Old Alk Manual 51000-18

Cat. No.
51000-18
APA 6000™ Alkalinity Process Analyzer

Model 51000
Instrument Manual
© Hach Company, 1998, 1999. All rights reserved. Printed in the U.S.A. hm/dp 1/99 2ed
Rev1, 5/00
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Table of Contents
Trademarks of Hach Company ................................................................................................................................. 2

Certification ............................................................................................................................................................... 7
Safety Precautions .................................................................................................................................................... 9
Specifications .......................................................................................................................................................... 11
Operation ............................................................................................................................................................. 13
Section 1 Introduction ...................................................................................................................................... 15

1.1 How to Use this Manual .................................................................................................................................... 15
1.1.1 Overview of the Analyzer Setup .............................................................................................................. 15
1.2 Packing Lists ..................................................................................................................................................... 16
1.3 Location and Operating Environment................................................................................................................ 16
1.4 Instrument Overview ......................................................................................................................................... 16
1.4.1 General Description................................................................................................................................. 16
1.4.2 Instrument Components .......................................................................................................................... 17
1.4.3 The AquaTrend Interface ......................................................................................................................... 19
1.4.4 Alkalinity Reagent Kit............................................................................................................................... 23
1.4.5 Installation Kit .......................................................................................................................................... 24
1.4.6 Maintenance Kit....................................................................................................................................... 24
1.4.7 Tool Kit..................................................................................................................................................... 24
1.5 Theory of Operation .......................................................................................................................................... 25
1.6 Method of Analysis............................................................................................................................................ 26
1.7 Basic Single-sample APA 6000 Analyzer System............................................................................................. 26
1.8 Options and Add-ons for the APA 6000 Analyzer ............................................................................................. 26
Section 2 Startup ............................................................................................................................................... 27

2.1 Introduction ....................................................................................................................................................... 27
2.2 The AquaTrend.................................................................................................................................................. 27
2.2.1 The AquaTrend Keypad ........................................................................................................................... 27
2.2.2 The AquaTrend Display ........................................................................................................................... 29
2.2.3 Time and Date Settings ........................................................................................................................... 32
2.2.4 Changing the Date Format ...................................................................................................................... 34
2.2.5 Programmable Functions......................................................................................................................... 34
2.3 Outputs and Relays........................................................................................................................................... 40
2.3.1 Alarms ..................................................................................................................................................... 40
2.3.2 Sensor Warning Options ......................................................................................................................... 42
2.3.3 Recorders or Controllers ......................................................................................................................... 43
2.4 Sample Conditioning Setup .............................................................................................................................. 48
2.4.1 When to Use Sample Conditioning Setups ............................................................................................. 48
2.5 Changing Reagents and Standards .................................................................................................................. 51
2.5.1 Changing Reagents and the Cleaning Solution....................................................................................... 51
2.5.2 Changing the Standard Solutions............................................................................................................ 52
2.5.3 Setting Solution Levels ............................................................................................................................ 53
2.6 Replacing the Soda Lime in the Standard Solution Scrubbers ......................................................................... 54
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51000-18TOC.fm Table of Contents
Table of Contents
2.7 Starting Analyzer Operation.............................................................................................................................. 55

2.7.1 Adjusting Sample Flow ............................................................................................................................ 55
2.7.2 Priming the Analyzer ............................................................................................................................... 55
2.7.3 Setting Up the Auto-Calibration Schedule ............................................................................................... 57
2.7.4 Setting Up the Auto-Calibration Check Schedule .................................................................................... 58
2.7.5 Changing Calibration Check Warning Limits ........................................................................................... 59
2.7.6 Changing Calibration Check Recalibration Limits.................................................................................... 60
2.8 Instrument Clean Function Setup ..................................................................................................................... 61
2.9 Adding Sample Streams ................................................................................................................................... 62
2.9.1 Setting the Number of Sample Streams .................................................................................................. 62
2.9.2 Setting Up the Sample Sequence ........................................................................................................... 63
2.9.3 Selecting a Measurement Type ............................................................................................................... 64
2.9.4 Measurement to Channel Connections ................................................................................................... 65
Section 3 Normal Operation ............................................................................................................................ 69

3.1 Measurements .................................................................................................................................................. 69
3.2 Process Analysis............................................................................................................................................... 70
3.2.1 Viewing Process Analysis Data ............................................................................................................... 70
3.3 Grab Sample Analysis....................................................................................................................................... 73
3.3.1 Grab Sample History ............................................................................................................................... 74
3.4 Calibration Options............................................................................................................................................ 75
3.4.1 Manual Calibration................................................................................................................................... 75
3.4.2 Manual Calibration Check........................................................................................................................ 76
3.4.3 Viewing the Calibration History................................................................................................................ 77
3.4.4 Viewing the Calibration Check History .................................................................................................... 78
3.5 Alarm Log Review ............................................................................................................................................. 79
3.5.1 Clear Alarm Log....................................................................................................................................... 79
3.6 Cleaning the Instrument.................................................................................................................................... 80
3.7 Temperature Control ......................................................................................................................................... 81
3.8 Shutting the Analyzer Down (Off or Standby) ................................................................................................... 82
Maintenance ........................................................................................................................................................ 83
Section 4 Routine Operator Maintenance .................................................................................................... 85

4.1 Maintenance Kit ................................................................................................................................................ 85
4.2 Scheduled Maintenance ................................................................................................................................... 85
4.3 Reagent Consumption ...................................................................................................................................... 86
4.3.1 Changing Solutions ................................................................................................................................. 86
4.4 Replacing Autoburette Seals............................................................................................................................. 87
4.5 Maintaining the Valve Rotor and Stator............................................................................................................. 90
4.5.1 Replacing the Tubing ............................................................................................................................... 92
4.6 Cleaning the Mixer Module ............................................................................................................................... 95
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Table of Contents 51000-18TOC.fm
Table of Contents
Section 5 Warnings, Alarms, and Troubleshooting ................................................................................... 97

5.1 General Troubleshooting Procedure ................................................................................................................. 97
5.1.1 Check Alarm Log ..................................................................................................................................... 97
5.1.2 Check Solutions....................................................................................................................................... 97
5.1.3 Examine the Rotor Valve ......................................................................................................................... 97
5.1.4 Examine the Autoburette ......................................................................................................................... 98
5.1.5 Examine the Tubing and Fittings ............................................................................................................. 98
5.2 Specific Alarm/Warning Messages ................................................................................................................... 99
5.3 Diagnostics ..................................................................................................................................................... 104
5.3.1 Hold Outputs.......................................................................................................................................... 104
5.3.2 Internal Relay Test................................................................................................................................. 105
5.3.3 Internal Output Test ............................................................................................................................... 106
5.3.4 Default Calibration ................................................................................................................................. 107
5.3.5 Show Software Version Number............................................................................................................ 108
Installation ......................................................................................................................................................... 109
Section 6 Sample Conditioning .................................................................................................................... 111

6.1 Sample Conditioning ....................................................................................................................................... 112
6.1.1 Basic Clean Water Sample Conditioning............................................................................................... 112
6.2 Adding To or Changing the Basic Sample Conditioning.................................................................................. 112
6.2.1 Unfiltered Sample Bypass ..................................................................................................................... 112
6.2.2 Cleaning Submersible Sample Pumps Automatically............................................................................ 119
6.3 Installing Multiple Sample Streams ................................................................................................................. 122
Section 7 Hardware Installation.................................................................................................................... 123

7.1 Selecting a Location for the APA 6000 Analyzer ............................................................................................. 123
7.2 Mounting ......................................................................................................................................................... 124
7.2.1 Bench Mount ......................................................................................................................................... 124
7.2.2 Wall Mount............................................................................................................................................. 124
7.2.3 Panel Mount........................................................................................................................................... 124
7.3 Electrical Connections .................................................................................................................................... 128
7.3.1 Power Connections At the APA Analyzer............................................................................................... 130
7.3.2 Alarm Relay Connections ...................................................................................................................... 133
7.3.3 Recorder Output Connections ............................................................................................................... 134
7.3.4 Network Connections ............................................................................................................................ 136
7.4 Fuse Replacement .......................................................................................................................................... 145
7.5 Changing Modules .......................................................................................................................................... 146
7.6 Air Purge ......................................................................................................................................................... 147
7.7 Plumbing Installation ....................................................................................................................................... 147
7.7.1 Sample Tubing Installation..................................................................................................................... 148
7.7.2 Determining Sample Lag Time .............................................................................................................. 152
7.7.3 Drain Line Connection ........................................................................................................................... 152
7.7.4 Waste Disposal...................................................................................................................................... 154
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51000-18TOC.fm Table of Contents
Table of Contents
Section 8 Network Menu Configuration ..................................................................................................... 155

8.1 Using the APA With a Signal Output Module (SOM)....................................................................................... 155
8.1.1 Getting the SOM to Communicate With the APA 6000.......................................................................... 155
8.1.2 Verify SOM Connections ....................................................................................................................... 155
8.1.3 APA 6000 Menu Options for SOM Relays & Analog Outputs ................................................................ 155
8.2 Using an APA With an SIO Module ................................................................................................................. 156
8.2.1 Getting the SIO to Communicate With the APA 6000............................................................................ 156
8.2.2 Verify SIO Connection to Computer/Printer........................................................................................... 156
8.2.3 RS232 Data Format: APA 6000 Menu Options for SIO ......................................................................... 157
8.2.4 APA 6000 Printer and Computer Formats ............................................................................................. 158
8.2.5 Remote RS232 Commands................................................................................................................... 158
8.3 Using an APA With a Digital Display Module (DDM) ....................................................................................... 161
Section 9 PID Control ...................................................................................................................................... 163

9.1 Analyzer Settings ............................................................................................................................................ 163
9.1.1 Set Point ................................................................................................................................................ 163
9.1.2 Dead Band............................................................................................................................................. 163
9.1.3 Proportional Band.................................................................................................................................. 163
9.1.4 Reset (Integral) ...................................................................................................................................... 163
9.1.5 Rate (Derivative).................................................................................................................................... 163
9.1.6 Output Action......................................................................................................................................... 163
Appendix A Bench Method Procedure .............................................................................................................. 165
Glossary ............................................................................................................................................................. 171
General Information......................................................................................................................................... 175

Replacement Parts ............................................................................................................................................... 176
How to Order......................................................................................................................................................... 179
Repair Service ...................................................................................................................................................... 180
Warranty ............................................................................................................................................................... 181
Index .................................................................................................................................................................... 182
Page 6
Table of Contents 51000-18TOC.fm
Certification
Hach Company certifies this instrument was tested thoroughly, inspected

and found to meet its published specifications when it was shipped from
the factory.
The APA 6000™ Alkalinity Process Analyzer has been tested and is certified
as indicated to the following instrumentation standards:
Product Safety
The APA 6000 Alkalinity Analyzer is ETL listed to UL Standard 3101-1
(Listing # H0492805390) and is ETL certified to CSA Standard C22.2 No. 142
(Certification # H0492805390).
Certified by Hach to EN 61010-1 (IEC1010-1), supporting test records by

Intertek Testing Services.
Immunity
EN 50082-2 (Generic Immunity Standard) per 89/336/EEC EMC:
Supporting test records by Hach Company, certified compliance by

Hach Company.
Required Standards include:
EN 61000-4-2 “1995” (IEC 1000-4-2) Electro-Static Discharge

EN 61000-4-4 “1995” (IEC 1000-4-4) Electrical Fast Transients/Burst
EN 61000-4-11 “1994” (IEC 1000-4-11) Voltage Dips, Interruptions and
Variations
ENV 50140 “1993” (IEC 801-3) Radiated RF Electro-Magnetic Fields
ENV 50141 “1993” Conducted Disturbances Induced by RF Fields
ENV 50204 “1995” Radiated Electro-Magnetic Field from Digital Telephones
Additional Standards include:
EN 61000-4-5 “1995” (IEC 1000-4-5) Surge
Emissions
EN 50081-2 (Generic Emissions Standard) per 89/336/EEC EMC:
Supporting test records by Intellistor O.A.T.S., certified compliance by

Hach Company.
Required Standards include:
EN 55011 (CISPR 11) Emissions, Class A Limits
Additional Standards include:
EN 61000-2 (IEC 1000-3-2) Harmonic Disturbances Caused by

Electrical Equipment
EN 61000-3 (IEC 1000-3-3) Voltage Fluctuation (Flicker) Disturbances
Caused by Electrical Equipment
Page 7
51000-18 certification.fm Certification
Certification
Canadian Interference-causing Equipment Regulation, IECS-003,

Class A:
Supporting test records by Intellistor O.A.T.S., certified compliance by

Hach Company.
This Class A digital apparatus meets all requirements of the

Canadian Interference- Causing Equipment Regulations.
Cet appareil numérique de la classe A respecte toutes les exigences du

Règlement sur le matériel brouilleur du Canada.
FCC Part 15, Class A Limits:
Supporting test records by Intellistor O.A.T.S., certified compliance by Hach

Company.
This device complies with Part 15 of the FCC Rules. Operation is subject
to the following two conditions:
(1) This device may not cause harmful interference, and (2) this device must
accept any interference received, including interference that may cause
undesired operation.
Changes or modifications to this unit not expressly approved by the party

responsible for compliance could void the user’s authority to operate
the equipment.
This equipment has been tested and found to comply with the limits for a
Class A digital device, pursuant to Part 15 of the FCC Rules. These limits are
designed to provide reasonable protection against harmful interference when
the equipment is operated in a commercial environment. This equipment
generates, uses, and can radiate radio frequency energy and, if not installed
and used in accordance with the instruction manual, may cause harmful
interference to radio communications. Operation of this equipment in a
residential area is likely to cause harmful interference, in which case the user
will be required to correct the interference at his own expense.
The following techniques of reducing the interference problems are

applied easily:
1. Disconnect the APA 6000 Alkalinity Analyzer from its power source to
verify that it is or is not the source of the interference.
2. If the AC power supply for the APA 6000 Alkalinity Analyzer is connected
into the same outlet as the device with which it is interfering, try
another outlet.
3. Move the APA 6000 Alkalinity Analyzer away from the device receiving
the interference.
4. Reposition the receiving antenna for the device receiving the interference.
5. Try combinations of the above.
Page 8
Certification 51000-18 certification.fm
Safety Precautions
Please read this entire manual before unpacking, setting up,
or operating this instrument. Pay particular attention to all danger and
caution statements. Failure to do so could result in serious injury to
the operator or damage the equipment.
To ensure the protection provided by this equipment is not impaired,
do not use or install this equipment in any manner other than that
which is specified in this manual.
Use of Hazard Information

If multiple hazards exist, this manual will use the signal word
(Danger, Caution, Note) corresponding to the greatest hazard.
DANGER
Indicates a potentially or imminently hazardous situation which, if not
avoided, could result in death or serious injury.
CAUTION
Indicates a potentially hazardous situation that may result in minor or
moderate injury.
NOTE
Information that requires special emphasis.
Precautionary Labels
Read all labels and tags attached to the instrument. Personal injury or
damage to the instrument could occur if not observed.
! This symbol, if noted on the instrument, references

the instruction manual for operation and/or safety information.
This symbol, if noted on the product, indicates the need

for protective eye wear.
! Section 2.5 Changing Reagents and Standards on page 51
! Section 2.6 Replacing the Soda Lime in the Standard Solution Scrubbers on page 54
! Section 4.2 Scheduled Maintenance on page 85
! Section 4.3.1 Changing Solutions on page 86
! Section 6 Sample Conditioning on page 111
! Section 6.1 Sample Conditioning on page 112
! Section 7.3 Electrical Connections on page 128
! Section 7.3.1 Power Connections At the APA Analyzer on page 130
! Section 7.3.2 Alarm Relay Connections on page 133
Page 9
51000-18 safety.fm Safety Precautions
Safety Precautions
! Section 7.3.3 Recorder Output Connections on page 134
! Section 7.3.4 Network Connections on page 136
! Section 7.4 Fuse Replacement on page 145
! Section 7.5 Changing Modules on page 146
! Section 7.7 Plumbing Installation on page 147
! Section 7.7.3 Drain Line Connection on page 152
Page 10
Safety Precautions 51000-18 safety.fm
Specifications
Specifications are subject to change without notice.
Performance
Range: 1 to 1000 mg/L for total alkalinity as calcium carbonate; 5 to
1000 mg/L for P alklanity as calcium carbonate
Accuracy: ±5% of reading or ±1.0 mg/L, whichever is greater
Repeatability: ±3% of reading or ±0.6 mg/L, whichever is greater
Response Time: For single sample stream instruments, less than 10 minutes
for 90% response to step change at sample inlet.
Cycle Time: 8 minutes (average)
Recorder Outputs: Two isolated, 4-20 mA outputs standard. Output span

programmable over any portion of the 0-1000 mg/L range (500 V isolation
from earth ground).
Alarms: 14 programmable internal alarms
Relays: Two SPDT relays with a maximum contact rating of 5 A resistive load
at 240 VAC. Additional relays available through optional Signal Output
Module.
Power Requirements: 95-240 VAC, 50 or 60 ±2 Hz, 150 VA
Sample Inputs: Up to three sample streams (with optional hardware)
Communications: Echelon®fieldbus compatible; utilizes LonTalk® protocol.

Maximum of 400 meters between devices with a 500 meter maximum per
segment; distances in excess of 500 meters require a repeater. Up to three
repeaters can be used for a total network length of 2000 meters.
Features
Instrument Enclosure: NEMA 4X (Indoor) and IEC 529 (IP 66) with
provision for air purge
Instrument Installation Category: II
Reagent Enclosure: Fully enclosed latch cases with protected ducting for
reagent and standard lines.
Waste Drain: Single plumbing connection for instrument drain; additional

plumbing connections for instrument case and reagent enclosure overflow
drains.
Instrument Weight: 25 kg (56 lb.)
Instrument Dimensions: 626.1 mm wide x 527.05 mm deep x 522.73 mm

high (24.65 x 20.75 x 20.6 inches)
Page 11
51000-18 specification.fm Specifications
Specifications
Sample/Environmental Requirements
Operating Temperature: 5 to 50 °C (41 to 122 °F)
Relative Humidity: 5 to 95% relative humidity, non-condensing
Sample Pressure: 2.5 to 100 psig (0.17 to 6.9 bar) to at Basic Water
Conditioning Filter; 0.5 to 30 psig (0.035 to 2 bar) maximum at sample inlet
block.
Sample Temperature Range: 5 to 50 °C
Sample flow: 25 to 1000 mL/min. maximum at Basic Water Conditioning

filter; 6 mL/min. maximum; filtered to 22 microns or less at sample inlet block.
Grab Sample:
Temperature: 5 to 50 °C
Volume: 100 mL minimum; filtered to 22 microns or better
Air Purge (optional): 15-scfh (7 L/min.) of dry instrument-quality air, ¼-inch

OD fitting
Page 12
Specifications 51000-18 specification.fm
Operation
DANGER
Handling chemical samples, standards, and reagents can be dangerous. Review the necessary Material
Safety Data Sheets and become familiar with all safety procedures before handling any chemicals.
DANGER
La manipulation des échantillons chimiques, étalons et réactifs peut être dangereuse. Lire les Fiches de
Données de Sécurité des Produits (FDSP) et se familiariser avec toutes les procédures de sécurité avant
de manipuler tous les produits chimiques.
PELIGRO
La manipulación de muestras químicas, estándares y reactivos puede ser peligrosa. Revise las fichas
de seguridad de materiales y familiarícese con los procedimientos de seguridad antes de manipular
productos químicos.
GEFAHR
Das Arbeiten mit chemischen Proben, Standards und Reagenzien ist mit Gefahren verbunden. Es wird dem
Benutzer dieser Produkte empfohlen, sich vor der Arbeit mit sicheren Verfahrensweisen und dem richtigen
Gebrauch der Chemikalien vertraut zu machen und alle entsprechenden Materialsicherheitsdatenblätter
aufmerksam zu lesen.
PERICOLO
La manipolazione di campioni, standard e reattivi chimici può essere pericolosa. La preghiamo di prendere
conoscenza delle Schede Techniche necessarie legate alla Sicurezza dei Materiali e di abituarsi con tutte
le procedure di sicurezza prima di manipolare ogni prodotto chimico.
Page 13
51000-18 operation stopper.fm Operation
Section 1 Introduction
1.1 How to Use this Manual

This manual is organized into two parts. After installation by a technician, the
analyzer is ready to be turned on and operated. Section 2–5 and Section 9
describe instrument start up, normal operation, and warnings/alarms that may
occur during daily operation. Section 6–8 (Installation) are intended for the
installation/repair technician. This portion describes how the installer should
wire and plumb the analyzer and accessories.
Figure 1 APA 6000™ Process Analyzer
1.1.1 Overview of the Analyzer Setup
1. As you unpack the analyzer and its accessories, refer to the packing lists
in Section 1.2 to ensure all the hardware required to install and operate
the analyzer arrived with the shipment.
2. See Section 1.3 on page 16 to choose a suitable installation location.
3. See Section 7.7 on page 147 to bring the sample from the process
stream to the APA. Only a qualified technician should complete the steps
in this section.
Page 15
51000-18 introduction.fm Introduction
Section 1
4. Refer to Section 7 on page 123 to complete the mounting and electrical
installation of the APA. Only a qualified technician should complete the
steps in this section.
5. Refer to Section 2 Startup to set up and start the analyzer.
1.2 Packing Lists

Table 1 describes the items shipped with the analyzer. Remove the instrument
from the shipping cartons and verify that no visible damage has occurred
during shipment. Verify the following items are included in the carton. Contact
Hach Customer Service at 1-800-227-4224 if any items are missing
or damaged.
Table 1 APA 6000 Alkalinity Analyzer

Item Catalog Number
APA 6000 Alkalinity Analyzer or APA 6000 Alkalinity Analyzer without AquaTrend® Interface 51000-10 or 51000-12
APA Alkalinity Reagent 1, Titrant, one 1-L bottle 26965-53
APA Alkalinity Reagent 2, Indicator, one 1-L bottle 26966-53
APA Alkalinity Standard 1, 0 mg/L, one 1-L bottle 26967-53
APA Alkalinity Standard 2, 2000 mg/L, one 1-L bottle 26968-53
Alkalinity Cleaning Solution, one 1-L bottle 26970-53
Installation Kit 51040-00
Maintenance Kit 51043-00
Tool Kit 51291-00
1.3 Location and Operating Environment

The analyzer is rated NEMA 4X (indoor) and IP66 when the front door is
latched and NEMA hardware is used to seal electrical connections.
Select the location of the APA 6000™ Alkalinity Process Analyzer so the
analyzer can be:
• Plumbed to the sample stream you wish to monitor.
• Plumbed to drain the waste fluids from the analyzer.
• Connected to a 95-240 VAC power source.
• In an area where the temperature will be 5 to 50 °C.
• Shielded from dripping/spraying fluids.
• Out of direct sunlight.
1.4 Instrument Overview
1.4.1 General Description

The APA 6000 Alkalinity Process analyzer (see Figure 1) is a microprocessor-
controlled process analyzer designed to continuously monitor a sample water
stream for alkalinity. The analyzer displays total, phenolphthalein, hydroxide,
carbonate, and bicarbonate alkalinity in the sample. Typical samples include
drinking water and boiler water.
Page 16
Packing Lists 51000-18 introduction.fm
Section 1
The analyzer uses a colorimetric method to determine concentration.
Data retrieval and communication with the instrument is done through
the AquaTrend® Interface keypad and display, mounted in the door of
the analyzer.
The reagent containers are sized to provide reagents for 30 days of

continuous operation. All reagent containers are factory-filled and meet
Hach’s quality standards.
The instrument case meets NEMA 4X (indoor) and IP66 industrial enclosure
requirements. The front door is constructed of corrosion-resistant materials
and opens for a full view of the analyzer’s modular components (refer to
Figure 3 on page 19). The analyzer can be used on a bench or mounted on a
wall or panel. Electrical connections are made through the back of the
analyzer. Sample and drain connections are made with standard tubing and
fittings on either side of the instrument.
Reagents and standards are plumbed from the reagent enclosures on the
side of the instrument (see Figure 2). All tubing enters the instrument at the
ports at the bottom of the instrument bezel.
The internal instrument temperature is factory pre-set at 50 °C. The design of

the analyzer door and instrument panel provide a small, insulated space
ensuring temperature control for accurate analysis. In order for the
temperature control system to function properly, the instrument door must
remain closed and latched during operation.
The analyzer has two analog outputs of 0-20 or 4-20 mA, which can be used
to drive a chart recorder or a process controller. Recorder span minimum and
maximum values can be programmed using the AquaTrend Interface keypad.
Two programmable alarm circuits provide relay closures, both normally open
and normally closed, for two selectable concentration set points. Set points
can be programmed anywhere within the overall range. System warning and
system alarm features may be used to provide alarm relay closures indicating
a need for operator attention.
If you need more than two relays or two analog outputs, external Signal
Output Modules (SOM) may be purchased.
1.4.2 Instrument Components

Four kits are necessary for operation:
• Alkalinity Reagent Kit
• Installation Kit
• Maintenance Kit
• Tool Kit
See Sections 1.4.4, 1.4.5, 1.4.6 and 1.4.7 for details about these kits
Instrument Enclosure
The instrument enclosure houses various modules, the instrument’s power
supply and control circuitry (see Figure 3). Within the enclosure, a module
panel separates sensitive electrical components from the wetted parts.
All openings to the module panel are gasketed to protect against leakage.
Page 17
51000-18 introduction.fm Instrument Overview
Section 1
The module panel folds out to allow access to the electrical connections at the
back of the instrument.
Electrical access points (power hookups, alarm outputs, etc.) are behind
the module panel in a grounded, covered area. A plastic upper cover
shields the power supply and control circuit board. Do not remove this cover!
The metal lower cover is removable for access to electrical connections
during installation.
Separate, spill-containing compartments on each side of the instrument

contain all chemical reagents and standards (see Figure 7 on page 23). This
allows changing of solutions without opening the instrument and upsetting the
temperature-controlled area.
Figure 2 APA 6000 Alkalinity Analyzer Components
The APA 6000 Alkalinity Analyzer consists of five basic components

(see Figure 3):
• Autoburette Module
• Colorimeter Module
• Rotor Valve Module and Holding Coil
• Mixer Module
• AquaTrend Interface
Page 18
Instrument Overview 51000-18 introduction.fm
Section 1
Autoburette Module
The analyzer uses a positive-displacement autoburette to measure and move
fluids through the various analytical components in the instrument. The
autoburette module consists of a clear acrylic block which houses a ceramic
piston, a double seal for the piston, a linear actuator, a two-way solenoid
valve, and control circuitry.
Colorimeter Module
Samples are measured in a temperature-controlled single-wavelength flow
cell. The light source is an LED, which passes through a 600 nm bandpass
filter. The path length is 8.75 mm (0.344 inches).
Rotor Valve Module, Holding Coil, and Reaction Coil

The rotor valve directs fluids to various components in the instrument.
All tubing is factory-assembled and labeled for each individual chemistry.
The valve head and holding coil are enclosed in a temperature-controlled
metal housing.
Mixer Module
The mixer module mixes reagents, sample, and standards.
Figure 3 APA 6000 Alkalinity Analyzer Modules
Valve Module ON/OFF Detector

and Holding Coil Switch Module
Module Panel
Mixer Module Autoburette Module
1.4.3 The AquaTrend Interface

The APA 6000 Analyzer has an AquaTrend® Interface built into the instrument
door. It provides a numerical or graphical display and a keypad for user input.
The AquaTrend allows networking of several Hach instruments. A remote
AquaTrend can be connected to the analyzer for access to the analyzer from
another location.
Page 19
Section 1
Data can be viewed in numeric or graphical format and reviewed on trend
graphs for details of measurement history. With the addition of the Hach Serial
I/O Module, data can be downloaded to a computer or printer.
A complete description of the AquaTrend’s capabilities can be found in the

AquaTrend Interface Manual, Cat. No. 51350-18, which can be ordered from
Hach Company.
1.4.3.1 Overview of Networking Options

One AquaTrend can link up to eight sensors or analyzers and other devices in
a variety of configurations. This section describes requirements and options
for setting up the AquaTrend network system with more than one sensor.
A “network” is the connection of one or more devices (at least one must be a
sensor) to a master AquaTrend. This master AquaTrend serves as the
network control panel.
Optional equipment (see Figure 4) is considered part of the system network.

