‘Apparatus + Burct, Burt Stan, Pipete, Conical ask, Glazed tie Principle: 2HC1+N,C0,—> _2N4C1+,0+0, i 2 mole HCL = nee eo, Procedure : a 1. Wash the barete swith Tap water then Distilled Water. Again Dburete rinse with given HICT solution, 2. Fillthe burette with given AICT solution without ir bubbles up othe rmark and fix it tothe stand. 13. Pipette out 20 ml of Na,CO, solution in to the clean conical flask and add Two to Three drops of Methyl orange. Then solution tums into yellow colou “4, ‘Note the initia reading of burette and then titrate this solution with HCI solution. ‘5. Atend point pale yellow colour solution tums into pale pink. Atthis point stop the burette and record fina reading. 16, Repeat the experiment til to get two identical consecutive readings Report : Moly of CI = 01M “The amount of Hydeachorie Acid pesentin__ml= =coma ease tnna manaertaM, Wenn 1 Motor i ot ane AEH = “ott or 20 20 108 ml 3 Maecbe Weight of GMLW of NCO, = [Estimation of Socium Carbonate J ‘Alma To etinate the amour of Sodium carbonate presatin _ ml ive solution Using standard 0.1. tdroclori aid wating: Principle intr Neco, ——> 3NatI+¥10+0, 2 ole Cl = I mateseD, == + Paleyeow topalépink xh with Tp wate then Distilled Water. Again ihgiven ACI solution. {C1 sotution without air bubbles upto the ie + Bure, Burt Stand, Pipe, Conical Mask, Glazed le, Basses HCI so) ie acuaeaualiancaiiasiiian pin op he ead. | Ferien ILAR Geocten Sork From Quiet) [Estimation of Oxaic Acid i tT esate he et of Ova Acid prmtin_ mo Be sen ‘aon Uninet 02 3S oie aon ‘Apparatus + Buret, Puree Stand, Pipette, Conical ask, Glazed ie Principle + axaon + (0h —> maycop +72 ,C,0, solution in tothe clean conical ask end tor then solution turns into colourless.pasar og atocda a Mote Pinal .. : sven ation, U Apparatus + Bure Bure Stam Prati. Comin sk azo le Principto * aNseat . son p.= 0 to, 082. ox 3 Mo 0 M, M5 1 Mole Wei of GM WD ol Dae tel Seven = 100 mfr 0 29001 4 Malar weigh of MW) OEKMNO, = 1 Section = [HR Question Bank From @:19t221) exxnnED ‘Aten To estmuic the amount of Ptnsium Permanganate present. the given solution. Using standard 0.95 M Oxalc Acid solution ‘Apparatus ; Burts, Burts Stand, Pipcte, Conical ask, Glazed ie 3H $0,+ 55004 ——» 2Ma50,+4,30,¢8810 +10 i 2mole KMnO, = Smale (00M, + No indicatoris nest KMnO it selfacts asa self indicator. + Colour less to pink.ask and 2d 10m of dil. 0, solution. ‘of burste and then titrate this sotion with solution turns into pink At this point stop thexno, solution tend point colour less solution turns into pink.Atthis point stop the burette and record final reading. ‘get two identical consecutive readings. 2 : 00M “Toe amount of Prasiatn permanganate present in =Systematic Procedure For Salt Analysis fests white 610 io ray be absent Bie May be Copper salt Groen (on) Pale Green “May be Ferrous salt Maybe Manganese salt May be Nickel salt Crystalline (or) Amorphous con Coo [rick red colon flame Ca? may be present Crimson red colour lame Se?imay be present ne upto no colOwE apps sultan [HCT*saltin watch glass,| Bright bluish-green colour flame Cur may be present. “eaten | omar | 2h ’ present. Dall bj -whit’Gobour ame Ph"? may be present Grassy green colour flame 1 rl quantity of sat itaken| ‘nevolved. ry testtube and strongly| b, Colour fxs gas with Asmonia smell ‘evolved and white subhimate formes. . Colourtess ess with Ammonia seve | May iu (NH, es wil isl | Maybe Armen (NH, aye Ammnium halide sal] se. othe test 4. Reddish Brown vapours are evolved, May be Nitrate (NOs) Salt ©. Cracking sound is observed, May be Lead Salt £ Yellow when hotand White when cold| Maye Zine Salt, Charatristics mel of Vinegar. May be Acetate ion. 1h Blue salt becomes white on heating. | May be Copper Salt. «Water dropsae formed onthe inner | Maybe Hydrated salt, eset | on ‘The gas putsoffa burning splinter. Ikturns Lime water into milky.pee poate Broan ening. | (Corie (CP) fon ate dicccbarmmraci | sy ‘ncentimad htoide (C1) ion ‘secntinned. vith | Bromide) ion ‘scontiened romide (Br ion ‘scouted.Confirmation Confirmation Test for ‘Confirmation Test for ‘Srontium (Sr Cation ation Test for (Mg *) Cation foltion NOOH solution is 1.0, solution sn Toate of Cattons pret SeCr0, ia formed rissolubleinpctic acid Whine pp formed tro gpringly soluble im acti acid and ihiy soluble in iL NCL White pp. is formes. Which is insoluble in excess of NaOH. White ppt is formed, Sanaa priiminary Tost 1. Colour Flame text Steom BIC + sith fouvodce this past oop to the flame