DAFTAR METODE STANDAR BATU BARA

Test BS ISO ASTM Repeatability Reproducibility

Sampling manual BS ISO 18283:2006 D2234/
18283:2006 D2234M-16
D2234/
D2234M-17
D6883-04(2012)
D6609-08(2015)
D6609-17
Preparation 13909-4 : 2016 D2013/
D2013M-12
Manual sampling D 6883-17
of stockpiles
Mechanical 13909-1,2,3, : 2016 D7430-16be1
sampling D7430-18a
Bias Testing a 13909-8:2016 D7430-16be1
mechanical D7430-18a
sampler
Size analysis BS ISO 1953 : 2015 1953 : 2015 D 4749-87: ASTM : Not Applicable ASTM : Not Applicable
(2012)
ISO : Not Applicable ISO : Not Applicable
Total Moisture 1016.1-1973 589 : 2008 D3302/ ASTM : ASTM :
D3302M-17 Bituminous 1.6-7.9% : Bituminous 1.6-7.9% :
0.14 0.62
Subbituminous & lignite Subbituminous & lignite
12.4-31.2% : 0.42 12.4-31.2% : 0.70
ISO ISO
Residual Moisture : 0.3% Residual Moisture : NA
Total Moisture : 0.5% Total Moisture :1.5%
Hal 1 dari 14 hal
Total Moisture D2961/D2961M- ASTM : 0.30% ASTM : 0.50%
(single stage) 17
< 15%
Practices for BS ISO 17246:2010 D3172-13 - -
proximate 17246:2010
analysis
Moisture in BS ISO 11722:2013 D3173-17 ASTM : ASTM :
analysis sample 11722:2013 D3173/D3173M- 1.0-21.9% : 0.09+0.01XA 1.0-21.9% : 0.23+0.02XA
17a
ISO : ISO : Not Applicable
<5 % : 0.10
≥5% : 0.15
Ash contents BS ISO 1171:2010 1171:2010 D3174-12 ASTM : (250µm) ASTM : (250µm)
2.68-17.86% (db) : 0.22 2.68-17.86% (db) : 0.32
ASTM : (2.36 mm) ASTM : (2.36 mm)
Bituminous 5.0-15.0% : Bituminous 5.0-15.0% :
0.30 % 0.49 %
Subbituminous & lignite Subbituminous & lignite
4.5-30.0% : 0.33 % 4.5-30.0% : 0.47 %
ISO : ISO :
< 10% : 0.2% < 10% : 0.3%
> 10 % : 2.0 % of the > 10 % : 3.0 % of the
mean result mean result
Volatile Matter BS ISO 562 :2010 562 :2010 D3175-17 ASTM : Using Pt Crucible ASTM : Using Pt Crucible
Anthracite : 0.3 Anthracite : 0.6
Semiantrachite, Semiantrachite,
bituminous : 0.5 bituminous : 1.0
Subbituminous : 0.7 Subbituminous : 1.4
Lignite : 1.0 Lignite : 2.0

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 ISO: ISO:
< 10% : 0.3% < 10% : 0.5%
> 10 % : 3 % XA > 10 % : 0.5 % atau 4.0 %
XA (nilai mana yang lebih
besar)
Volatile Matter 5071-1: 2013 ISO: ISO:
(2 furnace 1,0 % absolute 3,0 % absolute
method)

Total Sulfur BS ISO 334:2013 334:2013 Withdrawn ISO : ISO :

- Eschka Method

Total Sulfur BS ISO 19579 : 2006 (IR (D4239-17) ASTM (DB): ASTM (DB):
- High Temp 19579:2006 spectrometry) D4239-18e1 Metode A (Cal CRM) Metode A (Cal CRM)
1350°C 1350°C
0.28-5.61%: 0.02+0.03XA 0.28-5.61%: 0.02+0.09XA
Metode A (Cal BBOT) Metode A (Cal BBOT)
1350°C 1350°C
0.37-5.48%: 0.37-5.48%:
0.053+0.019XA 0.125+0.053XA

Metode B 1150°C Metode B 1150°C

0.38-5.6% : 0.04+0.05XB 0.38-5.6% : 0.07+0.07XB

ISO: ISO:
0.02+.03XA 0.02+0.09XA

Gross Calorific BS ISO 1928:2009 1928:2009 D5865-13 ASTM (DB): ASTM (DB):
value (250µm/Microprocessor (250µm/Microprocessor
Controlled Calorimeters) Controlled Calorimeters)
Bituminous 11300-14700 Bituminous 11300-14700
Btu/lb : 64 Btu/lb / 149 Btu/lb : 110 Btu/lb / 256
J/g J/g
Hal 3 dari 14 hal
 6282-8172 kcal/kg : 35.6 6282-8172 kcal/kg : 61.2
kcal/kg kcal/kg
Subbituminous-lignite Subbituminous-lignite
9400-11900 Btu/lb : 83 9400-11900 Btu/lb : 164
Btu/lb / 193 J/g Btu/lb / 381 J/g
5226-6616 kcal/kg: 46 .1 5226-6616 kcal/kg: 91.2
kcal/kg kcal/kg