Optional devices include Signal Output Modules (SOM), Digital Display
Modules (DDM), Serial I/O Modules (SIO), PS1201 Power Supplies, other
sensors, Remote AquaTrends, and Portable AquaTrends.
All AquaTrend devices use Echelon® LONWORKS® communication protocol to

ensure reliable digital network communications and compatibility with other
vendors’ equipment. Figure 5 on page 21 shows an example of a single-
sensor AquaTrend network system. An example of a multi-sensor system is
shown in Figure 6 on page 22.
Figure 4 Other Available Network Devices
AquaTrend AquaTrend with Signal PS1201 Signal Output Module

Output Module Power Supply Module (SOM)
Serial I/O Module
Digital Display Module
Portable AquaTrend Other sensors

(1720D Turbidimeter)
Page 20
Section 1
Each AquaTrend network device manual (AquaTrend, Digital Display Module,
Serial I/O Module, and Signal Output Module) provides setup instructions for
that component. The table below describes the maximum number of devices
that can be managed by one Master AquaTrend on a system. Additional
power supplies may be needed for devices other than the SIO.
One AquaTrend can link up to eight sensors (including the Alkalinity Analyzer)
and other devices in a variety of configurations. If you want to link any
additional sensors, consult the sensors’ manuals and the AquaTrend Interface
Manual. These manuals also contain all the information needed for setting up
an AquaTrend network and other network devices.
Table 2 Master AquaTrend Capabilities

Number that can be maintained by
Device
one Master AquaTrend
Signal Output Module (SOM) 8
Serial I/O Module (SIO) 2
Digital Display Module 8
Sensors 8
Remote AquaTrend 8
Figure 5 Example of a Single-Sensor AquaTrend Network
Page 21
Section 1
Figure 6 Example of Multi-Sensor AquaTrend Network
Page 22
Section 1
1.4.4 Alkalinity Reagent Kit

The APA 6000™ Alkalinity Process analyzer uses five reagents (see Figure 7
for location of each bottle).
APA Alkalinity Reagent 1 is an acid titrant that reacts with the alkalinity in
the sample.
APA Alkalinity Reagent 2 is a indicator used to determine the endpoints of

the titration.
APA Alkalinity Standards 1 and 2 are used together to perform a multiple-point

calibration. Standard 1 is a 0-mg/L as CaCO3 sodium carbonate solution.
Standard 2 is a 2000-mg/L as CaCO3 sodium carbonate solution. Both
require a CO2 scrubber for the air inlet, which is assembled and shipped
already attached to the reagent enclosure wall.
The fifth reagent, APA Alkalinity Cleaning Solution, cleans the system during
the Prime and Instrument Clean functions. This solution assures the system
stays free of precipitate buildup. Initially, a different cleaning solution (Cat. No.
26974-53) may be used to make sure all parts are wetted.
Figure 7 APA 6000 Analyzer Reagent, Standard, and Cleaning Solution Containers
Page 23
Section 1
1.4.5 Installation Kit

This kit includes the hardware for the basic clean water sample conditioning.
Installation Kit Components

Coupling, ¾″ NPT x ¾″ NPT Drain pipe, precut, 1″ diameter
Elbow fitting, ½″ ID x ¾″ NPT PP Tube connector fitting, male, ¼″ tubing
Reducer fitting, ¾″ MNPT x ¼″ NPT PVC Ball valve, ¼″ NPT
Teflon tubing, 0.170 ID x 0.250 OD Strainer housing, ¾″ w/o filter
Tygon tubing, ¾″ OD x 1/8″ W, black Filter, 22 µm
Conduit hanger clamp, 1-inch Teflon tape, 0.25″ wide
Tee fitting, 1x1″ SOC x ¾″ FNPT, PVC
1.4.6 Maintenance Kit

The Maintenance kit contains replacement parts for components subject
to wear.
Alkalinity Maintenance Kit Components

O-ring, fluorocarbon, 0.103 W x 0.424 ID
O-ring, fluorocarbon, 0.103 W x 0.237 ID
Autoburette piston seals, 0.25″ diameter
Rotor replacement for valve
1.4.7 Tool Kit

This kit contains the necessary tools and parts for normal operator
maintenance (see the table below and Figure 8):
Tool Kit Components

Cat. No. Description
51129-00 Hex nut fitting, 0.062 in. OD tubing
51130-00 Ferrule fitting, 0.062 in. OD tubing
51131-00 Flangeless nut fitting, 0.062 in. OD tubing
51132-00 Ferrule fitting, 0.062 in. OD tubing
51149-00 Autoburette force gauge tool
51169-00 Autoburette module wrench
51170-00 O-ring seating tool
51174-00 Flangeless nut extender tool
51345-00 Allen wrench, 7/64 in., long arm
51357-00 Valco valve wrench, ¼-in.
51356-00 Tubing cutter, for 1/16 in. tubing
51293-00 Flat bottom Tefzel plug, ¼-28
51178-00 Tefzel tubing, 0.030 in. ID x 0.062 in. OD, 2000 PSI
51359-00 Union fitting, ¼-28
51357-00 Valco valve wrench, ¼-in.
51356-00 Tubing cutter, for 1/16 in. tubing
Page 24
Section 1
Figure 8 Tool Kit Components

51149-00 51170-00 51174-00
51169-00
Tefzel Tubing
51178-00
51340-00
51345-00
51357-00
51131-00 51129-00
51356-00 51132-00 51130-00
51359-00
51293-00
1.5 Theory of Operation

The APA 6000® Alkalinity Process Analyzer is designed to provide
reproducible results through consistent solution handling. Every step in an
analysis is performed the same way each time, ensuring accurate results.
Accuracy can be verified and established by measuring grab samples with a
known concentration of analyte.
See Section 1.4.2 for descriptions of the various analyzer components.
The following steps describe how the analyzer works.
1. The instrument aspirates a representative sample and a small amount of

pH indicator.
2. The sample and indicator are delivered to the mixer and blended.
3. Another representative sample is aspirated and delivered to the detector

to obtain a reference measurement.
4. The sample/indicator mixture is aspirated from the mixer, followed by a

slug of acid.
5. The mixture is delivered to the detector, dispersing the acid through the
mixture and providing a characteristic titration profile.
Page 25
51000-18 introduction.fm Theory of Operation
Section 1
1.6 Method of Analysis

The analyzer aspirates and mixes the sample with a combination pH indicator
solution in the mixing chamber. The indicator changes color according to the
sample pH. The analyzer then aspirates more sample and delivers it to the
detector to obtain a reference measurement. This compensates for small
amounts of color or turbidity in the sample.
Some of the sample/indicator mixture is then aspirated from the mixer and
delivered to the detector, replacing the previous clear fluid. The remainder of
the mixture is aspirated from the mixer, followed by a slug of acid. This
acidified mixture is delivered to the detector via the reaction coil. As it travels
through the reaction coil, the acid becomes dispersed through the
sample/indicator mixture on both sides of the acid slug, forming a pH gradient.
There will be an small volume (band) of fluid on both sides of the acid peak
where the acid exactly neutralizes the alkalinity present in the sample, and the
pH indicator changes color.
As the fluid flows through the detector, the absorbance at 600 nm is recorded,
producing a characteristic titration peak. The peak width is determined at two
specific absorbance values. One width is determined at the absorbance
representing pH 8.3, and the other at the absorbance representing pH 4.5.
The first width represents the phenolphthalein alkalinity and the second width
represents the total alkalinity of the sample. The instrument automatically
calibrates using two standards (0 and 2000 mg/L as CaCO3) to establish a
multi-point calibration curve.
1.7 Basic Single-sample APA 6000 Analyzer System

The standard APA 6000 Analyzer provides measurements on one
process sample stream. The analyzer requires “clean water” sample
streams (particles smaller than 22 microns in diameter). The Basic
Sample Conditioning Kit brings the sample to the instrument and ensures
it meets this requirement. To measure 2-3 sample streams, additional
Basic Sample Conditioning Kits are necessary. Sample streams with
particles larger than 22 microns require additional sample conditioning;
see Section 6 on page 111.
1.8 Options and Add-ons for the APA 6000 Analyzer

Additional Basic Sample Conditioning Kits allow the analyzer to measure up
to three different sample streams.
Sample conditioning options allow measurement of dirty or turbid samples or

samples where biogrowth may be present. Sample conditioning options
include high bypass flow and air backflush for self-cleaning of the filter and
automatic submersible pump backflush. Provisions have been made for ultra-
filtration or micro-filtration. See Section 6 for more information.
Optional Signal Output Modules (SOM) provide the analyzer with additional
relay and recorder/controller outputs.
Serial Input/Output (SIO) modules can connect the analyzer to a computer
via an RS232 interface.
Digital Display Modules (DDM) provide a remote display of a given sample
stream’s measurement.
Remote AquaTrends allow for remote operation of the analyzer and
remote display of sample measurements. Portable AquaTrends provide
temporary operation/control of analyzers that do not have a built-in
AquaTrend® Interface.
Page 26
Method of Analysis 51000-18 introduction.fm
Section 2 Startup
2.1 Introduction
It is assumed that the analyzer has already been plumbed to the sample
source and a drain, as well as wired to a power source and any other
electrical wiring associated with 4-20 mA connections, relay connections, and
network connections by the installation technician according to the Hardware
Installation section. This section presents the steps, in sequence, an operator
should take to begin operation. This section will;
• give a general overview of the analyzer’s AquaTrend, display/keypad and

user interface.
• explain setup steps for changing default values and performing

measurements. Some of these selections have default settings that will
allow the analyzer to run without being changed (see Section 2.2.5 on
page 34).
• instruct you on setting up relay and alarm outputs.
• outline the steps required to choose sample conditioning options if the

analyzer is used to monitor a “dirty water” sample.
• describe the steps the operator will perform in getting the reagents and
standards set up.
• describe how to check for proper sample flow.
• list the steps required to prime the sample lines and reagents.
• discuss calibration of the analyzer.
• explain how to set up the clean cycle.
2.2 The AquaTrend

The AquaTrend integrated into the door of the APA 6000 Analyzer provides
the interface necessary to communicate with the APA 6000 and the Hach
network, if present. See Section 1.4.3 on page 19 for more discussion of the
AquaTrend. Before pressing any keys, turn the instrument on and put it in
standby (see Section 2.2.2).
2.2.1 The AquaTrend Keypad

The AquaTrend keypad is designed for simple navigation through the
AquaTrend menus (see Figure 9). The keypad contains four arrow keys, a
DISPLAY key, a MENU key, an EXIT key, and an ENTER key.
Page 27
51000-18 startup.fm Startup
Section 2
Figure 9 AquaTrend Keypad
1
2
4
DISPLAY EXIT
3 5
MENU ENTER
Table 3 AquaTrend Key Functions

Number Key Function of Keys
Allows you to navigate through the various menus, to change settings, and to move the
1 cursor when observing graph data.Table 4 summarizes the functions of the arrow keys in
each menu view.
Displays the data display screen. Once the data is displayed, pressing the DISPLAY key
2
toggles between data presented in numerical form and graph form.
3 Displays the main menu from any menu level or from the data display.
Accesses the data display screen from the main menu. From any other menu level, press the
4 EXITkey to display the previous menu screen. The EXIT key can also be used to abandon any
alphanumeric entry or selection process.
5 Selects menu options and confirms alphanumeric entries in any menu.
The arrow icons and their positions in the arrow field in the top right corner of
the screen (item 6 on Figure 11) indicate which of the arrow keys are available
for the screen you are in. Figure 10 shows the screen categories and Table 4
summarizes the function of the arrow keys for each screen category.
Table 4 Arrow Key Functions

Screen Category Function of Arrow Keys
Menu Screen Move the pointer or highlight to next (down) or previous (up) item.
Numeric Data Display Screen Up: go to previous channel. Down: go to next channel.
(1, 4 or 8 numeric readings) Will loop around at top or bottom of page, depending on which key is pressed.
Up: display previous channel graph. Down: display next channel graph. Right increases the
Graph Display Screen number of channels shown; Left decreases the number of channels shown. ENTER key
toggles between the single and multiple channel display.
Pop-up Alphanumeric Entry Increment (up) and decrement (down) currently highlighted character. Move highlight to next
Screen (right) or previous (left) character. Loop around at either end.
Page 28
The AquaTrend 51000-18 startup.fm
Section 2
2.2.2 The AquaTrend Display

Before pressing any keys, turn the instrument on and put it in standby
as follows:
1. Press the MENU key.
2. Select the SENSOR MENU.
3. Select the sensor by name.
4. Select SENSOR STATUS.
5. Select STANDBY.
6. Press ENTER.
Note: This puts the analyzer into AquaTrend screens appear in several different formats (see Figure 10).
Standby Mode and terminates all See Figure 11 and Figure 12 for descriptions of each field.
operations. When the analyzer is
restarted, it will automatically start When the MAIN MENU is displayed on the AquaTrend screen, press the EXIT
performing measurements. or display key to return to the data display mode. Consecutive presses of the
EXIT key from any menu takes you back, one screen at a time, to the data
display screen. Pressing DISPLAY from any menu immediately returns you to
the measurement display screen.
When changing settings or performing diagnostics on a device on

the network, temporarily exit the data display mode and return to the
main menu by pressing the MENU key. Press the DISPLAY key to view data
in the data mode.
The AquaTrend will display data from the APA 6000 Alkalinity Analyzer except
when the operator uses it for specific purposes. When viewing data, press the
DISPLAY key to alternate between displaying the data in numeric and
graphical mode.
• When viewing data in numeric mode, you can display a single

measurement or up to eight measurement channels at the same time.
• When viewing data in graph mode, you can see a history of readings
over the last 60 minutes, 24 hours or 30 days. The AquaTrend,
however, displays data for only one measurement channel at a time in
the graphic mode.
For details on selecting the preferred graph time and scaling, see
Section 3.2.1 on page 70.
Figure 10 AquaTrend Screen Categories
1. Menu Screen 2. Numeric Data 3. Graph Display Screen 4. Pop-up Entry Screen
Display Screen
Page 29
51000-18 startup.fm The AquaTrend
Section 2
Figure 11 AquaTrend Menu and Numeric Data Display Fields
Table 5 AquaTrend Display Fields

Number Field Information Shown in Field
Numeric Data display: shows DISPLAY DATA
1 Status Bar Main menu: shows MAIN MENU
Lower menus: shows top level menu
2 Text/Data Numeric data, graphical data, menus and pop up boxes appear here.
3 Date Current date
Check here to see if there are active alarms on the system.
Numbers that appear here—1 through 8—correspond to the sensor with active alarms.
For example, if an alarm becomes active on sensor 3, the number 3 appears in the
4 Alarms alarm field.
If “N” appears in this field, an active AquaTrend alarm is coming from a network device other
than a sensor. If no indicators appear in this field, no alarm on the system is active.
See Section 5.1.1 on page 97 to review alarms.
5 Time Current time displayed as military time (24 hour clock).
6 Arrow Field Direction of these arrow icons correspond to enabled arrow keys for each screen.
Page 30
Section 2
Figure 12 AquaTrend Graph Fields

1 16
15
2
AquaTrend™
14
3 13
12
6
11
7 Alarms
8 9 10
Table 6
Number Field Information Shown in Field
1 Status Bar Shows the active menu
2 Channel assignment Channel letter of the measurement shown in the graph
3 Graph data, upper limit (y-axis) Upper numeric limit of trend graph data (Y max)
4 Cursor Y-data Y value (measurement) value at cursor location
5 Units Unit of the measurement on the displayed channel (ppm or mg/L)
6 Species Chemical form of the measurement on the displayed channel
7 Graph data, lower limit (y-axis) Lower numeric limit of trend graph data (Y min)
Lower time limit If reviewing data with cursor, this fields is replaced by the
8 Graph time, lower limit (x-axis)
(oldest data) date and/or time, depending on selected time range.
9 Cursor time/date Time or date of data at the cursor position
Current time If reviewing data with cursor, this field is replaced by the
10 Graph time, upper limit (x-axis)
(latest data) date and/or time depending on selected time range.
Recalls value of data at its current position. Use the left and right arrow keys to
11 Graph cursor move the cursor to different times on the graph for data review. Move the cursor
all the way to the right or press EXIT to return to the current reading.
Line graph of 60 minutes, 24 hours of data, or one month of data. These
12 Graph Area
settings are selectable in the DISPLAY SETUP menu.
Depending on the sensor type and configuration, the display shows
13 Sensor name measurement channel and name or the sensor location, or a combination of
both.
14 Units and chemical form Units and chemical form of the measurement on the channel
Direction of these arrow icons correspond to enabled arrow keys for each
15 Arrow Field
screen.
16 Current Data Most recent measurement (same as numeric display)
Page 31
Section 2
2.2.3 Time and Date Settings

The current time and date have been factory set on the AquaTrend, but the
time may need to be adjusted to your time zone. If it is necessary to reset the
time and date, proceed as follows:
2.2.3.1 Setting the Time
1. Press the MENU key to start from the MAIN MENU.
2. Use the up/down arrow keys to select AQUATREND MENU and

press ENTER.
3. Select SET TIME/DATE and press ENTER.
4. Select SET TIME and press ENTER.
5. A pop-up screen will prompt you to enter the new time. The numbers
representing the hour will be highlighted. Press the up arrow key to
increase the hour setting and press the down arrow key to decrease the
setting. When the proper hour is displayed, press the right arrow key and
set the minutes in the same manner.
Note: The AquaTrend uses a 24-hour clock (military time), so there is no selection for
a.m. or p.m. If the current time is 4:00 p.m., for example, you would enter the
24-hour format equivalent of 16:00.
6. Press ENTER to save the change or EXIT to cancel.
Page 32
Section 2
2.2.3.2 Setting the Date

Use this procedure to change the current date:
2. Use the up/down arrow keys to select AQUATREND MENU and

press ENTER.
4. Select SET DATE and press ENTER.
5. A pop-up box will prompt you to enter the new date. The numbers
representing the month will be highlighted. Press the up arrow key to
increase the month setting and press the down arrow key to decrease the
setting. When the proper month is displayed, press the right arrow key
and set the day. Repeat to set the last two digits of the current year.
6. Press ENTER to save the change or press EXIT to cancel.
2.2.3.3 Setting the Correct Day of the Week

Use this procedure to change the current day of the week:
2. Select AQUATREND MENU and press ENTER.
4. Select DAY: and press ENTER.
5. A pop-up box will prompt you to select the day. Use the up or down arrow
key to highlight the desired day.
6. Press ENTER to save the change or press EXIT to cancel. The day will
change automatically. Check to be sure the clock is set at the correct time.
Page 33
Section 2
2.2.4 Changing the Date Format

Use the following procedure to change the format of the date displayed by
the AquaTrend:
4. Select DATE FORMAT: and press ENTER.
5. A pop-up box will appear with SELECT DATE FORMAT. Use the up and
down arrow keys to select a date format: MM/DD/YY is month/day/year,
and DD/MM/YY is day/month/year.
6. Press ENTER to save the change or press EXIT to cancel.
2.2.5 Programmable Functions

Programmable functions on the APA 6000 Analyzer have factory default
values. All programmable functions are set and reviewed via the AquaTrend
by responding to specific displayed prompts. The following sections describe
how to program the analyzer to meet specific needs.
2.2.5.1 Language Selection

English is the default language of the APA 6000 Analyzer. To display another
language follow the instructions below:
3. Select LANGUAGE and press ENTER.
4. Use the up or down arrow key to select the language you want to use and
press ENTER. All screens will be displayed in this language.
Page 34
Section 2
2.2.5.2 Editing the Analyzer Name

The name of the APA 6000 Analyzer must be unique to identify the analyzer
and its data on the network. The name may be changed at any time:
2. Select SENSOR MENU and press ENTER.
3. Select the sensor by name and press ENTER.
4. Use the up or down arrow key to select EDIT NAME and press ENTER.
5. Use the left and right arrow keys to choose the character to change and
use the up and down arrow keys to cycle through letters, numbers and
symbols until you reach the character you want.
Note: In order to distinguish between devices on the network, use a unique and
descriptive sensor name. The sensor name can be up to 12 characters long in any
combination of alphanumeric characters. The first character must be a letter or the
# sign.
6. Press ENTER to accept the displayed name.
Page 35
Section 2
2.2.5.3 Security Setup

To limit access and avoid unauthorized changes to the AquaTrend Network
setup features, set security options by;
• setting a password;
• setting the security level; or
• accessing a temporary unlock option. This temporarily suspends the full

or partial security levels, allowing access to the system without having to
use the password.
The default password is HACH. The default security level is NONE. This
security level allows access to all functions.
2.2.5.4 Changing the System Password
1. Press MENU to start from the MAIN MENU.
3. Select SECURITY SETUP and press ENTER.
4. Select SET PASSWORD and press ENTER.
5. Enter the current password for access to the AquaTrend menus. Pressing
the right and left arrow keys moves the cursor right and left; pressing the
up and down arrow keys scrolls through the available characters. The
default password is HACH.
6. Press ENTER to confirm or press EXIT to cancel.
7. Enter the new password by using the arrow keys as in step 5.
8. Re-enter the new password.
Page 36
Section 2
2.2.5.5 Setting the Security Level

The analyzer’s security level determines which of the menu parameters can
be modified by the operator. The three security levels are NONE, PARTIAL
and TOTAL.
TOTAL lockout means the operator is unable to change any of the analyzer’s
settings or cause the analyzer to perform any operations (priming, cleaning,
calibrating, etc.) from the keyboard. Any user will be able to review all settings,
but will be unable to modify them if they are locked out.
PARTIAL lockout allows user access to the following menus and functions:
• display setup (see Section 2.2.5.7 on page 39)

• language (see Section 2.2.5.1 on page 34)
• alarm log (see Section 3.5 on page 79)
• execute calibration (see Section 3.4.1 on page 75)
• read grab sample (see Section 3.3 on page 73)
• all solution level settings (see Section 2.5.3 on page 53)
• all priming operations (Section 2.5.3 on page 53 and Section 4.3.1 on
page 86).
• clean system now (Section 2.8 on page 61)
Setting the security level to NONE allows access, without a password, to any
of the menus except SECURITY SETUP.
Set the security level as follows:
4. Select SECURITY LEVEL: and press ENTER.
5. Enter the password (default is HACH). Use the left and right arrow keys to
choose the character to change and use the up and down arrow keys to
cycle through letters, numbers and symbols until you reach the character
you want.
6. Use the arrow keys to select NONE, PARTIAL, or TOTAL.
Page 37
Section 2
2.2.5.6 Using Temporary Unlock and Unlock Duration

Selecting temporary unlock allows the operator to temporarily override the
security level setting and have full access to all menu parameters. Unlock
duration allows the operator to select the length of time that the temporary
unlock is in effect.
4. Select TEMPORARY UNLOCK and press ENTER.
5. Enter the password (this is necessary only if the security level is set to
Partial or Total).
6. Choose the duration of time you want the keypad to remain unlocked:
30, 60, 120 or 360 minutes.
Page 38
Section 2
2.2.5.7 Adjusting the Display Contrast

Adjusting the contrast level setting of the AquaTrend Interface allows the
operator to choose the most readable display for the lighting conditions.
1. Press MENU to start from the MAIN MENU.
3. Select DISPLAY SETUP and press ENTER.
4. Select CONTRAST LEVEL.
5. A pop-up box provides a choice of settings between 0 and 24 (0 being the

lowest setting). Use the up and down arrow keys to adjust the contrast.
Press ENTER to accept the displayed contrast level.
2.2.5.8 Selecting Measurement Units

The analyzer displays measurements in ppm or mg/L. To change units, follow
the instructions below.
Important Note: Changing units causes the data log for the measurement to
be erased.
4. Select MEASUREMENT OPTIONS and press ENTER.
5. Select UNITS and press ENTER.
6. Select the units you want to use and press ENTER, or press EXIT to cancel
Note: When units are changed, the display shows new units with the next
measurement.
Page 39
Section 2
2.3 Outputs and Relays

The APA 6000 analyzer has internal and external outputs. The internal analog
outputs are used without an SOM and provide signals to recorders and
controllers directly from the instrument. There are also two internal alarm
(open or closed) signals and 12 external alarm signals. External analog and
alarm outputs should be routed to an SOM. The table below summarizes
the outputs.
Table 7 Output Signals

Output Name Location and Signal Type Function
RCA, RCB Internal (analog) Controller, Recorder
RC1, RC2 External (analog) Controller, Recorder
RC3-RC12 External (analog) Recorder
ALA, ALB Internal (open or closed) Alarm
AL1- AL12 External (open or closed) Alarm
2.3.1 Alarms
Each APA 6000 Analyzer provides 14 alarm signals for your system. Two of
these, ALA and ALB, are permanently attached to the analyzer’s internal
alarm outputs, labeled Relay A and Relay B. The remaining alarm signals,
AL1 through AL12, can be attached to relays in optional Signal Output
Modules (SOMs).
SOMs can be purchased separately, and provide two relays and two analog
outputs each. For information on attaching alarms to relays and recorders to
analog outputs, see Section 7.3.4 on page 136 and Section 8 on page 155.
Each of the alarm setup options provides a setting for measurement,

enabling/disabling alarms, alarm type, and alarm set point. Alarms can be
configured as one of 8 types: high, low, rate, sensor warning, sensor alarm,
air backflush, sample pump or unconfigured. Table 8 describes the
parameters available on each alarm type. Parameters in bold print indicate
default settings.
Table 8 Parameters for Setting Alarms

Options Setpoint Alarms Sensor Warnings and Alarms
TYPE High, Low, Rate, Unconfigured Sensor Warning, Sensor Alarm, Unconfigured
MEASUREMENT [Sensor measurement] ---
SET POINT [Legal value] ---
ENABLED Yes, No Yes, No
MEAS FAILURE Off, On, Hold ---
Page 40
Outputs and Relays 51000-18 startup.fm
Section 2
To set up the alarms:
4. Select ALARM SETUP and press ENTER.
5. Select the alarm you want to set up and press ENTER.
ALA and ALB are internal analog outputs connected to relays in the APA
analyzer and may be used to actuate the air backflush and submersible
pump cleaning cycles. AL1 through AL12 may be connected to relays in
an SOM.
6. Select TYPE and press ENTER.
7. Select one of the following to choose the type of alarm:
• To disable an alarm, select UNCONFIGURED and press ENTER.

• Select HIGH, LOW or RATE to configure a set point alarm within those
ranges and press ENTER. Go to Step 8.
• Select SENSOR WARNING or SENSOR ALARM to configure an alarm
that will be triggered by a sensor alarm or warning. Go to Step 9.
Note: Setup for Air Backflush and Sample Pump is described in Section 2.4.1.1 on
page 49 and Section 2.4.1.2 on page 50.
Page 41
51000-18 startup.fm Outputs and Relays
Section 2
8. If HIGH, LOW or RATE was selected in Step 7, the following setup options
are available:
• Select MEASUREMENT to change the sample measurement that is

monitored for alarm generation.
• Select SET POINT to specify a numeric value for the alarm.
• Select ENABLED to turn the alarm on or off.
• Select MEAS FAILURE to set the alarm’s response when sample is
not flowing to the analyzer or the analyzer experiences a fault that
prevents it from providing the selected measurement. ON and OFF
turn the alarm on or off; HOLD leaves the alarm in the state it was in
prior to the failure.
9. If you selected SENSOR WARNING or SENSOR ALARM in Step 7, select

ENABLED. Select YES or NO to turn the alarm on or off, respectively.
10. Press ENTER to save the alarm setting, or press EXIT to cancel.
2.3.2 Sensor Warning Options

This option allows you to enable/disable warnings generated by power failures
and low reagents/standards. The default settings for low solution levels is ON
and for power failure warning is OFF.
4. Select SENSOR DIAGNOSTICS and press ENTER.
5. Select SENSOR WARNING OPTIONS and press ENTER.
6. Select POWER FAILURE or FLUIDS LOW and press ENTER. A pop-up

menu will appear.
7. Select ON or OFF to enable or disable the warning. Press ENTER.
Page 42
Section 2
2.3.3 Recorders or Controllers

Each APA 6000 analyzer provides up to 14 analog output signals. Four of
these signals (RCA, RCB, RC1 and RC2) can be configured as controllers.
Two of these signals, RCA and RCB, are permanently attached to the
analyzer’s internal analog outputs, labeled Output A and Output B. RCA and
RCB may also be configured as recorder outputs. The remaining analog
signals, numbered RC1 through RC12, can be attached to analog outputs in
SOMs and used as alarm and warning outputs. SOMs can be purchased
separately and provide two relays and two analog outputs each (see the
AquaTrend Manual for networking information). Table 9 describes the
parameters available for recorders and controllers. Parameters in bold print
indicate default settings.
Table 9 Parameters for Setting Recorders/Controllers

Options Recorder Controller
TYPE Recorder, Unconfigured Controller, Unconfigured
MEAS [Sensor measurement] [Sensor measurement]
MIN [value] NA
MAX [value] NA
ENABLED Yes, No Auto, Manual, Off
MEAS FAILURE Go Max, Go Min, Hold Go Max, Go Min, Hold
OUTPUT SETUP Only RCA and RCB Only RCA and RCB
DEAD BAND NA [value]
PROP BAND NA [value]
RESET NA [value]
RATE NA [value]
SETPOINT NA [value]
OUTPUT ACTION NA Reverse, Direct
Page 43
Section 2
2.3.3.1 Configuring Analog Outputs as Recorder Signals

To set up an analog output to a recorder, perform the following steps:
4. Select RECORDER/CONTROL SETUP and press ENTER.
5. Select the analog output you want to use and press ENTER.
Select RC [1 -12] if you want to configure a SOM output to a recorder.
Select RCA or RCB if you want to configure one of the APA analog outputs
as a recorder output.
6. To change the type of output, select TYPE and press ENTER.
7. Select RECORDER to send the analog output to a recorder.
OR
8. Press ENTER to confirm the setting or press EXIT to cancel.
9. To change the measurement that the recorder output will track,

SELECT MEASUREMENT: XXXX and press ENTER.
10. Select the desired measurement and press ENTER.
11. To change the minimum measurement value that corresponds to the

minimum recorder output, select MIN: XXXX and press ENTER.
12. Modify the minimum value by using the arrow keys and press ENTER
when the value entry is complete.
13. To change the maximum measurement value that corresponds to the

maximum recorder output, select MAX: XXXX and press ENTER.
Page 44
Section 2
14. Modify the maximum value by using the arrow keys and press ENTER
when the value entry is complete.
15. To enable or disable the recorder output, select ENABLED and

press ENTER.
16. Select YES or NO to indicate that the recorder output is enabled or

disabled, respectively, and press ENTER.
17. To change the recorder output action when the analyzer is unable to
perform measurements in the selected measurement range, select
MEAS FAILURE: XXXX and press ENTER.
18. Select HOLD, GO MAX or GO MIN to indicate what the output action
should be when the analyzer cannot perform a selected measurement.
GO MAX sets the output to 20 mA, GO MIN sets the output to 4 mA, and
HOLD keeps the output at the current value. Press ENTER.
19. To complete the recorder setup for RCA or RCB, see Section 2.3.3.3. To
complete the recorder setup for RC1-12 see Analog Output Settings in
the SOM Manual.
Page 45
Section 2
2.3.3.2 Configuring Analog Outputs as Controller Signals

For an explanation of the PID control settings see Section 9 on page 163. The
following steps let you define the PID controller settings.
Only RCA, RCB, RC1, and RC2 can configured as controller outputs to
actuate controllers.
1. Follow Steps 1-7 in Section 2.3.3.1 to access the controller setup menu,
then choose CONTROLLER in Step 7.
2. To change the measurement that the analyzer uses to monitor for its
control action, select MEASUREMENT: XXXX and press ENTER.
3. Select the desired measurement and press ENTER.
4. To turn off the control output, enable automatic control or enable manual
control, select ENABLE: XXXX and press ENTER.
5. Select OFF, AUTO or MANUAL to indicate that the control action is

turned off, in automatic control, or set for manual control, respectively.
Press ENTER.
6. If MANUAL CONTROL was selected, a pop-up menu will appear. If

desired, the output can be manually modified by using the arrow keys
then pressing ENTER.
7. To change the dead band value, select DEAD BAND: XXXX and
press ENTER.
8. Modify the dead band value by using the arrow keys. Press ENTER.
9. To change the proportional band value, select PROP BAND: XXXX and
press ENTER.
10. Modify the proportional band value by using the arrow keys.
Press ENTER.
Page 46
Section 2
11. To change the reset value, select RESET: XXXX and press ENTER.
12. Modify the reset value by using the arrow keys. Press ENTER.
13. To change the rate value, select RATE: XXXX and press ENTER.
14. Modify the rate value by using the arrow keys. Press ENTER.
15. To change the set point value, select SET POINT: XXXX and press ENTER.
Modify the set point value by using the arrow keys. Press ENTER.
16. To change the output action setting, select OUTPUT ACTION: XXXX and
press ENTER.
17. Select REVERSE or DIRECT for the controller’s output action.

