clASSMAte

Date
Experi ment no. 1 Page
Dale
Aim: Preporatien ef erystals c pwe copper swlphate( u sO 5H0)
oom a given impwe sampfe the bu vitiss
heory :lhe aven Semple (e., impuu CusOq 5l40) is shakun
Nater A es drops o
ilute swlphweit aid aru added to
itm order to
prevent hydralysas sk copRur sulphate.
Copper sulphate preseni t h e cumpfe gefs dissswed
l e the mssfuukle
imgwutiss o u lefi ahimd. Thu ssuuin
is erel Th filtate is con
centaded to the cryslallkato
povwt Gnd than codied. Oncosing crystas a
Coppursulphae (CuSO4:5H, O) pepetate ou

Reqiremends Crude sample q Coppur Aulpkate a 10w

beaker a Chana dish a
funnel m evaporatmg
dish, Hilter bumsen
paper ,
bno
Procedwre
1. reparatin ssatutiom
Abow 25-30 oHaler was akdad to ihe qi
ven
copper sukpkate(pudered form) m a aaker.St aas
stred to dissdwe it Nor 2-3d e dilude sulph weic
aud en adled do it to prevent hydroly sis
c
Copper Auphate.
2. Filaticm 6 he soution :
The >auti on wa flHered to remove mdiss dve o{
1mp wutiio Om Hrade w Csllecte{ in a china

3.Concentanticon s he filbate do crstallisation pont:

he lade NC eated pto the Crystali sa Ron pot
by redmcmq vofume do abowl one tuird of it
 elAsSMAte
Date
Page
Expf 1 paje 2

Oigimal vofume
Kemovina a drop e k ssuehiam al the end s
gkas rod omd it N cooled by stonhng The
appestama.
CrusF o tiny crystals on l l% rool hos
Th he crystallisatiom povn has reachad. Than k
hot satwr aB ed_ ssuhont o o tromsferred m a

Crystallisvma dh:
4 Casinq lh Ka satweated bsutian:
Th ssution t e e slauly cssledfer Acmetime. Dup
blu crytas
0 sfCopRurAulpkate apReceLR
5 Separtation ocrystals omd
Th Crystals uàu
dug
Aeporated cmd elsu ed ome hn
CYytals tramsfered to a d r est tue rd
Coxk ra wsed to stojp ltu mout ot l l
tef fuke
The cryAals o pwte coppur (1D>ulphate ( Cuso SH2O) a e
Haielinác, tramsparunt amd btme.

recauthons
The ilhrate Ahold ke eveporated slasky bJ
2. The cAlhate is to ke
qentfehesting
evaporad ed owy wpto crustallisatim
pomt t showd mever lae heed ed to drunus
3.Thu>suhion haulA ee coofed lay wilbou distwbeit
Hamq o t thu crstslo wik Haskihq igud 3-4 time
usin Small Amomt ot iquid each time
 ASSMA-TE.
Date
Expeiment no. 2 Page

Pai3
Aimiomalyse he aiven salt to detect aud ralical.
Sample mumber : 101

Physical Exam natien

Cotswr NKite
Physical State: Crystaline so

Odouwe O doweles
Solubility Nater Soluble m ate

Doy heating test

Exper ment Observaton nfereme
Small CUmoumt the 2ven A cofowtless a G a
Salt Hoas stronly Keated evotve emd thi 1 Cn may e

cleam , dzy est +ube. qcs tutms lime-water present

C

milk
Dilute Sulphwue aud test
Expetment Obser atian mereme
Small am oumt o the 2iven A Colowtles odour lass co
Salt sGS taken m a cleam 20 Na evstved
may
4 est tuloe amd1-2 oki brisk_ eKecvescen PresemE

lute HS0q HGA aRLi d_ The evolived ate

twt me ater
The evslvel gom v7ky
passed hrous lime iater
Contmation o aud radicals bu Het tests
reparahon agu ater extract
Small Cm oumt sthe salt we taken a cle cm

test tuloe isHllel ater Has adLL o it Thn it

shaken AA clear AcfuHon forme Thessution
1S Nater ex act c W.E
 easSMAte
Date.
Page

Ept-2 Paje.
Expau ment
Obser vahan nerence
- 3 m o water ex ract u Brisk eevascencs c oior
taken m a cle am test tuke. Occws emd cofoweleu, Coftrmed.
1-2mm dilute_H C s eve addel | eodowdeu 2 a
toit evofved. Th evofved
The evdived _2aa nam passed 2 twens lims aker|
hrough lme_water. mlk

