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Very High Cycle Fatigue Properties of Bearing Steel Under Axial Loading Condition
Very High Cycle Fatigue Properties of Bearing Steel Under Axial Loading Condition
Very high cycle fatigue properties of bearing steel under axial loading condition
K. Shiozawa a,*, T. Hasegawa b, Y. Kashiwagi a, L. Lu c
a
Graduate School of Science and Engineering, University of Toyama, Toyama 930-8555, Japan
b
Okuma Co., Oguchi-cho, Niwa-gun, Aichi 480-0193, Japan
c
State Key Laboratory of Traction Power, Southwest Jiaotong University, Chengdu 610031, China
a r t i c l e i n f o a b s t r a c t
Article history: It has been observed to appear a step-wise or duplex S–N curve under the test of rotary bending fatigue
Received 29 October 2007 using high strength steel. This behavior was caused by the transition of fracture mode from surface-
Received in revised form 31 October 2008 induced fracture to subsurface inclusion-induced fracture. The aim of this study is to clarify the S–N char-
Accepted 2 November 2008
acteristic under an axial loading fatigue in the very high cycle fatigue regime. In order to investigate the
Available online 12 November 2008
mean-stress effects, fatigue tests were carried out in air at room temperature under three applied stress
ratios of 1, 0 and 0.5 using a hour-glass shaped specimen of high carbon–chromium bearing steel, JIS
Keywords:
SUJ2. From the results, three types of fracture mode were observed on the fracture surface, such as sur-
Very high cycle fatigue
Subsurface crack
face-induced fracture, subsurface inclusion-induced fracture without granular bright facet (GBF) area and
Fracture mode that with GBF area around an inclusion. Fatigue lifetime for transition in the fracture mode depended on
Axial loading the applied stress ratio. Shape of the S–N curve was a smooth and continuous under three testing condi-
Stress ratio tions in spite of the occurrence on the three types of fracture. Detail discussion for fatigue fracture behav-
Residual stress ior was made through the observation of fracture surface and from point in view of the fracture
mechanics. In addition, an effect of residual stress in the specimen surface layer on the transition of frac-
ture mode was discussed and compared with the experimental results.
Ó 2008 Elsevier Ltd. All rights reserved.
0142-1123/$ - see front matter Ó 2008 Elsevier Ltd. All rights reserved.
doi:10.1016/j.ijfatigue.2008.11.001
K. Shiozawa et al. / International Journal of Fatigue 31 (2009) 880–888 881
fatigue fracture mode were discussed based on the fracture 2.2. Fatigue testing method
mechanics.
Fatigue tests were performed using a newly developed multi-
2. Experimental procedures type fatigue testing machine in axial loading [20,21]. This testing
machine can simultaneously perform fatigue tests for four differ-
2.1. Testing material and specimen ent specimens at the frequency of 80 Hz, using a special hydraulic
system with rotary valve to distribute high-pressure oil into the
The material used in this study was a high carbon–chromium respective actuators. The loading capacity for each specimen is
bearing steel, JIS SUJ2. The chemical composition (mass percent- ±10 kN and the applied load can be given independently to the
age) of this steel is shown in Table 1. Hourglass-shaped specimens individual specimen. In this study, force-controlled fatigue tests
with a minimum diameter of 3 mm and round notch radius under axially-reversed loading of sinusoidal wave type were car-
of 15 mm with a flange, as shown in Fig. 1, were machined. The ried out at three applied stress ratios, R, of 1, 0 and 0.5 in an open
specimens were heated for 2400 s in a vacuum at 1008 K and environment at room temperature.
oil-cooled, tempered for 1200 s in a vacuum at 453 K and then
air-cooled. The round notch surface was polished by an emery
3. Experimental results
paper having a mesh of #2000 and buff polishing. The elastic stress
concentration factor of this specimen is 1.029.
