SPECIFICATION Stee OR UMITED ae SUERELSTINESSSTEGL AMO, 8.790018 Rev.0 sere aed ved ed wd ER Sere area tea sca @ feu farta SPECIFICATION FOR DUPLEX STAINLESS STEEL AND SUPER DUPLEX STAINLESS STEEL (0 28.12.08 ISSUED AS STANDARD SPECIFICATION ie a ; ‘Standards Committee Rev. spose Prepare Checked Coe chattaan Rev. ate Purpe iby by —Cofivenor_Chairmar ‘Approved by Format No. 6-00-000%-F1 Rev. 0 Copyright EI — Al rights reserves‘STANDARD SPECIFICATION No. 6-79-0015 Rev. 0 Page 20f 12 SGI Sy ENGINEERS SPECIFICATION FOR segeeee ORAL pun ecsramass Se Abbreviations: ABS American Bureau of Shipping ASME American Society for Mechanical Engineers ASTM : American Society for Testing and Materials BV Bureau Veritas CEIL Certification Engineers International Limited cPr ‘Chemical Process Industry csc Chloride Stress Cracking DNV Det Norske Veritas Dss Duplex Stainless Steel HAZ Heat Affected Zone Iso International Organization for Standardization Mss. ‘Manufacturers Standardization Society NACI National Association of Corrosion Engineers PREN Pitting Resistance Equivalent Number spss Super Duplex Stainless Steel ssc Sulphide Stress Cracking SMMS Standards Committee Convener Shri KK. Mallick (SMMS) ‘Members Dr. G. Saha (SMMS) Dr. V.R. Krishnan (SMMS) Shri P.P. Lahiri (SMMS) Shri M.R. Chakraborty (Piping) Shri AK. Tandon (Construetion) Dr. Mukesh Kumar (Metallurgy) Shri S.K. Sood (Refinery 1) Committee constituted to revise the standard: Chairman Shri BK. Raut (SMMs) Members Shri B.S. Gupta (HMTD) Shri MLR. Chakraborty (Piping) Shri Sheel Yadav nspection) Shri G.D. Goyal (Process) Format No. €.00-0001-F1 Rev. 0 ‘Copyright ETL — Al rights reservedSennen SPECIFICATION FOR ‘STANDARD SPECIFICATION No, INDIALIMITED _ DUPLEX STAINLESS STEEL AND - SRELEREE SROAINEED super ourtexstantess oree, 72.0018 Rev. CONTENTS Clause Title Page No. 10 SCOPE 4 2.0 CODES AND STANDARDS 4 3.0 STEEL MANUFACTURE 5 4.0 HEAT TREATMENT 5 5.0 APPLICABLE REQUIREMENTS FOR DSS & SDSS 5 6.0 PRE-QUALIFICATION CRITERIA FOR MILL / MANUFACTURER, 8 7.0 CORROSION TESTS FOR PRE-QUALIFICATION * 8.0 REQUIREMENTS FOR PRODUCTION TESTING ul 9.0 QUALITY SURVEILLANCE AND INSPECTION 2 10.0 DOCUMENTS TO BE SUBMITI Format No, 6-00-0001-F1 Rev. 0 ‘Copyright EIL — AT TGhTS reservedSOMONE sproricanoNron __sAmannereceranowa SEBBONR i oudsanee sree aw Sreagis mee SRRESONOAUWIED cGpeeouniensrancesseree, —_7EO01S Rev.0 1.0 SCOPE 1.1 This specification covers the specific requirements for manufacture, inspection, testing and supply of duplex stainless steels conforming to UNS No.(s) S 31803, $ 32205 or equivalent and super duplex stainless steel conforming to UNS No(s) $ 32760, S 32750, $ 39274, § 32550, J 93380 or equivalent. DSS and SDSS material shall be considered acceptable when they meet the pre-qualification criteria mentioned in this specification. 1.2 This specification shall be read together with the corresponding product specifications mentioned in the relevant piping material specifications or the equipment data sheets/design drawings intended to be used in sour and/or chloride containing environments, as applicable. 1.3 In case of conflict between this specification and the referted material codes/standard specifications, the requirement of this specification shall govern. 2.0 CODES AND STANDARDS ~ ‘The manufacture, inspection, testing, marking and supply of the item covered by this specification shall follow the latest editions of the following codes and standard specifications: ASTM A182 Forged or rolled alloy steel pipe, flanges, forged fittings and valves and parts for high temperature service ASTM A240 Heat resisting chromium and chromium - nickel stainless steel plate, sheet and strip for pressure vessels ASTM A276 Stainless steel bars and shapes ASTM A351 Casting - austenitic, austenitie-ferritie (duplex) for pressure containing parts ASTM A370. Standard methods and definitions for mechanical testing of steel ASTMA743. Castings - iron-chromium-nickel-base corrosion resistant, for general application ASIMA744 Casting - iron-chromium-nickel-base corrosion resistant, for severe application ASTMA789 Seamless and welded ferritic/austenitic stainless steel tubing for general service ASTMA790 Seamless and welded ferritic- austenitic stainless steel