Press ENTER.
18. To change the recorder or controllers output action when the analyzer is
unable to perform measurements in the selected measurement range,
select MEAS FAILURE: XXXX and press ENTER.
19. Select HOLD, GO MAX or GO MIN to indicate what the output action
should be when the analyzer cannot perform a selected measurement.
GO MAX sets the output to 20 mA, GO MIN sets the output to 4 mA, and
HOLD keeps the output at the current value. Press enter.
Page 47
Section 2
2.3.3.3 Adjusting Output for RCA and RCB (Trim)

Use the trim adjustments to set zero or full scale on a recorder without
adjusting the recorder itself. The range of adjustment is 0.0-11 mA for zero
scale and 13.2-22.5 mA for full scale. The current values are nominal values
and are accurate to ±1.5%. The recorder full scale (20 mA) may not exactly
match the APA full scale (20 mA). You can adjust the outputs so that full scale
on the APA is equal to full scale on the recorder. The same holds true for the
zero value.
If you wish to adjust (trim) the milliamp output range for the internal
recorder/controller outputs (RCA or RCB) or if you want to change the range,
select OUTPUT A SETUP or OUTPUT B SETUP. Press ENTER.
• To adjust the mA output at the bottom of the scale, select ZERO SCALE
TRIM and press ENTER. Use the up/down arrow to select FINE or
COARSE ADJUSTMENT. Press ENTER. The new trim mA value will appear.
Select ACCEPT NEW VALUE when done and press ENTER.
• To adjust the mA output at the top of the scale, select FULL SCALE TRIM
and press ENTER. Adjust as described above.
• To select either 0-20 mA or 4-20 mA as the output range, select OUTPUT

RANGE and press ENTER.
2.4 Sample Conditioning Setup

All samples are minimally conditioned by the Sample Conditioning Kit
installed with the analyzer. In addition, dirty or more turbid samples may
require additional conditioning to make them clean enough for the APA 6000
analyzer. See Section 6.2.1.1 on page 113 for installation of the Air Backflush
Kit or Section 6.2.2 on page 119 to install the submersible sample pump.
2.4.1 When to Use Sample Conditioning Setups

If you have dirty water applications such as effluent from sewer plants or other
sources with biogrowth, silt or turbidity, you may have purchased optional air
backflush or submersible sample pump equipment. The analyzer must be
equipped with the optional hardware necessary to perform the air backflush.
To perform the sample pump cleaning, the analyzer must use a submersible
sample pump. Section 6 on page 111 has more information about sample
conditioning applications and installation. Use this section to set up the
software necessary for sample conditioning options.
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Sample Conditioning Setup 51000-18 startup.fm
Section 2
2.4.1.1 Air Backflush Option
1. Press the MENU key on the AquaTrend to start from the MAIN MENU.
2. Select the SENSOR MENU by pressing the down arrow key. Press ENTER.
Note: An alarm relay should be used to actuate the air backflush valve.
5. Select the alarm output that drives the relay which controls the air
backflush (see Section 7.3.2 on page 133 for installation.)
7. Select AIR BACKFLUSH and press ENTER.
8. Ensure that ENABLED is set to YES. If not, select ENABLE and press
ENTER. Select YES and press ENTER.
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51000-18 startup.fm Sample Conditioning Setup
Section 2
2.4.1.2 Sample Pump Option

This option is used when a sample pump is supplying sample to the sample
conditioning filter. The sample filter is cleaned by cycling the pump off and on
periodically to dislodge debris.
5. Select the alarm output that drives the relay which controls the sample
pump (see Section 7.3.2 on page 133 for installation).
7. Select SAMPLE PUMP and press ENTER.
8. Ensure that ENABLED is set to YES. If not, select ENABLE and press
ENTER. Select YES and press ENTER.
Page 50
Sample Conditioning Setup 51000-18 startup.fm
Section 2
2.5 ! Changing Reagents and Standards

The solution bottles are labeled as Reagent 1, Reagent 2, Standard 1,
Standard 2, Cleaning Solution. The tubing into each of these bottles is also
labeled with the solution name to prevent reagent line mix-ups.
2.5.1 Changing Reagents and the Cleaning Solution

To change Reagents 1 and 2 and the Cleaning solution see Figure 13 and
follow these instructions:
1. Use a permanent marker to put a mark on the tubing where it exits

the bottle.
2. Remove the bottle vent cap assembly and tubing from the top of the
existing solution bottle.
3. Rinse the straw surrounding the tubing with deionized water and shake off
any residual water before inserting it into the new solution. This avoids
possible contamination. Be sure the tubing extends to the bottom of the
straw. If not, adjust it and re-mark the tubing.
4. Insert the straw into the new bottle and screw the vent cap on. Be sure the
mark on the tubing is still located where the tubing exits the bottle. This
assures the inner tube has remained at the bottom of the bottle.
5. Place the new bottle in the reagent compartment. Hach recommends

changing all the solutions at the same time.
6. Use the applicable prime function to fill the tubing with new solution
(see Section 2.7.2 on page 55 for priming procedures).
7. Set the solution level (Section 2.5.3 on page 53) using the
AquaTrend keypad.
Figure 13 Replacing Reagent Bottles
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51000-18 startup.fm Changing Reagents and Standards
Section 2
2.5.2 Changing the Standard Solutions
1. Remove the bottle vent cap assembly from the top of the existing
standard solution bottle. Keep the scrubber and reagent line in the same
position relative to the cap.
2. Rinse the straw surrounding the tubing with deionized water and shake
off any residual water before inserting it into the new solution. This
avoids possible contamination. Be sure the tubing extends to the bottom
of the straw.
3. Insert the vent cap assembly into the new standard bottle. Make sure the
scrubber tubing is above the level of the liquid. Make sure the reagent line
to the instrument is at the bottom of the bottle.
4. Place the new bottle in the reagent enclosure.
5. Use the applicable prime function to fill the tubing with new solution
(see Section 2.7.2 on page 55 for priming procedures).
6. Set the solution level (Section 2.5.3 on page 53) using the
AquaTrend keypad.
Figure 14 Vent Cap Assembly for Alkalinity Standards
Page 52
Changing Reagents and Standards 51000-18 startup.fm
Section 2
2.5.3 Setting Solution Levels

Each time a solution is changed in the analyzer, adjust the solution level
setting using the SOLUTIONS & CLEANING menu.
4. Select SOLUTIONS & CLEANING and press ENTER.
5. Select SOLUTION LEVELS and press ENTER.
6. The current “% full” for each reagent is displayed.
7. If you have refilled all the solutions at once, select RESET ALL TO 100%
and press ENTER. Go to Step 9.
If you have not refilled all the solutions, select the solution(s) you
are changing.
8. Press ENTER and a pop-up box will show a default setting of 100%. If
necessary, adjust the setting by pressing the up and down arrow keys.
9. Press the ENTER key to accept the value or press EXIT to cancel.
10. Repeat Steps 7-9 for each solution that was changed.
Page 53
51000-18 startup.fm Changing Reagents and Standards
Section 2
2.6 ! Replacing the Soda Lime in the Standard Solution Scrubbers

Note: Wear synthetic glove while Standard 1 and Standard 2 bottles require a scrubber (see Figure 15) that
working with the soda lime. contain soda lime to remove CO2 from the air that enters the reagent bottle.
Carbon dioxide reacts with the standard and causes a concentration change.
Replace exhausted soda lime (it will turn purple) as follows:
1. Gently remove the scrubber cap from the glass tube containing the soda
lime. Be sure to keep the inlet and outlet tubes in their proper positions.
2. Pour out the soda lime and dispose of it according to regulations.
3. Add new soda lime to the glass tube (a funnel may help). Be sure to leave
enough room to replace the top.
4. Gently insert the scrubber cap back into the glass tube. Be sure the seal
is tight.
Figure 15 Carbon Dioxide Scrubber
Page 54
Replacing the Soda Lime in the Standard Solution Scrubbers 51000-18 startup.fm
Section 2
2.7 Starting Analyzer Operation
2.7.1 Adjusting Sample Flow

See Figure 16, below, and Figure 54 on page 151 for the location of the
components used to adjust the sample flow.
1. Set the flow rate with the ¼-in. ball valve. When the lever is perpendicular
to the valve body, the valve is fully closed; when the lever is parallel with
the valve body, the valve is fully open.
2. Check the flow by pulling the ¼-in. OD tube from the push-in fitting at the
drain tee (the tubing from the sample inlet block to the drain tee). If
desired, measure the flow rate by directing the sample into a large
measuring container (flask or cylinder) over a set amount of time. Keep
the end of the tube at the same height as the push-in fitting.
3. Clean or replace the filter as required. This is usually indicated by a

significant decrease in flow to the sample inlet block when the sample
stream pressure has remained the same.
Figure 16 Adjusting the Flow Rate
2.7.2 Priming the Analyzer

If the analyzer is still in “standby” perform the following steps:
1. Press the MENU key.
2. Select the SENSOR MENU.
4. Select SENSOR STATUS.
5. Select RESTART.
6. Press ENTER.
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51000-18 startup.fm Starting Analyzer Operation
Section 2
Priming the analyzer assures that the standards and/or reagent fill the tubing
going to the rotary valve. When reagents, standards or cleaning solutions are
replaced, perform the applicable priming operations.
5. Select PRIMING and press ENTER.
6. Select one of the following:
• PRIME ENTIRE SYSTEM NOW. This will prime all the lines from
the solution bottles and sample lines. Use this option when all the
reagent bottles are replaced. The system prime will take about
12 minutes. The analyzer will display various messages about the
progress of the cycle.
• PRIME REAGENTS NOW. Use this option when only Reagent 1 and/or
Reagent 2 is replaced.
• PRIME STANDARDS NOW. Use this option when only the Standards
are replaced.
7. A pop-up window will indicate that priming will begin after the current
operation cycle. When priming starts, a pop-window will indicate the time
remaining to complete the prime cycle.
Page 56
Starting Analyzer Operation 51000-18 startup.fm
Section 2
2.7.3 Setting Up the Auto-Calibration Schedule

The analyzer accuracy specifications are based on an auto-calibration once
every week. The APA 6000 Analyzer can calibrate at any time. The default
setting is for the analyzer to auto-calibrate at 1:00 a.m. every Monday. To
change the calibration time, use the auto-cal setup procedure:
4. Select CALIBRATION and press ENTER.
5. Select AUTO-CAL SETUP and press ENTER.
6. The default is for the analyzer to calibrate once every week. To change
this, select one of the following:
• Select AUTO-CAL to turn the automatic calibration option off, or to set

the day or hourly interval you want the instrument to calibrate.
Choose any day of the week, every day of the week or every 12 hours
(as shown below).
Note: When auto-calibrate is set to 12 hours, the analyzer calibrates at the set
auto-cal time and again 12 hours later.
• Select AUTO-CAL TIME to specify the clock hour you want the
instrument to calibrate (use a 24-hour clock). Use the up and down
arrow keys to enter an hour between 1 and 24. For example, if you
want the instrument to calibrate at 2:00 p.m., enter 14.
Page 57
Section 2
2.7.4 Setting Up the Auto-Calibration Check Schedule

The default auto-calibration is performed weekly. An auto-calibration
measures four standards and takes about 1.5 hours. To check analyzer
accuracy without performing a full calibration, a calibration check is
automatically done once a day. The calibration check compares the
concentration level of one standard to the value of the same standard in the
current calibration curve. If the values are different by a specific percentage
(see Section 2.7.5), a full calibration is performed.
5. Select AUTO-CAL CHECK SETUP and press ENTER.
6. The default is for the analyzer to perform a calibration check once every
day. To change this, select one of the following:
• Select AUTO-CALCHECK to turn the automatic calibration check

option off, or to set the day or hourly interval you want the instrument
to calibrate.
Note: When auto-calibrate check is set to 12 hours, the analyzer checks the calibration
at the set auto-cal time and again 12 hours later.
• Select AUTO-CAL CHECK TIME to specify the clock hour you want the
instrument to check the calibration (use a 24-hour clock). Use the up
and down arrow keys to enter an hour between 1 and 24. For
example, if you want the instrument to calibrate at 2:00 p.m., enter 14.
Page 58
Section 2
2.7.5 Changing Calibration Check Warning Limits

A warning is issued if calibration check results are outside the warning limits
(i.e., ±10% of the calibration value). If the limit is set to 0, a warning will not be
issued. To change the warning limits, follow these steps:
6. Select WARNING LIMITS and press ENTER.
7. Set the warning limit to 0 to disable this feature. Otherwise, use the arrow
keys to choose a percent value by which the calibration value can vary.
For example, entering 05 will cause the analyzer to issue a warning if the
point being checked is different by ±5% of the current calibration value.
8. Press ENTER to accept the value.
Page 59
Section 2
2.7.6 Changing Calibration Check Recalibration Limits

A calibration is performed if calibration check results are outside the
recalibration limits (i.e., ±10% of the calibration value). If the limit is set to 0,
a recalibration will not be done. To change the recalibration limits, follow
these steps:
6. Select RECAL LIMITS and press ENTER.
7. Set the recal limit to 0 to disable this feature. Otherwise, use the arrow
keys to choose a percent value by which the calibration value can vary.
For example, entering 05 will cause the analyzer to recalibrate if the point
being checked is different by ±5% or greater of the current calibration
8. Press ENTER to accept the value.
Page 60
Section 2
2.8 Instrument Clean Function Setup

There are two cleaning cycles, NORMAL and EXTENDED. Use the normal
cycle to clean analyzers operating in clean water applications. Use the
extended cycle to clean analyzers operating in “dirty” water applications. The
extended cycle runs longer than a normal clean cycle.
5. Select INSTRUMENT CLEAN and press ENTER.
6. Verify the instrument is set to the appropriate type of clean cycle

(NORMAL or EXTENDED). To change it, press ENTER. Select the desired
cycle type and press ENTER.
7. Select AUTO-CLEAN and press ENTER.
8. Select the how often you want the analyzer to automatically clean itself
and press ENTER.
Note: Using the default settings is strongly recommended by the manufacturer and
should only be changed if sample components cause measurement problems.
If cleaning frequency is decreased, verify that the cleanliness and operation of the
analyzer is not degraded.
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51000-18 startup.fm Instrument Clean Function Setup
Section 2
2.9 Adding Sample Streams

To install more sample streams, see Section 6.3 on page 122 for instructions.
Then return to this section to set up the analyzer.
2.9.1 Setting the Number of Sample Streams

Note: The APA 6000 Alkalinity Once an additional sample stream is installed in the analyzer, the analyzer
analyzers will support three must be programmed to recognize and analyze that stream.
sample streams.
5. Select SAMPLE STREAMS and press ENTER.
6. Enter the registration number that came with your sample stream
expansion kit.
7. Select the number of sample streams the analyzer is plumbed for and
press ENTER.
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Adding Sample Streams 51000-18 startup.fm
Section 2
2.9.2 Setting Up the Sample Sequence

For analyzers with two or three sample streams, the measurement sequence
option lets you customize the sequence of sample stream measurements.
The analyzer will measure the sample streams based on the “step order” the
operator selects. The sample streams can be in any order; the analyzer will
sequence up to 8 sample cycles. For example: 1, 2, 3 or 1, 2, 1, 3, 1, 2.
5. Select SAMPLE SEQUENCE and press ENTER.
6. Select from the list of measurement sequences and press ENTER.
For each step (1–8), choose one of the measurement streams to

sequence. The instrument will analyze in this sequence down to the first
step left unused and will then repeat the sequence.
7. Select SAMPLE 1, SAMPLE 2, SAMPLE 3 or UNUSED (to remove a step

from the sequence) and press enter, or press exit to cancel.
Note: The sequence will terminate at the first unused step. Succeeding steps
will be cleared.
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51000-18 startup.fm Adding Sample Streams
Section 2
2.9.3 Selecting a Measurement Type

When analyzing one sample stream, the analyzer determines all five types of
alkalinity values listed below. To display each value, assign the measurement
type to a channel on the AquaTrend (see Section 2.9.4). Values will not be
displayed unless they are assigned a channel on the AquaTrend.
This option is used when the instrument is measuring more than one sample.
Analyzing two or three sample streams creates more than eight values that
can be displayed. Since the AquaTrend only has eight channels, the operator
must choose which eight values should be displayed.
For each sample stream, the choices are:

• Total (T) alkalinity
• Phenolphthalein (P) alkalinity
• Hydroxide alkalinity
• Carbonate alkalinity
• Bicarbonate alkalinity
To select the type of alkalinity measurement:
1. Press the MENU key to start at the MAIN MENU.
2. Select the SENSOR MENU and press ENTER.
4. Select MEASUREMENT OPTIONS.
5. Select ENABLE MEASUREMENTS.
6. Use the arrow keys to scroll to the desired measurement type and press
ENTER. An asterisk will appear next to the enabled measurement type.
This measurement may then be connected to a channel on the
AquaTrend (see Section 2.9.4)
7. To disable a selection, press ENTER to toggle it off. The asterisk

will disappear.
Page 64
Section 2
2.9.4 Measurement to Channel Connections
2.9.4.1 Attaching a Measurement to a Channel

Although more sample streams may be analyzed or sensors may be added to
the network, readings will not be displayed until the sensor output
(measurement) is attached to a channel. AquaTrend sensors can report one
or more measurements, depending on the type of sensor. Assign each sensor
measurement to one of the eight AquaTrend channels when setting up a
new sensor.
For example, APA Alkalinity analyzers can measure from 1-3 sample streams.
The alkalinity measurements for each sample stream can be displayed as five
types of alkalinity. To display any or all of these alkalinity types requires that
each measurement type be assigned a channel on the AquaTrend (see
Section 2.9.3). These could be called 1TAlk, 1PAlk, and 1HyAlk. To assign a
channel to a measurement, use the AquaTrend menu as described below.
1. Press the MENU key to begin at the MAIN MENU.
2. Use the up or down arrow key to select the AQUATREND MENU and
press ENTER.
4. Select MEASUREMENT TO CHANNEL and press ENTER.
5. Select ATTACH, and press ENTER. A list of available sensors will appear.
6. Select the sensor of interest and press ENTER.
• If the sensor has more than one measurement available, select the
desired measurement and press ENTER.
7. Select the channel (A or B) you want the data displayed on and

press ENTER.
8. Select ATTACH and press ENTER to attach, or select CANCEL to cancel

the attachment.
The message OPERATION COMPLETE will appear. The screen will return to
the display setup menu upon completion of the measurement to channel
setup. See Section 3.2.1 on page 70 for more information about viewing
process analysis data.
Page 65
Section 2
Attaching a measurement to channel with one sensor
Attaching a measurement to channel with more than one sensor
Page 66
Section 2
2.9.4.2 Detaching a Measurement From a Channel

Proceed as follows to detach a measurement from a channel:
1. Press the MENU key to begin at the MAIN MENU.
2. Use the up or down arrow key to select the AQUATREND MENU and
press ENTER.
4. Select MEASUREMENT TO CHANNEL and press ENTER.
5. Select DETACH, and press ENTER. A list of attached channels will appear.
6. Select the channel of interest and press ENTER. A description of the

channel will appear on the screen.
7. Select DETACH and press ENTER to detach, or select CANCEL to cancel

the operation.
The message OPERATION COMPLETE will appear. The screen will

return to the display setup menu upon completion of the measurement to
channel setup.
Page 67
Section 3 Normal Operation
3.1 Measurements
The specific steps of a normal measurement cycle are detailed in Table 11.
The measurement cycle carries out a colorimetric analysis to make an
accurate measurement of alkalinity in the sample stream (also see
Section 1.5 on page 25).
During normal operation the 10-port Rotor Valve rotates to various
positions to move sample and reagents through the analyzer. Table 10 lists
the port numbers and their function for each APA 6000™ Alkalinity Process
Analyzer. Table 11 describes the valve position and autoburette actions during
a normal cycle.
Table 10 Port Functions For Alkalinity Analysis
Port # Function Port # Function
1 Detector 6 Standard 2
2 Sample 1 7 Reagent 1
3 Sample 2 8 Reagent 2
4 Sample 3 9 Mixer
5 Standard 1 10 Grab sample
Table 11 Normal Alkalinity Cycle Sequence

Step # Valve Position Autoburette Action Comments
1 2 (sample port) Aspirates 300 µL sample into holding coil Flushes mixer out
2 9 (mixer port) Aspirates 300 µL from mixer Empties mixer
3 between ports Aspirates 100µL of Wash solution Goes to drain
4 10 (waste) Dispenses 700 µL ---
5 2 (sample port) Aspirates 1200 µL of sample ---
6 9 (mixer port) Dispenses 600 µL from mixer ---
7 9 (mixer port) Aspirates 800 µL Flushes mixer
9 2 (sample port) Aspirates 1450 µL into mixer Fills mixer with sample and indicator
10 9 (mixer port) Dispenses 950 µL ---
12 2 (sample port) Aspirates 1450 µL ---
13 9 (mixer port) Dispenses 950 µL ---
15 2 (sample port) Aspirates 1400 µL ---
16 8 (indicator port) Aspirates 50µL of indicator ---
17 9 (mixer port) Dispenses 900 µL. ---
18 10 (waste) Dispense 550 µL ---
19 2 (sample port) Aspirate 1600 µL Takes reference reading
20 1 (detector) Dispenses 1600 µL ---
21 9 (mixer port) Aspirate 1600 µL ---
22 1 (detector) Dispenses 1150 µL ---
23 9 (mixer) Aspirates 1117 µL ---
24 7 (titrant port) Aspirates 33 µL of titrant ---
25 1 (detector port) Dispenses 1600 µL to detector for measurement ---
Page 69
51000-18 normal operation.fm Normal Operation
Section 3
3.2 Process Analysis

The main function of the APA 6000 analyzer is to measure samples in the
sequence determined by the operator in the setup menu. Single channel
instruments simply measure one sample stream. Multi-channel instruments
measure 2-3 streams in the specified sequence. Grab sample measurement
and calibration interrupt the measurement cycle; once these special
measurement cycles are complete, the instrument continues with the normal
sample sequence.
3.2.1 Viewing Process Analysis Data
3.2.1.1 Numerical Display

The AquaTrend can display data from a 1-8 sensor channels at one time.
Access the display mode by pressing the DISPLAY key. Use the right arrow
key to increase the number of channels displayed on the screen. Press the
left arrow key to decrease the number of channels displayed. The up and
down arrow keys move up or down through the displayed channels. The most
current measurement is displayed for each channel. If a current measurement
for a channel is not available, the display will show “- - - -”.
When viewing more than one channel, the display will not identify the sensor
that is sending measurement data. If the APA is not networked, the
measurement channel is associated only with that specific APA. If the APA is
networked, you may see the same channel numbers displayed, even though
the channels show data from different analyzers. For example, you may see
two 1ALKALINITY channels displayed. To identify the instrument that is
sending the displayed data, highlight the measurement channel and press
ENTER. The display will show all the information for that measurement. Press
ENTER again to return to the multiple display screen.
3.2.1.2 Graphical Display

To monitor trends and obtain more details about a channel, use the graphical
display mode. The graphical mode displays only one channel at a time. First,
select the channel (in the numerical mode) you are interested in. Press
DISPLAY. Graph time appears on the x-axis (horizontal) and the range of
recent sensor readings appears on the y-axis (vertical). The default graph
time is 60 minutes for all channels.
A cursor may be used to examine the graph data in detail. The lower and
upper concentration limits are programmable as are the time intervals.
Three different display modes are available:
1. 60 minutes - displays the last 60 minutes of data where each point is

based on an average measurement value during a 30-second interval.
2. 24 hour - displays the last 24 hours of data where each point is based on
an average measurement value during a 12-minute interval.
3. 30 days - displays the last 30 days of data, where each point is based on
an average measurement value during a 6-hour interval.
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Process Analysis 51000-18 normal operation.fm
Section 3
3.2.1.3 Setting the Graph Time (x-axis)

1. Press the MENU key to access the MAIN MENU.
4. Select CHANNEL GRAPH SETTINGS from the DISPLAY SETUP MENU and
press ENTER. A list of available channels will appear.
5. Select the channel of interest and press ENTER.
6. Select TIMEBASE: and press ENTER. The pop-up screen shows: 60 min,
24 hrs, 30 days.
7. Select the desired time base and press ENTER to confirm the new setting
or press EXIT to cancel. The selected graph time will appear for a specific
channel on the x-axis on the graph each time a graph is displayed.
To change graph times for additional channels, select another channel as in

step 5, and repeat the remaining instructions in this section.
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51000-18 normal operation.fm Process Analysis
Section 3
3.2.1.4 Scaling the Graph Y-axis

To optimize the graphical display, establish the minimum and maximum values
you want displayed. If the expected range is 0-7 ppm, assign 0 as the
measurement minimum and 7 as the measurement maximum.
1. Press the MENU key to access the MAIN MENU.
4. Select CHANNEL GRAPH SETTINGS from the DISPLAY SETUP MENU and
press ENTER. A list of available channels will appear.
5. Select the channel of interest and press ENTER.
6. Select YMAX: and press ENTER.
7. Use the arrow keys to change the displayed values. Press ENTER to
accept the value or EXIT to cancel.
8. Repeat Step 6 and Step 7 to change the YMIN: displayed value. Enter
negative numbers by changing the first character to a negative sign with
the arrow keys.
3.2.1.5 Using the Graph Cursor

To examine specific data points on the graph, press ENTER from the display
data (measurement) screen. The graph cursor will appear as a long dashed
vertical line in the graph (see Figure 12 on page 31). Use the left and right
arrows to move the cursor to different time locations on the graph.The data for
the location of the cursor will change as the cursor is moved.
Time/date data for the cursor location will appear below the x-axis.
The measurement value at the cursor location will appear in the second field
from the top along the y-axis. The measurement value is an average of
several measurements. To examine the specific measurement data for the
point at the cursor location, press ENTER. The display will show the time, the
maximum and minimum concentration values and the average value. Press
EXIT to return to the graph.
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Process Analysis 51000-18 normal operation.fm
Section 3
3.3 Grab Sample Analysis

The grab sample capability of the APA 6000 Analyzer allows a quick analysis
of samples taken from alternative sample streams or analysis of a known
standard as a quality assurance check. See Figure 17.
Figure 17 Grab Sample Analysis
Grab Sample Plug
Grab Sample Block
1. Collect at least 100 mL of sample from the desired section of a sample

stream (or quality control sample). Hot grab samples must be cooled to
below 50 °C.
2. Filter the sample through a 22-µm filter.
Note: To filter sample, use a 60-cc syringe (Cat. No. 22587-00) and a 5-µm Acrodisc
(Cat. No. 22261-00). Draw sample into the syringe, attach the filter, then dispense
sample through the filter.
7. Select GRAB SAMPLE and press ENTER.
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51000-18 normal operation.fm Grab Sample Analysis
Section 3
8. Select MEASURE GRAB SAMPLE. The display will show PREPARING
SYSTEM FOR GRAB SAMPLE. PLEASE WAIT.
9. The display will read POUR GRAB SAMPLE. Remove the cap from the grab
sample block. Pour at least 100 mL of filtered sample into the grab sample
block (see Figure 17). Replace the cap.
10. The display will read MEASURING GRAB SAMPLE NOW. A pop-up menu
will display the time remaining to complete the grab sample analysis.
When the grab sample measurement is complete, the grab sample
reading will appear on the screen. The top reading is total alkalinity and
the bottom reading is P alkalinity
3.3.1 Grab Sample History

The following procedure allows you to view the date, time and readings of the
last eight grab samples taken.
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Grab Sample Analysis 51000-18 normal operation.fm
Section 3
5. Select GRAB SAMPLE and press ENTER.
6. Select GRAB SAMPLE HISTORY.
7. A pop-up box will appear with the most recent grab sample data, including
the time and date of the reading. Select REVIEW NEXT GRAB to step
through the eight most recent grab sample measurements. After the last
grab sample, press enter to return to the previous menu. Press Exit to
return to the grab sample history menu.
8. Pages that read ppm CaCO3 represent T alkalinity and pages that read just
ppm represent P alkalinity.
3.4 Calibration Options

Calibration prepares the APA analyzer to calculate concentrations in unknown
samples based on a calibration generated using two known standards. Two of
these standards are the high and low standard.
For immediate trend analysis, an electronic factory default calibration is

already established and allows the analyzer to provide approximate
measurements. The default calibration cycle is once a week at 1:00 a.m.
on Monday. This time may be changed to any other time during the day,
if desired.
The once-a-week auto-calibration interval may also be changed to every

12 hours, a specific day of the week or be turned off totally. The analyzer
accuracy specifications are based on an auto-calibration once every week.
Turning this option off will reduce reagent usage, but it may also reduce
measurement accuracy.
The analyzer automatically performs a calibration check every day to ensure

accurate measurements. This is not a calibration; the instrument checks the
value of one calibration point and compares it to the value of this point in the
current calibration. If the calibration check value is different than the user-
specified percentage, the instrument performs another calibration. To view
these calibration checks see Section 3.4.4 on page 78.
Calibration should only be performed after the analyzer has been

turned on for more than two hours. This allows the temperature inside the
analyzer to stabilize.
3.4.1 Manual Calibration

To start a calibration manually, proceed as follows. The instrument will finish
its current cycle, then perform the calibration.
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51000-18 normal operation.fm Calibration Options
Section 3
5. Select EXECUTE CALIBRATION and press ENTER. The CALIBRATION

PENDING message will appear.
The analyzer completes current measurement or priming cycles before

calibrating. Calibration typically takes 1.5 hours to complete. The maximum
calibration time is 2.5 hours It repeats a four-point calibration until two
readings match within a narrow acceptance band.
3.4.2 Manual Calibration Check

To start a calibration check manually, proceed as follows. The instrument will
finish its current cycle, then perform the calibration check.
5. Select EXECUTE CAL CHECK and press ENTER.
6. The CALIBRATION CHECK PENDING message will appear.
The analyzer will wait until any current measurement or priming cycle is
complete before doing the calibration check. Calibration checks typically takes
30 minutes to complete. The maximum calibration check time is 40 minutes.
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Calibration Options 51000-18 normal operation.fm
Section 3
3.4.3 Viewing the Calibration History

This option allows you to review calibration data of past calibrations.
5. Select CAL HISTORY and press ENTER.
6. A pop-up box will appear with the calibration date and time of the seven
most recent calibrations. Select REVIEW NEXT CAL to step through the
“pages” of the calibration history. After the last calibration, press ENTER to
return to the previous menu. To exit the CAL HISTORY MENU, press EXIT.
The calibration is a multiple point calibration, but the display will only show
the lowest and highest point values, which correspond to PT1 and PT2.
P alkalinity values will appear on the second line; T alkalinity values will
appear on the third line. These values represent what the new point would
have read on the previous curve.
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51000-18 normal operation.fm Calibration Options
Section 3
3.4.4 Viewing the Calibration Check History
This option allows you to review calibration check data of past

calibration checks.
5. Select CAL CHECK HISTORY and press ENTER.
6. A pop-up box will appear with the calibration check date and time of the
seven most recent calibrations. Select REVIEW NEXT CAL CHECK to step
through the “pages” of the calibration check history. After the last
calibration check, press ENTER to return to the previous menu. To exit the
CAL CHECK HISTORY MENU, press EXIT.
The display shows the calibration point checked in the first column and
the value measured during the calibration check in the second column.
The second line shows the T alkalinity value and the third line shows the
P alkalinity value.
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Calibration Options 51000-18 normal operation.fm
Section 3
3.5 Alarm Log Review

If an alarm warning is active, a number will appear at the bottom of the display
in the alarms area. Follow the instructions below to find out why the alarm
was triggered:
2. Select ALARM LOG and press ENTER.
4. Select either WARNING/ALARM LOG or SETPOINT ALARM LOG.