3.1. S–N Curve
Fig. 2 shows the microstructure of the heat-treated material ob-
served by an SEM, which was prepared with micro-etching by Nital
The S–N curve obtained from the axial loading fatigue tests un-
(a) and electro-etching (b). It can be seen from the photographs
der different applied stress ratio is shown in Fig. 3a. As observation
that many spherical carbide particles are distributed in the matrix
result of the fracture surface by SEM, fatigue fracture mode was
which is a tempered martensite structure composing of an average
classified into two types, such as surface fracture mode resulting
prior-austenitic grain size of 5.7 lm. Size of the carbide particle
from the surface crack initiation and growth (referred to as S-
distributed in the range of 0.2–2.0 lm and the average was
mode) and subsurface non-metallic inclusion-induced fracture
0.8 lm. The tensile strength and the Vickers hardness of the
mode with a fish-eye. Also, the subsurface fracture mode was di-
heat-treated material are 2316 MPa and HV749, respectively.
vided two types of fracture mode; One was formed the GBF area
in the vicinity of a non-metallic inclusion at the fracture origin in-
Table 1
side the fish-eye zone for the specimens ruptured at the high cycles
Chemical composition of tested materials (mass%).
of a lifetime of more than 106 cycles (IG-mode), plotted by solid
C Si Mn P S Cr Cu Ni Mo [O] mark in Fig. 3a. The other was not formed the GBF area at short
1.01 0.23 0.36 0.012 0.007 1.45 0.06 0.04 0.02 8 ppm lifetime bellow 106 cycles plotted by half-solid marks (I-mode).
Fig. 3b shows the comparison between the S–N curve obtained
from the axial loading fatigue test under the stress ratio of 1 and
that from the cantilever-type rotary bending fatigue test using
hourglass-shaped specimens with a minimum diameter of 3 mm
[2]. It can be seen from the figure that the S–N curve depends on
the applied loading mode. Even though the results obtained from
the rotary bending fatigue test shows the step-wise S–N curve or
a duplex S–N curve, shape of S–N curve obtained from the axial
loading fatigue tests is a smooth and continuous in spite of the
occurrence of the three types of fracture mode. The fatigue life in
surface-induced fracture mode can be found to have no difference
between loading modes. However, the fatigue life in subsurface-in-
duced fracture mode obtained from the axial loading fatigue test is
shorter than that from the rotary bending fatigue test. It is sug-
Fig. 1. Shape and dimension of specimen used. gested that a reason of the difference in lifetime between them is
R=0.5
1500
I IG mode
a,
106
Nf, cycles
Stress amplitude
103
0 -1.5 -1 -0.5 0 0.5 1
103 104 105 106 107 108 109 Stress ratio R
Number of cycles to failure Nf, cycles
Fig. 4. Experimental results for the effect of applied stress ratio on the transition
life of fracture mode.
b 2000
SUJ2
Cantilever-type Fig. 5 shows typical examples of SEM observation for the IG-mode
rotary bending fatigue
MPa
Surface fracture on the fracture surface of the specimen obtained under the
Subsurface testing condition of three applied stress ratios. Distinctive feature
Subsurface GBF
a,
SUJ2
GBF a 50
m
Surface Subsurface
inclusion inclusion
40 R=-1
20
10
Rotary bending fatigue (Subsurface inclusion)
20µm 0
10 3 10 4 10 5 10 6 10 7 10 8 10 9
(a) R= 1, a=850MPa, Nf=1.32 108 cycles Number of cycles to failure Nf, cycles
SUJ2
b 1500
Rotary bending fatigue
m
R=-1
R=0
R=0.5
500
240 m
20µ
0 20 m
10 3 10 4 10 5 10 6 10 7 10 8 10 9
(b) R=0, a=525MPa, Nf=1.03 108 cycles Number of cycles to failure Nf, cycles
Fig. 6. Experimental relationship between size of inclusion (a) and depth of
inclusion from specimen surface (b), and number of cycles to failure.
SUJ2
a 100
Axial loading fatigue SEM SEM
80
R=-1 Rotary bending fatigue
R=0
R=0.5
m
60
area GBF,
40
20µm 20µm
20
EPMA EPMA
0
106 107 108 109
Number of cycles to failure Nf, cycles
b 8
SUJ2
Axial loading fatigue
C C
m
R=0.5
4
area GBF/
0
Ti Ti
106 107
10 8
10 9
(a) R= 0, a=550MPa (b) R= 0.5, a=380MPa
Number of cycles to failure Nf, cycles
Nf =5.11 107 cycles Nf =7.12 107 cycles
Fig. 7. Experimental relationship between size of GBF area (a) and the ratio of GBF
area size to inclusion size to inclusion size (b), and number of cycles to failure. Fig. 8. EPMA analyzed results around an inclusion on fracture surface.
