Professional Documents
Culture Documents
for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: E1444/E1444M − 21
1. Scope* 1.6 This standard does not purport to address all of the
1.1 This practice establishes minimum requirements for safety concerns, if any, associated with its use. It is the
magnetic particle testing used for the detection of surface or responsibility of the user of this standard to establish appro-
slightly subsurface discontinuities in ferromagnetic material. priate safety, health, and environmental practices and deter-
This practice is intended for aerospace applications using the mine the applicability of regulatory limitations prior to use.
wet fluorescent method. Refer to Practice E3024/E3024M for 1.7 This international standard was developed in accor-
industrial applications. Guide E709 can be used in conjunction dance with internationally recognized principles on standard-
with this practice as a tutorial. ization established in the Decision on Principles for the
NOTE 1—This practice replaces MIL-STD-1949. Development of International Standards, Guides and Recom-
mendations issued by the World Trade Organization Technical
1.2 The magnetic particle testing method is used to detect Barriers to Trade (TBT) Committee.
cracks, laps, seams, inclusions, and other discontinuities on or
near the surface of ferromagnetic materials. Magnetic particle 2. Referenced Documents
testing may be applied to raw material, billets, finished and
semi-finished materials, welds, and in-service parts. Magnetic 2.1 The following documents form a part of this practice to
particle testing is not applicable to non-ferromagnetic metals the extent specified herein.
and alloys such as austenitic stainless steels. See Appendix X1 2.2 ASTM Standards:2
for additional information. E543 Specification for Agencies Performing Nondestructive
1.3 Portable battery powered electromagnetic yokes are Testing
outside the scope of this practice. E709 Guide for Magnetic Particle Testing
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1.4 All areas of this practice may be open to agreement E1316 Terminology for Nondestructive Examinations
between the cognizant engineering organization and the E2297 Guide for Use of UV-A and Visible Light Sources and
supplier, or specific direction from the cognizant engineering Meters used in the Liquid Penetrant and Magnetic Particle
organization. Methods
E3022 Practice for Measurement of Emission Characteris-
1.5 This standard is a combined standard, an ASTM stan- tics and Requirements for LED UV-A Lamps Used in
dard in which rationalized SI units and inch-pound units are
Fluorescent Penetrant and Magnetic Particle Testing
included in the same standard, with each system of units to be
E3024/E3024M Practice for Magnetic Particle Testing for
regarded separately as standard.
General Industry
1.5.1 Units—The values stated in either SI units or inch-
pound units are to be regarded separately as standard. The 2.3 ASNT Documents:3
values stated in each system are not necessarily exact equiva- SNT-TC-1A Personnel Qualification and Certification in
lents; therefore, to ensure conformance with the standard, each Nondestructive Testing
system shall be used independently of the other, and values ANSI/ASNT CP-189 Standard for Qualification and Certifi-
from the two systems shall not be combined. cation of NDT Personnel
1 2
This practice is under the jurisdiction of ASTM Committee E07 on Nonde- For referenced ASTM standards, visit the ASTM website, www.astm.org, or
structive Testing and is the direct responsibility of Subcommittee E07.03 on Liquid contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Penetrant and Magnetic Particle Methods. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved Sept. 1, 2021. Published October 2021. Originally the ASTM website.
3
approved in 1991. Last previous edition approved in 2020 as E1444/E1444M – 20. Available from American Society for Nondestructive Testing (ASNT), P.O. Box
DOI: 10.1520/E1444_E1444M-21. 28518, 1711 Arlingate Ln., Columbus, OH 43228-0518, http://www.asnt.org.
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the part or group of parts under examination. The procedure
shall be in accordance with the requirements of this practice.
4
Copies of standards, specifications, drawings, and publications required by The process, when conducted in accordance with the written
manufacturers in connection with specification acquisition should be obtained from procedure, shall be capable of detecting discontinuities speci-
the contracting activity or as directed by the contracting officer.
