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Q. Y. Lu & C. H. Wong
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detectability of these defects by NDT techniques are assessed. The applicability of each NDT
technique for different categories of AM process is discussed. The categories of AM are, namely,
material extrusion, powder bed fusion, vat photopolymerisation, material jetting, binder jetting,
sheet lamination, and directed energy deposition.
include visual inspection, liquid penetrant testing, mag- than 0.25 inches can be detected through magnification.
netic particle testing, eddy current testing, ultrasonic The sensitivity then varies with the type of equipment
testing, and radiography. Some of these techniques used (Matzkanin 2006).
including visual inspection, and ultrasonic testing can
also be used as in situ inspection NDT methods. 2.1.2. Advantages and disadvantages
Visual inspection can be applied to systems of any size.
From large systems, such as the aircraft skin, to small
2.1. Visual inspection
electrical circuitries, they can all be examined visually
Visual inspection is the most extensively used technique before deciding if further tests are required. Visual
among all the non-destructive tests (Allgaier et al. 1993). inspection systems including laptop-based systems and
It can be performed quickly, is simple, applies to most borescopes are field portable, and suitable for remote
specimens, and is typically low in cost. Visual inspection and field inspection applications. The relative cost of
often serves as a pre-inspection technique to ascertain inspection for visual inspection is low as compared to
the accuracy of the component’s fabrication, before it other methods, ranging from nothing to a moderate
is examined using other NDT techniques (Craig 2007). price (Smith 1991, Matzkanin 2006).
The basic principle governing visual NDT is based on Visual inspection is restricted to surface defects detec-
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the illumination of the specimen with light, which is tion. Internal and inaccessible regions of the test speci-
usually in the visible light region of the electromagnetic men cannot be visually examined. As this inspection
spectrum. The specimen is then examined with eye or technique is subjective, and the visual perception
light sensitive optical aids. The equipment required for across individuals varies, training for the inspectors is
visual inspection is very simple. However, ample illumi- essential. In addition, vision testing of the inspection
nation is critical. The amount of light falling upon the requiring examinations of the eye is compulsory (Smith
specimen can be quantified with a light meter. The 1991, Craig 2007).
surface of the test specimen should be cleaned before
inspection is carried out (Matzkanin 2006). 2.1.3. Applications of visual inspection in AM
The eye is the most invaluable NDT tool for visual Visual inspection has been integrated as part of the
inspection due to its exceptional visual perception, inspection system in some AM technologies. One
where it can assess visual characteristics and identify example is the Realizer 50, a desktop machine with selec-
different types of defect. It can also carry out accurate tive laser melting (SLM) technology, by ReaLizer GmbH
inspections on the size, shape, colour, depth, brightness, (ReaLizer GmbH 2012). The device is mainly applied in
contrast, and texture of the test specimen. Mechanical the dentistry industry for the manufacturing of crown
and or optical aids may be required for visual inspection. and bridge frameworks, and brackets made of cobalt
Mechanical aids include apparatus such as callipers and chrome. The process chamber of the machine is
micrometres. Optical aids are used when direct viewing equipped with a microscope for visual inspection
of the test specimen is not possible. The equipment during the printing of parts (Gebhardt et al. 2010).
ranges from simple mirrors to intricate devices, such as CassaMobile has successfully developed a prototype
microscopes and borescopes (Matzkanin 2006). material extrusion machine for local and versatile pro-
duction of highly customised parts in response to
2.1.1. Types of defect detectable and sensitivity improve adaptation to customers’ requirements for local
Cracks, holes, corrosion, blisters, and impact damage are fabrication solutions (CassaMobile 2013). The capability
some of the discontinuities that visual inspection can to identify part failures during the primary phase of man-
detect (Allgaier et al. 1993). Possible sources of mechan- ufacturing signifies the possibility to prevent premature
ical fragility such as sharp notches, and the presence or in-service failure of the part. The prototype is based on
absence of oxide film on the specimen’s surface can an in situ monitoring concept whereby images of the
also be identified. In general, defects that are surface layers captured by an optical camera during printing are
breaking or causes deformation at the surface are detect- compared against sliced reference images. The quality
able (Matzkanin 2006). of the printed part is quantified by identifying the pres-
The minimum size of defects that the human eye can ence of any deviation, if any, within an established toler-
distinguish is approximately 0.25 inches. The permitted ance between the captured and reference image
working period for a human inspector should be (Johnson et al. 2016). After the inspection of a given
limited to two hours on a continuous basis as errors layer, the printing process continues before another
may arise due to weakened visual discrimination and inspection is prompted. A live feedback is provided to
reliability. With the use of optical aids, defects smaller the operator regarding the quality of the printed part,
VIRTUAL AND PHYSICAL PROTOTYPING 3
and inspection can be activated at different rates. An voids was examined for thin wall features, and
appropriate selection of camera, lens, and lighting is warpage of 45° overhangs (Johnson et al. 2011).
necessary for the visual inspection of the captured This NDT technique is suitable for the detection of
images (Johnson et al. 2016). surface discontinues of additively manufactured parts.