Press ENTER. The Warning/Alarm Log provides information on the
operation of the analyzer. The Setpoint Alarm Log provides information
about sample measurements that exceed the setpoint values.
The most recent alarm/warning is listed first. A bell icon to the left of the
warning indicates the alarm/warning is active. Selecting a specific
alarm/warning and pressing ENTER provides more detailed information about
that alarm/warning (i.e., time, date, value).
3.5.1 Clear Alarm Log

Selecting the CLEAR ALARM LOG option lets the operator delete past alarms
and warnings from the alarm log. To clear the alarm log:
5. Select CLEAR ALARM LOG and press ENTER.
6. Select YES and press ENTER to clear the alarm log.
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51000-18 normal operation.fm Alarm Log Review
Section 3
3.6 Cleaning the Instrument

To clean the outside of the instrument, wipe with a damp cloth as needed. Be
sure to clean up all reagent spills as soon as possible with a dry cloth,
followed by a damp cloth.
To clean the wetted parts of the analyzer, the system default is set to run a
normal clean cycle every day. However, you may want to use this option in
other circumstances. During operation air bubbles may develop inside the
autoburette, tubing or the colorimeter. This is especially true of new
instruments where system components are not thoroughly wetted. In addition,
clean samples require more cleaning cycles because clean water does not
contain enough surfactants to keep the system thoroughly wetted. To clear
bubbles from the system, use the Normal Instrument Clean function. If
bubbles persist in a new analyzer, use the alternate Cleaning Solution
(Cat. No. 26974-53) for the first weeks of operation.
Note: The alternate cleaning The cleaning option dispenses the cleaning solution (an acid) through all the
solution is a weak surfactant and wetted parts in the analyzer. The cleaning operation has several functions:
will not eliminate metal precipitate
in the system. • It is used to prime the system (cleaning solution is pulled directly into
the autoburette).
• It is used routinely to assure the wetted parts stay free of precipitate

build-up.
• If the cleaning solution is a surfactant, it can help remove air bubbles

retained in the system.
Note: This alternative solution should only be used for a break-in period.
• When a selected sample stream is not supplying sample to the analyzer

and excessive air is introduced into the system, the analyzer
automatically performs a clean function to re-prime the wetted parts.
5. Verify the instrument is set to the appropriate type of clean cycle

(NORMAL or EXTENDED).
6. Select INSTRUMENT CLEAN and press ENTER.
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Cleaning the Instrument 51000-18 normal operation.fm
Section 3
Note: Using the default settings is 7. Select one of the following:
strongly recommended by the
manufacturer and should only be • To clean the entire system immediately, select CLEAN SYSTEM NOW
changed if sample components and press ENTER. The analyzer will complete the current cycle, then
cause measurement problems. If perform the cleaning operation.
cleaning frequency is decreased,
verify that the cleanliness and • The system default is set to clean the analyzer every day.
operation of the analyzer is To change this default, select AUTO-CLEAN and press ENTER.
not degraded. Select the how often you want the analyzer to automatically clean
itself and press ENTER.
• To change the type of cleaning cycle, select NORMAL or EXTENDED.
Press ENTER. The analyzer will complete the current cycle, then
perform the cleaning operation.
3.7 Temperature Control

The analyzer temperature is controlled by maintaining a fixed temperature
(50 °C) in the detector and valve modules. Maintaining a constant
temperature within the analyzer is essential for ensuring the analyzer
performs to its specifications. Proper temperature maintenance requires the
analyzer be operated with the door securely fastened, and that modules not
be modified and remain clean.
If the air temperature surrounding the instrument becomes higher than the
temperature control point of the analyzer, the analyzer can still function but
performance may fall outside of specifications. Recalibrating at the air
temperature allows the measurements to remain accurate. Best accuracy is
achieved if a constant ambient temperature is maintained, even if it is above
the analyzer setpoint. If the analyzer is calibrated and measures at the same
temperature, readings will be accurate. If the control temperature changes
between calibration and measurement, accuracy will be reduced.
Page 81
51000-18 normal operation.fm Temperature Control
Section 3
3.8 Shutting the Analyzer Down (Off or Standby)

Before changing solutions or inspecting/replacing parts, place the analyzer in
“standby” then turn the instrument off. To turn the instrument off, open the
front door and locate the on/off switch near the top of the analyzer. Move the
switch to the off position. Placing the instrument in standby moves the
autoburette and rotor between ports and leaves the analyzer in a “known”
condition so restarting begins at a consistent place.
If the analyzer will be shut down for an extended time, it is best to run a clean
cycle just before shutdown to fill all the wetted parts with cleaning solution and
help prevent fouling/biogrowth in the system. See Section 3.6 on page 80
for cleaning.
To place the analyzer in standby:
1. Press the MENU key, then press ENTER.
2. Select SENSOR MENU, then press ENTER.
3. Select the sensor name and press ENTER.
4. Select SENSOR STATUS and press ENTER. A pop-up menu will appear.
Use the arrow keys to select STANDBY. Press ENTER.
To re-start the instrument:
1. Press the MENU key, then press ENTER.
2. Select SENSOR MENU, then press ENTER.
3. Select the sensor name and press ENTER.
4. Select SENSOR STATUS and press ENTER. A pop-up menu will appear.
Use the arrow keys to select RESTART. Press ENTER.
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Shutting the Analyzer Down (Off or Standby) 51000-18 normal operation.fm
Maintenance
DANGER
Some of the following manual sections contain information in the form of warnings, cautions and notes
that require special attention. Read and follow these instructions carefully to avoid personal injury and
damage to the instrument. Only personnel qualified to do so, should conduct the maintenance tasks
described in this portion of the manual.
DANGER
Certains des chapitres suivants de ce mode d’emploi contiennent des informations sous la forme
d’avertissements, messages de prudence et notes qui demandent une attention particulière. Lire et suivre
ces instructions attentivement pour éviter les risques de blessures des personnes et de détérioration de
l’appareil. Les tâches d’entretien décrites dans cette partie du mode d’emploi doivent être seulement
effectuées par le personnel qualifié pour le faire.
PELIGRO
Algunos de los capítulos del manual que presentamos contienen información muy importante en forma de
alertas, notas y precauciones a tomar. Lea y siga cuidadosamente estas instrucciones a fin de evitar
accidentes personales y daños al instrumento. Las tareas de mantenimiento descritas en la presente
sección deberán ser efectuadas únicamente por personas debidamente cualificadas.
GEFAHR
Einige der folgenden Abschnitte dieses Handbuchs enthalten Informationen in Form von Warnungen,
Vorsichtsmaßnahmen oder Anmerkungen, die besonders beachtet werden müssen. Lesen und befolgen
Sie diese Instruktionen aufmerksam, um Verletzungen von Personen oder Schäden am Gerät zu
vermeiden. In diesem Abschnitt beschriebene Wartungsaufgaben dürfen nur von qualifiziertem Personal
durchgeführt werden.
PERICOLO
Alcune parti di questo manuale contengono informazioni sotto forma d’avvertimenti, di precauzioni e di
osservazioni le quali richiedono una particolare attenzione. La preghiamo di leggere attentivamente e di
rispettare quelle istruzioni per evitare ogni ferita corporale e danneggiamento della macchina. Solo gli
operatori qualificati per l’uso di questa macchina sono autorizzati ad effettuare le operazioni d’istallazione
e di manutenzione descritte in questa parte del manuale.
Page 83
51000-18 maintenance stopper.fm Maintenance
Section 4 Routine Operator Maintenance
4.1 Maintenance Kit

Use the Tool Kit and the maintenance kit for routine maintenance. The
maintenance kit contains:
• Small O-rings for piston seals, 0.103 W x 0.237 ID (2)
• Large O-rings for piston seals, 0.0103 W x 0.424 ID (2)
• Teflon piston seals (2)
• Rotor replacement (1)
4.2 ! Scheduled Maintenance

Note: Chemicals are present in the Table 12, Table 13, and Table 14 provide lists of items to check monthly,
pump, valve and reagent tubing. every six months or yearly. If any of the items are in need of repair at the time
Before doing any maintenance, of the scheduled maintenance check, follow the direction under the
review all MSDSs and use Maintenance Required column.
recommended safety measures to
prevent exposure to potential
chemical hazards.
Table 12 Monthly Maintenance

Item Maintenance Required
Reagents and standards Replace reagents and standards. Make sure the reagent compartment and tubing are clean.
Autoburette module Inspect for seal or fitting leaks. Inspect for particulate build up.
Valve module Inspect the module and associated tubing for leaks.
Colorimeter Module Clean if discolored. No customer serviceable parts.
Sample conditioning filter(s) Inspect the filter. Clean or replace the filter.
Mixer Module Inspect for particulate build up.
Table 13 Six-Month Maintenance

Autoburette module Check for need to replace piston seals. Inspect for signs of leakage.
Valve module Replace rotor. Inspect stator.
Tubing and Fittings Inspect for leaks or damage. Replace as needed.
Table 14 Yearly Maintenance

Reagents Replace bottle vent assembly and supply tubing.
Autoburette module Replace piston seals.
Page 85
51000-18 routine operator maintenance.fm Routine Operator Maintenance
Section 4
4.3 Reagent Consumption

The rate of reagent use depends on many factors, including the number of
times the instrument cycles, calibration frequency, and the number of clean
cycles. In addition, the analyzer utilizes smart software to perform certain
functions automatically to correct for problem conditions. The analyzer
monitors reagent consumption and displays a “FLUID LEVEL LOW” warning
when the solution level falls below 5%. The following table provides the
volume of the reagents consumed with each type of function.
Table 15 Reagent Consumption

Cycle Length Standard 1 Standard 2 Reagent 1 Reagent 2 Cleaner Sample
Cycle Type
(minutes) (mL) (mL) (mL) (mL) (mL) (mL)
Measurement 8 0 0 0.033 0.05 0.1 7.4
Calibration
17 13 3 0.099 0.15 0.3 0
Check (typical)
Calibration
34 26 6.2 0.132 0.20 0.4 0
Check (max)
Calibration
80 45 30 0.33 0.5 1 0
(typical)
Calibration
135 76 48 0.53 0.8 1.6 0
(maximum)
Normal Clean 1.2 0.00 0 0 0 1.6 0
Extended Clean 10 0.00 0 0 0 9.3 0
Prime
2.5 0 0 1.2 1.2 2.0 0
Reagents
Prime
2.5 1.6 1.6 0 0 1.6 0
Standards
System Prime 7 1.6 1.6 1.2 1.2 2.0 1.6
Grab Sample 13 0 0 0.033 0.05 0.1 9.4
4.3.1 ! Changing Solutions

Solutions should be changed every month. Before replacing the solution,
place the analyzer in standby, then turn the instrument off (see Section 3.8 on
page 82).
The solution bottles are labeled as Reagent 1, Reagent 2, Standard 1,

Standard 2 or Cleaning Solution. The tubing into each of these bottles is also
labeled with the solution name to prevent reagent line mix-ups.
Hach recommends changing both standards at the same time. To change any
of these solutions see Section 2.5 on page 51.
Page 86
Reagent Consumption 51000-18 routine operator maintenance.fm
Section 4
4.4 Replacing Autoburette Seals

Replace autoburette piston seals if:
• air leakage into the autoburette body through the seals is visible
• there are signs of leakage on the back side of the autoburette module
Use the following procedure, Figure 18, and Figure 19 to replace the
autoburette seals:
1. Place the instrument in standby, then turn it off (see Section 3.8 on
page 82). This is when the piston is fully forward.
2. Break the siphon to the cleaning solution by disconnecting the reagent

tubing from the reagent vent cap insert. Lift the reagent line until the
bottom of the reagent line is above the liquid level in the bottle.
3. Remove all four tubing connections to the autoburette body.
4. Remove the lock ring from the autoburette body; set aside.
Figure 18 Autoburette Module

Lock Ring
Autoburette Body Assembly
Solenoid Valve
Autoburette Module Base

Autoburette
Piston
Page 87
51000-18 routine operator maintenance.fm Replacing Autoburette Seals
Section 4
Figure 19 Autoburette Body Assembly
O-ring O-ring Seal Spacer

40215-00 51191-00 51176-00
Autoburette Body Piston Seal Piston Seal

51108-00 51225-00 51225-00
Counter Bore O-ring O-ring Seal Gland Nut

(Seal Gland) 51191-00 40215-00 51328-00
5. Gently slide autoburette body assembly off of the piston by pulling it away
from the module base.
6. Remove seal gland nut using spanner wrench and set aside (see
Figure 20).
Figure 20 Using the Spanner Wrench
7. Remove the back piston seal and 2 O-rings and discard.
8. Remove the seal spacer and set aside.
9. Remove the front piston seal and 2 O-rings and discard.
10. Push 2 new small O-rings onto each of the 2 new piston seals to make a
seal/O-ring assembly.
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Replacing Autoburette Seals 51000-18 routine operator maintenance.fm
Section 4
11. Insert one seal/O-ring assembly into the seal gland of pump block with the
Teflon base against the bottom of the seal gland.
12. Insert the large O-ring into the bottom of the seal gland, seating with the
seating tool.
13. Insert the seal spacer into the seal gland, with cross-drilled holes and
groove oriented toward the bottom of the seal gland.
14. Insert one large O-ring into the seal gland and seat against the
seal spacer.
15. Insert a second seal/O-ring combination into seal gland.
Note: It is best to push on the 16. Install the seal gland nut until finger tight. Wet the piston with a towel
autoburette body assembly with the moistened with deionized water. Slide the pump body assembly partially
piston assembly tool after each onto the piston and tighten the seal gland nut, using a spanner wrench,
quarter turn of the seal gland nut to until the plunger on the force gauge bottoms out just before the piston
assure that the seals don’t become moves (see Figure 21).
over tightened.
17. Seat the autoburette body fully into the autoburette motor housing.
18. Reinstall the knurled housing lock ring until it is full tightened.
Figure 21 Using the Force Gauge Tool
Force Gauge Tool
Autoburette Body Assembly
Autoburette Module Base
Lock Ring
Page 89
51000-18 routine operator maintenance.fm Replacing Autoburette Seals
Section 4
Note: There should NOT be any 19. Reinstall all four tubing connections.
movement of the autoburette body
once the lock ring is fully in place. 20. Reinstall the reagent line and bottle cap into the cleaning solution bottle.
Be sure the reagent line is at the bottom of the bottle.
21. Prime the instrument (see Section 2.7.2 on page 55).
4.5 Maintaining the Valve Rotor and Stator

It may be necessary to clean inside the rotary valve and or inspect the
surface of the rotor and stator. If the surface finish of the these two surfaces
become scored from normal wear or scratched by debris, analyzer
performance will deteriorate.
Servicing the Rotary Valve
Refer to Figure 22 and these instructions:
1. Place the instrument in standby, then turn it off (see Section 3.8 on
page 82).
2. Shut off the sample flow.
3. Break the siphon to the reagent bottles and standard bottles as follows:
a) Disconnect the reagent line from the reagent vent cap insert. b) Lift the
reagent line so the bottom of the reagent line is above the liquid level in
each reagent/standard bottle. c) Re-collar the reagent line in the vent cap
insert to prevent it from moving around.
Figure 22 Valve Rotor Part Identification

7/64" Allen Cap Screw
3 Places
Valve Stator
1
2 10
3
9
8
Spacer
4
5
6
Valve Rotor
Valve Body
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Maintaining the Valve Rotor and Stator 51000-18 routine operator maintenance.fm
Section 4
Note: Avoid contaminating the 4. Before removing the valve head, remove tubing to ports 4, 7 and 10 for
standards. wrench clearance (see Figure 23). There is no need to drain sample line 3
as the sample was turned off in step 2. The line to port 7 is the grab
sample line. This will not drip if there is no fluid in the grab sample port.
Figure 23 Removing Screws From Valve Stator
1 1
2 2
10 10
3
3
9
9
4
4
8
8
7
7
5 5
6 6
(The tubing has been removed for clarity.)
Note: Do not the scratch the 5. Using a 7/64-in. Allen wrench, loosen the three recessed socket head cap
surfaces of the rotor and stator. screws in the valve stator (valve head). Do not completely remove the
screws, but back them out far enough to remove the head. These screws
will help hold a ring spacer that lies under the valve head or stator. Be
careful not to lose this spacer. Pull the valve head away from the valve
module and inspect surfaces of the rotor and stator.
Note: A small amount of fluid may 6. Inspect the slot in the rotor for any plastic shavings or sample debris. If
drain from the stator. If the volume is these are visible, remove the rotor from its holder for cleaning. Carefully
larger, be sure the siphon to the clean this slot with a small stylus, or a soft bottle brush, taking care not to
reagent bottles was broken. scratch the valve surface.
7. Inspect the valve surface of the valve head/stator. If this surface is scored,
replace the valve head along with the rotor.
Reinstallation
Note: If you are not sure what 1. Before reinstalling the rotary valve, dry all surfaces with paper toweling.
position the valve is in, briefly turn Reposition the valve head with port 1 at 12 o’clock (top center) on the
the instrument on. The valve will valve body. Make sure the locating pins in the valve body engage the
move to port 1. Immediately shut the locating pin holes on the back side of the valve head/stator.
instrument off.
2. Hold the valve stator in place as you engage the three socket head cap
screws. Take care to evenly tighten these three screws. You will feel an
even resistance as the valve stator tightens down because a spring
washer is compressed during the rotor/stator mating. Tighten these
screws in even increments until tight (100 to 120 inch-ounces of torque).
Note: Do not over-tighten these 3. Re-attach lines 4, 7, and 10 to the valve head/stator. If the valve stator is
valve fittings. These fitting are replaced, connect the remaining lines to the new stator.
finger-tight fittings. Torque these
fitting to no more than 18 inch- 4. Return the raised reagent lines of the reagent/standard bottles to their
ounces (0.13 Joules of torque). original positions.
Page 91
51000-18 routine operator maintenance.fm Maintaining the Valve Rotor and Stator
Section 4
5. Start the analyzer. Go to the prime menu and select the
PRIME ENTIRE SYSTEM option (see Section 2.7.2 on page 55).
Recalibrate the instrument (see Section 3.4 on page 75).
4.5.1 Replacing the Tubing

Tubing replacement will be required for one or more of the following reasons:
• A tube becomes crimped or kinked and is interfering with fluid flow.

• The tubing becomes fouled due to sample conditioning upset (or
improper sample conditioning).
Replacing a single tube:
1. Isolate the tube to be replaced from others it is grouped with (see

Figure 26 on page 94). If it is an external tube (to reagent containers,
sample inlet, or drain) remove the tubing cover from the back, underside
of the instrument case.
2. Remove the fittings on either end of the tube from their ports. Note
whether it is a ¼-28 flat bottom fitting or a 10-32 rotary valve fitting.
3. Remove the fittings from the ends of the tubing and discard.
4. Prepare a section of tubing the appropriate length, according to Table 16

on page 94.
5. If the tube is an external tube, slide the rubber grommet onto the tubing
and insert into the appropriate position in the manifold on the inside
bottom of the instrument case.
6. Route the tubing to its appropriate place on the outside and inside of the
instrument (refer to Figure 26).
7. Install the nut onto the tubing, followed by the spacer and ferrule, as
shown in Figure 24 or Figure 25.
8. Tighten fittings in the ports using the tightening tool provided.
Warning: DO NOT overtighten the fittings. This will result in poor

analyzer performance.
9. Reinstall the tubing cover.
Page 92
Section 4
Figure 24 #10-32 Fitting Assembly (Valve Head Assembly)
Ferrule Tubing
#10-32 Nut
Figure 25 1/4-28 Fitting Assembly
Ferrule and Locking Ring 1/4-28 Flangeless Nut Tubing

(see Detail A)
Chamfered End Flat End

Chamfered End Flattened End
of Locking Ring of Locking Ring
Detail A
Page 93
51000-18 routine operator maintenance.fm Maintaining the Valve Rotor and Stator
Section 4
Figure 26 Plumbing Diagram for a Alkalinity Analyzer
1 10
2 APA 6000
HACH COMPANY
LOVELAND, CO
HOLDING COIL 2 1
5 4
2-Way 3 16
VALVE
OUT
MIXER 2
6 1 AUTO-
IN
BURETTE
7
15
CO AIN
CL
ST
Wa
MI
ST
RE
RE
DR
XE
LO
AN
AN
EA
AG
s
AG
te
RD
RIM
DA
DA
NE
E
E
NT
NT
8
R
R
R
RA
ET
D2
D1
2
IN
ER
9 11 12 13 14
Table 16 Replacement Tubing Lengths for Figure 26

Item Description Length From... To...
1 Reaction Coil - part of Temperature Control Block Port 1 Colorimeter in
2 Tefzel tubing, 0.03 ID x0.062 OD 24 in. (60 cm) Port 2 Sample 1
3 Blank port --- --- ---
4 Blank port --- --- ---
5 Tefzel tubing, 0.03 ID x 0.062 OD 54 in. (135 cm) Port 5 Standard 1
6 Tefzel tubing, 0.03 ID x 0.062 OD 66 in. (167 cm) Port 6 Standard 2
7 Tefzel tubing, 0.03 ID x 0.062 OD 61 in. (152.5 cm) Port 7 Reagent 1
8 Tefzel tubing, 0.03 ID x 0.062 OD 66 in. (167 cm) Port 8 Reagent 2
9 Tefzel tubing, 0.03 ID x 0.062 OD 8.5 in. (21.3 cm) Port 9 Mixer in
10 Tefzel tubing, 0.03 ID x 0.062 OD 32 in. (80 cm) Port 10 Grab sample
11 Tefzel tubing, 0.03 ID x 0.062 OD 30 in. (75 cm) Mixer module out Mixer drain
12 Tefzel tubing, 0.03 ID x 0.062 OD 9 in. (22.5 cm) Two-way NC Autoburette top
13 Tefzel tubing, 0.03 ID x 0.062 OD 7 in. (17.5 cm) Two-way out Autoburette bottom
14 Tefzel tubing, 0.03 ID x 0.062 OD 47 in. (117.5 cm) Seal wash bottom Cleaning solution
15 Tefzel tubing, 0.03 ID x 0.062 OD 29 in. (45 cm) Colorimeter out Colorimeter drain
Call Hach
16 Holding Coil Center Port Autoburette
service
Drain Tygon tubing, ¾ -in. OD x 1/8-in. wall 72 in. (180 cm) Drain ---
Page 94
Section 4
4.6 Cleaning the Mixer Module

It may be necessary to clean the mixing chamber and the surface where the
stir bar rests. This is usually indicated if the chamber becomes discolored by
biogrowth, staining or sediment.
1. For safety reasons, run an EXTENDED CLEAN cycle before disassembling

the mixer module (see Section 2.8 on page 61).
2. Put the instrument in standby, then turn the instrument off (see
Section 3.8 on page 82).
3. Notice the mixer housing is split. Loosen the two Phillips screws that hold
the top of the module housing in the module block.
4. Hold the part of the housing next to the block while pulling the top of the
housing out from the block. The part of the housing that holds the stir bar
should stay attached to the instrument. Let the top part of the housing
hang from the attached tubing.
5. Use a cotton swab soaked with a dilute bleach solution to clean the mixing
chamber and the module housing top. Rinse well with deionized water.
6. If necessary, use a cotton swab soaked with a dilute bleach solution to

clean the surface the stir bar sits on and the stir bar. Rinse with deionized
water.
7. Reassemble the housing, making sure the O-ring and stir bar are in place.
8. Tighten the Phillips screws that hold the top of the housing to the block.
9. Restart the instrument (see Section 3.8 on page 82).
Page 95
51000-18 routine operator maintenance.fm Cleaning the Mixer Module
Section 4
Figure 27 Mixer Module Parts
Mounting Screw
2 Places
To Mixer Drain
To Rotary Valve
Stir Bar
20549-59 O-ring
40788-00
Page 96
Cleaning the Mixer Module 51000-18 routine operator maintenance.fm
Section 5 Warnings, Alarms, and
Troubleshooting
5.1 General Troubleshooting Procedure

This section provides general procedures to solve problems that affect the
analyzer’s performance. The first sign of a problem may be an alarm or
warning, but erroneous or erratic readings may not always cause an alarm or
warning. Being familiar with the steps in Section 5.1 on page 97 will help to
quickly solve operational problems.
5.1.1 Check Alarm Log

If any alarm or warnings occur, this will help narrow the search to a specific
module or problem. See the tables in Section 5.2 on page 99 for specific
alarm and warning messages and corrective actions. See Section 3.5 on
page 79 to review the alarm log.
5.1.2 Check Solutions
• Verify Reagent 1, Reagent 2, Standard 1, Standard 2, and Cleaning

Solution bottles are not empty and are connected to the correct tube.
• Ensure the reagent line in the guide tube goes to the bottom of the
reagent 1 bottle.
• Make sure standards are the correct value.
• Check tubing at the rotary valve and make sure the tubing is filled with
fluid, not air.
• If ports on the rotary valve have been removed recently, refer to the
plumbing diagram and ensure the ports were reconnected properly.
• If reagent or standard is not delivered to the valve, check for kinks in the
tubing. Replace any tubing that is kinked.
• If reagents or standards are degrading, check the seal on the bottle caps
and the tubing connections. Replace if necessary.
5.1.3 Examine the Rotor Valve
• Watch the rotor valve movement during a cycle. If fluid is moving from the
common port to more than one outlet port, cross-leakage in the rotary
valve is occurring. Inspect the rotary valve per Section 4.5 on page 90. It
is likely that stator will need to be replaced.
• Verify fluid is aspirated in when the autoburette is aspirating. If air is pulled

into the tubing connected to the center port, and there is fluid at the
selected port, the selected port may be clogged. Inspect and clean the
rotor valve per Section 4.5 on page 90.
• If reagent or standard is not delivered, disassemble and inspect the valve

and stator for blockage or buildup. Also inspect the reagent and standard
port tubing.
• If fluid in the holding coil is not observed, the holding coil may be blocked.
Replace the valve module.
Page 97
51000-18 warnings alarms and troubleshooting.fm Warnings, Alarms, and Troubleshooting
Section 5
5.1.4 Examine the Autoburette
• If air is moving through the piston seals during operation, replace the
seals per Section 4.4 on page 87.
• If there is fluid movement in both directions in the Cleaning Solution

tubing, there may be several causes. To check for a blockage,
remove the center port tubing from the rotary valve and see if the fluid
movement in the Cleaning Solution tubing stops. If the movement does
not stop, it is likely the solenoid valve is clogged or fouled; replace the
autoburette module.
• If there is fluid leakage around the autoburette body, check the seals
using the Force Gauge Tool (see Section 4.4 on page 87). Tighten the
seals if they are loose. If they are not loose, replace them.
5.1.5 Examine the Tubing and Fittings
• Check the tubing for kinks which may cause reduced or blocked flow.
Reduced or blocked flow may also be caused by fittings that are
over-tightened.
• Examine the fittings for leakage and tighten if necessary. The fittings
should be fingertight.
Page 98
General Troubleshooting Procedure 51000-18 warnings alarms and troubleshooting.fm
Section 5
5.2 Specific Alarm/Warning Messages

• There are two types of alarms, system alarms and sample setpoint
alarms. System alarms cause the analyzer to shut down and require
operator intervention to correct the problem. Sample setpoint alarms do
not shut the analyzer down and are caused by sample concentrations
exceeding the user-selected setpoint values.
• Warnings warn the operator of potential problems which might degrade

the performance of the analyzer.
• When an alarm or warning occurs, it is placed in the alarm log, which

stores up to 14 alarm/warning messages. The alarm log can be reviewed
from the AquaTrend (see Section 3.5 on page 79).
• The following tables describe the possible warnings and alarms, along
with causes, analyzer actions and corrective actions. Use these tables
and Section 5.1 to return the analyzer to proper operation.
Table 17 APA 6000 Set Point Alarms

Alarm/Warning Cause Analyzer Action Corrective Action
Enable assigned relay
LOW ALARM value Sample below user setting for when alarm condition
None
units relay setpoints occurs. Disable assigned
relay when condition clears.
HIGH ALARM value Sample exceeds user setting when alarm condition
None
units for relay setpoints occurs. Disable assigned
Sample rate change exceeds
RATE ALARM value when alarm condition
user settings for relay None
units occurs. Disable assigned
setpoints
Table 18 APA 6000 System Alarms

Detector module main analog Restart the analyzer. Replace detector
A/D FAILURE Analyzer shuts down
to digital converter has failed. module if problem persists.
Analyzer shuts down.
A counter which
records the number of
errors which occurred
A combination of at least 5
EXCESSIVE RE- today has recorded 5 Review alarm history for errors that caused
errors specified in the system
INITS errors. Counter is the shut down.
warnings.
reinitialized at
midnight and by
cycling power to the
analyzer.
RAM on APA main circuit Restart the analyzer. Replace main board if
RAM TEST FAILED Analyzer shuts down
board has malfunctioned. problem persists.
ROM on APA main circuit Restart the analyzer. Replace main board if
ROM TEST FAILURE Analyzer shuts down
board has malfunctioned. problem persists.
Page 99
51000-18 warnings alarms and troubleshooting.fm Specific Alarm/Warning Messages
Section 5
Table 18 APA 6000 System Alarms (continued)
The dipswitch is set to
Unknown dipswitch setting on inform the analyzer Verify dipswitch setting is correct. If
INVALID DIPSWITCH
APA main board. which chemistry problem persists, replace the main board.
to run.
NO xyz module
Internal network bus error; Verify module is installed correctly and
RESPONSE (where
software time-out occurred connections are secure. Restart the
xyz = colorimeter, Analyzer shuts down
while waiting for response analyzer. Replace module if problem
mixer, autoburette, or
from xyz module. persists.
rotary valve module)
An xyz module was not
Verify correct module is securely installed.
detected on the internal
NO xyz MODULE Analyzer shuts down Check cable connections. Verify correct
network bus, but is required for
chemistry is selected via dipswitch.
the selected chemistry.
An extra xyz module was
Verify correct chemistry is selected via
EXTRA xyz MODULE detected, but is not required Analyzer shuts down
dipswitch. Replace with correct module.
for the selected chemistry.
This xyz module type was Verify correct module software is being
WRONG MODULE
detected, but is not required Analyzer shuts down used. Verify correct chemistry is selected
(xyz)
for the selected chemistry. via dipswitch. Replace with correct module.
Cannot properly install xyz
INSTALL ERROR xyz Analyzer shuts down Replace module.
module.
Internal network bus error;
NO INT NEUR software time-out occurred Verify modules are securely installed.
Analyzer shuts down
RESPONSE while waiting for response Check cable connections.
from module.
Verify module is installed correctly. Check
Communication failed with xyz backplane cable connections. Restart
xyz NV FAIL Analyzer shuts down
module. analyzer. Replace module if problem
persists.
Table 19 APA 6000 System Warnings