pipe ASTMA799 Steel _castings-stainless instrument calibration for estimating ferrite content ASTMAS8I5 Wrought ferritic, ferritic-austenitic and martensitic stainless steel pipe fittings ASTM A923 Standard test methods for detecting detrimental intermetallic phase in wrought duplex austenitie/ferritic stainless steels ASTM A928 Specification for ferritic/austenitic (duplex) stainless steel pipe electric fusion welded with addition of filler metal ASTME 18 Rockwell hardness testing of metallic materials, ASIME 562 —_ Determining volume fraction by systematic manual point count ASTM G36 Performing stress corrosion cracking tests in a boiling magnesium chloride ASTM G48 Standard test methods for pitting and crevice corrosion resistance of stainless steels and related alloys by use of ferric chloride solution ASME B 16.34 Valves- flanged, threaded, and welding end ASME Sec.V _Non-destructive examination MSS-SP-55 ‘Manufacturers Standardization Society of the Valve and Fitting Industry Standard — Quality Standard for Steel Castings for valves, flanges, and fittings and other components (visual method) Format No, €.00-0001-F1 Rev. 0 Copyright EIL— All rights reservedGRR By ENGINEERS. SPECIFICATION FOR ‘STANDARD SPECIFICATION No. Pee SAGA TRAD DUPLEX STAINLESS STEEL AND 6-79-0015 Rev.0 eGecmows — stwenaniemms _ SUPER DUPLEX STAINLESS STEEL. 3.11 4.0 4d 42 50 Sa Page 5 of 12 NACE MRO175/ Petroleum and natural gas industries-Materials for use in H:S-containing ISO 15156 environments in oil and gas production: Part 1 General principles for selection of cracking-resistant materials Part 3 Cracking-resistant CRAs (corrosion-resistant alloys) and other alloys NACE MRO103 Material resistant to Sulfide Stress Cracking in corrosive petroleum refining environments NACETM0177 Laboratory testing of metals for resistance to sulfide stress cracking and stress corrosion cracking in H;S environments SNT-TC-1A Personne! qualification and certification of nondestructive testing personnel, American Society for Nondestructive Testing (ASNT) STEEL MANUFACTURE The steel shall be manufactured / produced by the following or as specified in the applicable material specification: : ‘The steel shall be made by one of the following primary steel making processes: = electric are furnace, - electric induction furnace. The steel shall be subjected to tertiary steel refining treatments such as vacuum oxygen decarburization (VOD) argon oxygen decarburization (AOD), and vacuum are degassing (VAD) to minimize dissolved gas contents, inclusions content and to meet the chemical composition with close tolerances. HEAT TREATMENT Duplex Stainless Steel (DSS) All the finished product forms shall be solution annealed by holding it at 1020-1080°C followed by a fast cooling procedure. The duration of homogenizing treatment is dependent on the product forms and thickness, but shall be not less than 20 minutes per 25 mm of thickness. For product thickness is less than or equal to 10 mm, forced air cooling shall be carried out while for thickness greater than 10 mm, water quenching shall be carried out. All hot working/forging operations shall be carried out within a temperature range of 1020-1080°C. No hot working/forging operations shall take place at temperature less than 1020°C. Super Duplex Stainless Steel (SDSS) All the finished product forms shall be supplied in solution annealed condition. The product shall be homogenized at 1050-1100°C followed by a fast cooling procedure. The duration of homogenizing treatment is dependent on the product forms and thickness, but shall be not less than 20 minutes per 25 mm of thickness. For product thickness is less than or equal to 10 mm, forced air cooling shall be carried out while for thickness greater than 10 mm, water quenching shall be carried out. All hot working/forging operations shall be carried out within a temperature range of 1050-1100°C. No hot working/forging operations shall take place at ‘temperature less than 1050°C. APPLICABLE REQUIREMENTS FOR DSS AND SDSS Chemical Composition Chemical composition of DSS and SDSS shall be as per Clause Nos. 5.1.1 and 5.1.2 respectively. Format No, 6-00-0007-F1 Rev. 0 ‘Copyight ETL — Al fghts reservedSPECIFICATION FOR STANDARD SPECIFICATION