Armillotta has employed the use of visual inspection It can be employed during the printing process, and as
in the assessment of surface quality on textured FDM a post-process inspection technique for surveying the
prototypes (Armillotta 2006). As the stair-stepping quality of parts (Craeghs et al. 2011). There is no limit-
effect is ineluctable due to the layered manufacturing ation on the type of material and the part’s size for
principle in AM, it is a main concern in relation to the inspection. However, the detection of subsurface
surface quality of textured prototypes. Visual inspection defects is not possible with visual inspection. It can be
has been performed at two levels for examination of used as an inspection technique to assess the extent of
the surface quality of FDM prototypes. Firstly, the discontinuities formation before further investigation
texture appearance is verified against the reference can be performed using NDT techniques that are
shape. Secondly, optical microscopy provides a more capable of distinguishing subsurface defects.
detailed view for inspection, allowing investigation on
the possible sources of process constraints, and to
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detect the presence of local defects (Armillotta 2006). 2.2. Liquid penetrant testing
This aids in the investigation on the suitability of FDM
Liquid penetrant inspection is used to test for defects
technique to a direct fabrication of rapid prototypes
present at the surface of parts manufactured from non-
with textured surfaces.
porous materials, as illustrated in Figure 1(a). It employs
Visual inspection has also been used as a monitoring
the inherent accumulation of a fluid around a discontinu-
system for powder deposition process in SLM (Craeghs
ity to create noticeable indication of surface defects.
et al. 2011). A visual camera with focusing lens is
Capillary effects arising from surface tension due to
focused to the build platform to ensure an even distri-
cohesive force between the molecules of the liquid,
bution of the powder particles during each layer depo-
and wetting properties of the material cause the liquid
sition. Three light sources were present to provide
to penetrate the openings on the surface (Figure 1(b))
sufficient illumination to the powder bed. The reasons
(Boyes 2009).
for the degradation in the smoothness of the powder
The penetrating liquid, also known as the dye, is
bed include warping of parts due to high thermal stres-
usually either bright red (colour contrast) or fluorescent
ses during SLM printing, wear and damage of recoater
under ultraviolet (UV) light (brightness contrast) to ease
blade, and an insufficient amount of feed powder. With
visual inspection of defects. After the dye has penetrated
the aid of a visual camera and adequate lighting, these
into the surface cavities of the part, excess penetrant is
defects can be detected using simple image processing
removed before a thin layer of developer is applied as
algorithms. Craeghs et al. (2011) detected two types of
shown in Figure 1(c) and (d) respectively. The main
recoater defects with the visual inspection system. The
purpose of the developer is to enhance defect visibility.
first type of defect is due to wear of the recoater blade,
Visual inspection of the defect is then performed
resulting in small scratches distributed across the
(Figure 1(e)).
powder bed. The second type of defect is caused by
Penetrant inspection method is applicable on cer-
local damage of the recoater blade, leading to local
amics, plastics, moulded rubber, and glass. It is also suit-
deep scratches in the powder bed (Craeghs et al. 2011).
able for metals such as titanium, copper, aluminium, and
stainless steel (Federal Aviation Administration 2008).
2.1.4. Suitability of visual inspection for additively
manufactured parts 2.2.1. Types of defect detectable and sensitivity
Visual inspection is mainly employed during the prelimi- Penetrant inspection has the capability to detect discon-
nary part of the overall quality management system in tinuities such as fatigue cracks, shrinkage cracks, poros-
AM applications. Cookies printed using solid freeform ity, laps, and seams. It can also provide indication of a
fabrication technology were visually inspected for their lack of bonding between joined metals (Federal Aviation
geometric fidelity to determine the suitability of the Administration 2008).
recipe for thermally stable printable sugar cookies Sensitivity can be defined as the ability of the liquid
(Lipton et al. 2010). Benchmarking models produced by penetrant to reveal flaws in a material. In general,
FDM were also visually inspected for uniformity among cracks with width of approximately 5 µm can be
features printed. For example, the presence of core detected using visible dye penetrant while cracks with
4 Q. Y. LU AND C. H. WONG
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width ranging from 1 to 2 µm can be detected using flu- composition of the penetrant, making indications less
orescent penetrant (Raj et al. 2002). visible (Integrated Publishing 2017).
2.2.4. Suitability of liquid penetrant testing for 2.3.1. Types of defect detectable and sensitivity
additively manufactured parts Cracks, laps, inclusions, voids, seams, cold shuts, and
Without additional post-processing techniques, such as tears are the types of defect usually detected by mag-
machining and polishing, it is incompatible to use netic particle testing (Federal Aviation Administration
liquid penetrant testing on additively manufactured 2008).
metal parts for defects detection. This is primarily due The magnetic flux should be orientated perpendicu-
to the mismatch in operation principle of liquid pene- larly to the defect for maximum sensitivity. Hence, mag-
trant testing and the inherent surface finish of most netic flux must be induced in more than one direction
additively manufactured metal parts. Liquid penetrant since defects can exist at any angle to the major axis of
testing requires a smooth surface for testing, and is the part. Two magnetising set-ups, namely, longitudinal,
unsuitable with porous materials, while the surface and circular magnetisation should be performed for
finish of the additively manufactured metal parts from defect detection.
powder bed fusion and directed energy deposition pro- In longitudinal magnetisation, the magnetic field
cesses is rough. While it has been discussed that cracks induced is parallel to the long axis of the specimen, as
with width of approximately 5 µm can be detected illustrated in Figure 2(a). Defects that lie approximately
using visible dye penetrant, it may be a challenge for perpendicular to the axis of the part can be detected.
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additively manufactured parts, considering the rough In circular magnetisation, the magnetic field induced is
surface finish. concentric about and within the part, as illustrated in
Liquid penetrant testing is a surface defect detection Figure 2(b). Defects that lie approximately parallel to
technique; hence embedded defects present below the the axis of the part can be detected (Raj et al. 2002,
surface of the additively manufactured print part, such Federal Aviation Administration 2008).
as porosities are unidentifiable. Volumetric defects and In general, flaws which lie up to ±45° to the direction
delamination beneath the surface, which are the of the magnetic flux can be detected while flaws at less
common defects present in powder bed fusion pro- than ±30° to the direction of the magnetic flux are
cesses, such as SLM and electron beam melting (EBM) undetectable (Halmshaw 1987, Shull 2002). Incipient
produced parts will not be detected by this technique fatigue cracks and fine grinding cracks with sizes less
(Sames et al. 2016). than 0.02 mm deep and surface openings of one tenth
of that or less can be revealed by magnetic particle
testing (Raj et al. 2002). Detectability in magnetic particle
2.3. Magnetic particle testing
testing is dependent on the relation between the
Magnetic particle testing is used for inspection of ferro- defect’s surface opening and depth. Generally, a
magnetic materials, which encompass most iron, nickel, surface discontinuity with a depth that is at least five
and cobalt alloys. When a specimen is magnetised, times its width (opening) at the surface is detectable.
magnetic lines of force, also known as magnetic flux,
are predominately inside the ferromagnetic material.