Analyzer will check every
Verify sample is not flowing, then restore
Loss of sample x 30 minutes until sample is
SAMPLEx OUT sample flow. Then turn the analyzer off
detected. regained. Analyzer will
and back on to restart measurement.
restart measurement.
Check fluid level in each bottle. If fluid is
Standard, reagent or almost empty, replace the bottle and
STDx LOW REAGENT 1 Analyzer continues to
cleaning solution level reset fluid level. If fluid level is not near
LOW CLEANER LOW operate
is less than 5% full. empty, reset the fluid to the correct %
level.
Calibration is halted and a
Calibration failed with new calibration curve is not Check fluid levels. Verify standard values
CAL STDx FAILURE
standard x. calculated. Analyzer uses are correct.
previous curve.
Calibration standard Analyzer continues
CAL STDx OUT Check fluid level(s).
empty. operation
Loss of power to the Analyzer continues to
POWER FAILURE Check for loose power connections.
analyzer occurred. operate
Page 100
Specific Alarm/Warning Messages 51000-18 warnings alarms and troubleshooting.fm
Section 5
Table 19 APA 6000 System Warnings (continued)
Module xyz
temperature detector
Analyzer continues to If ambient temperature is well above this,
xyz TEMP VERY LOW measures below -10 °C
operate check the cable connections.
(clears when it is >-
5 °C).
Module xyz
Occurs on startup of analyzer and will
measure more than
clear after temperature control warms up
1 °C below the Analyzer continues to
xyz TEMP MARG LOW module to 50 °C. If ambient temperature
temperature setpoint. operate
is less than 5 °C, analyzer may not be
Warning clears when
able to get to temperature control range.
module temperature is
within 0.5 °C.
Module xyz
temperature detector Temperature is maintained at 40 °C by
measure more than 1°C heating. If ambient temperature is
above the temperature Analyzer continues to greater than 50 °C, this warning is
xyz TEMP MARG HIGH
setpoint. Warning clears operate displayed. If temperature changes are
when module rapid, analyzer may have trouble
temperature is within calibrating.
0.5 °C.
Module xyz
Analyzer continues to If ambient temperature is well below this,
xyz TEMP VERY HIGH measures above 58 °C
operate check all cable connections.
(clears when it is <
55 °C).
Module xyz
temperature is not
increasing to control Analyzer continues to Check cable connections. Shut heater off
xyz TEMP NOT MOVING
temperature setpoint operate and retry every 20 minutes.
with heater on full
power.
Analyzer restarts and tries
Unexpected xyz module to continue operation. If Verify module xyz is installed correctly.
xyz RESET reset (i.e., power loss or problem persists, it displays Check backplane cable connections.
low voltage). EXCESSIVE RE-INITS Replace module if problem persists.
alarm and shuts down.
to continue operation. If Check to ensure cable connections on
VALVE NO HOME Rotary valve cannot find
problem persists, it displays valve module are secure. Replace
SIGNAL the home location.
EXCESSIVE RE-INITS module if problem persists.
Valve home signal does
to continue operation. If Check to ensure cable connections on
not clear when valve
VLV HOME SIG ON problem persists, it displays valve module are secure. Replace valve
moves away from its
EXCESSIVE RE-INITS module if problem persists.
home position.
Rotary valve failed to Check valve for proper tightness and
to continue operation. If
arrive at its required obstructions to the valve rotor. Valve
VLV MOVE ERR problem persists, it displays
port after motor may be wearing out; replace valve
EXCESSIVE RE-INITS
request signal. module if problem persists.
Check valve for proper tightness and
Valve module required
Analyzer continues to obstructions to the valve rotor. Valve
VALVE STEPS ERROR extra steps to get to
operate motor may be wearing out; replace valve
final destination.
module if problem persists.
Page 101
Section 5
to continue operation. If Check for clogged lines in the analyzer.
Error in position
problem persists, and Check module cable connections.
BURETTEx HOME ERR detected since last
EXCESSIVE RE-INTS Replace Autoburette module if problem
cycle
alarm results and the persists.
analyzer shuts down.
Check for clogged lines in the analyzer.
to continue operation. If
The home position has Check module cable connections.
BURETTEx HOME DRIFT problem persists, it displays
drifted excessively. Replace Autoburette module if problem
EXCESSIVE RE-INITS
persists.
Home position is when autoburette is at
The module cannot find Analyzer restarts and tries
the fully dispensed position. Check
its home position (NO to continue operation. If
BURETTEx NO HOME module cable connections. If autoburette
HOME) or cannot move problem persists, it displays
BURETTEx HOME ON moves, check optical switch cable. If not,
away from its home EXCESSIVE RE-INITS
check motor cable connections. If
position (HOME ON). alarm and shuts down.
problem persists, replace Autoburette.
Autoburette system
hysteresis and Analyzer continues to Be sure seals are not too tight. If problem
BURETTEx HYST WARN
blacklash is greater operate persists, replace Autoburette module.
than 28 µL.
Analyzer main board Analyzer continues to May be problem with main board. Call
WATCHDOG TIMEOUT
processor times out. operate Hach Service.
Internal neuron cannot
INT NEUR HS TIME OUT communicate with main Analyzer shuts down If problem persists, call Hach Service.
board.
Analyzer tries to reconnect
Unexpected internal Cycle analyzer power. If problem
INT NEUR RESYNC with neuron and continue to
neuron reset occurred. persists, call Hach Service.
operate.
Analyzer tries to reconnect
Unexpected external Cycle analyzer power. If problem
EXT NEUR RESYNC with neuron and continue to
neuron reset occurred. persists, call Hach Service.
operate.
The AquaTrend was If problem persists, check cable
busy when analyzer Analyzer continues to connections. If communications between
AT NOT READY
tried to send operate the AquaTrend and analyzer are
a message. intermittent, call Hach Service.
If problem persists, check cable
The AquaTrend did not
Analyzer continues to connections. If communications between
AT NV FAIL respond after analyzer
operate the AquaTrend and analyzer are
sent message.
intermittent, call Hach Service.
External network bus
error - loss of Analyzer continues to
SIO NV FAIL Check cable connections to SIO.
communication with operate
SIO.
Voltage readings are made at the
VREF VOLT ERROR VDD
System voltage(s) are Analyzer continues to detector module. Check cable
VOLT ERROR VCC
outside specified limits. operate. connection at back panel. Ensure
VOLT ERROR
detector module is securely installed.
Attempt to perform
Analyzer continues to Be sure standard bottles contain
FAILED TO CAL CHECK check of calibration
operate. standard.
curve failed.
Page 102
Specific Alarm/Warning Messages 51000-18 warnings alarms and troubleshooting.fm
Section 5
A check of the
calibration curve
Analyzer continues to
CAL CHECK WARNING showed the check point Recalibrate the analyzer.
operate.
was outside the
specified range limit.
Unable to complete a Ensure calibration standard bottles are
CAL FAILURE operate using previous
calibration. not empty.
calibration curve.
Unable to complete a Ensure calibration standard bottles are
CAL STD OUT operate using previous
calibration. not empty.
calibration curve.
Detector A/D counts are
Analyzer continues to Replace colorimeter/detector module if
LED OUTPUT LOW below recommended
operate. problem persists.
operating range.
Detector A/D counts are
Analyzer continues to Replace colorimeter/detector module if
LED OUTPUT HIGH above recommended
operate. problem persists.
operating range.
Slope of calibration
MARG CAL (TALK Analyzer continues to
curve is outside nominal Check accuracy of calibration standards.
SLOPE) operate using new slope.
default slope.
Slope of calibration
MARG CAL (PALK Analyzer continues to
curve is outside nominal Check accuracy of calibration standards.
SLOPE) operate using new slope.
default slope.
P alkalinity calibration Analyzer continues to
CK STD2 P ACCURACY Check accuracy of calibration standards.
curve is questionable. operate using new slope.
Page 103
Section 5
5.3 Diagnostics
The diagnostic menu provides options to help the operator diagnose and
solve potential problems.
5.3.1 Hold Outputs

This option lets you interrupt the analyzer operation (e.g., maintenance
tasks, sample upsets) without affecting alarms or changing the
recorder/controller outputs.
5. Select HOLD OUTPUTS and press ENTER.
• Select HOLD OUTPUTS 30 MIN if you want to reset the timer to

30 minutes.
• Select ABORT OUTPUT HOLD if you want to return control of
outputs/relays to their appropriate status based on the current
sample measurements.
6. A pop-up window will show a countdown from 30 minutes. Normal

operation will resume after a time out.
Page 104
Diagnostics 51000-18 warnings alarms and troubleshooting.fm
Section 5
5.3.2 Internal Relay Test

This option allows you to activate and deactivate the relays to check
their function.
5. Select INTERNAL RELAY TEST and press ENTER.
6. Select the desired relay and press ENTER.
7. Select the desired state for the relay and press ENTER.
8. To return to normal operation, press ENTER or EXIT.
Page 105
51000-18 warnings alarms and troubleshooting.fm Diagnostics
Section 5
5.3.3 Internal Output Test

This feature allows the operator to manually set the current level of each of
the internal analog outputs to either the minimum, half (50%), or full output
level.
5. Select INTERNAL OUTPUT TEST and press ENTER.
6. Select the desired analog output and press ENTER.
7. Select the desired analog output value and press ENTER.
8. To return to normal operation, press ENTER or EXIT.
Page 106
Section 5
5.3.4 Default Calibration

If the analyzer is giving incorrect readings, you may want to re-set the
analyzer to use the default calibration. The default calibration allows the
analyzer to give good approximations of the measurement value. To ensure
that measurements meet analyzer accuracy specifications, perform a
calibration as described in Section 3.4 on page 75.
To set the analyzer to its default calibration, follow these steps:
5. Select DEFAULT CALIBRATION and press ENTER (press EXIT to cancel).

Select YES and press ENTER to set the analyzer to the default calibration.
Page 107
51000-18 warnings alarms and troubleshooting.fm Diagnostics
Section 5
5.3.5 Show Software Version Number

This selection informs the operator which version of primary software is
operating in the analyzer, as well as the software versions in each module.
This information is useful in determining replacement parts and service
information. To view the software version number:
5. Select SHOW VERSION NUMBERS and press ENTER.
6. Press ENTER to review the next page of version numbers.
Page 108
Installation
DANGER
Some of the following manual sections contain information in the form of warnings, cautions and notes
that require special attention. Read and follow these instructions carefully to avoid personal injury and
damage to the instrument. Only personnel qualified to do so, should conduct the installation/maintenance
tasks described in this portion of the manual.
DANGER
Certains des chapitres suivants de ce mode d’emploi contiennent des informations sous la forme
d’avertissements, messages de prudence et notes qui demandent une attention particulière. Lire et suivre
ces instructions attentivement pour éviter les risques de blessures des personnes et de détérioration de
l’appareil. Les tâches d’installation et d’entretien décrites dans cette partie du mode d’emploi doivent être
seulement effectuées par le personnel qualifié pour le faire.
PELIGRO
Algunos de los capítulos del manual que presentamos contienen información muy importante en forma de
alertas, notas y precauciones a tomar. Lea y siga cuidadosamente estas instrucciones a fin de evitar
accidentes personales y daños al instrumento. Las tareas de instalación y mantenimiento descritas en la
presente sección deberán ser efectuadas únicamente por personas debidamente cualificadas.
GEFAHR
Einige der folgenden Abschnitte dieses Handbuchs enthalten Informationen in Form von Warnungen,
Vorsichtsmaßnahmen oder Anmerkungen, die besonders beachtet werden müssen. Lesen und befolgen
Sie diese Instruktionen aufmerksam, um Verletzungen von Personen oder Schäden am Gerät zu
vermeiden. In diesem Abschnitt beschriebene Installations- und Wartungsaufgaben dürfen nur von
qualifiziertem Personal durchgeführt werden.
PERICOLO
Alcune parti di questo manuale contengono informazioni sotto forma d’avvertimenti, di precauzioni e di
osservazioni le quali richiedono una particolare attenzione. La preghiamo di leggere attentivamente e di
rispettare quelle istruzioni per evitare ogni ferita corporale e danneggiamento della macchina. Solo gli
operatori qualificati per l’uso di questa macchina sono autorizzati ad effettuare le operazioni di
manutenzione descritte in questa parte del manuale.
Page 109
51000-18 installation stopper.fm Installation
Section 6 Sample Conditioning
The nature of tasks described in this section requires individuals to

understand the associated dangers. Please read all caution statements in
the left-hand column of this section before installing the instrument. Burns,
shock, eye injury, fire and chemical exposure may occur. Hach Company
assumes individuals performing these tasks are qualified and aware of proper
safety procedures.
! DANGER DANGER
This instrument should be Cet appareil doit être installé par du personnel technique qualifié, afin d’assurer
installed by qualified technical le respect de toutes les normes applicables d’électricité et de plomberie.
personnel to ensure adherence to
all applicable electrical and PELIGRO
plumbing codes. Este instrumento debe ser instalado por personal técnico capacitado para
assegurar el cumplimiento con todos los códigos eléctricos y de plomería
aplicables.
GEFAHR
Um zu gewährleisten, daß alle elektrischen und sanitärinstallationstechnischen
VDE-Vorschriften und gegebenefalls die Zusatzvorschriften der zuständigen
Elektrizitäts- und Wasserwerke erfüllt werden, darf dieses Gerät nur von
geschultem Fachpersonal installiert werden.
PERIGO
Este instrumento deve ser instalado por pessoal técnico qualificado para
asegurar o cumprimento de todas as normas elétricas e de canalização
aplicáveis.
! DANGER DANGER
This instrument is not intended Cet instrument n’est pas conçu pour une utilisation avec des échantillons
for use with flammable samples inflammables ou des échantillons contenant des hydrocarbures.
or those containing
hydrocarbons. PELIGRO
Este instrumento no está destinado para uso con muestras inflamables o que
contengan hidrocarburos.
GEFAHR
Dieses Gerät nicht verwenden bei Tests mit brennbaren Lösemitteln oder
Lösemitteln mit Kohlenwasserstoffen.
PERIGO
Este instrumento não é feito com o fim de ser empregado com amostras
inflamáveis ou aquelas que contêm hidrocarbonetos.
Page 111
51000-18 sample conditioning.fm Sample Conditioning
Section 6
6.1 ! Sample Conditioning
6.1.1 Basic Clean Water Sample Conditioning

All samples must be “conditioned” using the single-sample, basic sample
conditioning kit shipped with each analyzer. The kit eliminates particles
greater than 22 µm and allows adjustments to provide proper sample flow
through the sample inlet block. See Section 7.7.1 on page 148 to install the
sample line into the analyzer.
The 22-µm Y-strainer filter protects the analyzer’s components and tubing by
allowing only particles smaller than 22 µm to pass on to the instrument
(a 22-µm particle is at the limit of visibility by the human eye). Use the ¼-inch
ball valve (refer to Figure 31 on page 117, item 21) to restrict and control the
flow rate of filtered sample from the filter through the sample inlet block (item
20). Install another on/off valve upstream of the filter for occasions when the
sample needs to be turned off or on. The filter housing valve (item 2) can be
opened to flush the unfiltered side of the filter element, or adjusted in any
partially open position for continuous bypass.
For samples that tend to clog the analyzer filter or tubing, additional
conditioning steps are required (see Section 6.2).
6.2 Adding To or Changing the Basic Sample Conditioning

The following sections cover available additions or changes to the Basic
Sample Conditioning kit. One or more of these additions or changes may be
necessary if the sample clogs the analyzer filter or tubing. The options are
presented from easiest to implement to more difficult to implement.
6.2.1 Unfiltered Sample Bypass

If the 22-µm filter clogs after a few days of use, use the sample bypass
procedure. Open the filter housing ball valve partially or fully (or remove the
valve completely) to increase flow and decrease clogging (see Figure 31 on
page 117). With this method, most of the sample coming to the instrument’s
filter is bypassed back to the sample stream without being filtered. This
bypassed sample flows axially through the tubular filter element and flows out
the filter housing’s bypass port without passing through the filter screen.
Some different applications for bypassing unfiltered sample through the filter
are as follows:
• Low to high flow bypass will let occasional sample upsets or slugs of
algae bypass through the filter rather than clogging the filter.
• High flow bypass will allow some self-cleaning of the filter as well as
provide the previously mentioned benefit of keeping the filter clear when
occasional sample upsets or slugs of algae occur.
• Unfiltered bypass flow may be used as a fast sample loop. If the sample is
a distance away from the instrument, the sample can be pumped through
a pipe to the filter. Unfiltered sample can then be returned back to the
sample site with pipe. This creates a fast flowing sample loop which can
minimize lag time between the process stream and the analyzer,
depending on the pump flow rate and pipe size selected. Use this concept
with clean or dirty water.
Page 112
Sample Conditioning 51000-18 sample conditioning.fm
Section 6
If the 22 µm filter clogs frequently, even when using the high flow unfiltered
bypass option, an air backflush kit may solve these problems. The 22-µm filter
will not collapse when using the air backflush option.
6.2.1.1 Using the Air Backflush Kit

The APA 6000 performs an air backflush each measurement cycle during a
time period when the instrument is not pulling sample into the instrument. Air
is injected on the filtered side of the filter element screen as controlled by the
APA 6000. The injected air pushes filtered sample and air backwards through
the filter element screen, and forces the debris into the fast flowing unfiltered
sample bypass stream. Additional air is injected which causes great
turbulence in the filter, along with the fast flowing unfiltered sample bypass
stream, further cleaning the filter element screen.
Installation
See Section 2.4.1.1 on page 49 to enable this option. The analyzer
automatically controls the timing of the air backflush by opening/closing the air
valve (item 28 in Figure 31) supplied with the kit. Electrical installation of the
air backflush is illustrated in Figure 28, Figure 29, and Figure 30. Only a
qualified technician should perform the electrical installation.
See Figure 31 on page 117 for plumbing the air backflush kit. Install the gray
female T-fitting (item 25) between the filter housing and the ¼-inch ball valve
(replace item 7 of the basic conditioning kit with item 25). The other
components of the air backflush kit attach to item 25. All the other
components are part of the Basic Water Conditioning Kit which must be
installed to route sample to the analyzer.
Figure 28 Air Backflush Wiring
Page 113
51000-18 sample conditioning.fm Adding To or Changing the Basic Sample Conditioning
Section 6
Figure 29 Schematic for Air Backflush Wiring, Single-Phase Relay*
* Refer to local electrical codes.
Page 114
Adding To or Changing the Basic Sample Conditioning 51000-18 sample conditioning.fm
Section 6
Figure 30 Schematic for Air Backflush Wiring, 2-Phase Relay*
Page 115
Section 6
Table 20 Parts List for Figure 31
Item Number Description Catalog Number
1 Screw, 6-32 x 1.5, pan head (2) 5593-11
2 Screw, 6-32 x 2.5, pan head (2) 19495-00
3 Fitting, elbow, ½-in. ID tubing x ¾-in. NPT (1) 30618-00
4 Fitting, reducer, ¾-inch NPT x ¼-inch FNPT (3) 31560-00
5 Teflon Tubing, 0.170 ID x 0.250 OD (10 feet) 45462-00
6 Tygon Tubing, ¾-in. OD x 1/8-in. wall (2 feet) 45543-00
7 Clamp, conduit hanger, 1-in. (2) 47349-00
8 Coupling, ¾-in. NPT x ¾-in. NPT (3) 49620-00
9 Manifold Grommet (1) 51036-00
10 Tee Fitting, 1 x 1 SOC x ¾-in. FNPT (1) 51080-00
11 Hex Nut Fitting, for 0.062 OD tubing (1) 51129-00
12 Ferrule Fitting, for 0.062 OD tubing (1) 51130-00
13 Flangeless Nut Fitting, for 0.062 OD tubing (1) 51131-00
15 Clean Water Label (affix to sample line) (1) Part of 51139-00
16 Tefzel Tubing, 0.030 ID x 0.062 OD (3 feet) 51178-00
17 PVC Pipe, 1-in. (1) 51239-00
18 Male Connector for ¼-in. tubing (3) 51246-00
19 Tube Fitting, ¼-in. tube x stem elbow (1) 51362-00
20 Sample Inlet Block (1) 51365-00
21 Ball Valve, ¼-in. NPT, PVC (1) 51395-00
22 Strainer Housing, ¾-in., without filter (1) 51396-00
23 Filter Element, 450 mesh (1) 51397-00
24 Teflon Thread Tape 70608-24
25 Female Tee Fitting, ¾-i.h NPT, gray (1) 31553-00
26 In-line Check Valve, for ¼-in. OD tubing 51172-00
27 Fitting, Tube, ¼-in. OD to ¼-in. OD 51179-00
28 2-way Air Solenoid Valve 51181-00
Page 116
Section 6
Figure 31 Assembly for Air Backflush and High-flow Unfiltered Sample Bypass
Page 117
Section 6
6.2.1.2 Ultrafiltration (Customer supplied)

Ultrafiltration is recommended to remove turbidity, algae, and
other biological components in the sample. See Figure 32 on page 118 for
the recommended plumbing configuration (numbers correspond to those in
Table 20).
Do not use the air backflush option with ultrafiltration.
Figure 32 Ultrafiltration Installation
Page 118
Section 6
6.2.2 Cleaning Submersible Sample Pumps Automatically

Some applications may use a submersible sample pump to pull sample from a
basin. In dirty water applications the pump inlet may clog frequently due to
large debris being pulled up against the filter screen of the pump. Turning off
the submersible pump will cause the sample in the pipe between the
submersible pump and the filter to siphon backwards through the submersible
pump. This will back flush most of the large debris from the inlet screen of the
submersible pump. The submersible pump can automatically be turned on
and off each cycle at the appropriate time by the APA 6000.
To turn the submersible sample pump off and on each cycle, you can program
one of the analyzer alarm relays to turn the power to the submersible sample
pump on and off. Use the analyzer alarm relays to control an appropriate
power relay which supplies power to the pump in use. See Section 2.4.1.2 on
page 50 to enable this option, and Figure 33 for installation. Also refer to
Section 7.3.2 on page 133 for information about the alarm contact
requirements and Figure 34, Figure 35, and Figure 36 for typical sample
pump connections.
Figure 33 Submersible Pump Installation
Page 119
Section 6
Figure 34 Sample Pump Control Using a Slave Relay*
Figure 35 Sample Pump Control Using An Intrinsically Isolated Solid State Relay*
Page 120
Section 6
Figure 36 Sample Pump Control Using the Voltage From the APA 4-20 mA Recorder Output For the
Control Voltage On a Solid State Relay*
To use the configuration in Figure 36, follow these steps:
1. Follow the steps for setting up alarm relays in Section 2.4.1.2 on page 50.
Choose one of the configured channels that receives sample from the
sample stream which the sample pump controls. For instance, if
measuring from sample stream 1, select that measurement as the alarm
relay between the recorder output and the solid state relay.
2. Follow the steps for setting up recorders output in Section 2.3.3.1 on

page 44. Set the minimum measurement value to 0.0 and the maximum
measurement value to 0.001. This ensures the recorder output is always
at 20 mA (maximum output). Select the 4-20 mA option after Step 16.
Page 121
Section 6
6.3 Installing Multiple Sample Streams

Order a Sample Conditioning Kit (Cat. No. 51045-00) for each stream added.
APA 6000 analyzers can measure up to three sample streams. To install a
second or third sample stream follow these instructions.
1. Plumb all components indicated in Figure 54 on page 151 as required by

the application. Assembly of some components is the same as for single
samples. Assembly of the components from the sample inlet block to the
rotary valve is described in the following steps.
2. Remove the two screws holding the sample inlet block to the side of
the analyzer.
3. Place the sample inlet block (item 20) from the kit on top of the original
inlet block. Install the next length screw from the kit through the holes in
both blocks and fasten to the side of the analyzer.
4. Open the analyzer door. Remove a blank rubber grommet from the
bulkhead on the same side of the analyzer as the sample inlet block.
5. Thread the tubing (item 16) through the manifold grommet (item 9). Push
the grommet into the empty hole in the bulkhead.
6. Thread the tubing out through one of the holes next to the original sample
tubing in the back of the analyzer.
7. Remove the plug at port 3 of the rotary valve. Put a hex nut fitting (item
11) and ferrule (item 12) on the tubing. Install it in port 3 of the rotary
valve. See Section 4.5.1 on page 92 for an illustration of this assembly.
8. Put the flangeless nut fitting (item 13) and ferrule fitting (item 14) on the
tube. Put the Sample 2 label on the tubing. Screw the nut and ferrule into
the sample inlet block.
If the APA 6000 relays are used to control air backflush or submersible pump
cleaning, it is possible to use these options on the added sample streams.
The APA internal alarm relays can be used in parallel to control them. See
Section 2.4.1.1 on page 49 and Section 2.4.1.2 on page 50 to set up these
options. Also refer to Figure 31 on page 117 and Figure 54 on page 151.
Page 122
Installing Multiple Sample Streams 51000-18 sample conditioning.fm
Section 7 Hardware Installation
7.1 Selecting a Location for the APA 6000 Analyzer

Locate the analyzers as close to the sampling point as possible. Shorter
distances between the process stream and the analyzer mean faster analyzer
response to changes in alkalinity concentration. Long sample lines are also
more vulnerable to sediment accumulation.
The instrument enclosure is designed for general-duty, indoor installation.

Do not mount the analyzer in direct sunlight. Ambient temperatures may
range from 5-50 °C (41-122 °F), but best performance will result if ambient
temperature is between 5 and 35 °C (41 and 95 °F).
To control the analyzer from a location other than the instrument location,
connect a Remote AquaTrend. The Remote AquaTrend can be mounted on a
bench, pole or panel as far away as 1320 feet (400 m).
Figure 37 Overall Dimensions of the APA 6000

20.58" (522.73 mm)
16.51" (419.35 mm)
AquaTrend™
DISPLAY EXIT
MENU ENTER
17.15" (444.75 mm) 20.75" (527.05 mm)
24.65" (626.11 mm)
Page 123
51000-18 hardware installation.fm Hardware Installation
Section 7
7.2 Mounting
7.2.1 Bench Mount

Important Note: It is mandatory the analyzer be bolted to the bench.
Secure the rear of the instrument to the bench or table with two ¼-20 UNC
screws to prevent the instrument from tipping while the module panel is open.
7.2.2 Wall Mount

The back plate of the instrument has four key-shaped holes for wall
mounting. The analyzer can be mounted directly to a wall or to rails capable
of holding 350 lbs (157.5 Kg). Leave at least 18-22 inches (46-56 cm) of
space above the top of the bolt pattern (see Figure 38) to allow access to the
reagent enclosures.
1. Make sure no power is supplied to the analyzer.
2. Locate appropriate mounting hardware for 3/8-16 UNC (Unified National

Coarse thread) hexbolts, according to the dimensions in Figure 38.
3. Install the top two 3/8-16 UNC hexbolts, leaving a ½-inch gap under each
bolt head.
4. Slide the bracket keyholes onto the bolts and lower the frame so the bolts
settle in the narrow part of the keyholes.
5. Install the two bottom bolts.
6. Tighten all four bolts securely.
7.2.3 Panel Mount

Note: Panel mounting is 1. Cut a hole in the panel using the dimensions in the template (Figure 39).
inconvenient because access to Leave at least 18-22 inches (46-56 cm) space above the top of the bolt
the reagents is limited. Hach pattern for access to the reagent compartments.
recommends you mount a remote
AquaTrend in the panel and wall or 2. Disconnect the reagent lines from the reagent bottles.
bench mount the analyzer near the
sample point.
3. Refer to Figure 40 and remove the reagent enclosures and supporting
brackets from the instrument. Each reagent enclosure has three brackets
which support the enclosure and act as tubing guides. Remove these
brackets from the instruments with a single pull. During operation, reagent
replacement will require access from the back side of the panel.
4. Remove the tubing cover from the bottom of the instrument.
Note: Be careful to not crimp or 5. Slide the instrument into the panel cutout so the back of the bezel is flush
compress the analyzer tubing when with the front of the panel.
panel-mounting the analyzer.
6. Install two #10-16 x 0.75-in. long self-tapping screws into the top
mounting holes (see Figure 39).
7. Install four #10-16 x 0.75-in. long, self-tapping screws into the side
mounting holes. Secure the reagent brackets with these screws also (see
Figure 39).
Page 124
Mounting 51000-18 hardware installation.fm
Section 7
8. Make all electrical connections described in Section 7.3.
9. Reattach the remaining brackets and reagent enclosures.
10. Mount the grab sample block to the front panel routing the tubing through
panel and into the tubing guide.
Figure 38 Mounting Dimensions
12.46" (316.40 mm)
11.50" (292.10 mm)
Page 125
51000-18 hardware installation.fm Mounting
Mounting
Page 126
Figure 39 Panel Mounting Dimensions
Section 7
17.086" (433.97 mm)
14.50" (368.30 mm)
14.00" (355.60 mm)
10.00" (254.00 mm)
.50" (12.70 mm) 4.00" (101.60 mm)
.31" (7.87 mm) 6.88" (174.77 mm)
1.90"
16.50" (419.10 mm)

(48.15 mm)
.213"
(5.41 mm)
11.87" (301.39 mm)
Cutout 8 Places
for
Instrument
1.150"
(29.21 mm)
15.00" (381.00 mm)
.725"
(18.42 mm)
.362"
.438" (9.21 mm)
(11.11 mm)
Cutout
(55.58 mm)
for
51000-18 hardware installation.fm
2.188"
Grab
Sample
.156" Block
(3.96 mm)
2 Places
.375"
(9.52 mm)
Section 7
Figure 40 Disassembly Required for Panel Mounting
Panel
#10-16 x 0.75" long

Self-tapping screws
(Customer Supplied)
Page 127
51000-18 hardware installation.fm Mounting
Section 7
7.3 ! Electrical Connections