No. TSWASS: — inmewmminns! SUPER DUPLEX STAINLESS STEEL eee Page S11 DSS Element wi% Carbon (C) 0.03 (max.) Manganese (Mn) 2.0 (max.) . Silicon (Si) 1.0 (max.) Sulphur (S) 0.02 (max.) Phosphorus (P) 0.03 (max.) Chromium (Cr) 21,00 - 23.00 7 Nickel (Ni) 4.50 - 6.50 Molybdenum (Mo) 25-3.50 Nitrogen (N) 0.15 -0.20 Copper (Cu) 0.50 (max.) ‘Tungsten (W) 0.50 (max.) 5.1.2 SDSS Element wi% Carbon (C) 0.03 (max.) Manganese (Mn) 1.0 (max.) Silicon (Si) 1.0 (max.) ‘Sulphur (S) 0.02. (imax.) Phosphorus (P) 0.03 (max.) Chromium (Cr) 24.0 - 27.0 Nickel (Ni) 6.0-8.0 Molybdenum (Mo) 35-45 Nitrogen (N) 0.20 - 0.35 Copper (Cu) 0.75 (max.) Tungsten (W) 1.00 (max.) 5.1.3 Ifany other elements are proposed to be added, such proposals shall be submitted to Company for specific written approval. Copper (Cu) and Tungsten (W) additions exceeding the limits as specified above shall be acceptable, provided the weldability and freedom from undesirable ‘metallurgical constituents are ensured. 5.2 Pitting Resistance Equivalent Number (PREN) 5.2.1 PREN shall be calculated by the following formula: PREN = % Cr+3.3 x (%Mo) + 16x (%N) 5.22 PREN for DSS The pitting resistance equivalent number of the duplex stainless steel materials shall be greater ‘than 35, when calculated as mentioned in Clause No.5.2.1 5.2.3 PREN for SDSS ‘The pitting resistance equivalent number of the super duplex stainless st greater than 40, when calculated as mentioned in Clause No. 5.2.1 53 Microstructure Format No, €-00-0001-Ft Rev. 0 Copyright EiL ~ Al ighis reserved‘SPECIFICATION FOR [STANDARD SPECIFICATION No. SBaRERSNTALMTED —_OUPLEX STAINLESS STEEL AND 6-79-0015 Rev. 0 “.Gwacet — vuaaeainanme SUPER DUPLEX STAINLESS STEEL. 53.1 53.2 53.3 534 34 54d 542 Page 7 of 12 DSS The duplex stainless steel shall have approximately equal proportions of austenite and ferrite phases and the ferrite content shall be in the range of 40-55% in the austenite-ferrite matrix, SDSS For super duplex stainless steel, the ferrite content shall be in the range of 35-55% in the austenite-ferrite matrix. Ferrite content measurement for DSS and SDSS material shall be carried out for each heat by metallography method in accordance with ASTM E 562. In case ferrite-scope is expected to be used during fabrication/erection for the ferrite measurement, then the testing at shop shall be carried out by the ferrite-scope also, and the correlation between the results from the two methods shall be established for future use. For DSS and SDSS products, either in the as-supplied condition, solution annealed condition, or in the as welded condition, the microstructure shall not reveal the presence of any carbide or any intermetallic phases to the extent that are detrimental to the toughness and corrosion resistance of the material. The detection of the detrimental intermetallic phases in the wrought products shall be carried out in accordance with ASTM A 923. The intermetallic phases shall not be more than 1%. Mechanical Properties DSS and SDSS ‘The material in the solution-annealed condition shall conform to the mechanical properties such as ultimate tensile strength, 0.2% & 1% offset yield strength, %elongation, hardness applicable for the respective UNS No. of the material. The tensile test shall be carried out as per ASTM A 370. The hardness test method shall be in accordance with ASTM E 18. If any other methods including portable hardness tester are to be deployed for checking production welds, then the correlation between the qualification method and the production method shall be established and the calibration graph shall be generated for use at the field/shop. Impact energy (Charpy V-notch) for DSS and SDSS ‘The impact test shall be carried out as per ASTM A 370. ‘Wrought materials at 20 120 J (Average)/ 90 J (Minimum) at-30°C 100 J (Average)/ 75 J (Minimum) Cast_materials at 206 75 J (Average)/ 55 J (Minimum) at-30°C 60 3 (Average)/ 40 J (Minimum) Format No. 6:00-0001-F1t Rav. 0 ‘Copyright ETL — AI ights reservedsand ress SPECIFICATION FOR ‘STANDARD SPECIFICATION No. g@areteies @INDIAUMTED _DUPLEX STAINLESS STEEL AND 7 “rGrcasee weatanssimarsi SUPER DUPLEX STAINLESS STEEL. eee Page 8 of 12 6.0 PRE-QUALIFICATION CRITERIA FOR MILL / MANUFACTURER 6.1 The DSS and SDSS material