The presence of a flaw in the specimen disturbs the 2.3.2. Advantages and disadvantages
flow of magnetic flux, resulting in local magnetic flux With almost no restrictions on the size and shape of the
leakage fields. The flaw essentially causes a sudden test specimen, magnetic particle testing is the most
local change in permeability, which is the ease with reliable technique for detecting surface discontinuities,
which a magnetic flux can be established in a mag- in particular, very shallow and fine cracks. In general,
netic circuit (Federal Aviation Administration 2008). results from magnetic particle testing are easy to inter-
The inspection of flaws in magnetic particle testing is pret and the equipment is simple to operate. This tech-
dependent on the detection of this local magnetic nique is capable of defect identification even for
flux leakage field. defects filled with foreign matter or if the specimen is
When fine magnetic particles are sprinkled coated with nonmagnetic painting and plating. Magnetic
onto surface of the magnetised specimen, they particle testing is a relatively low-cost method and the
accumulate at the flaw sites, creating a visual pattern test procedures can be fully automated (Shull 2002).
estimating the shape and size of the defect The major disadvantage of magnetic particle testing is
(Halmshaw 1987). In the case of a subsurface defect, its exclusiveness to ferromagnetic materials. It cannot be
a less sharply defined indication is observed since the used to test parts of nonferrous materials such as alu-
amount of flux leakage is lesser for discontinuities not minium and titanium. In addition, only surface and sub-
open to the surface (Federal Aviation Administration surface defects can be identified, providing no
2008). indication on the quality of the bulk or internal attributes
6 Q. Y. LU AND C. H. WONG
Figure 2. Effect of magnetic flux direction on defect indication in (a) longitudinal and (b) circular magnetisation.
of the part. During testing, local heating and burning ferromagnetic materials, restricting the breadth of appli-
may exist at electrode contact points, damaging the cability of this testing technique. The suitability of mag-
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specimen. Demagnetisation of the part, which is required netic particle testing for ferromagnetic material based
at the end of the test if it is to be returned to service, is alloys is further complicated by the interaction of
often time consuming. This is to avoid the accumulation various factors. For instance, the extent of magnetism
of filings and grindings in the part during operation of inconel 718 is dependent on the exact nickel and
(Sharratt 2015). iron content, the working temperature, and the limit of
magnetic susceptibility permitted for a given application
2.3.3. Applications of magnetic particle testing in (Goldberg et al. 1990).
AM As mentioned in Section 2.3.2, demagnetisation of the
There is limited research on the direct use of magnetic material is required after inspection for safety concerns,
particle testing on additively manufactured parts. AM which introduces post cleaning effort and increases the
has been widely adopted in the aerospace industry overall inspection time. Hence, this technique may not
throughout all processes and functions; from design con- be suitable as a rapid inspection method.
ceptualisation to near-end-of-life repairs (Hiemenz 2014).
High-performance titanium alloys, in particular, Ti-6Al-4V,
is favoured for the manufacturing of advanced aerospace 2.4. Eddy current testing
structures such as engine parts (Inagaki et al. 2014, Eddy current testing is based on Faraday’s law of electro-
Uhlmann et al. 2015). As a non-ferromagnetic material, magnetic induction and defined as oscillating electrical
this restricts the application of magnetic particle testing. currents induced in a conductive material due to electro-
magnetic induction, by an alternating magnetic field
2.3.4. Suitability of magnetic particle testing for (García-Martín et al. 2011). An alternating current,
additively manufactured parts usually with frequency ranging from 1 to 2 kHz, flows
The major drawback of magnetic particle testing is its through a primary (excitation) coil to produce an alter-
applicability to only ferromagnetic materials, which has nating (primary) magnetic field as shown in Figure 3(a).
accounted for the sparse research of this technique on When the primary coil is in close proximity to the electri-
additively manufactured parts. The commonly used cal conducting surface of a metallic material, an eddy
materials in AM are categorised in Table 1. As illustrated current is induced in the material due to electromagnetic
in Table 1, only nickel and cobalt based alloys are induction as illustrated in Figure 3(b). The presence of
Figure 3. Probe response (a) in the absence of conductive material (b) in the presence of conductive material.
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defects in the material causes perturbation to the flow of 2.4.2. Advantages and disadvantages
eddy current, which in turn, produces a secondary mag- A major advantage of eddy current testing over liquid
netic field that opposes the primary field. This reduction penetrant, ultrasonic and magnetic particle techniques
in the net magnetic field – primary and secondary, is lies in it being a non-contacting method, which
tracked by the pickup (receiver) coil (Raj et al. 2002). enables automated high-speed assessment. In addition,
The electrical conductivity, magnetic permeability, surface preparation of the test specimen is not required
and geometry of the material are the main drivers when employing this technique. Eddy current testing is
affecting the magnitude of the eddy currents, and one of the few inspection techniques that are suitable
hence of the secondary field. For an ideal conductor, for high-temperature applications (Shull 2002). In the air-
there will be a complete cancellation between the craft industry, this technique can be used to measure the
primary and secondary field. Response signals are rep- conductivity of heat treated aluminium components in
resented in a range of formats, all of which indicates quantifying the hardness and tensile strength of the
impedance changes in the receiver coil. In many appli- part. Measurements can be taken during heat treatment
cation-specific systems, changes in the amplitude of instead of after, offering more information about the
the electromotive force are computed while the process (Jochen et al. 2003).