DANGER DANGER
All electrical connections should Tous les branchements électriques doivent être effectués par un technicien
be made by a qualified technician qualifié pour assurer la conformité à toutes les normes électriques applicables.
to assure compliance to all
applicable electrical codes. PERIGO
Todas las conexiones eléctricas deben ser ubstaladas por personal técbico
cualificado a fin de asegurar su conformidad con las normas eléctricas
vigentes.
GEFAHR
Alle elektischen Anschlüsse müssen van qualifizierten Techniekem
durchgeführt werden, damit die Übereinstimmung mit allen elektrischen
Anschlussdaten gewärhrleistet ist.
PELIGRO
Todas as lagções eléctricas devem ser feitas por técnicos qualificados, para
assegurar o cumprimento de todos os regulamentos em vigor.
To access electrical connections in the APA 6000, remove the 2 hold-down

screws in the upper corners of the module panel. Slowly pull the panel forward
until it is fully supported by the steel restraining cable (see Figure 41 and
Figure 42).
Four access holes for electrical connections are provided along the back of
the instrument enclosure (see Figure 44). Remove the cover seals by
loosening the wing nuts from inside the instrument.
This product is designed to meet NEMA 4X (INDOOR) and IEC 529 I.P. 66
enclosure requirement when the front door is securely latched. Achieving
these protection levels, however, depends on the use of proper hardware in
the installation of this product. Standard off-the-shelf NEMA-approved conduit
hardware is required for proper installation of all electrical connections.
For process or industrial applications, the national electrical codes of most

countries require that AC service feeds be hard-wired and contained in
conduit systems. The APA 6000 Analyzer has been designed to conform to
this requirement.
Hach recommends conduit for two reasons:
1. It is generally required by most local electrical codes, and
2. Use of metal conduit can improve immunity to lightning surges and

AC power transients.
In hard-wired electrical applications, the power and safety ground service

drops for the analyzer should be no longer than 6 meters (20 feet) unless
metal conduit is used to shield the AC power wiring. In applications where
power cords are allowed by local electrical codes and power surges and
transients are not a great concern, an 18-gauge, 3-conductor power cord
(including a safety ground wire) can be used, but its length must not exceed
3 meters (10 feet).
The power cord or power cable is not supplied with the APA 6000
Analyzer and must be selected to meet applicable electrical codes for
the installation site.
Page 128
Electrical Connections 51000-18 hardware installation.fm
Section 7
Hach recommends that care be taken with hook-up configurations other than
shown in these illustrations. First, be sure your configuration satisfies local
electrical codes and second, ensure that your configuration does not cause
susceptibility to lightning, power surges, or transients upsets.
Figure 41 Looking Inside the APA 6000, with Hinged Module Panel Down
Panel Hold–Down Fasteners
Door Open
THIS CLASS A DIGITAL APPARATUS CET APPAREIL NUMERIQUE DE LA WARNING: FOR CONTINUED ADVERTISSEMENT: POUR UNE
NEMA 4X (INDOOR), IIP66
Instrument
PROTECTION AGAINST FIRE PROTECTION CONTINUE CONTRE
MEETS ALL REQUIREMENTS OF THE CLASSE A RESPECTE TOUTES LES HAZARD REPLACE ONLY WITH LE FEU REMPLACER LE FUSIBLE
CANADIAN INTERFERENCE CAUSING EXIGENCES DU REGLEMENT SUE LA SAME TYPE AND RATING OF PAR UN DU MEME TYPE ET
REGULATIONS. MATERIEL BROUILLEUR DU CANADA. FUSE DE MEMES CARACTERISTIQUES
! F1 & F2
On/Off NETWORK
A B
RECORDER
A
+ -
B
+ -
A
ALARM
NO COM NC NO COM NC
B
BLACK
1
WHITE
2
T, 1.6A, 250V
Switch J4?
Steel
Restraini
Cable
Module Panel
(Shown in
Open Position)
Page 129
51000-18 hardware installation.fm Electrical Connections
Section 7
Figure 42 Looking Inside the APA 6000, Removing the Customer Access Cover
Wingnuts
Door Open
NEMA 4X (INDOOR), IIP66
Instrument
PROTECTION AGAINST FIRE PROTECTION CONTINUE CONTRE
! F1 & F2
On/Off NETWORK
A B
RECORDER
A
+ -
B
+ -
A
ALARM
NO COM NC NO COM NC
B
BLACK
1
WHITE
2
T, 1.6A, 250V
Switch J4?
Module Panel is not Customer Access Cover

shown in illustration.
7.3.1 ! Power Connections At the APA Analyzer

Note: If power cords are allowed The APA 6000 Analyzer operates on any AC line voltage from 95-240 VAC,
by local electrical code, a 125 V 50 or 60 Hz. A 12- to 18-gauge power lead supply wire (power cord), with
UL/CSA-approved power cord with insulation rated at 300 V (600 V peak), is required. The analyzer is designed
an approved NEMA-style strain for hard-wire connection to ensure conformation to local electrical codes.
relief and a standard 115 V North
American-style plug (Hach Cat.
Route the power leads through the access hole on the back of the enclosure.
No. 46306-00) or a 230 V VDE-
Line voltage connections are wired directly to the terminal strip J10 (see
approved power cord with an
approved NEMA-style strain relief Figure 43). The ground connection is made to the adjacent ground stud using
and a Continental European-style an appropriate closed loop connector (see Table 21).
plug (Hach Cat. No. 46308-00) can
be ordered.
Table 21 sWiring Color Codes

Connector North American IEC
line conductor black brown
neutral conductor white blue
ground conductor green/green with
green with yellow stripe
(#8 stud) yellow stripe
Page 130
Section 7
Figure 43 Looking Inside the APA 6000, Locating and Identifying the Customer Connections
J11
Network Terminator
(enabled)
Door Open
THIS CLASS A DIGITAL APPARATUS CET APPAREIL NUMERIQUE DE LA

MEETS ALL REQUIREMENTS OF THE CLASSE A RESPECTE TOUTES LES
NEMA 4X (INDOOR), IIP66 WARNING: FOR CONTINUED
PROTECTION AGAINST FIRE
HAZARD REPLACE ONLY WITH
ADVERTISSEMENT: POUR UNE
PROTECTION CONTINUE CONTRE
LE FEU REMPLACER LE FUSIBLE
Instrument
On/Off
! F1 & F2
NETWORK RECORDER ALARM T, 1.6A, 250V
A B
A
+ -
B
+ -
A
NO COM NC NO COM NC
B
BLACK
1
WHITE
2
! Switch
J11
J10
Power
Terminal
Strip
Ground Stud
Module Panel is not J7 Ground J8 J9
shown in this illustration. Network Stud Recorder Alarm
Terminal Terminal Terminal
Strip Strip Strip
Back View of Air Purge

Instrument
Power Connections Network Connections

Alarm Connections Recorder Connections
Drain
Page 131
Section 7
Figure 44 Wiring Connections
Approved NEMA Instrument On/Off Switch

style strain relief
External
5 Amp
Circuit Breaker
NEMA 4X (INDOOR), IIP66 PROTECTION AGAINST FIRE PROTECTION CONTINUE CONTRE
! F1 & F2

A B A B
A B + - + - NO COM NC NO COM NC
BLACK
1
WHITE
2
!
J11
Permanent
Connection (Conduit)
#8 Ground Stud
Instrument On/Off Switch
Approved NEMA
style strain relief
! F1 & F2

A B A B
BLACK
1
WHITE
2
!
J11
Please adhere to the

guidelines required
for using power cords.
#8 Ground Stud
Page 132
Section 7
7.3.2 ! Alarm Relay Connections

DANGER DANGER
The relay connection area is La zone de raccordement des relais est conçue pour des connexions soit tout
designed for either all low voltage en basse tension (<30 V) soit tout en haute tension (>30 V). Un risque
(<30 V) or all high voltage (>30 V) d’électrocution existe si des connexions basse et haute tension sont faites dans
connections. A shock hazard la zone de raccordement des relais.
exists if low and high voltage
connections occur PELIGRO
simultaneously in the relay El área de conexión de los relés esta diseñada para conexiones que sean todas
connection area. de baja tensión (inferior a 30V o bien todas de alta tensión (superior a 30V).
Existe riesgo de descargas si se combinan conexiones de alto y bajo voltaje en
el área de conexión de los relés.
GEFAHR
Die Ralaisanschlüsse sind entweder für Niederspannung (< 30V) oder für
Hochspannung (>30 V) vorgesehen. Wenn sowohl Nieder-als auch
Hochspannung an die Relais angeschlossen wird, kann es zu einem
Stromschlag kommen.
PERIGO
A área de ligaçõ do relé é designada só para ligações de baixa voltagem (<30 V)
ou só para ligações de alta voltagem (>30 V). Dá-se um curto-circuito se fizerem-
se simultaneamente ligações de baixas e altas voltagens na área de ligaçõa do
relé.
Note: If voltages >30 Vrms are The Analyzer contains two alarm relays designed for use with either high
connected to the relay contacts, you voltage (greater than 30V-RMS and 42.2V-PEAK or 60 VDC) or low voltage
must limit current to the relay (less than 30V-RMS and 42.2V-PEAK, or less than 60 VDC), but not a
contacts to 5 amps and be able to combination of both high and low voltage. Hach recommends using these
remove power from the relays relays to control air backflush or submersible pumps.
locally in case of an emergency or
for servicing of the product. This can
Wire alarm relays to the connectors labeled Alarm A or Alarm B on the back
be accomplished with an external
switch and a 5-amp fuse or with a electrical panel (see Figure 45). SPDT relay contacts are unpowered and
switched 5-amp circuit breaker. rated to carry up to 5 amperes at 240 VAC with a resistive load. If high-current
or inductive-load devices are to be controlled by analyzer alarms, use a
heavy-duty slave relay actuated by the alarm relay. Both normally open and
normally closed contacts are available. The connector will accept 22- to 12-
gauge wire, insulated as appropriate for the voltage. Size the wires according
to the load and local electrical code regulations.
If more relays are desired, supplement your system with the AquaTrend
Signal Output Module (SOM). Each SOM provides two additional relays.
See Section 8.1 on page 155.
Page 133
Section 7
Figure 45 Alarm Relay Connections
Approved NEMA
style strain relief

CANADIAN INTERFERENCE CAUSING EXIGENCES DU REGLEMENT SUE LA
REGULATIONS. MATERIEL BROUILLEUR DU CANADA.
SAME TYPE AND RATING OF
FUSE
PAR UN DU MEME TYPE ET
DE MEMES CARACTERISTIQUES
Instrument
!
NETWORK RECORDER
A B A
ALARM
B
F1 & F2
T, 1.6A, 250V On/Off

!
+ - + -
Switch
BLACK WHITE
A B NO COM NC NO COM NC 1 2
J11
Relay
Permanent
Connection
(Conduit)
#8 Ground Stud
2 Places
7.3.3 ! Recorder Output Connections

DANGER DANGER
Facility power systems may have Les installations électriques dans les usines développent des tensions de
ground potentials if poor masse si de mauvaises techniques de mise à la terre sont utilisées. Pour réduire
grounding techniques have been les risques d’électrocution, prendre des précautions pour le branchement
used. To reduce the chance of d’équipements raccordés à la terre à des emplacements différents. Suivre
shock hazards, care must be attentivement les instructions données dans ce chapitre.
taken when connecting
equipment grounded at different PELIGRO
locations (potentials). Carefully Si no se emplean técnicas adecuadas de conexión a tierra, los sistemas
follow the instructions given in eléctricos de la instalación pueden generar tensiones de masa. Con el fin de
this section. disminuir el riesgo de descarga eléctrica, haga la conexión a tierra en lugares
diferentes. Respecte las instrucciones que se indican en esta sección.
GEFAHR
Spannungsversorgungsanlagen führen evlt. Erdpotential, wenn eine schlechte
Systemerdung vorgenommen wurde. Vosicht ist geboten, wenn das
angeschlossene Gerät an verschiedenen Orten geerdet ist. Die Anweisungen in
diesem Abschnitt sind genau zu befolgen.
PERIGO
Os sistemas eléctricos de aparelhos podem densenvolver tensões de massa se
forem utilizadas técnicas de ligação à terra fracas. Para reduzir a possibilidade
de perigo de choques, há que ter cuidado em ligar o equipamento à terra em
lugares diferentes. Siga escrupulosamente as instruções contidas neste
manual.
Page 134
Section 7
The analyzer contains two isolated 4-20 mA analog outputs which can drive
a recorder or control a process (see Figure 46). Recommended output
impedance is 3.6 to 500 ohms. Route 22-to 12-gauge recorder wires through
the access hole below the terminal strip and connect them to the terminal
strip J4, labelled “Recorder”. Use shielded, twisted-pair cable to connect
the analyzer to the recorder. Tie the shield to earth ground only at the
analyzer end to avoid ground loops. To ensure the analyzer meets
NEMA 4X and I.P. 66 enclosure ratings, use only the supplied NEMA-style
enclosure strain relief fittings.
If more analog outputs are desired, you can supplement your system with the
AquaTrend Signal Output Module (SOM). Each SOM provides two additional
analog outputs.
Figure 46 APA to Recorder Connections
! F1 & F2

A B A B
BLACK
1
WHITE
2
!
J11
Strip Recorder
Page 135
Section 7
7.3.4 ! Network Connections

DANGER DANGER
Facility power systems may have Les installations électriques dans les usines développent des tensions de
ground potentials if poor masse si de mauvaises techniques de mise à la terre sont utilisées. Pour réduire
grounding techniques have been les risques d’électrocution, prendre des précautions pour le branchement
used. To reduce the chance of d’équipements raccordés à la terre à des emplacements différents. Suivre
shock hazards, care must be attentivement les instructions données dans ce chapitre.
taken when connecting
equipment grounded at different PELIGRO
locations (potentials). Carefully Si no se emplean técnicas adecuadas de conexión a tierra, los sistemas
follow the instructions given in eléctricos de la instalación pueden generar tensiones de masa. Con el fin de
this section. disminuir el riesgo de descarga eléctrica, haga la conexión a tierra en lugares
diferentes. Respecte las instrucciones que se indican en esta sección.
GEFAHR
Spannungsversorgungsanlagen führen evlt. Erdpotential, wenn eine schlechte
Systemerdung vorgenommen wurde. Vosicht ist geboten, wenn das
angeschlossene Gerät an verschiedenen Orten geerdet ist. Die Anweisungen in
diesem Abschnitt sind genau zu befolgen.
PERIGO
Os sistemas eléctricos de aparelhos podem densenvolver tensões de massa se
forem utilizadas técnicas de ligação à terra fracas. Para reduzir a possibilidade
de perigo de choques, há que ter cuidado em ligar o equipamento à terra em
lugares diferentes. Siga escrupulosamente as instruções contidas neste
manual.
Note: The network supports The APA analyzer can be connected into a network to communicate with other
distances of up to 1650 ft sensors/analyzers and accessory modules. Refer to Table 22 to determine
(500 meters) with a maximum what wiring connections are necessary.
distance between any two devices
of 1320 ft (400 meters).
Table 22 APA 6000 Network Connections

APA 6000 Operated as a... Refer to Hardware Installation Section Gauge and Grounding Requirements
...single sensor system with no
No connection necessary in this section NA
external accessories
...single sensor system with an Shielded, 2-conductor, 18 ga. Tie shield
7.3.4.1 APA 6000 with SIO Module
SIO module at one end only.
Shielded 2-conductor 18 ga. from APA to
...single sensor system with PS1201. Shielded 4-conductor from
7.3.4.2 APA 6000 with SOM module
SOM(s) module PS1201 to other accessories. Ground at
PS 1201.
...single sensor system with SOM PS1201. Shielded 4-conductor from
7.3.4.3 APA 6000 with SIO and SOM(s)
and SIO modules PS1201 to other accessories. Ground at
PS 1201.
...a single sensor with an external
AquaTrend
or 7.3.4.4 APA 6000 With Other Sensors, SOMs PS1201. Shielded 4-conductor from
and SIO Modules PS1201 to other accessories. Ground at
...part of a Hach network system
PS 1201.
with other sensors and accessory
modules.
Page 136
Section 7
7.3.4.1 Connecting the APA 6000 Analyzer To a Serial Input/Output Module (SIO)
Refer to the Installation section of the SIO Module Manual for SIO electrical
connections. In Network Connections, the SIO manual refers you to connect
into the network via the appropriate sensor manual. At this point, proceed to
Section 7.3.4.5 on page 142 of this manual. See Figure 47 for an illustration
of the connection.
Figure 47 APA Analyzer to SIO Connections
Page 137
Section 7
7.3.4.2 Connecting the APA 6000 Analyzer to a Signal Output Module (via the PS1201)
1. Connect the SOM(s) to the power supply (PS1201) as directed in the

SOM Manual and the PS1201 Power Supply Manual.
2. In Network/Device Interconnect Between Two Power Supplies of the

PS1201 Power Supply Manual you will be connecting the network from
the PS1201 to the network connection inside the APA analyzer instead of
a second PS1201 power supply. Complete this section in the PS1201
Power Supply Manual for one end of the network cable. At that point,
proceed to step 3, below.
3. Connect the SOM(s) relays and analog outputs as directed in the SOM
Manual in SOM Power and Network Connections.
4. Proceed to Section 7.3.4.5 on page 142 of this manual.
Figure 48 APA Analyzer to PS1201 Connections
Page 138
Section 7
7.3.4.3 Connecting the APA 6000 Analyzer to SIOs and SOMs

If both a SIO and SOM will be used with the APA 6000 Analyzer, both the
analyzer and the SIO network connections should be made at the PS1201
Power Supply. Follow the steps below. (See Figure 49 for an example.)
1. Make electrical connections at the SIO. Refer to the SIO Manual for
electrical connections. The Network Connections section of the SIO
Manual refers you to connect into the network via the appropriate sensor
manual. At that point, proceed to Step 2, below.
2. Connect the other end of the SIO network cable to the PS1201 Power
Supply Module as directed in the PS1201 Manual in the SIO to PS1201
Connection section.
3. Connect SOM(s) to the Power Supply Module (PS1201) as directed in the

SOM Manual and the PS1201 Power Supply Manual. In Network/Device
Interconnect Between Two Power Supplies of the PS1201 Manual you will
be connecting the Network from the PS1201 to the network connections
inside the APA 6000 instead of a second PS1201 Power Supply.
Complete this section in the PS1201 Power Supply Manual for one end of
the network cable.
4. Connect the SOM(s) relays and analog outputs as directed in the

SOM Manual.
5. Proceed to Section 7.3.4.5 on page 142 of this manual.
Page 139
Section 7
7.3.4.4 Connecting the APA 6000 Analyzer to Other Sensors, an SIO Module and SOMs
Use the following guidelines to connect the analyzer into the network.
• The recommended way to connect an APA 6000 analyzer to a network is

to wire it to a PS1201 Power Supply (refer to preceding section).
• The APA 6000 has one opening for the network cabling connection. If only
connecting two APA 6000 analyzers together with no other sensors, refer
to Section 7.3.4.5 on page 142 and connect them directly to each other.
• If connecting multiple sensors, SIOs, and SOMs on the same network, it

may be necessary to add electrical junction boxes where the network
cabling can be spliced together. See Figure 57 on page 173 in the
glossary for examples of possible network configurations. Determine a
configuration that works for your application. Connect the network
connections for the other sensors, SIOs, and SOMs per their respective
manuals. For the APA 6000 network connections proceed to
Section 7.3.4.5 on page 142.
Page 140
Section 7
Figure 49 Connecting the APA to an SIO and SOM
Page 141
Section 7
7.3.4.5 Network Connections in the APA 6000

The connections described below use the following parts:
• Shielded, two-conductor cable (Cat. No. 52157-00)
• Cable Termination Kit (Cat. No. 52156-00) - includes:
• Strain Relief (2) (Cat. No. 52025-00)

• Sealing Washer (2) (Cat. No. 10338-14)
• Locknut (2) (Cat. No. 10596-12)
• Insulated Quick Connects (6) (Cat. No. 52143-00)
• Heat Shrink Tubing (1 foot) (Cat. No. 40825-00)
The Cable Termination Kit is supplied with the SIO, SOM, or PS1201
Modules. If connecting the APA 6000 to another APA 6000, order this kit and
cable along with the additional APA 6000.
1. Make sure there is no power supplied to the APA 6000.
2. Open the APA 6000 Door and remove the screws on the Hinged Panel
holding the modules to access the electrical connections at the back of
the instrument. Refer to Figure 41 on page 129.
3. Remove the two lower wingnuts on the lower back panel, then remove the
lower terminal strip cover. Refer to Figure 42 on page 130.
4. Remove the Wire Access Plug below the Network terminal strip where the
network cable will be routed into the APA 6000. Refer to Figure 43 on
page 131.
5. Take one end of the network cable and strip 6 inches (15 cm) of outer
insulation from the cable.
6. Put the strain relief and sealing washer (supplied with the cable) over the
cable and slide the strain relief and sealing washer 7 inches down from
the end of the cable. Tighten the strain relief nut until the cable does not
slip through the strain relief. See Figure 51 on page 144.
Note: Connect shield at one end of 7. Remove ¼ inch of insulation from the white and green wires. Either
cable only. If connecting to another insulate the shield wire with appropriate length of heat shrink tubing or
analyzer, then connect shield in only remove ¼ inch of insulation from the shield wire.
one of the analyzers. Insulate the
non-connected end with tape or 8. Add a insulated quick connect to each wire using a crimping tool.
heat-shrink tubing.
9. Pull the cable through the APA 6000 wire access opening until the strain
relief /sealing washer is pulled flush with the opening. From inside the
analyzer, screw the locknut onto the strain relief and tighten.
10. Connect the white wire to the APA 6000 position “A” on the Network
terminal block. Connect the green wire to position “B” on the Network
terminal block. If connecting the shield wire, connect the ground wire of
the cable to the terminal stud near the network terminal block.
11. If the AquaTrend in the analyzer will be the master AquaTrend or if the
analyzer is not connected to a network, connect network terminator by
Page 142
Section 7
placing the jumper over pins 2 and 3 on the J11 connector (see
Figure 50). If this is not the master AquaTrend, place the jumper over pin
2 (See J11 Disabled, below).
12. Replace the lower terminal strip cover over the electrical connections and
install the two wingnuts to secure the cover.
13. Close the Hinged Panel holding the modules and reinsert and tighten
screws holding the module door shut.
Figure 50 Network Terminator
J11 is shown Enabled
! F1 & F2

A B A B
BLACK
1
WHITE
2
!
J11
J11 Connector Jumper J11 Disabled J11 Enabled
3 3 3
1 1 1
Page 143
Section 7
Figure 51 APA 6000 Electrical Terminals and Fuse Location
J11
Network Terminator
(enabled)
Door Open

Instrument
On/Off
! F1 & F2
A B
A
+ -
B
+ -
A
NO COM NC NO COM NC
B
BLACK
1
WHITE
2
! Switch
J11
J10
Power
Terminal
Strip
Ground Stud
Module Panel is not J7 Ground J8 J9
shown in this illustration. Network Stud Recorder Alarm
Terminal Terminal Terminal
Strip Strip Strip
Fuse Holders
! F1 & F2

A B A B
BLACK
1
WHITE
2
!
J4?
Page 144
Section 7
7.4 ! Fuse Replacement

DANGER DANGER
Instrument power and power to Si l’alimentation de l’appareil l’alimentation des contacts des relais est
the relay contacts (if greater than supérieur à 30 volts, l’alimentation doit être débranchée avant de retirer ou
30 V) must be disconnected prior installer les fusibles de l’alimentation secteur de l’appereil. Un interrupteur ou
to the removal or installation of un coupe-circuit externe doit être utilisé. L’interrupter général de l’analyseur ne
the instrument input power fuses. coupe pas l’alimentation des fusibles.
This is accomplished by way of a
remote power switch or circuit PELIGRO
breaker system. The analyzer Si la tensión de alimentación del aparato y de los contactos de los relés es
power switch does not remove superior a 30 voltios, conviene desactivarlo antes de poner o quitar los fusibles
power from the fuses. de le alimentación de entrada. Para esta operación, es necesario emplear un
interruptor remoto o un dispositivo para cortar el circuito, ya que el interruptor
de conexión del analizador no desconecta la alimentación de los fusibles.
GEFAHR
Wenn der Gerätestrom und der Strom an den Relaiskontakten mehr als 30 Volt
beträgt, muss die Stromzuführung unterbrochen werden, bevor die
Eingangsssicherungen des Geräte eingesetzt bzw. entfernt werden. Ein
Fernleistungschalter oder ein Abschalter müssen benutzt werden. Durch den
Stromschalter des Analysators wird der Strom nicht von den Sicherungen
genommen.
PERIGO
Se a corrente no instrumento e a corrente nos contractos do relé é superior a 30
Volts, a alimentação tem de ser desligada antes de remover ou instalar os
fusíveis de entrada do instrumento. Deve-se usar um interruptor de corrente
remoto ou um interruptor no circuito. O interruptor do analisacor não remove
corrente dos fusíveis.
The analyzer contains two T, 1.6 A, 250 V, AC-line (5mm x 20 mm) fuses
(Cat. No. 52083-00. These are located on the power supply board in the back
of the instrument. They protrude through the power supply cover on the lower
right side and are labeled F1 and F2 (see Figure 51). It is not necessary to
remove the power supply cover to replace the fuses.
Follow the instructions below to replace the fuses:
1. Disconnect all AC power to the analyzer.
2. Turn the fuse carrier ¼ turn counterclockwise to remove it from the

fuse holder.
3. Replace the fuse (T 1.6 A, 250 V, Cat. No. 52083-00) inside the carrier.
4. Turn the fuse carrier ¼ turn clockwise to reinstall it in the fuse holder.
5. Reconnect AC power to the analyzer.
Page 145
51000-18 hardware installation.fm Fuse Replacement
Section 7
7.5 ! Changing Modules

Refer to Figure 52 and follow the instructions below to replace a module:
Note: Chemicals are present in the 1. Put the analyzer in standby (see Section 3.8 on page 82). Turn off power
pump, valve and reagent tubing. to the instrument by toggling the on/off switch at the top center of the
Before doing any maintenance, module panel to off.
review all MSDSs and use
recommended safety measures to 2. Break the siphon of any reagent/cleaning tubing that is connected to the
prevent exposure to potential
module by removing the tubing from the bottles (see Section 2.5 on
chemical hazards.
page 51). Shut off the sample stream to the analyzer.
3. Remove all fittings from the module.
4. Loosen the two captive screws that secure the module to the instrument
panel with a Phillips screwdriver.
5. Pull the module straight out to remove.
6. Reverse the process to reinstall the module.
Figure 52 Part Identification for Module Removal
Loosen these
captive screws to
remove modules.
Page 146
Changing Modules 51000-18 hardware installation.fm
Section 7
7.6 Air Purge

Air purge may be necessary if the analyzer is located in an environment with
high humidity and/or caustic vapors. The goal is to maintain a slight positive
pressure in the instrument with dry instrument air.
The air purge connection is located in the middle of the back of the
instrument. To connect an air supply, remove the plug in the quick connect
fitting using the Quick Connect Release tool. Connect ¼-in. poly tubing by
pushing the tubing into the fitting. You should feel two distinct “stops” as you
push. If the tubing is not seated, it will pop out when air pressure is applied.
Use only dry instrument air at 15 scfh.
7.7 ! Plumbing Installation

The nature of tasks described in this section requires individuals to
understand the associated dangers. Please read all caution statements in the
left-hand column of this section before installing the instrument. Burns, shock,
eye injury, fire and chemical exposure may occur. Hach Company assumes
individuals performing these tasks are qualified and aware of proper safety
procedures.
CAUTION PRUDENCE
This instrument is not intended Cet instrument n’est pas conçu pour une utilisation avec des échantillons
for use with flammable samples inflammables ou des échantillons contenant des hydrocarbures.
or those containing
hydrocarbons. CAUDAD
Este instrumento no está destinado para uso con muestras inflamables o que
contengan hidrocarburos.
VORSICHT
Dieses Gerät darf nicht für Tests mit brennbaren Proben oder Proben, die
Kohlenwasserstoffe enthalten, benutzt werden.
ATENÇÃO
Este instrumento não é feito com o fim de ser empregado com amostras
inflamáveis ou aquelas que contêm hidrocarbonetos.
DANGER DANGER
This instrument should be Cet appareil doit être installé par du personnel technique qualifié, afin d’assurer
installed by qualified technical le respect de toutes les normes applicables d’électricité et de plomberie.
personnel to ensure adherence to
all applicable electrical and PELIGRO
plumbing codes. Este instrumento debe ser instalado por personal técnico capacitado para
assegurar el cumplimiento con todos los códigos eléctricos y de plomería
aplicables.
GEFAHR
Um zu gewährleisten, daß alle elektrischen und sanitärinstallationstechnischen
VDE-Vorschriften und gegebenefalls die Zusatzvorschriften der zuständigen
Elektrizitäts- und Wasserwerke erfüllt werden, darf dieses Gerät nur von
geschultem Fachpersonal installiert werden.
PERIGO
Este instrumento deve ser instalado por pessoal técnico qualificado para
asegurar o cumprimento de todas as normas elétricas e de canalização
aplicáveis.
Page 147
51000-18 hardware installation.fm Air Purge
Section 7
7.7.1 Sample Tubing Installation

