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    10 views18 pages

    РД 52.18.191-2018. Массовая доля кислоторастворимых форм металлов в пробах почв, грунтов и донных отложений

    Uploaded by

    Anila Moa

    Copyright:

    © All Rights Reserved
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Heastomarwecxoro geiicreus cpearers (Il) xnacca TowHocrA c MaKcumansHol HarpyaKol 200 r no FOCT §3228-2008, 5.1.7 Bann soqnnan no TY 64~1-2850-80. 5.1.8 CywansHes onekpyecrnt umacb c Teumeparypot Hanpesanus oT 30 0 200°C. 5.1.9 Axeaguctunnstop [19-4-2 no TY-16-10721-79 Pa s2.18.19 14.3 Oneparueibit KOHTponb norpeulHocTH c Mcnonb30BaHMeM MeTopa BapbMposaHia HasecKH 2018 14.3.1 Oneparueniih KoHTpons NPoueRyPS! MaMepeHHi NoogonAT nyTéM CcpaBHenus pesynsrara OTAeNbHO BIRTOM KOHTDONEHOM mpoUEAypA! Ki, ¢ Hop: aragow Koxrpons K 14.3.2 PesynstatT KOHTPOnbHOM NPoUeAyPE Ky paccunTelRaIoT NO chop- wyne Ky = (XX, (12) rae X— peaynetar mamepenus maccoBoll gon meTanna 8 npoGe sexoRHOA aces, mri: X’ — peaynbrat vamepenun waccosoi Aonu weTanna 8 npobe nonoaKHHOR acess, mir 14.3.3 HopwaTue KoHTpona K paccunTsiaatoT no chopmyne _——— k= Jai +a (13) Re Day WByy! ~ aHaveHiNR norpeUHOcTH peaynéraTOB MIMepeHiit, YCTaHoBNeH- Hole 8 naSoparopinn Np peanusaunn weToAMKH, cooTBeTCrayoU\Ne MaccoBol one Meranna 8 npoBe WexORHOM Macchi HB NPOGe NONoBMAHO Macc, COOT- Berersenno, Mike 14.3.4 Moueaypy Hamepennit npuaHalor yaoaneTsopuTeNsHOl NpH abi- nonkenna yenoana Ky ek (14) Nx Heabinonwenun yenosua (14) KOHTpONbHYIO NPOYeAYPY NoBTOPAIOT, Tp noeropHom HeauinonHehiw yonoans (14) BsIRCHRIOT NpHNME, NpHBOARUNE k HeyAoBneTBopHTenbHbiM peaynbTaTaM, W NpMHMIMAIOT MEPEI nO Mx YCTPAHE- Ho, 3 PQ 52.18.191-2018 - oneparwsHbilt oHTpon® norpewHocTH c McnonbaoBaHneN OBpaayoe ANA korTpons (OK) m meToqoM sapsuposanna Hasecox - onlepaTwsHeili KoHTOONS NoBTOpREMOCTH PesynbTaTOB HaMepeHHi, 14.2 OnepaTwaneit ronTpont norpewHocTH ¢ McnonbsoBaHHeM OK 14.2.1 Obpasuan ana konTpona cnymar craHaaprable o6paausi cocrasa owas, (pyHTa HMM AOKMEX OTHOMeHNI. ZINF KOKTPONA NorpeUNOcTH NpOBOAAT xoHTponsHoe vamepenue OK 8 cooreercrenn c pasenamm 10. 