results reflect the parameters of interest, such as the The main limitation of eddy current testing is that only
thickness of the coating (Shull 2002). electrically conductive materials can be tested (Shull
2002). The probe used in eddy current testing does not
solely respond to the desired material characteristics
2.4.1. Types of defect detectable and sensitivity
such as discontinuities and conductivity, but also
Conductive specimens with defects such as cracks and
detects unwanted signals related to conductivity and
inclusions, which cause a change in the output impe-
magnetic permeability, leading to increased complexity
dance, are detectable by eddy current testing. Surface
in results interpretation. Hence, sophisticated algorithms
and subsurface corrosion can be distinguished. Variation
and professional operator trainings are required to segre-
in the thickness of coating can be investigated based on
gate the desired and unwanted signals. This technique
the differences in conductivity between the conductive
can only detect discontinuities that are positioned per-
specimen and the coating. This technique does not
pendicular to the inspected surface (Shull 2002).
require the removal of surface coatings such as paint
and anodised films for inspection (Federal Aviation 2.4.3. Applications of eddy current testing in AM
Administration 2008). AM techniques are capable of printing a wide range of
The sensitivity of discontinuity detection is dependent materials, which include both metallic and non-metallic
on the material, the type of defect and its orientation, the materials (Wong and Hernandez 2012). As the inherent
depth of the defect, and the surface quality of the use of eddy current testing is on electrically conductive
material. Eddy current testing can be used to inspect materials, parts fabricated from biomaterials, polymeric,
conductive parts of thickness up to 6 mm with adequate and ceramic materials are not suitable for this NDT
sensitivity (Raj et al. 2002). technique.
8 Q. Y. LU AND C. H. WONG
Multi-layer metallic structures are commonly Additively manufactured parts have surface roughness
inspected by eddy current tests for the detection of in the range of 1.6–25 µm while parts produced from
cracks and corrosion. Eddy current testing is able to die casting and hot forging have values between 3.2
examine different levels of material’s depth based on and 6.4 µm, and 6.4 and 13 µm, respectively (Ippolito
the frequency of the induction coil. Despite the limited et al. 1995). The consistently higher surface roughness
references of eddy current applied to AM, it is worth values for additively manufactured parts is attributed
noting the indications to its application in this area. to the inherent staircase effect due to layer-by-layer
NASA has been actively engaging in AM activities. At deposition principle present in most AM processes
the Johnson Space Centre, manufacturing and qualifica- (Grimm et al. 2015).
tion of laser engineered net shaping (LENS) and electron Eddy current testing is valid for only electrically con-
beam freeform (EBF) components for manned space ducting materials, which include metals. The AM tech-
flight applications, which include in-space manufactur- nologies suitable for metal printing are the powder
ing, have been carried out. NDT methods such as con- bed fusion processes which produce parts with inher-
ventional ultrasonic and eddy current testing have ently higher surface roughness due to the aperiodic
been applied to EBF components (Albakri et al. 2015). profile caused by random powder distribution (Grimm
Additively manufactured components are expected to et al. 2015). Other testing techniques can be used in
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produce similar results to conventional metal com- addition to eddy current testing to obtain more accu-
ponents in eddy current testing. The success rate of rate results for defects detection in additively manufac-
detecting critical defects is largely dependent on the tured metallic parts.
surface finish and grain structure of the test component
subjected to eddy current testing. In a study conducted
2.5. Ultrasonic testing
by Albakri et al. (2015), the inspection of an inconel
Pogo-Z baffle produced a large amount of background Ultrasonic inspection is one of the most established NDT
noise, illustrating that the holes were not processed techniques as it is applicable to most materials. The fun-
appropriately. Without post-processing, the surface damental understanding of ultrasonic testing is based on
finish was not suitable for the test and had to be comple- the transformation of a voltage pulse into an ultrasonic
tely smoothened to achieve a good baseline signal pulse by a transducer. The transducer is positioned on
(Albakri et al. 2015). Areas of the component that were the specimen and transmitted pulses (ultrasonic waves)
machined smoothly had lower degree of background travel through the object. Ultrasonic waves with frequen-
noise. cies ranging from 1 to 10 MHz are usually used. As the
Ekrami et al. (2011) employed radiography and sup- ultrasonic waves are reflected by inhomogeneities,
plementary techniques including eddy current testing evaluation of the transmitted and reflected energies
to characterise fatigue crack growth, and subsurface can be used to relate to the material’s integrity
cracks at various angles of EBF produced 316 stainless (Schmerr 2016b).
steel specimens. Three basic methods of ultrasonic inspection include
It has also been encouraging to note that eddy the normal incident pulse-echo, angle beam pulse-
current testing can be integrated into in-process moni- echo and through-transmission method. In all cases,
toring of powder bed fusion processes, as seen from a the signals captured are transformed back into electrical
patent application by MTU Aerospace (Bamberg et al. pulses and are displayed on a cathode ray tube (CRT).