DK inc;s and DK inc;i decrease for increasing Nf, and depends on the ap- 4.2. Effect of applied stress ratio on the roughness of GBF area
plied stress ratio. To evaluate the effect of the stress ratio on crack
initiation at an inclusion, modified stress intensity factor range, Fig. 10 shows a typical example for the birds-eye pattern of the
DK inc and DK GBF , was calculated using a stress amplitude of tensile GBF area observed by scanning probe microscope (SPM). Some
range, Dr (for R = 1; rmax ¼ ra , for R = 0 and 0.5; rmax rmin ¼ granular convex particles can be seen on the fracture surface of
2ra ), instead of the value of Dr. The results are shown in Fig. 9b. the each specimen ruptured under the stress ratio of 1, 0 and
It can be see from this figure that DK inc;s and DK inc;i do not depend 0.5. It has been reported by the previous paper [15,16] that the for-
on the applied stress ratio and decrease continuously with increas- mation of convex and rough surface on the GBF area related to the
pffiffiffiffiffi
ing Nf. The values of DK inc;i are below 4 MPa m for the specimens carbide particles in the microstructure of the specimen.
ruptured in the range of long fatigue life over 106 cycles and by the Surface roughness measurements of the fracture surface were
IG-mode fracture. On the other hand, the DK inc;i are above taken by three-dimensional SEM analysis. The roughness of the
pffiffiffiffiffi
4 MPa m for the specimen ruptured by the I-mode. This value GBF area was 2–2.5 times greater than that outside the GBF area
may be the limit, DK th , to bring the I-mode cracking. Below the in fish-eye zone. Fig. 11a shows values of the surface roughness,
DK th , the GBF area is formed in the vicinity of non-metallic inclu- Rmax and Ra, on the GBF area for every specimen obtained from
sion during fatigue process and the fracture is occurred by the each applied stress ratio. An average distance of roughness on sur-
pffiffiffiffiffi
IG-mode. The values of DK GBF are in the range of 4–6 MPa m, not face roughness curve, S [see Ref. [15] for detail definition], is also
depended on applied stress ratio, and above the value of DK th . shown in this figure. The Rmax and Ra decreased and the S increased
Therefore, it is expected that the internal fracture mode initiated with increasing applied stress ratio. Fig. 11b shows the relation-
from an inclusion in very high cycle fatigue regime is controlled ship between the values of Rmax, Ra and S, and stress intensity fac-
by the formation of the GBF in the vicinity of the inclusion. This tor range for subsurface inclusion, DK inc;i . These values depend
mechanism is the same as the result of a rotary bending fatigue only on DK inc;i and do not depend on the applied stress ratio.
and does not depend on the applied stress ratio. From above dis- Roughness of the GBF area increases for increasing DK inc;i . It was
cussions, the mechanical factor to control the internal crack initia- pointed out in previous papers by authors [15,16] that the rough-
tion, propagation and fracture will be tensile stress amplitude, that ness on GBF area causes from decohesion of spherical carbide in
is, equivalent to the effective stress intensity factor range. the matrix. Therefore, it is suggested that the decohesion of spher-
K. Shiozawa et al. / International Journal of Fatigue 31 (2009) 880–888 885
a 20
SUJ2 a 2
SUJ2
Kinc,s, Kinc,i, KGBF, MPa m
1
10
Subsurface inclusion
Stress intensity factor range
µm µm µm µm µm µm
(a) R= -1, a =850 MPa (b) R= 0, a =525 MPa (c) R= 0.5, a =390 MPa
8 8 8
Nf = 1.32 10 cycles Nf = 1.03 10 cycles Nf = 1.13 10 cycles
Fig. 10. SPM observation of the GBF area on fracture surface of specimen obtained from fatigue tests under stress ratio of 1, 0 and 0.5.
