘composed an xia sos oxlsvelyo paseo sr ‘oxide, SO, Moire and parclts te removed rm he {530s fles The ps seam passed troagh acelin wich Slur dione 5 measured by an ifred CIR) stsoton (Sacco Sefer inde ebb I energy at ree wate™ eng within the IR spect. Energy bored a the a Pesto the cel body in wach the IR ener sb enemies tun, a the ecto lew energy i vcrved A ‘te enesy is elimina fom reaching the detector y Presive wavelength le Ths, sopion of ery ca [S'auited only 1 sulur donde whose coment is Proportions the change nergy a detector. Ose ca (et a both a reference and'2 measuemest chamber To ‘illu ae alu dione tected on onouous bs 3.11 One proce for Mathod A uses cal or cake rsferace mateals ocala he slfer anayrer A eco Procedre for Method A wes 8 pte substance, BBOT, 1 ‘arate te efor amie 132 Combusion Method B (1S0°C}—A weighed west sr- tion of sample stared in quae combustion tbe fa Suc of oxygen with an egal or excess weight of tangs "Ai ie rin Sant 0 1 cmap 7S Sli ip vs229 14 oxide (WOD, Sule i xiied during the reaction of he ample ad WO. The be furnace i oped tks ‘Stone operating empertre of 150°C and (Sa) ‘ample tents ae ized. Mote ad pls att ‘moved fom te combustion gas by Gen. The ps seam ‘hen passed hgh cel in which fer xsd meaeted by amined (UR) abodon detec ull dod aburts 1k energy a2 precte wavelength within te TR spec. Energy absorbed atthe gs pases trough th ell body In which he IR energy is eigenstate detector, Tes energy rcetvd Allee IR energy is liad reaching the dtr by presse wavelength le Ths the ‘sorption of energy ean be atibuted ony sul deide ‘war coscnaion fs properioclohe change nen st The deter One cell is sued th a reference apd ¢ ‘meajrementchanter. Toa slr as sulfur date i de 4. Sininennce and Use “4. Sal par of he inate nly of ol and coke coal prepanon snd caning, auton of penal sal ‘mistons from coal and coke comtuion or conversion process an evleton of ol and coke quay a laion ental speciation, aswell frente paps 143 The comptency of lborois with respect owe of ts sand ean be esublsbed dough reference to Price pra 5. Sample 51 Palverize he sample pas No 60 250m sev and ‘nix homughiy ie cconace With Practice D2013 or Practice Dae 52 Amiyze a separate prion of te analysis sample for smisre content in accordance wits Test Method DBI, oe [EVSt2 or ISO. 11722 for ealclaon 10 ober than the ‘edt tasi, 153 Procedures fo escalating a-Si slr values otined fom the amas sample oo bes re esrbed In Prices DSIT5 and S80 6. Apparatas Combustion Method A (135°C) 61 Measurement Eauippa 10 combust the sampler deerbed in 81 (See Fe I (62 Tube Femace—Capbl of eating he ot 06 or oter surice of te combustion ibe, or bath (tates 1350. Ws nomaly heed elaceicly sing reitnce rol = ‘essa wie oF maghdewim dsiie ements. Spec linesions cn vary wih manufrs ds {3 Combustion TaeMade of multe, poresnozeon wit rovson for routing the ater pode by combtion through tena ell The abe may ve a boat stop mae tf eclted ceramics ested 138°C tha serves om Pete the conbusion of ur conning mis {4 Sample Combustion Bots, made of ro-fee meal aod of convenient sine sable forthe diane of he (65 Boat Pllr—Where rogue, a rol fs etext rer with a bent or disk endo inet sd remove bots fom he combution tite, 66 Ralance—A wnt sloe lnc ra lane iterated seth he instrens, with resolton of a est 15 relative (fhe es portion mas Qi vazs0—14 Combustion Method 8 (180°C) 6:1 Measurement Apparans—Ealpped © combust the sample as dese in"? (See Fig 2 (68 Tabe Furnace —Copsbe of heting he ol zone ooter sue ote conboson be, or bof (59) toat ast 130°C. Ieisnomally bese electra uigreutance wie Specie limesions can vary with musufoctae’s sig. 69 Conbuson Tabe—Madeof que with provisions for rotingte pac produc by combo ugh ened oi 610 Sample Combustion Boat—Isde ofan irons tn mated and convenient se ule forthe imerions of {he combustion ae 7 Reagents 1 Party of Reagents—Use reagent rte chen in al test, nla ther inne rnened that legen fern the specications ofthe Commits on Avalale Reagents of the Areca, Chemical Society, whee sich ‘pecitcalons ae avalable* Oter grades canbe ed, pro- ‘ies a serie the eget of sey igh ‘ity peri is se witout Tseng the scary of he feteninaion 112 Mops Perclorate

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