2014). Eddy current testing can potentially be used to Figure 4 shows the block diagram of a simple normal
evaluate layer properties of metal printed parts such as incident pulse-echo set-up and the pulse-echo display
bonding defects within the layer through the use of associated to flaw detection, respectively. A couplant,
eddy current sensors (Satzger et al. 2013). usually grease or oil, is applied to the specimen to
couple the transmission of ultrasonic energy between
2.4.4. Suitability of eddy current testing for the face of the transducer and surface of the specimen
additively manufactured parts (Schmerr 2016b). When the transmitted ultrasonic
The effectiveness and accuracy of eddy current testing energy encounters a discontinuity in the specimen, a
on additively manufactured parts may be reduced as fraction of the energy will be reflected back and the
the surface finish and roughness of the part will cause remaining fraction propagates through the material.
unwanted perturbation to the flow of eddy current. The reflected ultrasonic energy captured by the probe
The surface finish of additively manufactured parts is is the source of defect detection shown on the CRT, as
generally inferior to those produced through conven- illustrated in Figure 4. Regions of the specimen that are
tional processes such as die casting and hot forging. free from defects will allow the complete transmission
VIRTUAL AND PHYSICAL PROTOTYPING 9
opposite sides of the specimen must be accessible (Raj the surface. Palanisamy et al. (2007) tested aluminium
et al. 2002). sample castings using ultrasound with frequencies
Ultrasonic testing, like other NDT methods, has some ranging from 5 to 20 MHz. Results have shown that the
disadvantages. Obtaining quantitative information of the defect signal amplitude decreases drastically when the
specimen and the accurate interpretation of results surface roughness of the sample castings is above
require a skilled operator. Typically, planar cracks with 50 μm. For surface roughness above 150 μm, the
length that lie parallel to the direction of ultrasonic defect signal amplitude becomes negligible for all fre-
wave travel are not detectable. In addition, ultrasonic quencies (Palanisamy et al. 2007).
testing equipment can be expensive (Shull 2002). Additively manufactured parts have a nominal surface
roughness on the order of 10–20 μm for powder bed
2.5.3. Applications of ultrasonic testing in AM processes and less than 80 μm for powder feed pro-
Ultrasonic testing has been proven to be an efficient cesses (Sharratt 2015). Hence, it can be predicted that
technique for the detection of discontinuities and parts printed from powder feed processes, such as
measurement of mechanical properties of material refer- LENS, will encounter similar difficulties in ultrasonic
ences (Lawley 2015, Sharratt 2015). It has the potential testing as for highly rough castings. Large amount of
for monitoring and testing of defects present as each noise and appreciable reduction in the defect signal
layer is being built during powder bed fusion processes. amplitude will be observed. Generally, ultrasonic
The use of ultrasonic testing has been examined sub- testing is more suitable for parts manufactured from
stantially for castings. It has, however, been hindered by powder bed processes as they have lower surface
the surface roughness for the detection of defects near roughness.
VIRTUAL AND PHYSICAL PROTOTYPING 11
Intelligent Optical Systems, Inc. has embarked on laser ultrasonic system has proven its potential for detec-
developing an in situ layer-by-layer part qualification tion of flaws during manufacturing (Cerniglia et al. 2015).
process using laser ultrasonic testing. During the build
process, each layer will be examined in real time and 2.5.4. Suitability of ultrasonic testing for additively
completed parts will not require any further tests (Navy manufactured parts
STTR 2015a, Navy STTR 2015b). One of the main challenges currently faced in the AM
At NASA’s Johnson Space Centre, ultrasonic testing community, is the lack of feedback sensors and measure-
has been used for examining embedded porosities and ment techniques for obtaining the necessary data for
flawed deposition layers in 2219 aluminium EBF parts. qualification and certification of additively manufactured
Illustrations can be found in (Waller et al. 2014). parts. Developing NDT techniques specialised for in situ
Lawley (2015) conducted a study on the feature monitoring of the printing process can rectify and
detection capabilities of ultrasonic testing on additively reduce defects produced through feedback control
manufactured parts. Two separate experiments were systems.
carried out. In the first experiment, 3D printed test speci- Laser ultrasonic testing, being a non-contact measure-
mens were designed with varying thickness and the ment technique, is a potential candidate for in situ
same geometrical features such as sunk in square and process monitoring of metallic AM processes (Bamberg
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rectangle shapes in varying sizes, on the back surface. et al. 2015, Everton et al. 2016). A laser pulse is focused
The smallest surface feature designed had a measure- at the material’s surface and an ultrasonic pulse is gener-
ment of 1 mm. Through the use of a C-scan, the effect ated to disseminate into the material. Rayleigh wave,
of sample thickness on the detection capabilities of ultra- which is a surface wave, is the dominant wave mode pro-
sonic testing could be validated. C-scan results have duced. Longitudinal and shear waves are also generated.
shown that shape features with sizes of 5 mm or greater In the presence of subsurface defects, diffraction and
are detectable, while parts of the features were detectable scattering of the Rayleigh wave occurs, and when
for sizes less than 5 mm (Lawley 2015). The latter is most returned to a receiver, it comprises of shear waves and
likely due to rough, layered surface that is inherent in mode converted compressional waves. The returned
additively manufactured specimens. Lawley (2015) has signal, which is received by the detection laser, is pro-
successfully demonstrated the detection of surface fea- cessed for further investigation on the details of the
tures on the back of test specimens using ultrasonic defects (Everton et al. 2015).
C-scan. The second experiment involved studying the This technique allows the inspection of inaccessible
internal features of test specimens. Intentional defects of areas and on curved surfaces, and can be applied at elev-
rectangular boxes with different sizes were introduced ated temperatures. Everton et al. (2015) have successfully
into the test specimens. From the results of the C-scan, used laser ultrasonic testing for holes detection with
it has been concluded that an internal feature of size diameter ranging between 0.563 and 1.265 mm, in tita-
as small as 10.9 mm2 is detectable at a distance of nium alloy Ti-6Al-4V blocks produced by laser-based
1.27 mm from the external surface of the specimen. powder bed fusion process through B-scans. Future
Cerniglia et al. (2015) explored the use of laser ultra- work in further optimisation of the laser ultrasonic
sonic for in-line inspection of laser powder deposition testing system to significantly reduce the scanning
process. A proof-of-concept laser system prototype was time will grant in situ process monitoring achievable.