886 K. Shiozawa et al. / International Journal of Fatigue 31 (2009) 880–888
10 µm
5 µm
FRASTA method for specimens tested under R = 0 and 0.5, and sively initiated by decohesion of spherical carbide from the matrix
ruptured by the IG-mode. In these plots of the figure, the dark areas in the vicinity of a non-metallic inclusion. The decohesion occurs
indicate the unfractured areas and white areas are the fractured with dislocations pilled-up to around spherical carbide particles
ones. The number in each plot of the figure gives the topographic in the zone of stress concentration due to an inclusion. These
displacement relative to the reference state, which corresponds microcracks grow and coalesce with each other during fatigue cy-
to fatigue process. At the stage of a small displacement, small cles. At this time, the microcracks propagate along a boundary be-
spotty white area can be seen in the vicinity of an inclusion. These tween spherical carbide and the matrix, and therefore the
areas are microcracks initiated during fatigue cycling. As the sepa- roughness of the size of the carbide grade is generated on the frac-
ration between the conjugate maps increased, the multiple micro- ture surface. After formation of an appropriate size for the GBF area
cracks increased in size and number, and then coalesce with each to enable propagation as an ordinary crack, the crack propagates
other into the GBF area. The phenomena were also observed on without depending on the microstructure of the materials and
the specimen tested under R = 1 and same as the results of rotary forms a fish-eye.
bending fatigue reported previous paper [15,16].
Fig. 13 shows cross-sectional plots (XSPs) of crack growth ob- 4.4. Effect of residual stress on transition of fracture mode
tained by displacing topographic contours along the white line in
Fig. 12. The darkly shaded areas are areas where the two topo- Three types of fracture mode, such as S-, I- and IG-mode, were
graphic surfaces overlap, and indicate that plastic deformation observed on the S–N curve. In this section, transition of the fracture
formed at a crack front during crack propagation. In these views, mode was discussed from a viewpoint of the fracture mechanics.
the white area is the fractured area. From this figure, microcracks Initial stress intensity factor range of surface inclusion, DK inc;s ,
initiate at a short distance from an inclusion and different points. and subsurface inclusion, DK inc;i , are calculated as Eqs. (1) and
Based on the experimental results and computational simula- (2), respectively, based on the discussion mentioned above section.
tion of the fracture process by the FRASTA method, a mechanism The value of DK inc;s is usually larger than that of DK inc;i , if both size
for formation of the GBF area is explained by the ‘‘dispersive dec- of inclusion are same. Fig. 14 shows a schematic relation between
ohesion of spherical carbide” model not only under the condition the DK inc;s indicated as dot-dashed line and DK inc;i as dashed line,
of the stress ratio R = 1 but also R = 0 and 0.5. Outline of the and applied stress amplitude. Above the threshold stress intensity
mechanism is as follows; initially, multiple microcracks are disper- factor range of surface crack growth, DKth, crack will initiate at a
5µm 5µm
0.581µm 1.219µm
(a) R=0, IG-mode fracture (b) R=0.5, IG-mode fracture
Fig. 13. Analytical results for a series of cross-sectional plots (XSPs) generated by the FRASTA method.
K. Shiozawa et al. / International Journal of Fatigue 31 (2009) 880–888 887
MPa
K*inc,s r=-373MPa
m
B 1200 *
K th= K'th C
a,
**
S I
Kinc, MPa
Stress amplitude
KTinc,s
IG-mode I-mode S-mode 800 * S IG
r =0
600 S IG *
Internal crack S : Surface fracture mode Experimental results
*
K inc,i I : Subsurface fracture mode without GBF 400 S I *
IG : Subsurface fracture mode with GBF I IG
200 * T. Sakai(Ritsumeikan Univ.)
S IG ** M. Nakajima(TCT)
Stress amplitude a, MPa 0
-1.5 -1 -0.5 0 0.5 1
Fig. 14. Schematic diagram to explain the transition of fracture mode.
Stress ratio R
Fig. 15. Diagram for stress amplitude on the transition of fracture mode relating to
surface inclusion and propagate to final fracture. Below the DKth, applied stress ratio, the comparison of calculated and experimental results.