(i Magnegium Sulohate est A Hhite precipitate Co on

12 m s ater ex bact formeA Cerntrmek
treated wilt.
maamei um Sulhate

Souhon
Kesult: CO on dae detected

Chemm cal eaciont Imvsved m dilute H,s©4 Test

On tTeatm gthe sohd catbanate ilb lute H2 SO4

CO2 2ven of wi brik eferves cence

C
cOO t 1HS O4 Co t H20_+ SO
C O , tHO + NaSO4,
e q N4 O2t H SOq

Keachom Cer bonmáte wi dolude HC &sutan

2 2H C
cO2 +
cO2 H0 + 2 C
COa-
Na O2 2HC cO + 4 , o+ 2 Nact
Maameiuum Sulshate est
CO_Ca2)+M5O4cag) MaCo(t SOtags
5 0 C a g ) > M a C O(s) t a SO4Cas
t e Ppt-
 ClASSMALE.
Date
Expeviment mumber; 3 Page.
Pa-5
Aim To emalyse the qtven. salt to detect add radical
Sample mumber : 305
Pbysical ExemunaHen
Physica state: Cyskalli'ne solid
Colow ite
Odowe Odoweles s
Solubility : Seluble ater

Dry heatingest
EXperment Observation Imferen ce
Small amaunt sthe selt waoA 400 evotved ukich ss2 ion
ion.
may 6 e
taken m drey test duleeSmells Cke rdten ega
heated lhe evefved aa twms pT2LenE
bums en bWmer lead a c e BsBe pppur
Has_tested_blak
The evdved 3
ead au tate paROA

Dilute swlphuwic add test

Obsevaton Tnference
Ex peu ment

Small a m a u n t ot hL l tA ceioureless gase

tube:evsfved hich has S im may
N s a taken m a teyt
offen egg Smell omnd be present.
2- dilute H So4 ka
w n elead acchste
addad to i t The evafve
pper black_
26 Han tested l
lead acetate_papet
atey extract WE):
epoeatiem agueCws Aouhom r clecm text-
Small_ amaunt e he sat tap taken
it: Thwn i t aA.
tuloe s t illed water was added o T s
v a e formek h aá
shaken A clease atuian
suhem a t e exacE (HE)
 elasSMAte
Date
Page t-3
Pos-6
Confirmatim saud radical by Het isfsi
txperiment Observation Inference
DLeadAcetate Test
2- d atey axbact| A Lfack precipitate s iom
NGAtaken cleam NaA osmed Cottsmed,_
+e_ du lat Fe dcops
l e a d alutate soutiam

C)Sodi um nibrusside test

2-3 e ater exhacE pwepfe r iolel- s om
t a k e n m_a test tube Cofowea Han Cem firmed
amd e r dops o obseved

Bsuhm aAlrd 4o it

(n Wa detected.
Resut s 2

Chemi cal Teachow mvstved n dalute H,s0A Test

Swphmde sadt ives H2S gus hun reactel wm dal. H,S
Na S t12s04 HS(a t N SO4

Leadacetate Test
NG2 5tns1 tC4,coo) Pb PESLs) t
2CHa Ceo NaLag)_
Back

Sedium ibe2prusside Test

NaS ag) t NaFe CNNO Na,lFeCcNNOS
Violet or_psepe
cefow
 Experi ment number Date

Aim: To Cmaly se the qiven saut to detect aud ra

dical
Smple mwmber 202
Physi cal Exami
naion
Physical state
HiBeCrteiline
s i d
Cafowe
Odagwt Odoweles
Solurlit Seluble Nater

syheatingest
Experiment Observatian
Small amoumt othe 1nference
sadt
N Shrungly heate ma Smellslke bwtning|
clecm dre test tulbe The Sulphwc. soin
may b e
evslved gGp_ NGS paKed Oromap smhon presennt
hreugk au dified potassi um 4wuns heen
dachromate sdutian
Dilute sulphwric autest
Expenment Obsevahon Inference
Small am ount heBalt iasA cotoweleu qes evsfvek
aken m
cle Cm test tue.Kich ke
2-3 _dilute H,s04 R
smells
soi
buting Sushwe may
adlad to ItTheevved quOkomas ssuhen present.
HG pased fhrous aidijed 4wns een
pstaium dichrom ate Sahution.