11 14.2.2 Peaynsrar Kowrpontworo usmepenin OK cpasrusaror ¢ ero aTrecronanitim sHavennen. Pesynetat KoMTpOnkNOl nNpoueaypal Ky, MPIKT, paccuTseaeT no popmyne Ki = Xo = Bs @) THe Xoo ~ WaMEpeHHoe sKaveHNe MaccoBoli ons Meranna @ OK. Mr 3B — artecropannioe shasenne waccosol gona weranna 8 OK, writ 14.2.3 Hopwatue KowTpona K. srikr, paccunrseaior no cbopuyne k=, (10) tae A, ~ xaparrepucraxa norpewnocta pesynsraros HaMepeHi = 0.84 A 142.4 Mpowonsr conocrasnenne pesynsrara KONTpONBHOM NpOUeAYPS! © Hopwartaom ‘orTpona. Mpoueaypy vaMepeHH npuoHaoT ynoBneTsopH- ‘TenbHoli, eons peaynbrarh! KOHTpoNsHOM npoLIeAypH! yAoBNeTaopAIOT yenoaINO Kel any Tipw HeBbinonHeHin ycnosua (11) KOHTpoNbHyo NpoYeAyPYy NoBTOpAWT. Tipu nostopom Hessinonvenin ycnosns (11) BSiRcHRIOT NpMMuH, NRHBORAUIME K MeygoaneTeopirensHii pesynbtataM, MM npwHuMaCT eps! nO Hx yerpanexino. 22 PA 52.18.191-2018 5.1.10 Annapar ana nonysennA soabi ana na6opaTopHoro auanusa Tuna B02 no TY 25-11-1592-81 6.1.11 OnHoKanansHeie nnneTkn nepemeHHoro Obtema BMeCTHMOCTBIO or 0,2 go 1,0 cw? c norpewiMocrsto gosmposaHna He Goree 2% chupm Eppendort ~ 2 ur 5.1.12 Mlonnnponunenosbie HaKoHeNHnKn K nuneTkam Eppendorf awecr#- MocTeto oF 0,2 20 1,0 cm? 100 usr 5.1.13 OnHoKanansiie nineTkx nepemeHHoro obkéma amectHmocrsio oT 1,0 0 5,0 cw® ¢ norpewnocTeo qosHposahia He Gonee 0,6 % cpupwe! LAB MATE® ~ 1 ur. 5.1.14 Tlonunponinevosbie HaKoHeNHiKM K nieTkam LAB MATE®, auectamocToio oF 1,0 20 5,0 cM? 100 us. 5.1.15 Muneran rpaaywposantie 2-ro knacca TosHocr#, MenonHeHus 1, 2 no FOCT 2927-91 amectumocteio 1 cw 2 uir., 10 cm? — 2 wir 5.1.16 Kon6ts Tuna Ki wcnonennn 2, TXC no [OCT 26336-82 HomMnanb- Hoh smectamocrsto 50 cw? — 50 wr. 5.1.17 Kon6si mepiole wcnonweHun 2, 2-ro xnacca ToNHocTH no TOCT 1770-74 ewectamocroio: 25 cw? ~ 10 wr. §0 cm* ~ §0 wr, 100 cw? ~ 25 wi, 500 cm? ~2 ws, 1000 om? — 5 ws. 5.1.18 MpoGupkm mepxbie wononHenwa 2 no OCT 1770-74 emectamocrsto 10 mn ~ $0 ur 5.1.19 Cink H Bahn creKnsHibie ¢ SMHTOBEIM ropnoM, ¢ npoKNaAKoH KObUKOH NK CG NpWTepTOR npoGKOH ANA xpAHeHNA peaKTWBCS no TY 6-19-4574 emecramocrsto: 50 cu? — 10 usr, 100 cm? — 10 wr, 500 cw? —2 usr 5.1.20 OnaKonb w Banke URNHHApUNECKHE NONMSTINEHOBLIE ¢ HABHHMH- BaIOUMICR KPWKAMA AANA xPAHEHHR POE M peaKTHBOS 110 TY 6-19-45-74 auectumocroie: 25 cM? ~ 50 usr, 50 eM? ~ 100 wx., 100 ew? ~ 10 wr, 200 cm? — 3 wi., 600 cM? —2 wi. 1000 om? —2 wr 5.1.21 Crynka Ne 4 no fOCT 9147-20. Pas2.t8.s91-2018 5.1.22 Cwro naGopatopHoe BT 206.01.000-01 no TY 4846-010- 11149834-2014. 