Selecting a good, representative sampling point is important for optimum
performance from the analyzer. The sample analyzed by the analyzer must be
representative of the condition of the entire system. If a sample is drawn from
a location too close to points of chemical additions to the process stream,
inadequate mixing or an incomplete reaction can result in erratic readings
from the analyzer.
Note: Plumbing connections should Run sample lines with small diameter tubing to the analyzer to minimize
be made only by qualified personnel lag time (the time required for sample to flow from sample point to the
to assure conformance to all analyzer). Route the tubing as directly as possible between the sampling
applicable plumbing codes. point and the analyzer. Long sample lines and low flow rates result in
significant lag time between actual process line conditions and the sampling
point of the instrument.
Install sample line taps into larger process pipes to minimize the chances of
ingesting sediment from the pipe line bottom or air bubbles from the top. A tap
projecting into the center of the pipe is ideal (see Figure 53).
Figure 53 Sample Line Location in Process Stream
Air (Typical)
Sediment (Typical)
Poor Poor Good Best
New tubing, valves and other sample conditioning equipment may be

contaminated with substances (oils, dust, etc.) which may contribute to low or
high readings on initial startup. Flush the sample line with sample for 1-2
hours before calibration. For faster cleaning, inject 1-4 liters of a dilute caustic
solution such as 1 N (5%) sodium hydroxide solution into the sample line and
force it through to clean sample system components. Waiting for the sodium
hydroxide solution to flow through the system and into the analyzer is
sufficient time to remove the contaminants.
All samples are “conditioned” using the single-sample, basic sample

conditioning kit shipped with each analyzer (see Figure 54 on page 151). The
kit eliminates particles greater than 22 µm and allows adjustments to provide
proper sample flow through the sample inlet block.
For samples that tend to clog the analyzer filter or tubing, additional
conditioning steps are required (see Section 6.2 on page 112).
The 22-µm Y-strainer filter protects the analyzer’s components and tubing
by allowing only particles smaller than 22 µm to pass on to the instrument
Page 148
Plumbing Installation 51000-18 hardware installation.fm
Section 7
(a 22-µm particle is at the limit of visibility by the human eye). Use the ¼- inch
ball valve to restrict and control the flow rate of filtered sample from the filter
through the sample inlet block. The customer should install another on/off
valve upstream of the filter for occasions when the sample needs to be turned
off or on. The ball valve on the filter housing can be opened to flush the
unfiltered side of the filter element, or adjusted in any partially open position
for continuous bypass.
The filtered sample then flows through the sample inlet block, from which the
instrument draws sample when needed. The analyzer is very flexible
concerning the sample flow rate through the sample bypass block. Within
reasonable bounds, the instrument is not affected by how fast the sample is
flowing through the block (it should be between 25 and 1000 mL per minute).
From the sample inlet block, the filtered sample flows to the filtered sample
bypass drain tee. It is very important to mount the bypass drain tee 6 inches to
3 feet (15 to 90 cm) higher than the sample inlet block. When properly
mounted, the vacuum breaker design of this bypass drain tee prevents
negative sample pressure and establishes the needed positive sample
pressure for sample flow through the analyzer. Connect the filtered sample
bypass drain tee to 1-inch PVC pipe, and run the pipe to the drain location.
PVC pipe is generally less expensive than hose or tubing, and is more
permanent and trouble-free than flexible hose or tubing.
7.7.1.1 Assembling the Basic Clean Water Sample Conditioning Kit
1. Assemble the parts of the system in the configuration shown in Figure 54.
2. All threaded fittings need to be sealed with two wraps of the teflon
tape provided.
3. Unscrew the top of the filter housing. Insert the filter element (either end
first) and push until it stays in place. Replace the filter housing top.
4. When pushing tubing into the push-in fittings, make sure you push the
tubing all the way in. Two distinct “clicks” should be felt when pushing in
the tubing. The first is when the tubing clears the gripper ring, and the
second is when the tubing bottoms out in the fitting.
Note: This may be a little difficult. To 5. Be sure to cut the ¼-inch O.D. tubing for use in the push-in fittings with a
help grip the tubing, try using rubber sharp knife so the ends are round, cleanly cut and not cut at an angle.
gloves or other material that grips
and forcefully push the tubing into 6. The push-in fittings are designed to use with soft ¼-inch OD plastic tubing
the fitting. Two stops should be felt; as included in the kit. Tubing material such as PTFE or HDPE is
otherwise the tubing will not be fully
recommended. The push-in fitting will not grip hard plastic or metal tubing
inserted and will leak.
and the tubing will slip out.
Page 149
51000-18 hardware installation.fm Plumbing Installation
Section 7
7.7.1.2 Using the Basic Clean Water Sample Conditioning Kit
1. Set filtered sample bypass flow by adjusting the ¼-inch ball valve, item 21
in Figure 54. The valve is fully closed when the lever is perpendicular to
the valve body and fully open when the lever is parallel with the valve
body. Hach recommends a filter bypass flow of 200–500 mL/min., but
25-1000 mL/min. is acceptable (see discussion in Determining Sample
Lag Time, Section 7.7.2 on page 152).
2. Check the flow by pulling the ¼-OD tube from the push-in fitting at the
drain tee (the tubing from the sample inlet block to the drain tee). If
desired, measure the flow rate by directing the sample into a large
measuring container (flask or cylinder) over a set amount of time. Keep
the end of the tube at the same height as the push-in fitting.
3. Clean or replace the filter as required. This is usually indicated by a

significant decrease in flow to the sample inlet block when the sample
stream pressure has remained the same .
Table 23 Parts List for Figure 54

Item Number Description Catalog Number
1 Screw, 6-32 x 1.5, pan head (2) 5593-11
2 Screw, 6-32 x 2.5, pan head (2) 19495-00
3 Fitting, elbow, ½-inch ID tubing x ¾-in. NPT (1) 30618-00
4 Fitting, reducer, ¾-inch NPT x ¼-in. FNPT (3) 31560-00
5 Teflon Tubing, 0.170 ID x 0.250 OD (10 feet) 45462-00
6 Tygon Tubing, ¾-inch OD x ¼ in. wall (2 feet) 45543-00
7 Clamp, conduit hanger, 1-in. (2) 47349-00
8 Coupling, ¾-inch NPT x ¾-in. NPT (3) 49620-00
9 Manifold Grommet (1) 51036-00
10 Tee Fitting, 1 x 1 SOC x ¾-in. FNPT (1) 51080-00
11 Hex Nut Fitting, for 0.062 OD tubing (1) 51129-00
12 Ferrule FItting, for 0.062 OD tubing (1) 51130-00
13 Flangeless Nut Fitting, for 0.062 OD tubing (1) 51131-00
15 Clean Water Label (affix to sample line) (1) Part of 51139-00
16 Tefzel Tubing, 0.030 ID x 0.062 OD (3 feet) 51178-00
17 PVC Pipe, 1-in. (1) 51239-00
18 Male Connector for ¼-in. tubing (3) 51246-00
19 Tube Fitting, ¼-in. tube x stem elbow (1) 51362-00
20 Sample Inlet Block (1) 51365-00
21 Ball Valve, ¼-in. NPT, PVC (1) 51395-00
22 Strainer Housing, ¾-in., without filter (1) 51396-00
23 Filter Element, 450 mesh (1) 51397-00
24 Teflon Thread Tape 70608-24
Page 150
Section 7
Figure 54 Sample Line and Basic Water Conditioning Assembly
Page 151
Section 7
7.7.2 Determining Sample Lag Time

The internal volume of the 22 µm filter shipped with the analyzer is 225 mL.
Take this volume into consideration along with the length of sample tubing
when deciding on a sample bypass flow rate. Generally, three volume
exchanges through the filter body, after a step change in the sample, will allow
90% of the change to be seen by the analyzer. Therefore, if the flow rate
through the filter is 100 mL/min, the number of minutes to achieve a 90%
change through the filter is:
(3 x 225 mL)/100 mL per minute = 6.8 minutes.
The lag time for sample to flow through the 0.25 O.D. X 0.17 ID tubing
supplied with the instrument must also be taken into account. The internal
volume of a 10 foot length of the tubing is 44.6 mL. Therefore, if the flow rate
is 100 mL/min, it will take (44.6 mL)/(100 mL/min) = 0.45 minutes for the
sample to flow through 10 feet of tubing.
The total lag time for the sample to reach the instrument would be the lag time
due to the filter plus the lag time through the tubing. Add the results for the
filter and 10 foot length of tubing as calculated above for the flow rates
indicated in Table 24.
It is best if sample bypass flow is 200–500 mL/min., but 25–1000 mL/min

is allowable.
Table 24
Lag time for 10 ft of Total Filtered Sample
Flow rate (mL/min) Filter lag time (min) Total lag time (min)
Tubing (min) Used L/day (gal/day)
100 6.8 0.45 7.2 144 (38)
200 3.4 0.22 3.6 288 (76)
500 1.4 0.10 1.5 720 (190)
7.7.3 ! Drain Line Connection

The analyzer is connected to a drain system through a ½-inch hose barb
fitting on a drain block on the side of the analyzer case. After analysis, the
waste exits the instrument through the manifold at the bottom of the
instrument and into the drain block. This block connects to a ½-inch ID hose
and provides a vented vacuum break at this point. The block vent, located on
the top of the drain block, has a barb fitting which can be used to ventilate the
tubing away from the instrument. Also see Section 7.7.4 on page 154.
Page 152
Section 7
Figure 55 Drain Line Connection
Drain Block
All drains must be at least one foot

below the bottom of the instrument.
Drains from Reagent Enclosures
Drain from Instrument Drain Block

(Customer supplied 3/4 inch tubing.)
From Catastrophic Drain
Route instrument waste through a ½-in. ID hose to a PVC pipe assembly,

which must be located at or below the level of the instrument drain block.
Note: It is imperative to mount this This assembly can be installed with the sample bypass and run into the same
drain point below the instrument drain or plumbed to a different drain than the sample bypass. Refer to
drain block. Failure to do so may Figure 55.
result in improper functioning of the
instrument or backflow of waste into The cabinet overflow drain is located in the middle of the tubing manifold and
the instrument cabinet.
is sized to accommodate a 1-in. ID hose. This drain is used if an upset inside
the instrument results in a significant leak. The supplied hose from this drain
port must be connected and run to a drain which is at or below the level of the
drain fitting.
The reagent enclosures each have an overflow fitting in the bottom of the
case. You can plumb these to the drain by punching out the knock-out in the
fitting, attaching a 3/8-inch ID hose to each fitting and running it to a drain
which is lower in elevation than the bottom of the reagent enclosure.
Page 153
Section 7
Figure 56 PVC Drain Assembly for the Instrument/Grab Sample Block Drain
From Drain Block

(Customer supplied 3/4 inch tubing.)
7.7.4 Waste Disposal

The effluent from the APA Alkalinity analyzer is non-hazardous per federal
RCRA regulations and may be safely discharged to a sanitary sewer based
solely on federal rules. Other state and local regulations or permitting
requirements may apply and it is the responsibility of the end-user to know
and apply state or local requirements to their specific applications. Hach
Company does not advocate the pouring, dumping or discharging of any
chemicals, hazardous or nonhazardous, to the ground or to septic systems.
Page 154
Section 8 Network Menu Configuration
8.1 Using the APA With a Signal Output Module (SOM)

This section describes how to set up the APA 6000™ Alkalinity Process
Analyzer to operate relays and/or analog outputs that reside in an SOM. For
initial setup and installation of the SOM to the APA 6000, follow all the steps in
the order listed below.
1. Perform the installation steps in Section 7.3.4.2 on page 138.
2. Perform the steps in Section 8.1.1.
8.1.1 Getting the SOM to Communicate With the APA 6000
1. Ensure step 1 of Section 8.1 has been completed.
2. Refer to Adding a Signal Output Module to the Network in the SOM

Manual. After successful completion of Section 2, the APA 6000 and the
SOM will be communicating over the network cable.
8.1.2 Verify SOM Connections
1. Ensure step 1 and step 2 of Section 8.1 have been completed. After
completion of these two steps it is assumed that electrical connections to
the SOM relays and analog outputs have been made.
2. Set up and test the SOM Relays and Analog Outputs per Section 2 of the
SOM Manual.
8.1.3 APA 6000 Menu Options for SOM Relays & Analog Outputs
Now you must assign the relay and analog outputs of the SOM to specific
alarm and recorder outputs of the APA 6000. Perform the steps in Alarm to
Relay Connections and Analog Output Settings in the SOM Manual. Then go
to Section 2.3 on page 40 to select the desired options.
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51000-18 network menu configuration.fm Network Menu Configuration
Section 8
8.2 Using an APA With an SIO Module

This section describes how to set up the APA 6000 to send data out to a
computer or to a printer through a SIO and describes the format of the data
sent. For initial set up and installation of the SIO to the APA 6000, follow all the
steps in the order listed below.
1. Perform the installation steps in Section 7.3.4.1 on page 137.
2. Perform the steps in Section 8.2.1 on page 156.
If the SIO is connected to a computer, refer to Section 8.2.5 on page 158

for computer remote operation commands for the APA 6000.
8.2.1 Getting the SIO to Communicate With the APA 6000
1. Ensure Step 1 of Section 8.2 has been completed.
2. Refer to Network Setup in the SIO manual. After successful completion of

that section, the APA 6000 and the SIO will be communicating over the
network cable.
8.2.2 Verify SIO Connection to Computer/Printer
1. Ensure steps 1 and 2 of Section 8.2 have been completed.
2. Verify SIO can transmit to Computer/Printer. Perform the PRINTER TEST

diagnostic in the Diagnostics section of the SIO Manual. This will verify
that the SIO and computer/printer cable connection is working properly for
data sent out from the SIO. If the test fails, troubleshoot the SIO per the
SIO Manual.
3. Verify the computer can transmit to SIO. If a computer will be used for
remote operation of the APA 6000, verify commands can be sent to the
analyzer. This can be done by transmitting xRID, where x = 1 to 8,
corresponding to channels 1 to 8. Follow this command with a carriage
return from the computer.
To find out what channel number data is being sent, turn the analyzer off and
on. On power up, the APA 6000 will send a message similar to the one below.
[1] Alkalinity V1.0 C1.0
This is the power up message. The number between brackets is the SIO
channel number for the APA analyzer.
If there is no return response, troubleshoot the SIO per the SIO Manual.
Page 156
Using an APA With an SIO Module 51000-18 network menu configuration.fm
Section 8
8.2.3 RS232 Data Format: APA 6000 Menu Options for SIO
The APA 6000 sends out measurement readings, alarms, and warnings
through the SIO. This section instructs how to select a particular format.
For a more detailed explanation of the format types, refer to Section 8.2.4.
4. Select SENSOR DIAGNOSTICS.
5. Select SIO1 SETUP or SIO2 SETUP.
Note the selections under SIO1 SETUP and SIO2 SETUP are the same. Up to
two SIOs can be connected to the APA 6000. If installing a second SIO or the
analyzer is connected to the second SIO on the network, select SIO2 SETUP.
If COMPUTER format is selected and OUTPUT is set to AUTO, the readings,

alarms, and warnings will be sent out as they occur. If OUTPUT is set to
QUERIED the information is sent only when a query command is sent from the
computer (see Section 8.2.4). The TIME/DATE will be sent with readings if
YES is selected and can be turned off by setting to NO.
If PRINTER format is selected, the OUTPUT and TIME/DATE options are

ignored and not shown in the menu.
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51000-18 network menu configuration.fm Using an APA With an SIO Module
Section 8
8.2.4 APA 6000 Printer and Computer Formats
8.2.4.1 Printer Format

Since the SIO can receive data from up to 8 analyzers, the SIO channel is
shown in the first three characters - i.e. [1] specifies information is from the
analyzer connected to SIO channel 1.
[1]01/01/97 00:23: 3.234 S1P1
[1]01/01/97 00:23: 0.527 S1P2
[1]01/01/97 11:28: 3.977 S1P1 *W
[1]01/01/97 11:28: SMP1 OUT ALARM *A
[1]01/01/97 11:28: 0.611 S1P2 *A * W
[1]01/01/97 11:29: End SMP1 OUT ALARM *A
First occurrence of any alarm or warning will be sent out. The time/date of the
alarm or warning is printed followed by either ALRM or WARN to specify it is
an alarm or warning. The specific alarm or warning is then printed on the next
line. When the alarm or warning condition clears it will be sent preceded by
END: to indicate the condition is cleared. Some alarms and warnings provide
information only and do not have an end (i.e. a fail to calibrate message is
printed out only when the condition occurs). If a alarm or warning condition is
active, then a *A for alarm or a *W for warning is appended to the
measurement readings.
8.2.4.2 Computer Format

When the SIO is setup to transmit to a computer, the format is similar to the
printer format described above. In addition, the year is included in the date
and the alarms and warnings are printed out on the same line as the time and
date. When using PC format, the time/date stamp can be disabled and the
readings can be queried instead of being sent out in real-time. If the SIO is in
Queried mode, the readings are sent out only when the analyzer receives
RMR command, alarms and warnings are sent only when receive RAR
command (refer to Section 8.2.5 for more on RMR and RAR commands).
8.2.5 Remote RS232 Commands

Table 25 lists the commands that can be sent to the APA 6000 Analyzer for
remote analyzer operation.The analyzer response to remote commands will
be OK if changing instrument settings. Commands which query settings or
values will be responded to with the current settings or readings. If the
analyzer does not recognize the command then a BAD CMD message is
returned. If the analyzer recognizes the command but the settings are invalid
then BAD SETTINGS is returned.
Messages to the analyzer must be terminated with a carriage return character

to signify end of command. Linefeed characters and spaces are ignored. All
incoming characters are converted to uppercase before evaluated.
When sending commands through the SIO, the channel number must
precede the command. For example, if the analyzer is connected to SIO
channel 1 and you wish to restart the analyzer, 1SRT should be sent. The
analyzer will reply with OK and the SIO inserts the channel assigned for the
analyzer (i.e. [1]OK will be the response to the computer).
Page 158
Section 8
Table 25 APA 6000 Remote RS232 Commands
Description of Remote Command Command Description of Command/Settings
Restart system SRT Restarts the system
Put instrument in standby HLT Puts the analyzer in standby
Perform a calibration CAL Performs a calibration at end of the current cycle
Perform a clean cycle CLN Performs a clean cycle at end of the current cycle
Prime entire system PMA Primes all the reagent and sample lines now
Prime reagents PMR Primes reagents lines at end of current cycle
Prime standards PMS Primes standard lines at end of current cycle
Prime electrolyte PME Refreshes electrolyte in the system at end of current cycle
Set/query Auto-Calibration setting
CTM Sending just first three characters CTM will result in current auto-cal.
settings to be returned. Add the equal sign and one of the characters
listed in the Command column to the left to set new auto-calibration
interval.
CTM=4,x Calibrate every 12 hours.
x = 0 to 23 indicates time of day to calibrate (using a 24-hour clock).
If x=22, the analyzer calibrates at 10:00 p.m. and a.m.
CTM=5,x Calibrate daily.
x = 0 to 23 indicates time of day to calibrate (using a 24-hour clock).
CTM=x,y Auto-Calibrate Weekly.
x = 6 to 12 which signifies the day of week to calibrate where Monday=6
and Sunday=12. y = 0 to 23 to indicate time of day to calibrate
(using 24-hour clock).
Recall Calibration RCL=A Sending just first three characters recalls the calibration values from the
last calibration. Adding “=A” will recall all calibrations stored (up to 7).
Reset to Default calibration RDC Resets calibration curve to factory default values.
Recall Grab Sample RGB=A Sending just first three characters recalls the grab sample value(s) from
the last grab sample cycle.
Adding “=A” will recall all grab samples stored (up to 8).
Get/Set Auto-Refresh settings ELI=x Sending just first three characters results in current settings being
returned. Adding =x will result in following settings where x =1=6 hours,
x=2=12 hours and x=3=24 hours.
Set Type of Auto-Clean cycle ACT=x Sending just first three characters results in current settings being
returned. Adding =x will result in following settings:
x=0=Normal Clean, x=1= Extended Clean
Get/Set Auto-Clean settings CLI=x Sending just first three characters results in current settings being
returned. Adding =x will result in following settings:
x =1=6 hours, x=2 =12 hours and x=3=24 hours.
x=4 to 10 signifies clean weekly where the day of the week to clean is 4
for Monday to 10 for Sunday.
Get/Set sample sequence SEQ Returns “SEQUENCE=123...1” which represents the order in which the
samples are measured.
SEQ=123.. Can have up to 8 values in sequence. The numbers after the equal sign
represent the order in which sample measurements are performed.
Measure Grab sample GRB Perform a grab sample measurement
Recall Grab Sample RGB=A Sending just first three characters recalls the grab sample value(s) from
the last grab sample cycle.
Adding “=A” will recall all grab samples stored (up to 8).
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51000-18 network menu configuration.fm Using an APA With an SIO Module
Section 8
Table 25 APA 6000 Remote RS232 Commands (continued)
Description of Remote Command Command Description of Command/Settings
Get Instrument ID RID Nitrate V1.0 C1.0
Ammonium V1.0 C1.0
Amm and Nitr V1.0 C1.0
Hardness V1.0 C1.0
Alkalinity V1.0 C1.0
Output latest alarms/warnings RAR Output up to last 10 alarms/warning messages since last “RAR”
command. Only enabled if SIOx setup in Query mode.
Output latest readings. RMR Output last measurement reading for all cycles (grab and normal
measure-ment readings & calibrations). Only enabled if SIOx setup
in Query mode.
Reset all fluid levels to 100% RFL Resets all standards, reagents and cleaning solutions to 100%.
Query/Set reagent levels. RG1=xxx Send just first three characters if requesting level.
The third character is the number of the reagent.
Add “=” followed by reagent level in percent if setting to new level.
Allowed values are between 0 and 100%.
Query/Set standard levels. SD1=xxx Send just first three characters if requesting level.
The third character is the number of the standard.
Add “=” followed by standard level in percent if setting to new level.
Allowed values are between 0 and 100%. The percent sign is optional.
Query/Set pump wash fluid level. WSH=xxx Send just first three characters if requesting level.
Add “=” followed by fluid level in percent if setting to new level.
Allowed values are between 0 and 100%. The percent sign is optional.
Request all Instrument settings and ALL Sends out all instrument settings.
information.
Set/Query Instrument name. RIN=xxx Send first three characters to get instrument name. Default name is
“#1 APA 6000”. Add equal sign plus text to set new name. Maximum
length of name is 12 characters. Note: all letters will be converted to
upper case.
Test internal recorder channel A. RCA=x Set x = F or H or Z for output recorder full-scale, half-scale or zero
respectively. Send just first three characters to stop test.
Test internal recorder channel B. RCB=x Set x = F or H or Z for output recorder full-scale, half-scale or zero
respectively. Send just first three characters to stop test.
Test internal relay A. RLA=x Set x = 0 or 1 for relay off or on. Send just first three characters to stop
test.
Test internal relay B. RLB=x Set x = 0 or 1 for relay off or on. Send just first three characters to stop
test.
Get Software Version numbers. RVN Get version numbers of instrument and its modules. For Alkalinity V1.0
C1.0
EXT NEURON: EXT0101
INT NEURON: INT0101
(and following if used:)
VALVE MODULE: VLV0103
DETECT MODULE: DET0102
BURETTE1 MODULE: PMP0102
BURETTE 2 MODULE: PMP0102
MIXER MODULE: PMP0102
Query alarm/warning logs TAL Transmits all messages in current alarm log
Clear alarm/warning logs WAL Clears alarm logs.
Page 160
Section 8
8.3 Using an APA With a Digital Display Module (DDM)

See the Digital Display Manual to connect it to the network. Then go to
Section 7.3.4.5 on page 142 in this manual for the connection in the APA
analyzer. Use this section to select the APA channel you want to display on
the module.
3. Select the sending sensor by name and press ENTER.
5. Select DISPLAY: and press ENTER.
6. Select a measurement from the available measurements listed and

press ENTER.
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51000-18 network menu configuration.fm Using an APA With a Digital Display Module (DDM)
Section 9 PID Control
The APA 6000 Analyzer uses a PID (Proportional, Integral (reset), Derivative
(rate) control algorithm. Each of the analyzer settings in Section 2.3.3.2 on
page 46 are described below.
9.1 Analyzer Settings
9.1.1 Set Point

The set point is the desired value of the parameter in the process stream.
PID control is used to keep this value stable.
9.1.2 Dead Band

This is the window or range around the setpoint where the controller takes no
action. Any measurement that falls within this window is considered to be
“at the setpoint” by the analyzer.
9.1.3 Proportional Band

The proportional band is the measurement range (in ppm or mg/L) that
adjustments via the controller can be made. Measurements above or below
this range cause a fully opened or fully closed valve (pump).
The proportional band setting determines the analyzer’s sensitivity to an error

(the difference between the setpoint and the correct value of the measured
parameter). If the proportional band is doubled, then the output signal is cut in
half for a given error signal. For a proportional only controller (reset and rate
settings off), the steady state error decreases with a smaller proportional
band. However, if the proportional band is set too low, the loop goes into
oscillation. This occurs because the proportional output is the error divided by
the proportional band, which does not give the necessary error term, unless
the required output happens to equal the preset value. By using the integral
action, the steady state error is reduced to zero.
9.1.4 Reset (Integral)

The reset action is used to drive the loop to maintain a zero long-term error.
For example, on a proportional controller where the steady state parameter is
too high, the integral component of the output starts ramping up until the
increased chemical feed brings the parameter level down to the set point. The
higher the setting, the faster the loop reaches a steady state, but it should not
be set faster than the delay time in the loop. If the setting is too high the loop
will oscillate (this is usually a slower oscillation than an oscillation caused by a
proportional band setting that is too low or a rate setting that is too high). The
reset action is turned off by setting it to zero.
9.1.5 Rate (Derivative)

The derivative action reacts to a rate of change of the input and attempts to
counter fast changes. The rate action is turned off by setting it to zero.
9.1.6 Output Action

The output action refers to addition of reagents to the process stream to
increase or decrease the parameter concentration. It is assumed that a higher
output current causes increased addition of reagent. If adding reagents
causes the parameter to increase, the output action should be set to
REVERSE. If the addition of reagents causes the parameter reading to
decrease, set the output action to DIRECT.
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51000-18 pid control.fm PID Control
Appendix A Bench Method Procedure
The precision of the APA 6000 analyzer is specified at 3%, however the
precision of the bench method is estimated to be 10%. This may lead to
apparent discrepancies between measurements obtained on the instrument
and with the bench procedure.
Contact with carbon dioxide in the air reduces the sample P alkalinity with
time. While the measurements given by the APA analyzer are representative
of the sample P alkalinity where it is sampled, the results from the bench
method may only be representative of the sample P alkalinity after some of it,
over time, has reacted with carbon dioxide in the air.
Also note that alkalinity measurements on the instrument are made at 50 °C,
while the bench method is performed at room temperature. Depending on the
sample matrix, this may contribute to apparent differences between
instrument and bench method results.
Select sample size
1. Select the sample 2. Insert a clean 3. Turn the delivery knob 4. Use a volumetric pipet
volume and Sulfuric Acid delivery tube into the to eject a few drops of to measure the sample
(H2SO4) Titration Cartridge titration cartridge. titrant. Reset the counter volume from Table 1.
corresponding to the Attach the cartridge to to zero and wipe the tip. Transfer the sample into
expected alkalinity the titrator body. a clean 250-mL
Note: For added convenience
concentration as mg/L Erlenmeyer flask. Dilute
Note: See General use the TitraStir Stir Plate.
calcium carbonate (CaCO3) See General Description to about the 100-mL
Description, Step-by-Step
from Table 1. in the Digital Titrator Digital Titrator Manual, Step 3 mark with deionized
Manual for assembly in Step-by-Step. water, if necessary.
Note: See Sampling and
Storage following instructions, if necessary.
these steps.
Table 1
Range Sample Titration Cartridge Catalog Digit
(mg/L as CaCO3) Volume (mL) (H2SO4) Number Multiplier
10-50 100 0.1600 N 14388-01 0.1
50-100 50 0.1600 N 14388-01 0.2
100-500 100 1.600 N 14389-01 1.0
500-1000 50 1.600 N 14389-01 2.0
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51000-18 bench method procedure.fm Bench Method Procedure
Appendix A
5. Add the contents of 6. If the solution turns 7. Calculate: 8. Add the contents of
one Phenolphthalein pink, titrate to a colorless one Bromcresol Green-
Digits Required x Digit
Indicator Powder Pillow end point. Place the Methyl Red Indicator
Multiplier = mg/L CaCO3 P
and swirl to mix. delivery tube tip into the Alkalinity Powder Pillow to the flask
solution and swirl the flask and swirl to mix.
Note: A solution of one pH
while titrating with sulfuric
8.3 Buffer Powder Pillow and Note: Four drops of Methyl
one Phenolphthalein Powder acid. Record the number
Purple Indicator Solution may
Pillow in 50 mL of deionized of digits required. be substituted for the
water is recommended as a Note: If the solution is Bromcresol Green-Methyl
comparison for determining colorless before titrating with Red Indicator Powder Pillow.
the proper end-point color. sulfuric acid, the Titrate from green to a gray
Phenolphthalein (P) Alkalinity end point (pH 5.1).
Note: Four drops of
Phenolphthalein Indicator is zero; proceed with Step 8.
Note: Four drops of
Solution may be substituted Bromcresol Green-Methyl
for the Phenolphthalein Red Indicator Solution may
Indicator Powder Pillow. be substituted for the
Bromcresol Green-Methyl
Red Indicator Powder Pillow.
Page 166
Bench Method Procedure 51000-18 bench method procedure.fm
Appendix A
9. Continue the titration 10. Calculate:

with sulfuric acid to a light Table 2
greenish blue-gray (pH Total Digits Required x Digit
Multiplier = mg/L as CaCO3 Sample Composition End Point
5.1), a light violet-gray
Total (T or M) Alkalinity
(pH 4.8), or a light pink Alkalinity about 30 mg/L pH 5.1
(pH 4.5) color, as required Note: Carbonate, Alkalinity about 150 mg/L pH 4.8
by the sample bicarbonate and hydroxide
composition; see Table 2. concentrations may be Alkalinity about 500 mg/L pH 4.5
Record the number of expressed individually using Silicates or Phosphates present pH 4.5
digits required. the relationships shown in
Industrial waste or complex system pH 3.7
Table 3.
Note: A solution of one
Bromcresol Green-Methyl Note: meq/L Alkalinity = mg/L
Red Powder Pillow and as CaCO3 ÷ 50.
one pillow of the appropriate
pH buffer in 50 mL of
deionized water is
recommended as a
comparison for judging
the proper end-point color.
If the pH 3.7 end point is
used, use a Bromphenol
Blue Powder Pillow instead of
a Bromcresol Green-Methyl
Red and titrate to a green
end point.
Page 167
Appendix A
Sampling and Storage

Collect samples in clean plastic or glass bottles. Fill completely and cap
tightly. Avoid excessive agitation or prolonged exposure to air. Samples
should be analyzed as soon as possible after collection.
Alkalinity Relationship Table

Total alkalinity primarily includes hydroxide, carbonate and bicarbonate
alkalinities. The concentration of these alkalinities in a sample may be
determined when the phenolphthalein and total alkalinities are known
(see Table 3).
Table 3 Alkalinity Relationships

Hydroxide Alkalinity is Carbonate Alkalinity Bicarbonate Alkalinity is
Row Result of Titration
equal to: is equal to: equal to:
Phenolphthalein Alkalinity = 0 0 0 Total

1
Alkalinity
Phenolphthalein Alkalinity equal to Total Alkalinity 0 0
2
Total Alkalinity
Phenolphthalein Alkalinity less 0 2 times the Total Alkalinity minus two
3 than one half of Total Alkalinity Phenolphthalein times Phenolphthalein
Alkalinity Alkalinity
Phenolphthalein Alkalinity equal to 0 Total Alkalinity 0
4
one half of Total Alkalinity
Phenolphthalein Alkalinity greater 2 times the 2 times the difference 0
than one half of Total Alkalinity Phenolphthalein minus between Total and
5
Total Alkalinity Phenolphthalein
Alkalinity
To use the table follow these steps:
1. Does the phenolphthalein alkalinity equal zero? If yes, use Row 1.
2. Does the phenolphthalein alkalinity equal total alkalinity? If yes, use

Row 2.
3. Multiply the phenolphthalein alkalinity by 2.
4. Select Row 3, 4, or 5 based on comparing the result of Step c with the

total alkalinity.
5. Perform the required calculations in the appropriate row, if any.
6. Check your results. The sum of the three alkalinity types will equal the
total alkalinity.
Page 168
Bench Method Procedure 51000-18 bench method procedure.fm
Appendix A
Required Reagents
(varies with sample characteristics)
Alkalinity Reagent Set (about 100 tests) ...................................................................................................... 22719-00
Includes: (1) 942-99, (1) 943-99, (1) 14388-01, (1) 14389-01
Description Unit Cat. No