components shall be procured from a pre-qualified supplier. The supplier shall be qualified for specific UNS No. for which the mill was pre-qualified. Any change in UNS No. shall require a fresh pre-qualification, 6.1.1 Pre-Qualification Criteria for Vendors with Prior Experience Track Record Vendors/manufacturers who have proven track record of supplying DSS and SDSS materials for sour service and chloride containing environments in chemical process industries (CPI) to any of the reputed operating companies/Engineering Consultants or Process Licensors such as UOP, IFP, EXXON, BP, CHEVRON, IOCL, HPCL, BPCL, and EIL shall be considered as “pre-qualified vendors/manufacturers’, on production of the relevant Purchase Orders and test certificates, certified by a witnessing third party inspection agency such as DNV, Lloyds, BV, ABS, TUV, SGS, CEIL, and BIL for the conformance of the materials to the respective materials specification of the mentioned operators / engineering consultants. For pre-qualified vendors, Clause No.6.1.2 is not applicable. 6.1.2 Pre-Qualification Criteria for New Vendors without Track Record ‘A vendor who has no track record of supplying DSS and SDSS materials for sour service and chloride containing environments in chemical process industries (CPI) to any of the reputed engineering consultants/operators, as mentioned above in Clause No.6.1.1, shall be considered. as a new vendor. The chemical, the mechanical and all the corrosion tests shall be carried out as mentioned in Clause Nos. 5.0, 7.0 for pre-qualification by any one of the reputed third party inspection agencies like Lloyds, BV, CEIL, DNV, TUV, and EIL. 6.2 The corrosion tests for DSS and SDSS in accordance with the Clause No. 7.0 shall be conducted for the pre-qualification of the manufacturers/mills. 63 All the tests reports including the corrosion fests shall be based upon the tests conducted on the product specimen drawn from a single heat, and shall bear the same heat number. 64 Incase the manufacture(s) had already conducted all the corrosion above tests on a product of the same material in the past, and has an approved quality assurance system in place, and the test results are certified by a witnessing a third party inspection agency approved by the ‘Company, the test results shall be furnished by the bidder, along with his bid, for Company's review. ‘The manufacturer(s) shall be qualified based on the satisfactory review of the submitted test results. The Company's decision in this regard shall be final and binding on the bidder. While selecting and procuring the duplex stainless steel and super duplex stainless steel materials for a specific project, care shall be taken to use the same UNS No. for the entire system. Bidder shall note that, subsequent to qualification, a change in combination of ‘mill/manufacturer and UNS No. shall call for a fresh qualification exercise to be conducted. 6.5 Examination for DSS and SDSS Castings 65.1 Visual All castings for valves, flanges, fittings and other components of DSS and SI visually examined in accordance with the quality levels mentioned in M! procedure for visual examination, and the acceptance criteria shall be as per MSS-SP-55. Format No, 6.00-000%-F1 Rev. 0 Copyright BIL — Alights reserved65.2 70 TA 72 721 722 ‘SPECIFICATION FOR STANDARD SPECIFICATION No, ENGINEERS BORAGE wo SRCWACE SS (Enunstwes — SUPERDUPLEX STAINLESS STEEL «© 70018 Rev.0 Page 9 of 12 Radiography Radiography examination shall be performed on all DSS and SDSS valve castings (in accordance with ASME B16.34 with the acceptance criteria mentioned therein) and flanges, fittings and other components of DSS and SDSS in accordance with Article 2 of ASME Section V. The operator’s certification to SNT-TC-1A or equivalent is required. Penetrant Test Wet fluorescent penetrant examination shall be performed on the exterior and accessible interior surfaces of all DSS and SDSS valve castings (in accordance with ASME B16.34 with the acceptance criteria mentioned therein) and flanges, fittings and other components of DSS and SDSS in accordance with Article 6 of ASME Section V. The operator's certification to SNT-TC-1A or equivalent is required, CORROSION TESTS FOR PRE-QUALIFICATION Sulphide Stress