5.1.23 Bopown tuna B, XC no TOCT 25336-82 aramerpow 56 mit ~ 50 ust AvanteTpom 36 wat — 50 usr 5.1.24 Llvnuigps! mepibie wcronienia 1: no TOCT 1770-74 eéectamo- ereio 500 eM? ~ 2 wr 5.1.25 Omnwtpsi oGessonennbie «Genan newray no TY 2642-001- 168085491-2011 quawerpow 14,0 cM 5.1.26 Cravanunkn secosbie anioumueenie c xpsuuxann, BC-1 ~50 wi. 5.1.27 Skcaxatop enonnenns 2 no FOCT 2536-82 awamerpow Kopryca 250 nem 5.1.28 YrnsepcansHan uaukaropHan Gymara no TY 6-09-1181-89 5.1.29 Focynapcreenseia crangeprHit oOpaseu (nanee - TCO) cocrasa pacreopa HoHos amiounnus [CO 7269-96. 5.1.30 TCO coctasa pacrsopa novos Sap FCO 7760-2000, 5.1.31 TCO coctasa pacrsopa wonos sanaqus [CO 7267-96. 5.1.32 TCO cocrasa pacrsopa woHoe xenesa CO 7766-2000, 5.1.33 TCO coctasa sonnoro pacrsopa woos Kaas [CO 7773-2000 5.1.34 CO coctasa pactaopa wovos xoGansra TCO 7268-96. 5.1.35 ICO cocrasa pacrsopa novos wapranuia (Il) [CO 7875-2000. 5.1.36 [CO cocrasa sonoro pacrsopa woHos wen TCO 7764-2000, 5.1.37 FCO cocrasa pacrsopa wowoe mbiuibaKa (Il) [CO 7284-96 5.1.38 CO coctasa eonHoro pacteopa woKos Hixena [CO 7785-2000 5.1.39 TCO coctasa sogHoro pacreopa wovos cama [CO 7778-2000 5.1.40 CO cocrasa eoaworo pacreopa nono xpowa (VI) [CO 7781-2000 5.1.41 TCO coctasa sogHoro pactaopa HoHos yunKa TCO 7770-2000. 5.1.42 CO cocrasa nowess (T9M K-11) CO 9231-2008. Tlpwmewa wwe Alonyeraeres venomsoeanive apyrix Taree cpeacre vaMepeni cnoworarenivoro oBopyaoaanin # marepuaoe €xapartepHcTaauM, OB€creeBOUyN NO rpeunocre raMepeni, yetennyo a paagerte 4c xBaNMuKaLMeR, He He yradeHHOR 85.1 PA s2.18.181-2018 13 Ocbopmnenme pesynbTaTos usmepeHnit 19.1 Sa peayneTar uamepennit npunumaior peaynerar eAMHitsHoro onpe- Renews, Maccosyto nom werannos e npoBax X urlkr npeacrasnsior 8 suqe xta, © Tae £A— a6coniorHoe sHaveHne noKasaTena ToxHocTH MeToAW, rik, paceuurasHoe no cbopmyne 4= a9 ” rae 6 — noKasaTene TouHocri, %. Ecnu maccosaa gona meranna 8 npoSe Hike HiKkHel rpaHitub! AKaNAIOHa vamepenini, nporssopsr cneayroulyio sanucy: «Maccosaa gons meTanna meHee Hueciel rpanmubi QanasoHe HaMepeHiih, mr/Kr> 18.2 lonyctumo npencrasnars peaynsrat 8 BMqe XE, (P=0,95) npaycnosmn A, < 2, ® Fae A, ~ mpaxnusi norpewHoctH pesynsTaToB aHanwsa, ycranosnenHele npu Peanwsaynn weroamKm 8 naSoparopum 4 oGecneynBaembie KoHTponew, cTaGuneHocTH peaynstaros uamepeniii, M/k 13.3 Peaynerarsi usmepenun o@opmnsior npoToKonoM HnM sanwcbIo & >eypiane no cbopman, npuBeneniei B PyxoBogcrse no xavecTay na6oparopin 14 BuyTpenHiii KoHTpont Ka4ecTBa pesynbTaToR MaMepeHHit 14.1 CSume nonoxeHna Buyrpenuith xonrpone KavecTs2 pesynstaros uamepeni 8 na6oparopHn Bbinonisetes 8 coorsercTenn ¢ PMT 