5
Available from SAE International (SAE), 400 Commonwealth Dr., Warrendale,
fied in the acceptance criteria. The written procedure may be
PA 15096-0001, http://www.sae.org. general if it clearly applies to all of the specified parts being
6
Available from Standardization Documents Order Desk, DODSSP, Bldg. 4, examined and meets the requirements of this practice. All
Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http:// written procedures, including technique sheets for specific
dodssp.daps.dla.mil.
7
Available from U.S. Government Printing Office Superintendent of Documents, parts, shall be approved by an individual qualified and certified
732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401, http:// at Level 3 (III) for magnetic particle testing in accordance with
www.access.gpo.gov.
8
the requirements of 5.1. Procedures shall be submitted to the
Available from American National Standards Institute (ANSI), 25 W. 43rd St.,
cognizant engineering organization for review, or approval, or
4th Floor, New York, NY 10036, http://www.ansi.org.
9
Available from International Organization for Standardization (ISO), ISO both, when requested.
Central Secretariat, Chemin de Blandonnet 8, CP 401, 1214 Vernier, Geneva,
Switzerland, https://www.iso.org.
10
Available from Aerospace Industries Association of America, Inc. (AIA), 1000
11
Wilson Blvd., Suite 1700, Arlington, VA 22209-3928, http://www.aia-aerospace.org. Available from ASD-STAN, asd-stan.org.
be used between shots; of 0.0008 in. [0.02 mm] or less shall be examined either before
5.3.1.12 The current level, or the number of ampere turns, to or after electroplating, or grinding, or both.
be used and the duration of its application; 5.4.3.3 Electroplated surfaces with a final plating thickness
5.3.1.13 Type of magnetic particle material to be used, the of between 0.0008 in. [0.02 mm] and 0.0050 in. [0.13 mm]
particle concentration limits, and the method and equipment to shall be examined both before and after electroplating, or
be used for its application. If a suspension dwell time is grinding, or both, of electroplated surfaces.
required, the length of suspension drain time prior to exami- (1) Electroplated surfaces with a final plating thickness of
nation shall be defined; 0.0050 in. [0.13 mm] or greater shall be examined before
5.3.1.14 Type of records and method of marking parts after electroplating, or grinding, or both, of electroplated surfaces.
examination; (2) Magnetic particle examination after electroplating is
5.3.1.15 Acceptance requirements to be used for evaluating not required for steels with a tensile strength less than or equal
indications, arc burns, and disposition of parts after evaluation; to 160 ksi.
0.4 mL in a 100 mL bath sample for fluorescent particles shall for magnetic particle testing, they shall meet the requirements
not be used. of 7.4.4.
5.6 Safety—The safe handling of magnetic particles and oil 6.2.3 Magnetizing Current Application—Alternating current
vehicles, water baths, and water conditioner concentrates is is to be only used for the detection of discontinuities open to
governed by the suppliers’ Material Safety Data Sheets the surface. Full-wave direct current has the deepest possible
(MSDS). Material Safety Data Sheets, conforming to 29 CFR penetration and must be used for examination of sub-surface
1910.1200, or equivalent, must be provided by the supplier to discontinuities when using the wet magnetic particle method.
any user and shall be prepared in accordance with FED-STD- Half-wave direct current can also be used for examination of
313. sub-surface discontinuities, and due to the pulsating nature of
5.6.1 Flammability—Flash point of oil vehicles shall be in the waveform, it has the advantage of increased particle
accordance with AMS 2641, Type I carriers. The suppliers’ mobility.