Bromcresol Green-Methyl Red Powder Pillows.....................................................................100/pkg.............. 943-99
Phenolphthalein Powder Pillows ...........................................................................................100/pkg.............. 942-99
Sulfuric Acid Titration Cartridge, 1.600 N...................................................................................each.......... 14389-01
Sulfuric Acid Titration Cartridge, 0.1600 N.................................................................................each.......... 14388-01
Water, deionized .......................................................................................................................... 4 L .............. 272-56
Required Apparatus
Digital Titrator.............................................................................................................................each.......... 16900-01
Flask, Erlenmeyer, 250 mL ........................................................................................................each.............. 505-46
Select one or more based on sample concentration:

Pipet, volumetric, Class A, 50 mL ..............................................................................................each.......... 14515-41
Pipet, volumetric, Class A,100mL ..............................................................................................each.......... 14515-42
Pipet Filler, safety bulb ...............................................................................................................each.......... 14651-00
Page 169
Glossary
AquaTrend Network System - A system which provides a digital interface

link between sensors and communication devices and can receive data from
these devices at a maximum distance of up to 500 meters (1640 feet.). The
fieldbus communications that makes such configuration possible is provided
by Echelon® LONWORKS® technology.
The network software may configure up to 35 devices including: one

Master AquaTrend, as many as two Serial I/O Modules, and up to eight
sensors, eight Signal Output Modules, eight Digital Display Modules and eight
Remote AquaTrends.
channel - Where data is displayed and logged on the AquaTrend. The

AquaTrend has eight channels (represented by the letters A through H) to
which you can attach measurements from sensors.
configure - Setting up a Hach network device for operation after hardware

installation is complete. This involves selecting various software options and
establishing communications between devices.
device - Any of the Hach network instruments, including sensors,

communications modules, display modules, outputs and AquaTrends.
Digital Display Module (DDM) - An eight-character display device that can

be used with sensors or analyzers to display a single measurement. It can be
mounted as far away as 400 meters (1310 feet) from the sensor and 30.5
meters (100 feet) from a PS1201 power supply.
Echelon® technology - communications technology used by the AquaTrend

Network System and developed by Echelon Corporation, producer of
LONWORKS fieldbus technology.
fieldbus - Any of several techniques allowing multiple devices to be

connected on a single set of wires.
LONWORKS - The fieldbus protocol used by the AquaTrend Network System.
Master AquaTrend - Acts as the main network data control center for setup
and operation of the network. The network can contain as many as nine
AquaTrends but only one can be the Master AquaTrend. Only through the
Master AquaTrend can you perform network operations.
network - The connection of one or more devices (of which at least one is a
sensor or analyzer) to a Master AquaTrend.
pop-up box - A selection or message box at the end of a menu chain. This
box either provides a choice of options—selectable by moving the cursor and
pressing ENTER—or allows you to use the arrow keys to enter an
Page 171
51000-18 glossary.fm Glossary
Glossary
alphanumeric response, or states the status of the current operation. These

three possibilities respectively are shown below.
Portable AquaTrend - Mobile device designed to setup and calibrate sensors

already setup on the network. Portable AquaTrends can access all menus
except the network menu and can not perform network operations.
PS1201 - A power supply that provides 25 watts to AquaTrend network

devices.
Remote AquaTrend - Any AquaTrend on a network that is not a Portable or

Master AquaTrend. Remote AquaTrends can display all sensor readings and
access all sensor menus.
repeater - A device capable of amplifying signals when total cable distance is

exceeded in order to extend the network’s capabilities.
SCADA - Supervisory Control and Data Acquisition. General term for any
automated (and usually PLC or computer-controlled) system for control and
data acquisition.
sensor - Any one of the Hach devices designed to take measurements for
specific parameters and for use with the AquaTrend Network System (e.g., the
1720D Turbidimeter)
Serial I/O Module ((SIO) - Communication device for two-way communication

with a PC or one-way communication with a printer.
Signal Output Module (SOM) - Network device that provides two relays,
each with normally open and normally closed contacts rated at a maximum of
5 A/250 VAC, and two analog outputs, selectable through the AquaTrend
keypad at either 4-20 or 0-20 mA. Sensor alarms can be configured to trigger
one the relays in the SOM and/or a recorder, or controller signal from a
sensor can be attached to the analog outputs of the SOM.
The SOM can either be a stand-alone device (model 51250) or can be internal
to the AquaTrend/SOM (model 51350).
terminator - Impedance stabilizing component that maintains network signal

integrity. One terminator is required for proper network operation, either on an
AquaTrend (without SOM) or on a stand-alone SOM.
topology - Any wiring configuration. See Figure 57 for examples.
Page 172
Glossary 51000-18 glossary.fm
Glossary
Figure 57 Wiring Topologies
1720D 1720D
SIO or MOD I/O
PS1201 PS1201 PS1201

Master
AquaTrend w/ SOM
PS1201 PS1201
1720D 1720D 1720D DDM
1650 feet (500 meters) Total maximum distance for network communication.
SOM PS1201
1720D PS1201 SOM PS1201

Master AquaTrend
Other
Device
SOM
PS1201 DDM
Other Device
Master Other
AquaTrend Device
1720D
Distances in excess of 1650 feet (500 meters) require a repeater.
100 feet (30.3 meters) Maximum distance between the power supply and the device it is powering.
1320 feet (400 meters) Maximum distance between two network devices.
20 feet Fixed distance between power supply and 1720D.
Only one enabled terminator is allowed for network.

(Terminators are located in SOMs, AquaTrends, and SIOs)
Page 173
51000-18 glossary.fm Glossary
General Information
At Hach Company, customer service is an

important part of every product we make.
With that in mind, we have compiled the following

information for your convenience.
Page 175
51000-18 general information stopper.fm General Information
Replacement Parts
Instrument Configurations
Description unit Cat. No.
APA 6000™ Alkalinity Analyzer, with AquaTrend® Interface ......................................................each.......... 51000-10
APA 6000™ Alkalinity Analyzer, without AquaTrend® Interface .................................................each.......... 51000-12
Reagents and Standards

APA Alkalinity Reagent 1, Titrant ................................................................................................. 1 L.......... 26965-53
APA Alkalinity Reagent 2, Indicator.............................................................................................. 1 L.......... 26966-53
APA Alkalinity Standard 1, 0 mg/L................................................................................................ 1 L.......... 26967-53
APA Alkalinity Standard 2, 2000 mg/L.......................................................................................... 1 L.......... 26968-53
APA Alkalinity Cleaning Solution .................................................................................................. 1 L.......... 26970-53
Optional Equipment and Supplies

AquaTrend Instrument, portable.................................................................................................each.......... 51400-00
AquaTrend Instrument................................................................................................................each.......... 51200-00
AquaTrend Instrument with SOM ...............................................................................................each.......... 51350-00
Basic Sample Conditioning Kit (for adding sample steams) ......................................................each.......... 51045-00
Digital Display Module (DDM) ....................................................................................................each.......... 52400-00
Power Cord, UL/CSA, 115 V, w/ NEMA-style strain relief ..........................................................each.......... 46306-00
Power Cord, VDE, 230 V, w/ Continental-style plug and NEMA-style strain relief .....................each.......... 46308-00
PS1201 Power Supply ...............................................................................................................each.......... 52010-60
Signal Input/Output Module (SIO) ..............................................................................................each.......... 52074-02
Signal Output Module (SOM) .....................................................................................................each.......... 51250-00
Sample Conditioning
Air Backflush Kit, automatic, 115 Vac ........................................................................................each.......... 51068-00
Air Backflush Kit, automatic, 230 Vac ........................................................................................each.......... 51068-01
Basic Sample Conditioning Kit w/ 22-µm filter ...........................................................................each.......... 51045-00
Filter, 0.2-µm membrane ............................................................................................................each.......... 51042-00
APA 6000 Micro Filter System, model 9700, 115 V ...................................................................each.......... 51339-00
APA 6000 Micro Filter System, model 9700, 230 V ...................................................................each.......... 51339-01
Filter Element, 450 mesh ...........................................................................................................each.......... 51397-00
Filter, support element ...............................................................................................................each.......... 51034-00
O-ring, Viton, filter seal ..............................................................................................................each.......... 51038-00
Page 176
Replacement Parts 51000-18 replacement parts.fm
Replacement Parts
Replacement Parts
AquaTrend Instrument Manual ...................................................................................................each.......... 51350-18
Binder, D-ring, for AquaTrend manual .................................................................................each.......... 52001-77
Autoburette Module, with 2-way valve only ................................................................................each.......... 51020-02
Autoburette Block .......................................................................................................................each.......... 51108-00
Bulkhead Union, 0.25 OD tubing to tubing (for air purge bulkhead) ..........................................each.......... 51104-00
Cable, backplane .......................................................................................................................each.......... 51161-00
Cable, AquaTrend ......................................................................................................................each.......... 51164-00
Cable Termination Kit .................................................................................................................each.......... 52156-00
Colorimeter, APA 6000 Alkalinity................................................................................................each.......... 51026-01
Colorimeter Temperature Control Block .....................................................................................each.......... 51116-00
Faceplate Assembly, APA 6000..................................................................................................each.......... 51022-00
Fitting, Ferrule, 0.062 OD...........................................................................................................each.......... 51130-00
Fitting, Ferrule, with ring, 0.062 OD ...........................................................................................each.......... 51132-00
Fitting, Union, Tefzel, ¼-28 ........................................................................................................each.......... 51359-00
Flangeless Hex Nut Fitting, 0.062 OD........................................................................................each.......... 51129-00
Flangeless Nut Fitting, 0.062 OD ...............................................................................................each.......... 51131-00
Fuse, 1.6 A, 250 V, 5 mm x 20 mm, UL, CSA, VDE approved...................................................each.......... 52083-00
Grab Sample Port Cap...............................................................................................................each.......... 51317-00
Grab Sample/Drain Block Assembly ..........................................................................................each.......... 51503-00
Grommet, manifold, APA 6000 (for tubing).................................................................................each.......... 51036-00
Hex Nut Valve Plug, 10-32 .........................................................................................................each.......... 51393-00
Manual, Alkalinity, APA 6000......................................................................................................each.......... 51000-18
Mixer Module Assembly, APA 6000, 3-mL .................................................................................each.......... 51021-01
Plug, air purge, for ¼-in. tubing ..................................................................................................each.......... 51140-00
Plug, manifold, APA 6000...........................................................................................................each.......... 51224-00
Plug, flat bottom, Tefzal, ¼-28....................................................................................................each.......... 51293-00
Power Switch, 4A, 250 VAC .......................................................................................................each.......... 51155-00
Quick Reference Card................................................................................................................each.......... 51000-44
Reagent Bottle Vent Cap Assembly ...........................................................................................each.......... 51215-00
Reagent Housing Assembly.......................................................................................................each.......... 51048-00
Restraining Cable, steel, w/eyelets (for module panel) ..............................................................each.......... 51417-00
Rotary Valve, 10-port, with actuator ...........................................................................................each.......... 51150-00
Sample Inlet Block .....................................................................................................................each.......... 51365-00
Seal, oil tight, 0.88-in. diameter .................................................................................................each.......... 42210-00
Scrubber, CO2, for standard bottles ...........................................................................................each.......... 51431-00
Scrubber, CO2, soda lime absorbant ........................................................................................ 500g.......... 27476-00
Stator, for 10-port valve (replaces 51150-00).............................................................................each.......... 51347-00
Stir Bar, micro, 3 mm x 10 mm...................................................................................................each.......... 20549-59
Teflon Tubing, 0.170 ID x 0.250 OD .............................................................................................feet.......... 45462-00
Teflon Thread Tape, 0.25-in wide ...............................................................................................1 roll.......... 70608-24
Temperature Control Block Assembly ........................................................................................each.......... 51046-01
Tubing, Tefzel, 0.030 ID x 0.062 OD, 2000 psi .............................................................................feet.......... 51178-00
Valve Body Replacement, 10-port valve ....................................................................................each.......... 51507-00
Valve Module Assembly, APA 6000............................................................................................each.......... 51029-01
Washer, sealing, ½-in. NPT .......................................................................................................each.......... 10338-14
Page 177
51000-18 replacement parts.fm Replacement Parts
Replacement Parts
Kits
Installation Kit ..........................................................................................................................each.......... 51040-00
Fitting, elbow, ½ ID tubing x ¾ NPT PP (2) .........................................................................each.......... 30618-00
Fitting, reducer, ¾ MNPT x ¼ FNPT PVC (3)......................................................................each.......... 31560-00
Tubing, Teflon, 0.170 x 0.250 OD .............................................................................. 3 m (10 ft.).......... 45462-00
Tubing, Tygon, ¾-in OD x 1/8-in. wall, black ............................................................. 1.8 m (6 ft.).......... 45543-00
Clamp, for hanging conduit, 2.5 cm (1 in.) (2) .....................................................................each.......... 47349-00
Coupling, ¾-in. NPT x ¾-in. NPT (3)...................................................................................each.......... 49620-00
Tee Fitting, 1-in. x ¾-in. x 1-in. PVC (2)...............................................................................each.......... 51080-00
Drain Pipe, pre-cut, 1-in. PVC (2) ........................................................................... 15 cm (6 in.).......... 51239-00
Fitting, ¼-in. tube connector, push-fit (3) .............................................................................each.......... 51246-00
Ball Valve, ¼-in. NPT, PVC (1) ............................................................................................each.......... 51395-00
Filter Housing, ¾-in., w/o filter .............................................................................................each.......... 51396-00
Filter Element, 22 µm, 450 mesh (1) ...................................................................................each.......... 51397-00
Teflon Thread Tape, 0.25-in wide (1 roll) .............................................................................each.......... 70608-24
Tool Kit ......................................................................................................................................each.......... 51291-00

Hex Nut Fitting, 0.062-in.OD tubing (4) ...............................................................................each.......... 51129-00
Ferrule Fitting, 0.062 in. OD tubing (4) ................................................................................each.......... 51130-00
Flangeless Nut Fitting, 0.062 in. OD tubing (10) .................................................................each.......... 51131-00
Ferrule Fitting w/ Ring, 0.062 in. OD tubing (10) .................................................................each.......... 51132-00
Autoburette Force Gauge Tool (1) .......................................................................................each.......... 51149-00
Autoburette Module Wrench (1)...........................................................................................each.......... 51169-00
O-ring Seating Tool (1) ........................................................................................................each.......... 51170-00
Flangeless Nut Extender Tool (1) ........................................................................................each.......... 51174-00
Allen Wrench, 1/8 in., long arm (1) ......................................................................................each......... 51340-00
Allen Wrench, 7/64 in., long arm (1) ....................................................................................each.......... 51345-00
Valco Valve Wrench, ¼-inch (1)...........................................................................................each.......... 51357-00
Tubing cutter, for 1/16-in. Tubing (1) ....................................................................................each.......... 51356-00
Flat-bottom Tefzel Plug, ¼-28 (4) ........................................................................................each.......... 51293-00
Tefzel tubing, 0.030 ID x 0.062 in., 2000 PSI .......................................................................feet.......... 51178-00
Hex Nut Valve Plug Fitting, 10-32 (3) ..................................................................................each.......... 51393-00
Quick Release Tool (1) ........................................................................................................each.......... 51289-00
Maintenance Kit, Alkalinity analyzer ......................................................................................each.......... 51033-00

O-ring, fluorocarbon, 0.103 W x 0.424 ID, large autoburette o-ring (2) ...............................each.......... 40215-00
O-ring, fluorocarbon, 0.103 W x 0.237 ID, small autoburette o-ring (2) ...............................each.......... 51191-00
Autoburette piston seals, 0.25-in. diameter (cylinder seal) (2) ............................................each.......... 51225-00
Rotor Valve (1).....................................................................................................................each.......... 51348-00
Page 178
Replacement Parts 51000-18 replacement parts.fm
How to Order
U.S.A. Customers
By Telephone: By Mail:
6:30 a.m. to 5:00 p.m. MST Hach Company
Monday through Friday P.O. Box 389
(800) 227-HACH (800-227-4224) Loveland, Colorado 80539-0389 U.S.A
By Fax: Ordering information by E-mail:

(970) 669-2932 orders@hach.com
Information Required
• Hach account number (if available) • Billing address
• Your name and phone number • Shipping address
• Purchase order number • Catalog number
• Brief description or model number • Quantity
Technical and Customer Service (U.S.A. only)

Hach Technical and Customer Service Department personnel are eager to
answer questions about our products and their use. Specialists in
analytical methods, they are happy to put their talents to work for you.
Call 1-800-227-4224 or E-mail techhelp@hach.com.
International Customers
Hach maintains a worldwide network of dealers and distributors.
To locate the representative nearest you, send E-mail to
intl@hach.com or contact:
Hach Company World Headquarters; Loveland, Colorado, U.S.A.

Telephone: (970) 669-3050; Fax: (970) 669-2932
Page 179
51000-18 general information section.fm How to Order
Repair Service
Authorization must be obtained from Hach Company before sending

any items for repair. Please contact the HACH Service Center serving
your location.
In the United States:

Hach Company
100 Dayton Avenue
Ames, Iowa 50010
(800) 227-4224 (U.S.A. only)
Telephone: (515) 232-2533
FAX: (515) 232-1276
In Canada:
Hach Sales & Service Canada Ltd.
1313 Border Street, Unit 34
Winnipeg, Manitoba
R3H 0X4
(800) 665-7635 (Canada only)
Telephone: (204) 632-5598
FAX: (204) 694-5134
E-mail: canada@hach.com
In Latin America, the Caribbean, the Far East, the

Indian Subcontinent, Africa, Europe, or the Middle East:
Hach Company World Headquarters,
P.O. Box 389
Loveland, Colorado, 80539-0389 U.S.A.
Telephone: (970) 669-3050
FAX: (970) 669-2932
E-mail: intl@hach.com
Page 180
Repair Service 51000-18 general information section.fm
Warranty
Hach warrants most products against defective materials or workmanship

for at least one year from the date of shipment; longer warranties may apply
to some items.
HACH WARRANTS TO THE ORIGINAL BUYER THAT HACH

PRODUCTS WILL CONFORM TO ANY EXPRESS WRITTEN
WARRANTY GIVEN BY HACH TO THE BUYER. EXCEPT AS
EXPRESSLY SET FORTH IN THE PRECEDING SENTENCE,
HACH MAKES NO WARRANTY OF ANY KIND WHATSOEVER
WITH RESPECT TO ANY PRODUCTS. HACH EXPRESSLY
DISCLAIMS ANY WARRANTIES IMPLIED BY LAW, INCLUDING BUT
NOT BINDING TO ANY WARRANTY OF MERCHANTABILITY OR
FITNESS FOR A PARTICULAR PURPOSE.
LIMITATION OF REMEDIES: Hach shall, at its option, replace or

repair nonconforming products or refund all amounts paid by the buyer.
THIS IS THE EXCLUSIVE REMEDY FOR ANY BREACH OF WARRANTY.
LIMITATION OF DAMAGES: IN NO EVENT SHALL HACH BE LIABLE FOR

ANY INCIDENTAL OR CONSEQUENTIAL DAMAGES OF ANY KIND FOR
BREACH OF ANY WARRANTY, NEGLIGENCE, ON THE BASIS OF STRICT
LIABILITY, OR OTHERWISE.
This warranty applies to Hach products purchased and delivered

in the United States.
Catalog descriptions, pictures and specification, although accurate to the

best of our knowledge, are not guarantee or warranty.
For a complete description of Hach Company’s warranty policy, request

a copy of our Terms and Conditions of Sale for U.S. Sales from our
Customer Service Department.
Page 181
51000-18 general information section.fm Warranty
Index
A Controllers ..................................................43, 46, 47

Air backflush ...........................................49, 113, 134 adjusting output .........................................48, 163
dead band ..........................................43, 46, 163
Air bubbles ............................................................... 80
output action .........................................43, 45, 47
Air purge ................................................................ 147 proportional band ...............................43, 46, 163
Alarm log ...........................................................97, 99 rate .....................................................43, 47, 163
Alarms ........................................................30, 40–42 reset ...................................................43, 47, 163
alarm messages ................................................ 99 set point ..............................................43, 47, 163
clearing the alarm log ........................................ 79 Cursor .........................................................28, 70, 72
diagnostics ...................................................... 104
log ...............................................................79, 97
D
relay connections ............................................ 133
sensor ............................................................... 41 Date ......................................................................... 30
troubleshooting .................................................. 97 Date format .............................................................. 34
types of .............................................................. 40 Date setting .............................................................. 33
Analyzer name ......................................................... 35 Day of the week ....................................................... 33
AquaTrend ................................................19, 27, 171 Dead band ................................................43, 46, 163
display ............................................................... 29 Diagnostics ............................................................ 104
keypad ............................................................... 27 hold outputs ..................................................... 104
menu ................................................................. 30 internal output test ........................................... 106
portable ............................................................. 20 internal relay test ............................................. 105
remote .........................................................19, 20 Digital dispaly module ............................................ 161
setup ...........................................................32–42
Digital display module ......................................20, 171
Arrow keys ............................................................... 28
Display ..................................................................... 29
Autoburette .................................................85, 87, 98 access to ........................................................... 70
alarm messages .............................................. 102 graphical ...............................................29, 31, 70
seal replacement ............................................... 87 setting the graph time ................................. 71
Auto-calibration ..................................................57, 58 setting the unit axis ...............................71–72
numeric .......................................................29, 70
B Display contrast ....................................................... 39
Bench method ....................................................... 165 Display key .............................................................. 28
Drain lines .............................................................. 152
C
Cable termination .................................................. 142 E
Calibration ............................................................... 75 Echelon® LonWorks® .....................................20, 171
alarm messages .............................................. 100 Electrical connections ............................................ 128
auto-calibration ............................................57, 58 Enclosure ................................................................. 17
default ............................................................. 107
Exit key .................................................................... 28
history ................................................................ 77
manual .............................................................. 75
temperature control ........................................... 81 F
Calibration check ..................................................... 76 Fuse replacement .................................................. 144
Calibration check history ......................................... 77
Channel G
number .............................................................. 31 Grab sample ............................................................ 73
Channels ............................................................... 171 history ................................................................ 74
measurement ..............................................65, 67 Graphical display ..................................................... 31
Cleaning cycles .................................................61, 80
Cleaning solution ........................................23, 80, 82 I
Cleaning the instrument .....................................61, 80 Installation
Clearing the alarm log ............................................. 79 air backflush .................................................... 113
Computer connections ...................................156, 157 air purge .......................................................... 147
alarm relays ..................................................... 133
Computer format .................................................... 158
Page 182
Index 51000-18IX.fm
Index
Bench mount ................................................... 124 connections .............................................136, 142
Drain lines ....................................................... 152 printer connections .......................................... 156
electrical connections ...................................... 128
network connections ...............................136, 142 O
panel mount .................................................... 124
Operating environment ....................................16, 123
plumbing .......................................................... 147
power connections .......................................... 130 Operation
recorders ......................................................... 134 normal ............................................................... 69
sample pump ................................................... 119 starting .............................................................. 55
sample streams .........................................62, 122 theory of ............................................................ 25
wall mount ....................................................... 124 Optional equipment ................. 20, 26, 155, 161, 172
Output ......................................... 40, 43, 44, 46, 138
K 4-20 mA .......................................................17, 27
adjusting ............................................................ 48
Keypad ..............................................................27–28
hold ................................................................. 104
Keys ......................................................................... 28 internal output test ........................................... 106
Kit RS 232 ....................................................157, 158
installation ...................................................17, 24 sensor ............................................................... 65
maintenance .........................................17, 24, 85
reagent .............................................................. 17
P
sample conditioniong ........................................ 48
tool ..............................................................17, 24 Password ................................................................. 36
PID settings .....................................................46, 163
L Port .......................................................................... 69
Lag time ................................................................. 152 Power connectionsl ................................................ 130
Language selection ................................................. 34 Priming ..................................................................... 55
Printer connections ........................................156, 157
M Printer format ......................................................... 157
Maintenance ............................................................ 85 Proportional band .....................................43, 46, 163
autoburette ........................................................ 85
changing modules ........................................... 146 R
changing solutions ......................................51, 53 Reagents ....................................................23, 51, 85
colorimeter ........................................................ 85 changing ............................................................ 86
kit ....................................................................... 24 consumption ...................................................... 86
mixer module ..................................................... 95 priming .............................................................. 55
scheduled .......................................................... 85 Recorders .......................................... 40, 43, 44, 134
tubing ................................................................ 92 adjusting output (trim) ....................................... 48
valve rotor and stator ........................................ 90 internal output test ........................................... 106
Measurement ........................................................... 69 Relays .....................................................40, 105, 133
attaching to a channel ....................................... 65
Replacement parts ................................................. 176
channel .............................................................. 67
Restarting the instrument ......................................... 82
Module
alarm messages ................................................ 99 Rotor ...........................................................69, 90, 97
autoburette ...........................................18, 85, 87 alarm messages .............................................. 101
changing modules ........................................... 146 RS 232 commands ................................................ 158
colorimeter ..................................................18, 85 RS 232 output ........................................................ 157
mixer ....................................................18, 85, 95
rotary valve ........................................................ 18 S
rotor valve ............................................85, 90, 97
Sample conditioning .................................48–50, 112
Mounting the analyzer ........................................... 124 air backflush .....................................49, 113, 133
sample pump ....................................50, 119, 133
N setup .........................................................48, 149
Network ................................................................... 20 ultrafiltration ..................................................... 118
computer connections ..................................... 156 Sample flow ............................................................. 55
configuration .................................................... 155 Sample lag time ..................................................... 152
Page 183
51000-18IX.fm Index
Index
Sample lines .......................................................... 148 Specifications ........................................................... 11
Sample pump .........................................50, 119, 133 Standards ..........................................................23, 51
Sample sequencing ................................................. 63 priming .............................................................. 56
Sample streams Standby ..............................................................29, 82
adding .......................................................62, 122 Stator ..........................................................85, 90, 97
sequencing ........................................................ 63
Security .................................................................... 36 T
level ................................................................... 37 Temperature control ................................................ 81
password ........................................................... 36 alarm messages .............................................. 101
unlocking the keypad ........................................ 38
Theory of operation .................................................. 25
Setpoint ....................................................43, 47, 163
Time setting ............................................................. 32
Setup
Tools ...........................................................24, 88–89
alarms ............................................................... 40
analyzer name ................................................... 35 Trim .......................................................................... 48
auto-calibration .................................................. 57 Troubleshooting ...............................................97–102
auto-clean ......................................................... 61 Tubing ................................................................97, 98
date ................................................................... 33 replacement ...................................................... 92
date format ........................................................ 34 replacement lengths .......................................... 94
day of the week ................................................. 33
language ........................................................... 34 U
measurement units ............................................ 39
Ultrafiltration ........................................................... 118
overview ............................................................ 15
sample conditioning .......................................... 48 Units of measure ................................................31, 39
sample measurement channels ........................ 65 Unlocking the keypad .............................................. 38
sample streams ................................................. 62
security ........................................................36–38 W
time ................................................................... 32 Warnings
unlocking the keypad ........................................ 38 alarm log ........................................................... 79
Shutdown ................................................................. 82 clearing the alarm log ........................................ 79
SIO .............................. 20, 137, 139, 156, 157, 172 sensor .........................................................41, 42
Software version .................................................... 108 troubleshooting .................................................. 97
Solution levels ......................................................... 53 warning messages ............................................ 99
SOM ..................................... 20, 138, 139, 155, 172 Waste disposal ...................................................... 154
Wiring topologies ................................................... 173
Page 184
Index 51000-18IX.fm

Old Alk Manual 51000-18

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Cat. No.

APA 6000™ Alkalinity Process Analyzer

AccuGrow® H2O University™ Pond In Pillow™

Visit http: //www.hach.com

Trademarks of Hach Company ................................................................................................................................. 2

Section 1 Introduction ...................................................................................................................................... 15

Section 2 Startup ............................................................................................................................................... 27

2.7 Starting Analyzer Operation.............................................................................................................................. 55

Section 3 Normal Operation ............................................................................................................................ 69

Section 4 Routine Operator Maintenance .................................................................................................... 85

Section 5 Warnings, Alarms, and Troubleshooting ................................................................................... 97

Installation ......................................................................................................................................................... 109

Section 6 Sample Conditioning .................................................................................................................... 111

Section 7 Hardware Installation.................................................................................................................... 123

Section 8 Network Menu Configuration ..................................................................................................... 155

Section 9 PID Control ...................................................................................................................................... 163

Appendix A Bench Method Procedure .............................................................................................................. 165

Glossary ............................................................................................................................................................. 171

General Information......................................................................................................................................... 175

Index .................................................................................................................................................................... 182

Hach Company certifies this instrument was tested thoroughly, inspected

Certified by Hach to EN 61010-1 (IEC1010-1), supporting test records by

Supporting test records by Hach Company, certified compliance by

Required Standards include:

EN 61000-4-2 “1995” (IEC 1000-4-2) Electro-Static Discharge

Additional Standards include:

EN 61000-4-5 “1995” (IEC 1000-4-5) Surge

Supporting test records by Intellistor O.A.T.S., certified compliance by

Required Standards include:

EN 55011 (CISPR 11) Emissions, Class A Limits

Additional Standards include:

EN 61000-2 (IEC 1000-3-2) Harmonic Disturbances Caused by

Canadian Interference-causing Equipment Regulation, IECS-003,

Supporting test records by Intellistor O.A.T.S., certified compliance by

This Class A digital apparatus meets all requirements of the

Cet appareil numérique de la classe A respecte toutes les exigences du

FCC Part 15, Class A Limits:

Supporting test records by Intellistor O.A.T.S., certified compliance by Hach

Changes or modifications to this unit not expressly approved by the party

The following techniques of reducing the interference problems are

5. Try combinations of the above.

Use of Hazard Information

! This symbol, if noted on the instrument, references

This symbol, if noted on the product, indicates the need

! Section 2.5 Changing Reagents and Standards on page 51

! Section 4.2 Scheduled Maintenance on page 85

! Section 4.3.1 Changing Solutions on page 86

! Section 6 Sample Conditioning on page 111

! Section 6.1 Sample Conditioning on page 112

! Section 7.3 Electrical Connections on page 128

! Section 7.3.1 Power Connections At the APA Analyzer on page 130

! Section 7.3.2 Alarm Relay Connections on page 133

! Section 7.3.4 Network Connections on page 136

! Section 7.4 Fuse Replacement on page 145

! Section 7.5 Changing Modules on page 146

! Section 7.7 Plumbing Installation on page 147

! Section 7.7.3 Drain Line Connection on page 152

Specifications are subject to change without notice.

Accuracy: ±5% of reading or ±1.0 mg/L, whichever is greater

Repeatability: ±3% of reading or ±0.6 mg/L, whichever is greater

Cycle Time: 8 minutes (average)

Recorder Outputs: Two isolated, 4-20 mA outputs standard. Output span

Alarms: 14 programmable internal alarms

Power Requirements: 95-240 VAC, 50 or 60 ±2 Hz, 150 VA