Cracking (SSC) test as per Clause No. 7.2, Chloride Stress Cracking (CSC) test as per Clause No. 7.3, Pitting Corrosion test as per Clause No. 7.4, Crevice Corrosion test as per Clause No.7.5, are mandatory when DSS and SDSS steel materials are intended to be used for sour service and chloride containing environments. IEDSS and SDSS materials are intended to be used for chloride containing environments only, the SSC test as per Clause No.7.2 shall be waived off. The remaining corrosion tests spec in this section shall be carried out for DSS and SDSS materials meant for use in the chloride containing environments. The corrosion tests applicable for DSS and SDSS materials shall be as furnished in the following paragraphs: Sulphide Stress Cracking (SSC) Test DSS. SSC test on duplex stainless steel shall be carried out by using the following test solutions and test conditions: i) a) Test solution NACE T0177 b) Test temperature we ¢) Stress value 350 Nim? 4) Acceptance criteria test sample failure at or after 720 hours. ii) a) Test solution NACE TM0177 b) Test temperature 290°C ©) Stress value 2325 Nimm? 4) Partial pressure of HjS__: 16 bars ©) Acceptance criteria : test sample failure at or after 720 hours. SDSS The Sulphide Stress Corrosion Cracking tests on super duplex stainless steel shall be carried out by using the following solutions and test conditions: i) a) Test solution NACE TMO177 +b) Test temperature 24°C Format No, €.00-0001-F1 Rev. 0 ‘Copyright ETL — A rights reservedSHERI bm ENGINEERS, SPECIFICATION FOR ‘STANDARD SPECIFICATION No. Fee SAGARA DUPLEX STAINLESS STEEL AND 6-79-0015 Rev.0 ‘seGircnoos osananieman; SUPER DUPLEX STAINLESS STEEL 73 Tat 14 74.1 742 15 151 752 Page 10 0f 12 ©) Stress value 2425 Nim? 4) Acceptance criteria = test sample failure at or after 720 hours. ii) a) Test solution NACE TM0177 b) Test temperature 290°C ¢) Stress value £390 N/mm? 4) Partial pressure of HS 16 bars ©) Acceptance criteria : test sample failure at or after 720 hours. Chloride Stress Cracking (CSC) Test DSS and SDSS a) The CSC tests shall be conducted on a representative specimens of DSS and SDSS, in accordance with the testing procedure mentioned in ASTM G-36, in aerated, boiling 40% calcium chloride (CaCI,) solution at 100? C with the pH of the solution maintained around 6.5. b) Acceptance criteria: stress to cause rupture in 500 hours shall exceed 0.85 times the ultimate tensile strength values of the duplex stainless steel and the super duplex stainless steel individually. Pitting Corrosion Test Dss a) The pitting corrosion test shall be conducted on the representative DSS specimen, in accordance with ASTM G-48 method A, using 6% ferric chloride (FeCh.6 H,0) solution by weight at 30°C, as well as at 50°C, for duration of 24 hours. b) Acceptance criteria: no pitting shall occur on the surface of the test sample at 30°C. For the testing at 50°C, the weight loss shall be reported to company for review. spss a) The pitting corrosion test shall be conducted on the representative SDSS specimen, in accordance with ASTM G-48 method A, using 6% ferric chloride (FeCl.6 H,0) solution by weight at 40°C, as well as at 50°C, for duration of 24 hours. b) Acceptance criteria: no pitting shall occur on the surface of the test sample at 40°C. For the testing at 50°C, the weight loss shall be reported to company for review. Crevice Corrosion Test DSS a) The crevice corrosion test shall be performed on the representative DSS specimen, in accordance with ASTM G-48 method B, using 6% ferric chloride (FeCl.6 HO) solution by weight, at 25°C for duration of 24 hours. b) Acceptance criteria: no crevice shall form on the surface of the test sample at 25% spss Format No, 6-00-000%-F1 Rev. 0 ‘CopyIgREETL — All Fights reservedSREZICT Sy ENGINEERS SPECIFICATION FOR ‘STANDARD SPECIFICATION No. seateee ORK UMITED 81 82 83 84 DUPLEX STAINLESS STEEL AND 6-79-0015 Rev. 0 “msercnses derdiseimeni SUPER DUPLEX STAINLESS STEEL agente a) The crevice corrosion test shall be performed on the representative SDSS specimen, in accordance with ASTM G-48 method B, using 6% ferric chloride (FeCl,.6 1,0) solution by weight, at 30°C for duration of 24 hours. b) Acceptance criteria: no crevice shall form on the surface of the test sample