MSDS shall certify the flash point. 6.2.4 Magnetic Field Directions—Discontinuities are diffi-
5.6.2 Personnel Hazards—Precautions against inhalation, cult to detect by the magnetic particle method when they make
skin contact, and eye exposure are detailed in the suppliers’ an angle less than 45° to the direction of magnetization. To
MSDS. These precautions shall be observed. ensure the detection of discontinuities in any direction, each
part must be magnetized in a minimum of two directions at
5.6.3 Electrical Hazards—Magnetizing equipment shall be approximately right angles to each other. Depending on part
maintained properly to prevent personnel hazards from elec- geometry, this may consist of circular magnetization in two or
trical short circuits. Care must be taken to reduce arcing and more directions, multiple circular and longitudinal
the possible ignition of oil baths. magnetization, or of longitudinal magnetization in two or more
5.6.4 UV-A Lamps—Replace cracked or broken ultraviolet directions.
filters immediately. Broken filters can allow harmful ultraviolet
energy to be emitted and must be replaced immediately. NOTE 2—For further guidance, see Guide E709.
Spectacles designed to absorb ultraviolet energy are suggested 6.2.5 Multidirectional Magnetization—Multidirectional
for close, high-intensity UV-A examination. LED UV-A lamps magnetization may be used to fulfill the requirement for
used for evaluation purposes shall comply with Practice magnetization in two or more directions if it is demonstrated
E3022. See 7.3.2. that it is effective in all areas, which require examination as
NOTE 1—Only a changing magnetic field will generate a resulting eddy current in the ring-shaped part, such as when the magnetic field in the
magnetizing coil suddenly collapses, or when using a moving waveform such as AC; no eddy current is produced in the part by a non-moving waveform.
The resultant toroidal shaped magnetic field may be used to detect circumferential discontinuities in the part.
FIG. 2 Example of Induced Current Magnetization
the required concentration shall be applied by gently spraying of parts, which because of geometric constraints, cannot be
or flowing the suspension over the area to be examined. examined with the continuous method. The residual method
6.4.1.1 Proper sequencing and timing of part magnetization shall be used only when specifically approved by the cognizant
and application of particle suspension are required to obtain the engineering organization or when it has been documented that
proper formation and retention of indications. This requires it can detect discontinuities or artificial discontinuities in parts
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that the stream of suspension be diverted from the part under examination. The test parts shall have the same material
simultaneously with, or slightly before, energizing the mag- and processing steps, and similar geometry, to the actual parts
netic circuit. being examined.
6.4.1.2 The magnetizing current shall be applied for a
duration of at least 0.5 second for each application, with a 6.5 Evaluation—Following magnetization, particle applica-
minimum of two shots being used. The second shot shall tion and before demagnetizing, the parts shall be examined for
follow the first while the particles are still mobile on the indications. All indications will be identified as relevant or
surface of the part. nonrelevant. Relevant indications will be compared to the
6.4.1.3 Under special circumstances, such as the use of proper accept/reject criteria and the parts accepted or rejected
automated equipment or for critical parts, the 0.5–second accordingly.
duration and the two-shot requirement may be waived, pro- 6.5.1 Eye Glasses—Personnel shall not wear eye glasses
vided it is demonstrated that the procedure can detect known that are photochromic (transition lenses) or that have perma-
discontinuities in reference parts. nently darkened lenses. This is not intended to prohibit the use
6.4.1.4 Care shall be exercised to prevent any damage to the of eyeglasses with lenses treated to absorb ultraviolet light.
part due to overheating or other causes. Weakly held indica- 6.5.2 Dark Adaptation—Personnel must wait at least 1 min
tions on highly finished parts are readily washed away, and after entering a darkened area for their eyes to adjust to the
care must be exercised to prevent high-velocity flow over low-level lighting before performing fluorescent magnetic
critical surfaces. Surfaces to be examined shall not be handled particle testing.
or contacted until the examination is complete. 6.5.3 Acceptance Requirements—The acceptance require-
6.4.1.5 Particle application by continuous immersion shall ments applicable to the part or group of parts shall be
be used only when specifically approved by the cognizant incorporated as part of the written procedure either specifically
engineering organization or when it has been documented that or by reference to other applicable documents containing the
it can detect discontinuities or artificial discontinuities in parts necessary information. When parts are zoned, the acceptance
under examination. criteria for each zone shall be specified.
