K SPECTRA Laboratories 2221 Ross Way * Tacoma, WA 98421 (253)272-4850* Fax (253) 572-9838 www.spectra-lab.com 11/18/2015 Project: King Co. KCIT Radio Client ID: Rattle Snake LK WO-29224 D Square Energy Systems Sample Matrix: Antifreeze 201 W North Bend Way Date Sampled: 10/30/2015 North Bend, WA. 98045-8196 Date Received: 11/12/2015 Spectra Project: 2015110339 Spectra Number: | Analyte Result Units Method Bot. Sediment and Water = 0.05 vol. % ASTM D-2709 Percent Antifreeze 34 vol. % ASTM D-287 Specific Gravity at 60 °F 1.078 ASTM D-287 pit 9.50 pH Units SM 4500-H B Aluminum 05 mg/L. SW846 6010C Boron 500 mg/L SW846 6010C Calcium 37 mg/L 'SW846 6010C Copper 13 mg/L. 'SW846 6010C Iron 0.91 mg/L SW846 6010C Lead 68 mg/L, SW846 6010C Magnesium <0.06 mg/L SW846 6010C Nickel <0.03 mg/L SW846 6010C Phosphorus 46 mg/L. ‘W846 6010C Silicon 2 mg/L. W846 6010C Sodium 1900 mg/L 'SW846 6010C Tin 2.0 mg/L SW846 6010C Zine 23 mg/L SW846 6010C Lead is very high, and could indicate a problem with corrosion or wear. SPECTRA LABORATORIES, = SS Steve Hibbs, Laboratory Manager Page 1 of 4 Sighh SPECTRA Laboratories 2221 Ross Way * Tacoma, WA 98421 11/18/2015 D Square Energy Systems 201 W North Bend Way North Bend, WA 98045-8196 Analyte Bot. Sediment and Water Percent Antifreeze Specific Gravity at 60°F pH Aluminum, Boron Caleium Copper Iron Lead Magnesium Nickel Phosphorus Silicon Sodium Tin Zine SPECTRA LABORATORIES Steve asiseh Laboratory Manager © (253)272-4850* Fax (253) $72-9838 * www.spectra-lab.com Result Trace 52 1.074 9.69 3.0 441 18 3.0 0.37 32 < 0.06 < 0.03 79. 23 1510 49 0.55 Project: King Co. KCIT Radio Client ID: ‘Squak Mt WO-29228 Sample Matrix: Antifreeze Date Sampled: 10/29/2015 Date Received: 11/12/2015 Spectra Project: 2015110339 Spectra Number: 2 Units vol. % vol. % pH Units mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L. Method ASTM D-2709 ASTM D-287 ASTM D-287 SM 4500-H B SW846 6010C SW846 6010C SW846 6010C SW846 6010C SW846 6010C SW846 6010C SW846 6010C ‘SW846 6010C SW846 6010C ‘SW846 6010C SW846 6010C ‘SW846 6010C SW846 6010C Page 2 0f 4i SPECTRA Laboratories 2221 Ross Way * Tacoma, WA 98421 14/18/2015 D Square Energy Systems 201 W North Bend Way North Bend, WA 98045-8196 Analyte Bot. Sediment and Water Percent Antifreeze Specific Gravity at 60°F pH Aluminum Boron Calejum Copper Iron Lead Magnesium Nickel Phosphorus Silicon Sodium Tin Zine SPECTRA LABORATORIES ———oe Steve Hibbs, Laboratory Manager “aSiseh © (253)272-4850 * Fax (253) 572-9838 © www.spectra-lab.com Result < 0.05 57 1.082 8.09 41 140 <0.06 38 0.12 1 < 0.06 0.05 3440 28 1100 <01 0.23 Project: King Co. KCIT Radio Client ID: Ring Hill WO-29226 Sample Matrix: Antifreeze Date Sampled: 11/03/2015 Date Received: 11/12/2015 Spectra Proj Spectra Number: 3 Units vol. % vol. % pH Units mg/L, mg/L, mg/L, mg/L. mg/L mg/L mg/L. mg/L mg/L mg/L mg/L mg/L. mg/L 2015110339 Method ASTM D-2709 ASTM D-287 ASTM D-287 SM 4500-H B SW846 6010C SW846 6010C SW846 6010C SW846 6010C 'SW846 6010C SW846 6010C SW846 6010C SW846 6010C SW846 6010C SW846 6010C SW846 6010C SW846 6010C SW846 6010C Page 3 of 4K SPECTRA Laboratories 2221 Ross Way * Tacoma, WA 98421 11/18/2015 D Square Energy Systems 201 W North Bend Way North Bend, WA 98045-8196 Analyte Bot. Sediment and Water Percent Antifreeze Specific Gravity at 60°F pH Aluminum Boron Caleium Copper Iron Lead Magnesium Nickel Phosphorus Silicon Sodium Tin Zine SPECTRA LABORATORIES ot Steve Hibbs, Laboratory Manager aSseh © (253)272-4850* Fax (253)572-9838 © www.spectralab.com Result <0.05 51 1.073 8.49 7.0 515 0.10 25 15 6.0 < 0.06 < 0.03 2030 161 1510 0.5 0.85 Project King Co. KCIT Radio Client ID: Federal Way WO-29223 Sample Matrix: Antifreeze Date Sample 10/30/2015 Date Received: 11/12/2015 Spectra Project: 2015110339 Spectra Number: 4 Units vol. % vol. % pH Units mg/L mg/L mg/L mg/L. mg/L mg/L, mg/L mg/L mg/L mg/L mg/L mg/L mg/L Method ASTM D-2709 ASTM D-287 ASTM D-287 SM 4500-H B SW846 6010C SW846 6010C 'SW846 6010C SW846 6010C ‘SW846 6010C SW846 6010C SW846 6010C SW846 6010C SW846 6010C SW846 6010C SW846 6010C SW846 6010C SW846 6010C Page 4 of 4“ouy eopATeuy eoeds “eNUGA V/A "0D BAe%\d Uf POIL &| UNE J4FEYM JO SBeIpYeBas UOADEIIOD JO S}S00 Ja\YO IIe pUE $29) | AOWIONE eiqeuoseall Suprouuopaeyyo Jo sj00 fed 0 spas etic ele \QUOU Jed % 2s cl efans sudo enp see “ep OF YON Sle, wouuhed Ong TH me TEU Tye aU ‘Ag canso2y| 7 f "| wanenome MAT | 1 g a yacanoa COZ | Cefoi al MW UTC, —— EnTy a Tawa SN GaN RABE SINNNOD/SNOLONELSNI TWId3ds| lo 6 oi T lL le fatal wrt I] WD) Cl HZ] WOT Pq | ee | BE TTRTETETETS1E] IF Hee ATEE TE eee elt S] 1 VHaST lel (elle aile fle fEFWa——_______ Fuscuoasvnaung z rab g 9 lo F EL le i ' i ? tl ig SE he _woodiouscpoejaes "WWF r | FP ef 3 VE (SCH) NOH t g 4 ‘Bis arenbs "TOVINOO al “TO Gash aL Tan TWAGIAIGNI POE LID" WE ToaroHa| eee ‘SP086 VM “PUP: ION O2# SS MN AV WleOd SFST “SSANCOV ‘ASsxoug arent “INSTTO} Clsemscov oe Fert vacroony «eye zz Hsny |X GYVGNVLS worgr-edvane 5 s — Lim Ey SEENEID sauowiogey VULOTdS | fe says