76 npenycmarpneaer: a Pa s2.t6.191-2018 Gon @PAHAR MaCcoBaA KOMUEHTpAKNA MeTANMA 8 xonOCTOH npobe. want? V ~ o6u8m pacrsopa noobs, av P — xosibebnunent nepecséra Ha cyxoi Bec; m — acca npobei, easTaa wa aNanus, B cayuae pasbasnenun pacTeopa npo6ti CpeaHAA MaccOBaR KOHYeHTpa- us meranna 8 pacteope npoSti paccuursisaroT no cbopmyne Cap = G8 a on = Oo FE (4) ‘ae Cy — maccoban KoHWeHTpalWNA MeTanna B pacTEOPe pasGaeneHHon NpoGs, saxrlaw V, — o5b€m Kon6ts, 8 KoTOPOR npoBoaNnh pasBasnenne, CM V, — 066M pacraopa npobs\, saRTom aria pas6asnenna, cM 12.2 fina onpenenenus Kostxdmyvenre nepecséra peaynbTaTos wamepe- His Ha cyxOH Bec npobe! maCCOM oF §,00 90 10.00 r nepenoesT 8 npoHymepo- BaHHbIe, BUICYWEHHEIE H RISELUEHHEIC BECORLIC CTaKAHNKH, SAKPHIBAIOT KPbILI- kam w eaneumearor c ToAHOCTEIO Ao 0,01 r. CraKaHuinkn orkpblsaior W eMecTe kpsluikamn NOMEWAIOT 8 WarPeTEIA CYLUMNEHBIM UikaCh W BbICyLAMBAIOT flO NocTO- ‘HHO Mach! npn Teunepatype (10542) °C 8 TeveHne 5 4, Mocne BbicyamBanus weconbie CTaKaHuMKi SaKpEiBAIOT KDBILUKAMM, OXNAKABIOT B OKCHKATOPE C XTOpH- cram KanbuvieM 4 BoReWNBAIOT C TOWNOCTEIO AO 0,01 r. Mocne ssBeuMBaHIIA ‘npoBs NaBTODHO sbicyuMaaIOT 8 TeveHHe 24, OXTAKAAIOT H B3BEUMBAIOT. Bbicy- umBaie NPoBOAAT AO nONyHeHNA pasHocTH Macc NpOBE NPM Aayx Nocneay!o- ux sssewnsannax He Bonee 0,02 r Koachebuunenr nepecuera Ha cyxon Bec P onpenensiot no bopmyne my ma Pe (5) rae m, ~ Macca sosaywHO-cyxOlt npoGe! c RECOBEIM CTAKAHUNKOM Mt KDEILKDA, img ~ Macca nycToro BECOBOrO CTAKaHMMKa C KPBILIKOA, F; im, ~ Macca cyxoi NPOBw! ¢ BECOBLIM CTAKAHUMKON HW EPBILKOA, F 20 Pa s2.18.491-2018 5.2 Mp ebinoriMeHnn vavepenii npumeHRior cneayoUue peaKriAsb! 5.2.1 Kucnora asomHan no TOCT 11125-84, oc. 4 5.2.2 Kucnora conanan no FOCT 14261-77, oc. 4 5.2.3 Boga quctunnuposanias no TOCT 6709-72 5.2.4 Bona ana naboparopHoro axanusa 2-A crene sicTOTs! no TOCT P 52501-2005 (nanee ~ sona ANA aToMHo-a6copGuMoHHoro anannsa): 5.2.5 Kann xnopucreili no FOCT 4234-77. x. 5.2.6 Mlannaanesbin MarpwuHbih MozNcbuKaTOP cbpme! Merck (pacTsop nuTpata nannagus 8 15 %-HoR as0THONl KucROTe c KOKUeHTPAUMeN NannaaWA 10 rem) 5.2.7 Coa rarounsnposannan TexHitieckan no FOCT 5100-86 5.2.8 Kansumii xnopucreii no TY 6-08-5077-87, 4 Tp ww e4 aH we —flonycraercn vcnonssosanne aPyrHx peaxr¥B08, 8 TOM Wicne vunoprHenx ¢ KeannbaKeune We Winke yresenHot 8 5 2. 