at 30°C. REQUIREMENTS FOR PRODUCTION TESTING Test Samples ‘Separate test blanks shall be required for each process of manufacture of the finished products. Each test sample shall receive the same working / heat treatment as the finished products it represents. If the test specimen cannot be taken from a finished product, then a representative test specimen shall be taken from the same heat, heat treated in the same batch, and be subjected to the same extent of working as the most worked section of the finished product. In case the finished product is of welded type, then the test piece shall be so chosen as to include the parent metal, the weld metal and the heat affected zone. Testing Frequency ‘The product analysis and the mechanical properties evaluation shall be conducted strictly as, per requirements of the relevant material product specifications. Micro-structural examination, ferrite measurement and hardness testing on the finished product, shall be carried out for one sample per heat per method of manufacturer. The test results shall be submitted to the Company as a part of the product documentation. Mandatory Production Tests (First Heat) On placement of order, a vendor who has met the pre-qualification criteria, shall carry out the following production tests, to meet the acceptance criteria mentioned in the respective clauses. All the following tests shall be witnessed and certified by a reputed the third party Inspection Agency duly approved by the Company, on the first heat: = Chemical composition analysis as per Clause No.5.1 - _ Pitting Resistance Equivalent Number as per Clause No.5.2 - Microstructure examination and ferrite measurement as per Clause No.5.3, - Mechanical properties evaluation as per Clause No.S.4 p Visual examination on casting as per Clause No. 6.5.1 : Radiography examination for casting as per Clause No.6.5.2 - Wet fluorescent penetrant examination for casting as per Clause No.6.5.3. Routine Tests The routine testing of product of each heat shall be carried out on a regular basis, in house. The chemical composition, the pitting resistance equivalent number, the mechanical properties, the micro-structural examination and for casting, the visual examination, the radiography and the wet fluorescent penetrant examinations shall conform to the requirements, specified in the respective Clauses of this specification. Format No, 6:00-0001-F1 Rev. 0 ‘Copyright EIL — Alrights reservedSERGI ly ENGINEERS SPECIFICATION FOR ‘STANDARD SPECIFICATION No. Pee SNA tiaeD ‘cence uwianavwan; SUPER DUPLEX STAINLESS STEEL 9.0 10.0 DUPLEX STAINLESS STEEL AND 6-79-0015 Rev. 0 Page 120f 12 QUALITY SURVEILLANCE AND INSPECTION ‘The supplier shall perform all the tests and inspection procedures mentioned above to ensure that the materials conform to the requirements of this specification. Company, or the representative duly approved by the Company, shall have unhindered access to the material ‘being manufactured for inspection and/or witnessing the selection of test samples, the preparation of test specimens, and the performance of tests. The company or its representative shall have the right to indicate the pieces from which the specimens are to be drawn for various tests. In case of any reasonable doubts regarding the quality of the product, Company shall have the option to ask for the re-qualification of the mill at the vendor’ s/contractor's cost. Inspection by the Company or its authorized representative shall not relieve the supplier of his responsibility for ensuring the compliance of the materials supplied to this specification, DOCUMENTS TO BE SUBMITTED The vendors/suppliers shall submit the following records of the tests and inspection conducted on the materials, as per the applicable Clauses mentioned in this specification, to the company in quadruplicate: - Chemical composition analysis report - Heat treatment records and charts A Micro-structure examination and ferrite measurement reports - Mechanical properties evaluation reports = Corrosion testing results (Pre-qualification records) - Visual examination report for castings - Radiography examination report for castings - _ Penetrant test report for castings. Format No, 6:00-0001-F1 Rev. 0 ‘Copyright EL — Alights reserved