constructed. Intentional defects were fabricated in stan- The application of this NDT technique allows the examin-
dard geometries to evaluate the sensitivity of this tech- ation of defect information during each build layer,
nique for defect identification. Holes with varying which accentuates the processing errors, and enables
diameters and depths below the surface of inconel speci- real-time alteration of processing parameters. Laser ultra-
mens were created. Results have confirmed the feasi- sonic testing presents opportunities for the in situ moni-
bility of utilising laser ultrasonic for detecting defects of toring of AM processes with improved part quality.
micro sizes in inconel specimens. Minimum defect size Rieder et al. (2014) have demonstrated the possibility
of 0.1 mm in diameter near the surface and larger of obtaining online ultrasonic measurements by ultra-
defect of up to 0.8 mm deep can be detected. As addi- sonic testing during the SLM process of cylindrical speci-
tively manufactured parts can be complicated in geome- mens. The set-up consisted of the ultrasonic probe fixed
try, it is challenging to use conventional NDT techniques to the lower side of the build platform. Acquisition of
for flaw detection. The quality of components produced data is executed layer-by-layer, and the ultrasonic
by laser powder deposition is commonly evaluated by signals were stored for further offline processing. The
destructive testing or by X-ray computed tomography presence of a void is detected through A- and C-scan.
(CT) after fabrication. Successful demonstration of the The current inspection system can acquire data for up
12 Q. Y. LU AND C. H. WONG
to eight hours. The inspection system can be refined to a recording medium (film). The specimen is placed
examine parts with complex geometries (Rieder et al. between the radiation source and a film. The projection
2014). of X-rays onto the specimen produces white areas on the
Both studies have established confidence in the use of film in regions where the X-ray has high absorption
ultrasonic testing as a NDT technique for in situ and post- (without defects), and gray areas in regions where the
process defect inspection of additively manufactured X-ray has low absorption (with defects) (Shull 2002).
parts. It should be noted that conventional ultrasonic The detection of defects can then be achieved through
testing requires contact between the probe and the inspection of the film density (darkness).
surface of the material. Hence, the surface finish and CT is a way to recover the 3D representation of a com-
roughness of the printed part play an important role in ponent. A stack of projection radiographs is captured of
ensuring the quality of the ultrasonic signals received the component at various angles. The reconstruction of
for post-process NDT inspection. the component from these radiographs is achieved
through computer algorithms. Hundreds to thousands
2.6. Radiography of digital project radiographs are usually necessary to
obtain a reconstructed component with high fidelity
The motivation in the employment of radiography is to (Shull 2002).
demonstrate the presence and nature of flaws in the
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A highly experienced operator is required for the design stage (Witvrouw 2017). Results from X-ray CT
analysis and interpretation of the radiograph. Recog- are used to compare against the images captured by
nition of flaws, however, can often be achieved with an optical system during SLM for process optimisation
ease for beginners even without the skills of a trained (Witvrouw 2017). This aids in improving part precision
specialist. Safety issues are of major concern as the and accuracy of the features.
necessity for a high voltage needed for the generation du Plessis et al. (2015) applied the use of X-ray micro
of X-rays can be dangerous. In addition, heavy shielding CT to the NDT of an additively manufactured Ti-6Al-4V
materials must be used (Shull 2002). component with a complex geometry. The illustrations
Radiography has its constraint in the detection of can be found in du Plessis et al. (2015). Defects formed
cracks. A crack that is embedded in the material will between layers of print by direct metal laser sintering
not be detected by this technique. For a crack to affect process due to imperfect melting were characterised
the transmission of radiation, a local absence of material by this technique. Results from X-ray micro CT scanning
resulting from an opening must exist. Furthermore, the revealed that the average porosity in the components
crack must also be parallel to the direction of radiation decreased from 0.005% to 0.002% before and after HIP
travel or be sufficiently large for it to be registered on treatment.
the radiograph (Shull 2002). This optimum orientation Several works have been published on the use of X-
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is contrary to ultrasonic testing where reflections from ray CT for quality control and measurement of internal
a crack positioned perpendicular the wave path will features and defects of additively manufactured com-
maximise the signal. In radiography testing, the size of ponents (Palmer and Jones 2016, Pavan et al. 2016).
the discontinuity must be at least 2% of the thickness
of the material for it to be detected (Raj et al. 2002). 2.6.4. Suitability of radiography for additively
X-ray machines, as compared to other NDT techniques, manufactured parts
are very costly. The inspection of thick components is One of the underlying reasons for the advent of AM is its
time consuming. This is predominantly due to the ability to manufacture complex structures in a single
requirement of heavy shielding to ensure the safety of print as compared to conventional methods, which
the operator. have limited success. Structures with complex geome-
tries often feature hollow spaces or undercuts (EOS
2.6.3. Applications of radiography in AM e-Manufacturing Solutions 2017). Fabrication of parts
The standard radiography and CT NDT techniques are by AM technologies provide a designer with the
both of interest in the AM field, with the latter being freedom to create structures with complex geometries
more appealing despite its longer computational and such as hollow metal cellular artefacts, and hip implant
imaging time. with lattice structures for improved osseointegration
CT carried out by NASA on adiabatic refrigerator com- (McCarthy and Williams 2012). X-ray micro CT is a suit-
ponent, nozzles, and injectors has exhibited its effective- able NDT technique for defect detection of parts with
ness in the detection of induced internal defects and complex shapes, without the need for any disassembly.
internal features that are inaccessible. In addition, CT There are, however, constraints on the use of this tech-
can be used to identify high-density inclusions in EBM nique. The size of the specimen which can be inspected
as-built Ti-6Al-4V specimens and to validate whether is limited by the size of the instrument’s sample holder
porosities are closed by hot isostatic pressing (HIP) which varies among machines (Texas Geosciences 2016).