6 Meron usmepennit Meron wavepennl ochoBaH Ha MaMepenin pesoH@HcHOro NormOWeHNR M3 AYMeHHa cBoGoAKbIMn aToMamn OnpegenseMoro SneMeHTa npn nPOXOXdeHMM sera vepes aToMHbii nap, obpasoBaRuunlics a peaynbTaTe snexrporeprenveckor ini nnaweHHom aTowmsaynn pacTBopa axanusupyeMor npoGe! 7 TpeSopanua GesonacHocTH, oxpavb! OKpyxKarowen Cpemb 7.1 Mpa sbinonkennn vamepennit maccosel Aon xucnoropacTsopHMeix hopm werannos 8 npoBax coBniogaioT TpeCosaHiun CesonachoctH 8 cooTEeT- crann ¢ FOCT 12.1.007 w OCT P 12.1.019 7.2 Mlomewenne, 8 KoTopOM npoBOART HaMepEHNE, AOMKHO BbiTe OBOpy- ROBaHO NpHTOHNO-BEITAMHOI SeTHNAYEN cornacko [OCT 12.4.021, coorser- cTaosar TpeGosaHnsm noxapHol Gesonacnocta comacho FOCT 12.1.004 w mere cpeqctea noxaporyulenia cornacko fOCT 12.4.009 PA 52.18.191-2018 7.3 pw pabore kucnoTamn pykn AOMKHe! Gbire saLuNWyeNb! NepHaTKaNAN, nasa — saunrnbian ovKanen 7.4 OtpaSoranisie pacTBOpe! KNCHOT CnnBAIOT 8 KAHARHZaKN Nocne Heirpannsauin# cogoit. Ina sT0To ovpaBoraHHbie pacrsops! KrcnoT pas6as- jnaloT 6 2-3 pasa eononposomHolt somo” w GoGaBNRIOT HeGonbwnMH NOPUMAMN KanbunnHpoBallyto copy AO HelITpaNBHOA peaKUMM cpeRbI no yHNBEPCANDHOR nauKaTopHol 6yware 8 TpeGonatinn x KeanucbuKaynn oneparopos. K sbinonieHiio HamepeHni o6paGorke wx peaynsTaros gonycKaroT My © Bbicunm nn cpemtite npocbeccHonantHum obpasosahveM, NpoweAUinx co- oreererayroulyro nogroTORKy, uMeoLYNX HaseiKn paBoTe! 8 xHMMMECKOH NaBOPa- Topwn n ocBonsumx MeTORIKY. 9 Tpe6opanua k ycnosmam MsMepeHHi Tipw epinonHeHin vaMepennit coSnioaaioT cheayioulme ycnosust ~ Tenmeparypa oKpyxaroujero sosayxa, °C. 2210: - atmocrbepnoe aasnenne, xa (tw pr. CT). (07 84,0 go 106,7 (01 630 go 800}, - sriaxHocrs Bosayxa npu TeMneparype 25 °C, %, He Gonee. 80, - Hanpamenue s cern, B 220 + 10; = dactora nepemeHHoro ToKa 8 ceTH nHTaHHR, Fu. 5041 10 Pp §2.18.191-2018, 11 Nopavok sbinonHenua uamepeHnit 11.4 Mamepenun waccossx KoMuenTpauwh wcnoTopacrsopamex cbopl etannos 8 pacTeope npo6 nposogsT 8 cooTseTCTEHN C PyKLBOACTBOM NO 3KC- Inyaraynn cnexrpomerpa. B KaxOM cryYae nposogsT Mea NocneAoBATENLHEIK auepenins W eeToMaTnecnn pacowrToIBalor cpegHee SHENENME MaCcOBOH KOM UueHrpaunn metanna 8 pacteope npo6sx. 