6.4.2 Residual Magnetization Method—In the residual mag-
netization method, the magnetic particles are applied to the part 6.6 Recording of Indications—When required by the written
under examination after the magnetizing force has been dis- procedure, the location of all rejectable indications shall be
continued. The residual method is not as sensitive as the marked on the part, and permanent records of the location,
continuous method. It can be useful on materials with high direction, and frequency of indications may be made by one or
retentivity. It is also useful for the examination of parts or areas more of the following methods:
(Mandatory Information)
A1.1 Application of Shims—The Reference Standard A1.9 Determining Field Strength and Direction—Use of the
Notched Shims of AS 5371, as shown in Annex A2, require circle or cross configuration shims will indicate fields in any
specific handling, attachment, and care for accurate indication direction.
of magnetic field strength and direction. To select amperage A1.9.1 In developing a magnetic particle procedure, first
settings for multi-directional magnetization, the use of determine the locations the shims should be placed to ensure
AS 5371 shims or parts described in 6.3.1.1 is mandatory. adequate coverage to monitor the field strength and direction,
A1.2 Shims 0.002 in. [0.05 mm] thick shall be used on and then attach the shims.
curved or complex surfaces. A1.9.2 Using the continuous method, begin by starting with
the amperage selection at a minimum level and increasing the
A1.3 Shims are manufactured of low carbon steel and must amperage slowly until the shim indications are readily ob-
be protected from corrosion when not in use. They may be served. When magnetized, one leg of the X will be indicated
submerged in a solvent such as MEK or naphtha for storage. perpendicular to the field direction and the circle shim will
Before attaching the shim to the part, both the shim and part show quadrants that are approximately perpendicular to the
shall be clean and dry. Prior to use, the protective coating shall direction of the applied field.
be removed from both faces of the QQI. Care shall be utilized
A1.9.3 In multi-directional magnetization, longitudinal and
when removing the protective coating. Excessive pressure to
circular fields shall be determined separately as follows:
remove the coating may imprint the face of the QQI, presenting
A1.9.3.1 Field strength for the first direction shall be deter-
nonrelevant indications during technique development.
mined by slowly increasing the amperage until a satisfactory
NOTE A1.1—Polar solvents such as water, will break down the
cynoacrolate based (super glue) adhesives commonly used to apply these indication is observed on each shim.
shims. A1.9.3.2 Record the amperage setting and indication re-
sults.
A1.4 The shim shall be placed in intimate contact with the A1.9.3.3 Demagnetize the part and carefully clean the shims
part with the flaw side next to the material to be examined. prior to determining the amperage in the next direction.
A1.9.3.4 Field strength for the second direction shall be
A1.5 The shim shall be securely fastened to the part by
determined by incrementally increasing the amperage until a
using an adhesive or tape (such as Scotch Brand 191, 471, or
satisfactory indication is observed on each shim.
600 series12) that prevents the magnetic particle suspension
A1.9.3.5 Record the amperage setting and indication re-
from entering between the shim and part. Whatever means is
sults.
used to secure the shim to the part shall not interfere with the
visibility of the indications. A1.9.4 Place the selector switch in the multi-directional
mode and magnetize the part at the previously recorded
A1.6 Tape may be used to secure the shim and shall have settings. If the entire circle on the shims is observed, the fields
the following properties: (1) Good adhesion to steel, (2) are in balance. If any portion of the circle has a weak
impervious to the suspension used, and (3) the tape shall be indication, adjust the amperage accordingly and repeat the field
non-fluorescent under UV-A. verification process until the magnetic fields are balanced.