post-processing. Hence, the characterisation and qualifi- Attenuation due to the interaction between the X-ray
cation of as-built additively manufactured components, and the specimen, accounted by photoelectric effect and
detection of internal flaws, examination of unreachable Compton scattering, is another issue for consideration.
features, and the affirmation on the effectiveness of For low X-ray energies of approximately 50–100 keV,
post-processing treatments are achievable by CT the photoelectric effect is the dominant attenuation
(Waller et al. 2014). mechanism. Attenuation is proportional to Z 3, where Z
X-ray CT has been employed in the quality control of is the atomic number of an atom in the attenuating
AM processes. In order for AM technologies to gain sig- material. At higher X-ray energies ranging from 5–10
nificant confidence from the market, parts produced MeV, Compton scatter is preeminent. Attenuation is pro-
have to be precise. Hence, production has to be robust portional to only Z (Ketcham and Carlson 2001). Hence,
whereby crucial parameters during printing can be con- materials with high atomic numbers, such as bone or
trolled, and the production has to be predictable, allow- metals, have significantly increased attenuation at
ing for effects such as part shrinkage after printing to be lower energies of X-ray which results in beam hardening
taken into consideration and compensated during the effects (Boas and Fleischmann 2012, NDT Resource
14 Q. Y. LU AND C. H. WONG
Center 2014). CT may not be able to provide accurate radiography, thermography, and acoustic emission
detection of defects in specimens with high atomic testing. Contact methods may not be efficient in the
numbers, such as stainless steel. In addition, the selection detection of surface defects due to the resolution of
of the right combination of parameters during material parts printed by material extrusion. X-ray CT is one of
scanning, which includes voltage, requires extensive the promising techniques to survey microstructural
training to train skilled operators. defects in additively manufactured parts. Precise infor-
CT is applicable to all specimens of any surface, shape, mation regarding the porous network induced by pro-
and material to a certain density and thickness that is cessing, amount of support material, and surface
penetrable with X-rays. It is the only NDT technique roughness can be acquired (Guessasma et al. 2015).
that allows the attainment of a complete model with
both the internal and external surface of a specimen.
3.2. Powder bed fusion
CT scans are uninfluenced by material characteristics
such as dark, reflective or transparent surfaces, and Powder bed fusion process employs the use of thermal
shaded areas, which may cause hindrance with other energy to selectively fuse region of a powder bed
3D scanning methods (Noel 2008). Another advantage (ASTM International 2015). The thermal source can be
of applying CT to additively manufactured parts is the either a laser or an electron beam. Powder is sintered
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available option to directly compare the 3D CT recon- or melted, layer-by-layer. The resolution of the printed
struction models to CAD models to display any part is dependent on the powder size. The common
peculiarities or commonalities in measurements and materials used in powder bed fusion include nylon,
densities (Noel 2008). 316L stainless steel and titanium Ti-6-Al-4V (Loughbor-
ough University 2017c).
Liquid penetrant testing is applicable; given the con-
3. NDT methods for different categories of AM
dition that post-processing is performed before inspec-
AM has seven categories of technologies, namely, tion. Eddy current testing is suitable for parts made
material extrusion, powder bed fusion, vat photopoly- from electrically conductive materials such as 316L stain-
merisation, material jetting, binder jetting, sheet lami- less steel. Radiography is useful in examining the surface
nation, and directed energy deposition (ASTM and internal defects after printing of the part. Visual
International 2015, Gao et al. 2015). inspection, laser ultrasonic testing, and thermography
have been discussed as potential candidates for in situ
process monitoring and quality control of parts fabri-
3.1. Material extrusion
cated by powder bed fusion.
In material extrusion, the material is dispensed through a
nozzle where it will be heated before being deposited in
3.3. Vat photopolymerisation
a layer-by-layer fashion (ASTM International 2015). The
materials used in material extrusion are usually thermo- Liquid photopolymer in a vat is selectively cured by light-
plastics such as ABS, and nylon, in a spool of filament activated polymerisation during vat photopolymerisa-
(Stratasys 2017). The resolution of the printed part is tion. UV light is used to cure the vat of liquid photopoly-
highly dependent on the geometry of the nozzle and mer resin where required. The build platform lowers
the layer thickness. Typical layer thickness ranges from from the top of the resin vat by the layer thickness
0.178 to 0.356 mm (Loughborough University 2017a). after each new layer is cured (Gibson et al. 2015c). Poly-
Surface defects including the staircase and chordal mers are used as materials for vat photopolymerisation.
effect often arise in parts fabricated by incremental Parts produced have high level of accuracy and a good
addition of material (Van Weeren et al. 1995). The surface finish as compared other AM technologies.
former is caused by the slicing procedure of fabrication, The surface roughness of the produced part is depen-
which can be minimised by adjusting the thickness of dent on the type of technology used. Parts produced
the slice, reducing the scale of error. The latter is due from SLA, under the category of vat photopolymerisa-
to the STL file format usually used in AM. Surfaces are tion, have significantly better surface roughness than
approximated as a mesh of triangles in the STL file those from powder bed fusion processes, such as SLM.
format. Curvilinear surfaces are approximated as a Both techniques use focused laser beams for the solidifi-
chain of linear segments, resulting in a non-smooth cation of the build material (Antu 2015). The laser spot
surface of the part (Van Weeren et al. 1995). size used in these techniques is one of the main factors
Appropriate NDT techniques for the inspection of that define the print resolution (Partanen 1996). SLA,
parts include visual inspection, laser ultrasonic testing, which employs the use of an UV laser to selectively
VIRTUAL AND PHYSICAL PROTOTYPING 15
cure a vat of liquid photopolymer resin to build a part, are commonly used in binder jetting; water-based
has a minimum laser spot size (diameter) of 75 µm binders, phosphoric acid-based and citric acid-based
(Sager et al. 2003, 3D Systems 2017). SLM, which binders, and polymer solution binders (Shirazi et al.
employs the use of an infrared laser to selectively scan 2015).
a powder bed, has a laser spot size typically in the Snelling et al. (2014) utilised binder jetting technology
range of 80–115 µm (Rombouts et al. 2006, SLM Sol- in the direct printing of patternless sand casting moulds.
utions 2017). The smaller laser spot size for lasers used One of the common issues in such application is the gas
in SLA in comparison to SLM is one of the main generation when binders are exposed to high tempera-
reasons accounting for the lower surface roughness of ture of the molten metal, generating an excessive
SLA printed parts. amount of gas producing defects in castings (Snelling
Liquid penetrant testing can be applied as an inspec- et al. 2014). X-ray CT would be particularly useful for
tion technique as the parts have a smooth surface finish. the inspection of internal defects in the printed part.