subsurface crack can start to grow after forming a GBF area in
the vicinity of subsurface inclusion. Therefore, surface fracture Stress amplitude occurred the transition of fracture mode, such
mode, S-mode, occurs in the region of high stress amplitude level as from S-mode to I-mode and from I-mode to IG-mode, was calcu-
and changes into an internal fracture mode with GBF area, IG- lated for each stress ratio using the compressive residual stress on
mode, at the low stress amplitude level (point C in Fig. 14). In this the specimen surface of 373 MPa measured by X-ray diffraction
case, only two fracture modes appear on a S–N curve and an inter- method, an average inclusion size of 17.0 lm and DK th ¼ DK 0th ¼
nal fracture mode without GBF area, I-mode, does not occur at any pffiffiffiffiffi
4 MPa m. The classical sin2 w method was applied to the determi-
stress amplitude level against the experimental facts. nation of residual stress, using the diffraction pattern of the (2 1 1)
In order to explain an occurrence of three fracture modes on a crystal plane by Cr Ka. Solid lines in Fig. 15 are the calculated re-
S–N curve, an effect of residual stress on surface layer of specimen sults of stress amplitude for transition of fracture mode relating
will be considered for the above discussion. It is assumed that the to the stress ratio. From this figure, stress amplitude of the transi-
residual stress, rr, acts on the fatigue behavior as a mean stress ef- tion from S-mode to I-mode and I-mode to IG-mode are clearly
fect, and stress range in tension side affects the crack initiation and separated each other, and decreased with increasing the stress ra-
propagation, according to the experimental facts mentioned above tio below about zero. On the other hand, at the range of higher
section. Based on the assumption, initial stress intensity factor stress ratio above zero, fracture mode changes from the S-mode
range of the surface inclusion, DK inc;s , is rewritten to DK Tinc;s using to the IG-mode and I-mode fracture does not occur, because of
DrT defined by Eq. (3) instead of Dr*. rmin P jrr j and no effect of residual stress on the fracture. In case
that there is not the residual stresses on the specimen surface, the
rmax rmin for rmin P jrr j
DrT ¼ ð3Þ transition of fracture mode from S-mode to IG-mode occurs at low
rmax þ rr for rmin < jrr j stress amplitude level, indicated as fine dot-dashed line in Fig. 15.
In addition, it is considered that the residual stress in surface The experimental results obtained from this study and reported by
layer affects only surface inclusion and does not affect on subsur- other researchers [18] are shown in this figure. It can be seen from
face inclusion. Therefore, initial stress intensity factor range of this figure that agreement of predicted results and the experimen-
subsurface inclusion, DK inc;i , does not change without regard to tal results is fairly good.
existence of residual stress on surface layer.
As schematically shown in Fig. 14, the value of DK Tinc;s indicated 5. Conclusions
as solid line becomes to small by the effect of compressive residual
stress comparing with the DK inc;s , relating with a constant applied 1. Three types of fracture modes, such as surface-induced fracture
stress amplitude. The value of DK Tinc;s against a stress amplitude mode, subsurface inclusion-induced fracture mode without for-
intersects the DK inc;i at a point A in Fig. 14, and the fracture mode mation of GBF area and subsurface inclusion-induced fracture
changes from S-mode to I-mode at the stress amplitude level. Be- mode with formation of GBF area, were observed on fracture
cause DK inc;i at the point A is above the DK 0th , a subsurface crack surfaces obtained under an axial loading fatigue. The fatigue
can initiate and propagate without forming the GBF area around lifetime at which different fracture modes appear depends on
the inclusion. Where, DK 0th is a threshold stress intensity factor the applied stress ratio.
range for subsurface crack growth without formation of a GBF area 2. S–N curve under the axial loading fatigue tests showed a
and same as the DK th from the experimental fact. The line of DK inc;i smooth and continuous shape under three testing conditions
is correspondent to DK 0th ð DK th Þ at a point B with decreasing in spite of the fact the fracture mode changes with depending
stress amplitude. Below this corresponding stress amplitude, a on applied stress. This was different from the clear duplex S–
subsurface crack cannot directly initiate and propagate from an N curve obtained from a rotary bending fatigue test.
inclusion, and the formation of GBF area around an inclusion is re- 3. Fatigue fracture in very high cycle fatigue regime was con-
quired for initiation and propagation of subsurface crack, that is, trolled by formation of the GBF in the vicinity of non-metallic
IG-mode fracture appears. Therefore, due to the existence of the inclusion without regard to applied stress ratio. The GBF area
compressive residual stress on the specimen surface layer, three couldn’t be observed clearly at higher applied stress ratio by
types of fracture modes will be occurred depending on the applied SEM, but large roughness and rich carbon distribution was
stress amplitude. detected in the vicinity of subsurface inclusion.
888 K. Shiozawa et al. / International Journal of Fatigue 31 (2009) 880–888
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