A1.7 If the tape becomes loose and allows the suspension to A1.9.5 Use care when applying the suspension to the shims.
seep under the shim, the tape and shim shall be carefully Proper shim indications may not form unless the suspension is
removed from the test piece. The shim and the part shall be applied in a gentle manner.
cleaned and dried, and then the shim shall be reattached to the A1.10 The shims are made of a low retentivity and high
test piece. permeability material that cannot be used for indicating re-
A1.8 Re-use of the shims is acceptable, provided they are sidual fields when developing magnetic particle testing proce-
not distorted when removed and intimate contact is achieved dures.
when replaced. A1.11 In unidirectional applications, the actual field
strength measurements can be obtained by placing a Hall Effect
probe adjacent to the shim or at a nearby location where probe
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12
The 191, 471, and 600 series are trademarks of Scotch Brand. placement can easily be replicated.
A2. REFERENCE STANDARD NOTCHED SHIMS FOR MAGNETIC PARTICLE TESTING IN ACCORDANCE WITH AS 5371
A2.1 The following standard flawed shims are typically square of Fig. A2.2. The shims of Fig. A2.2 are cut, by the user,
used to establish proper field direction and ensure adequate into four 0.395 in. [10 mm] square shims for use in restricted
field strength during technique development in magnetic par- areas.
ticle testing. The shims shown in Fig. A2.1 may be used to
ensure the establishment of fields in the unidirectional magne- A2.1.3 Shims shall be low carbon steel, AMS 5062, or
tization method and to ensure the establishment and field equivalent.
balance in the multidirectional magnetization method. A2.1.4 Shims shall be used as specified in AS 5371. Shims
A2.1.1 Except for shims illustrated in Fig. A2.2, the shims are placed in the area(s) of interest with the notches toward the
are available in two thicknesses, 0.002 in. [0.05 mm] and 0.004 surface of the part being examined. Use enough shims by
in. [0.10 mm]. Thinner shims are used when the thicker shims placing the shims in multiple areas to ensure proper field
cannot conform to the part surface in the area of interest. directions and strengths are obtained.
A2.1.2 The shims are available in two sizes, 0.75 in. [19
mm] square for Figs. A2.1 and A2.3 and 0.79 in. [20 mm]
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A3. AS 5282 TOOL STEEL RING SPECIMEN FOR SYSTEM PERFORMANCE TEST
A3.1 A ring specimen similar to Fig. A3.1 may be used to perform the system performance verification of 7.1.
Hole 1 2 3 4 5 6
Diameter 0.07 0.07 0.07 0.07 0.07 0.07
Note 1 [1.78 [1.78 [1.78 [1.78 [1.78 [1.78
mm] mm] mm] mm] mm] mm]
“D” 0.07 0.14 0.21 0.28 0.35 0.42
Note 2 [1.78 [3.56 [5.33 [7.11 [8.89 [10.67
mm] mm] mm] mm] mm] mm]
Hole 7 8 9 10 11 12
Diameter 0.07 0.07 0.07 0.07 0.07 0.07
Note 1 [1.78 [1.78 [1.78 [1.78 [1.78 [1.78
mm] mm] mm] mm] mm] mm]
“D” 0.49 0.56 0.63 0.70 0.77 0.84
Note 2 [12.45 [14.22 [16.00 [17.78 [19.56 [21.34
mm] mm] mm] mm] mm] mm]
NOTE 1—All hole diameters are 60.005 in. [60.13 mm]. Rings with holes 10 through 12 are optional.
NOTE 2—Tolerance on the D distance is 60.005 in. [60.13 mm].
NOTE 3—All other dimensions are 60.03 in. [60.76 mm].
FIG. A3.1 Tool Steel Ring Specimen
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A4.1 Hall-Effect Meter Usage Overview—Care must be the length of the part as the tangential circular field is
exercised when measuring the tangential applied field strengths consistent across the length. The transverse probe should be
as specified in A4.2. The active area of the Hall-Effect probe positioned upright such that the circular field is normal to the
shall be no larger than 0.2 in. [5.1 mm] by 0.2 in. [5.1 mm] and major dimension of the Hall-Effect sensor and within 5° of
should have a maximum center location 5 mm from the part perpendicularity to the part. More than one measurement
surface. The plane of the probe must be perpendicular to the should be taken to ensure consistent readings. On parts with
surface of the part at the location of measurement to within 5 more than one diameter/thickness, multiple measurements
degrees. This is difficult to accomplish by hand orientation; should be taken to ensure a minimum measurement of 30 gauss
therefore, the probe should be held in a jig or fixture of some
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(Nonmandatory Information)
X1.1 Some materials are far more suitable for magnetic as the PH steels, to use a high enough amperage to provide
particle testing than others. In some cases, liquid penetrant proper field strength.
testing may be a more reliable testing method.