NDT techniques that are not restricted to ferromagnetic Other NDT techniques may be applied to defect inspec-
or electrically conductive materials can be applied as tion of binder jetting printed parts, depending on the
post-process inspection methods for fabricated parts. type of material used.
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Q. Y. LU AND C. H. WONG
Type of Sensitivity for general applications, not Challenges for inspecting additively
NDT technique inspection limited to AM Applicable AM process manufactured parts References related to AM
Visual inspection Surface . Minimum size of discontinuities that . Material extrusion . The use of optical aids is often required to Armillotta (2006), Gebhardt et al. (2010), Lipton et al.
human eye can distinguish is . Powder bed fusion monitor AM processes (2010), Craeghs et al. (2011), Johnson et al. (2011),
approximately 0.25 inches . Vat photopolymerisation ReaLizer GmbH (2012), CassaMobile (2013), Johnson et al.
. Using optical aids, defects smaller . Material jetting (2016)
than 0.25 inches can be detected . Binder jetting
through magnification . Sheet lamination
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Liquid penetrant testing Surface . Cracks with width of approximately • Powder bed fusion . Prerequisite for testing is a relatively smooth Caiazzo et al. (2013), Waller et al. (2014), Waller et al.
5 µm can be detected using visible • Vat photopolymerisation examination surface (2015)
dye penetrant . Additional post-process machining and
. Cracks with width ranging from 1 µm polishing of parts required, which may close
to 2 µm can be detected using up or remove the surface flaws
fluorescent penetrant
Magnetic particle testing Surface . Flaws which lie up to ±45° to the . Powder bed fusion . Applicable to only ferromagnetic materials Goldberg et al. (1990), Hiemenz (2014), Inagaki et al.
direction of magnetic flux can be . Directed energy deposition . Among the commonly used materials in AM, (2014), Uhlmann et al. (2015)
detected only nickel and cobalt based alloys are
. Flaws at less than ±30° to the ferromagnetic materials, restricting the
direction of magnetic flux are breadth of applicability of this testing
undetectable technique
. Incipient fatigue cracks and fine
grinding cracks with sizes less than
0.02 mm deep and surface openings
of one tenth of that or less
Eddy current testing Surface . Dependent on material, type of . Powder bed fusion . Surface finish and roughness of the part will Ippolito et al. (1995), Ekrami et al. (2011), Wong and
defect and its orientation, depth of . Directed energy deposition cause unwanted perturbation to the flow of Hernandez (2012), Satzger et al. (2013), Bamberg et al.
the defect, and surface quality of eddy current (2014), Albakri et al. (2015), Grimm et al. (2015)
material . Post-processing of part is required to
smoothen the surface, in order to achieve a
good baseline signal
Ultrasonic testing Surface / . With the use of a particular frequency . Material extrusion . Large amount of noise and appreciable Palanisamy et al. (2007), Rieder et al. (2014), Waller et al.
subsurface probe, defect size of the order of half . Powder bed fusion reduction in the defect signal amplitude will (2014), Bamberg et al. (2015), Cerniglia et al. (2015),
the wavelength can be inspected . Vat photopolymerisation be observed for parts with rough surface Everton et al. (2015), Lawley (2015), Navy STTR (2015a),
. Material jetting finish Navy STTR (2015b), Sharratt (2015), Everton et al. (2016)
. Binder jetting
. Sheet lamination
. Directed energy deposition
Radiography Surface/ . The amount of exposure penetrating . Material extrusion . CT may not be able to provide accurate Ketcham and Carlson (2001), Noel (2008), Boas and
subsurface through the material is a crucial factor . Powder bed fusion detection of defects in specimens with high Fleischmann (2012), McCarthy and Williams (2012), NDT
. Vat photopolymerisation atomic numbers Resource Center (2014), Waller et al. (2014), du Plessis
. Material jetting et al. (2015), Palmer and Jones (2016), Pavan et al. (2016),
VIRTUAL AND PHYSICAL PROTOTYPING 17
Difficulty lies in recognition of the source that Wang et al. (2008), Yoon et al (2014), Everton et al. (2016)
complicates the calibration of infrared camera et al. (2013), Fedala et al. (2014), Krauss et al. (2014),
gases in gas-atomised powders. Lack-of-fusion defects
4. Conclusion
The broad temperature range of the melt
.
Directed energy deposition
AM processes.
Powder bed fusion
Material extrusion
Sheet lamination
Material jetting
Material jetting
Binder jetting
Binder jetting
Binder jetting
.
.
.
.
.
.
.
.
.
.
.
.
Surface
Successful detection of critical defects is highly depen- Boyes, W., 2009. Instrumentation reference book. Oxford:
dent on the surface finish and grain structure of the Butterworth-Heinemann.
Caiazzo, F., et al., 2013. Experimental analysis of selective laser
test component subjected to eddy current testing.
melting process for Ti-6Al-4V turbine blade manufacturing.
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No potential conflict of interest was reported by the authors. Symposium, Austin, TX, 212-226.
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