reporahon s a4msow setuho Watem extract (HE)

Small amownt slt He takn a clecm test +ube.
Diskilled water n _addud o i t S + &hakin emd a
clear A6uhn es tomad. Thi Ater extrac
 SSMAte
Date,

Con fixmati om s aud radi cal b Net 4ets :

Page
-y4
Expeiment Observatan LferAnce
Basuwm chlam de test A Aite pxecipitaie |
To 2-8 ater exrac formed hich S O ion

T um chlmdde ssutiam saeonssdwel m i l . Cenfirmed

added 1H C Ssiui on
The preipitate_waeeated
wi ilute H sautiem

(IPafagtiwmcichromate test
2-3 Hatex ex hac omge sahuhicn so
NG reat ed wlb i ute twtns een= Cona'rmed.
Sulph wuc au& eme than
whpåtagium ohchromate
Samtcm
Regut SO m asdetected

Chemicel Reachions lnvafved dilute HSd4Test

Sulphite Aalt aives s0ac isk ilute H,so Aud.
Na, sO t H SO4 SO, +_ HO + Na2 SÔ

Botti um chlonde est

NA S03( Badz Caq) Basoz(3)t 2
NaC (ag-
BaSO2
L s +2Hacag)_ S02 (g) + 1420(1)+Badz cas:

Pofassiwm dchromate test :

Na
S0+ H2 S0, + 1A2 O + Na2 SO

KCr,O7 H2 S04 t3s02 Cr (s04)g(ks) t K S04 Lag) t H20

Oxoms een
 la.SSMAte.
Expeiment mwmber 5 Dafe
Page

Pa-9
Aim lo omalyse 1he given slt to eetect acid Tadical

CUmple numbe: 307

hysteal Examinatien
Physical state : Crystalline solid
Cafowe Hite

Odow Odowrlecs
Solubili Salwkie Hater
Dsy heatingTest
Expezment Observahom lnetemce
Small amcumt s the gdven Redlish b maA NO
salt wGA shranady heated a evdved hich
clecum d test tulas.twns ferroww Skyhate may be
presemt
Ihe evetve gA a paded |ssutian black
Througk ferowo sulpkate
souem
Diute Sulphwic audest
Observation 1nferemce
Experiment_
NO, 1an
Small amoumt s He sautA eddish baam may be
WEA takim_ a eam NG evofved HKich
presenF
test tuke 2-3 mo dilute twtne eryo
|HSO4aR added to it Sukphate Bdtuticn
The evsved qae wa passeR | lack
hrugb ferraue Sulpkate
sautian
extrack (E)
sepacatien s aquioue sotuhon or dater
SUt Wa takim m
Small amoumt ok the
adlid to t Thin
tuke. d istilled Later ro
cleam t e s t
obfcwined
IE HV shaken A clear Loutan hee
Naterexhet (HE)
T h Aomhcn knaum Ge
 cassMAte.
Date
Page
Eyp-5
Cnfirmatiom acidrad'cal by wet tests
ExpeT| m e n t Observahann lnterence
(1 Fexrous suphate test _ A dack braum NO on
2-3 e Natey ex bact predptaten e Cantismed
Han taken m a
eleam test | formed.
tube. Fer dops o lute
acent aud wa added t
itThum ferreune sulpkate
wc added .

CiDStascch - Iodide test:

To 2- s water exhact A btue ssutionm NOin
stamel. Canfrmed
added Thn es draps
pofassi wm iodiele sstution
a adled to it Thm
fer drops o reshly
1prepaned_starrch sution
Aeadled to i t
Resuut: NO m detected

Chemi caR Te ac hics mvsved dilute HSO4 est

Nate salt ves NO_gO dil. H,SO hich readil
ve denge broumumes o NO, nl6 OXy m m aUr
3KNO t H2 SO4 3KHS O4 t HNO t Hz Ot 22NO
NO Cg)
NOLgp t0, cg) 2O2 (9) ume s
1run

ero we Suehate Test

KNO_+ CH COD H C aCoo K +HO
3 HO, +2 O + 420
Fe SO + Fes O CD aek braum2
ota sSTUm iaide test
+2 H2SO+2 H NO2 2KHSO4 + l2 t 2NO + 2 426
12 wm Staech papUr ue .