X1.4 Steels with very high permeability are easily magne-
X1.2 Some of the precipitation hardening (PH) steels are tized but should not be examined with the residual method.
austenitic in the annealed or low heat treat ranges. Austenitic X1.5 Fig. X1.1 is a tabulation of stainless and corrosion
materials cannot be examined by the magnetic particle testing resistant steels and their suitability for examination with the
method. magnetic particle testing method.
X1.3 Care must be taken with low permeability steels, such X1.6 Aluminum and aluminum based alloys, copper and
X2. FORMULAS FOR DETERMINING PROPER CURRENT VALUES FOR CIRCULAR MAGNETISM
SUMMARY OF CHANGES
Committee E07 has identified the location of selected changes to this standard since the last issue
(E1444/E1444M – 20) that may impact the use of this standard. (Sept. 1, 2021)
(1) Updates were made in 6.2.7.1, 7.1, and 7.4.7. (2) Fig. 1 was updated.
Committee E07 has identified the location of selected changes to this standard since the last issue
(E1444/E1444M – 16ε1) that may impact the use of this standard. (Dec. 1, 2020)
(1) Updated the title to include “for Aerospace.” (8) In Table 1, changed the title and changed UV-A integrity
(2) Added 1.3, 5.3.1.17, 6.2.7.1, 6.3.3, 6.3.4, 6.3.5, A4.2, A4.3, check to daily.
and A4.4 (9) Deleted previous 5.5.1, 6.2.2, 6.3.1.3, 6.4.1, 6.4.1.1,
(3) Replaced “Cognizant Engineering Organization” with 6.4.1.2, 6.4.4, 6.4.5, 6.4.6, 6.6.2, 6.6.3, and 7.4.8
“cognizant engineering organization” throughout the document (10) Reworded 7.2.1.2, 7.3.3, 7.4.5, 7.4.7, and A1.7.
for consistency. (11) Changed title of 7.4.6 to read “Hall-Effect Gauss/Tesla
(4) Replaced “standard practice” with “practice” throughout. Meters and Field Indicators.”
(5) Added and removed referenced documents from Section 2 (12) Deleted previous Annex A3, Appendix X2, and Appendix
based on updates made in the text. X5 entirely.
(6) Updated 5.2 to say “The agency performing this practice (13) Appendix X2: deleted the previous text and subsections
may be evaluated in accordance with Specification E543” to and replaced with “For guidance using formulas for determin-
conform with Practice E1417.
ing current values, see Guide E709. See 6.2.7.1.”
(7) Made edits to 5.1, 5.3, 5.3.1.1, 5.3.1.6, 5.3.1.10, 5.3.1.13,
(14) Appendix X3: deleted the previous text and subsections
5.3.1.15, 5.4.3.2, 5.5.4, 5.6.4, 6.1.1, 6.1.3, 6.2.4, 6.2.6, 6.2.10,
and replaced with “For guidance using formulas for determin-
6.3.1.2, 6.4.1, 6.4.1.4, 6.5, 6.5.1, 6.5.3, 6.9, 7.1, 7.2.1.1, 7.2.2,
7.2.3, 7.3.1.1, 7.3.2, 7.4.1, 7.4.2, 7.4.4, 7.4.5.2, A1.3, A1.6, and ing current values, see Guide E709.”
A4.1.
This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years and
if not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standards
and should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of the
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make your views known to the ASTM Committee on Standards, at the address shown below.
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