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K, = 5% ANA pexuma naMenHO atomnsauun 7 % Ans pexua sneKTPOTepMINYECKOR aTOMNZaUHK 11.2 Eenn yenosne (2) He BtinoniseTcA, To SHIFCHSIOT NpHNMHES, YCTPAHSIOT wx NOBTOPAIGT uaMEpeHNs 8 COOTRETCTEMM ¢ TpeBOSeHnAM HacTORLIEM MEV, 11.3 Ecna wamepennar maccosan KoNueHTPayNA MerTanna npesbilieer MaKcuMansiyo maccosy'o KOHLIEHTPALIWO Ha YCTAHOBNEHHOM rpaAyUPOBONHOA 3ABCHMOCTA, TO pacTaop npOOb, NoAyYeNHBI Nocne KNCROTHOrO pasnoKeHHN, pasGasnaior 12 O6paGorka pesynstaTos mamepeHnit 12.1 Maccosy'o Aono xncnoTopacteopumsnx cbopm MeTannoa 8 npobax xX, hurler, paccunTbiBaioT Ha cyxol Bec (BEC NPOGHI, BbICYWEHHOA non 105 °C) no cbopmyne (Cop = Gros) “V-P x (3) Te Cay cpenHAR MaccoB|R KOHLIEHTpALIMA MeTanna ® pacrsope npoBEs, saxcfaw: 19 PA 52.18.191-2018 10.6 Ycrahosnenne rpaaynposoHol xapakrepucTuKH 10.6.1 fina ycravoanenns rpanyuposo¥Hoh xapamrepHcT¥K wonaMbayercR He meee Tpex rpanynpoeownbix PacTsopos. FpanyAPOBONHyIO xapaKTepHCTAKy yoranaenueaior aBTomarivecks 8 CooTREToTEM c NporpaMMIM OBecreveHHEM Cnekrpowerpos nepen KaMo# cepnelt vaMepenn®, B xavecrse pacrsopa c Hynesoh KonueHTpaueR Now YCTaHOBNeHHH TpaRyMPOBOSHOA XepaKTepHCTHKH ononpsyior 0,1 Monb/aw? pactsop asorHoi Kncnores Mion yerahosnenun rpaayupoBosHolt xapakrepucrukn Gapus 8 pexnwe nawesHor aromnsayi X 10 cu! paBounx rpaayupoBoritesx pacrEapoe, noUro- ToaneHibix ® coorseTcTBHH c 10.3.6, aobasnaiT 0.2 cm 5 %-r0 pacrBopa Ka- ‘hus xOPMCTOrO, NpHToTOBNENHOTS No 10.3.4 10.6.2 Konpons cra6unsHocrH rpaayHpoBoNHOl xapaKTepHcTuK™ Bbinon- savor wepes Kexiqnie 25-30 uamepeniti no rpazyupoBoNHoMy PACTEOpy, 8 KOTO- Pom waccosan KOHUeHTpALINA MeTaNna HaXOAMTER B CepeqNNe ANANEsONa vo~ mepexnit, Ppagyuposounyio xapakTepucruky cnexrpomerpa cuMTaior craGunb- Holt, eons abinonHieTcs yenoane [C= Gu oS ne C— pesynetar konrponsHoro HaMepensia MaccoBol KOHUeHTpaUMA MeTanna 100 < Ky, «) © cpanynposourioM pacrsope, mur/am’ Gor — NPUNKCAHNOS BHavEHNe MaccOBOH KOHUeNTPAUMM WeTENna 8 rpAAy- mpogo4nom pactsope, mirigy! Kp ~ HopMarva KOHTponA CTaGuneHoctH MpaayupOBONHOR xapaKTepw- TMK, %, Koy = 10. B cnyyae Hessnonvenus yonosus (1) raayHPoBoUHyIO xapaKTepycrHKy yoranasnusait saHo80, 18 PA $2.18.191-2018 40 Moprorogka Kk BLINoNHeHMIo waMepeHnit 10.1 Nloproroska nocyabi 40.1.4 Ana orGopa w xpanenis nP06, pacr#0p08 wn peaKrHsoe AOMAHA Ho- nanssosarecn nocyaa Wa nnacTaka unn creKna 10.1.2 Nocyay ana or6apa u xpareHn npo6, pacreopoe v peaxrieos cne- ayer roroaiTs cnenyiouyn oSpasoM = TulaTenbio sbimbiTe sononpoBOANO! Bono ¢ MoVOUNMM cpencTEan = 3aMOUMTb He MeHee eM Ha 1 ¥ 8 ropRYet 2 MonbIAM? consHOA KucnoTe; = MPOMBIT BOROMPOBAAHOM BORON, - ononocnyre avcTunnuposansoi aozoft

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