(2.36mm/Microprocessor (2.36mm/Microprocessor
Controlled Calorimeters) Controlled Calorimeters)
: have not been : have not been
developed developed
ISO: ISO:
120J/g / 28.66 Kcal/Kg 300J/g / 71.65 Kcal/Kg
HGI BS ISO 5074:2015 5074:2015 D409/ D409M- ASTM /ISO: ASTM/ISO:
16 3 index of HGI 7 index of HGI

Hal 4 dari 14 hal

Ash fusibility BS ISO 540:2008 540 :2008 D1857/D1857M- ASTM ASTM
17 For reducing For reducing
D1857/D1857M- atmosphere: atmosphere:
17a Initial deformation Initial deformation
temperature, IT 30°C temperature, IT 70°C
Softening temperature, Softening temperature,
ST 30°C ST 55°C
Hemispherical Hemispherical
temperature, HT 30°C temperature, HT 55°C
Fluid temperature, FT Fluid temperature, FT
30°C 85°C
For oxidizing For oxidizing
atmosphere: atmosphere:
Initial deformation Initial deformation
temperature, IT 30°C temperature, IT 55°C
Softening temperature, Softening temperature,
ST 30°C ST 55°C
Hemispherical Hemispherical
temperature, HT 30°C temperature, HT 55°C
Fluid temperature, FT Fluid temperature, FT
30°C 55°C

ISO: (all atmospheres) °C ISO: (all atmospheres) °C

Deformation Temp.: 30 Deformation Temp.: 80
Sphere Temp. : 30 Sphere Temp. : 60
Hemisphere Temp. : 30 Hemisphere Temp. : 60
Flow Temperature : 30 Flow Temperature : 80

Ultimate analysis BS ISO 17247:2013 D3176-15 -

17247:2013
Carbon/Hydrogen
- High Temp BS 609:1996 ISO: (at same moisture ISO: (at same moisture
1016.106.1.1:1996 content) content)

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 ISO 609:1996 C : 0.25% C : 0.5%
H : 0.12% H : 0.25%
- Liebig Method 1016.106.1.2:1996 625:1996
Carbon, hydrogen BS ISO 29541:2010 D5373- 16 ASTM method A(DB): ASTM method A(DB):
Nitrogen 29541:2010 Carbon 54.9 to 84.7 : Carbon 54.9 to 84.7 :
instrumental 0.45 1.00
Hydrogen 3.25 to 5.10 : Hydrogen 3.25 to 5.10 :
0.10 0.25
Nitrogen 0.57 to 1.80 : Nitrogen 0.57 to 1.80 :
0.05 0.15

ASTM method B(DB): ASTM method B(DB):

Carbon 57.7 to 84.0 : Carbon 57.7 to 84.0 :
0.55 2.31

ISO: ISO:
Carbon (db) : 0.3% Carbon (db) : 1.0%
Hydrogen (db) : 0.06% Hydrogen (db) : 0.25%
Nitrogen (db) : 0.03% Nitrogen (db) : 0.15%

Oxygen content BS ISO 17247:2013 D3176-15 ASTM : Not Applicable ASTM : Not Applicable
17247:2013
ISO : Not Applicable ISO : Not Applicable
Analysis of ash D3682-13 SiO2 33.14 – 57.73% SiO2 33.14 – 57.73%
(AAS method) 0.33 + 0.04 x¯ –1.21 + 0.14 x¯
Al2O3 11.32 – 31.83% Al2O3 11.32 – 31.83%
0.80 –0.24 + 0.09 x¯
Fe2O3 2.93 – 41.11% Fe2O3 2.93 – 41.11%
0.01+ 0.06 x¯ 0.36 + 0.06 x¯
MgO 0.45 – 7.12 % MgO 0.45 – 7.12 %
0.04 + 0.03 x¯ 0.04 + 0.09 x¯
CaO 1.46 – 22.19% CaO 1.46 – 22.19%
0.21 + 0.04 x¯ 0.15 + 0.11 x¯
TiO2 0.57 – 1.44% 0.13 TiO2 0.57 – 1.44% 0.19
Hal 6 dari 14 hal
 K2O 0.45 – 2.99 % K2O 0.45 – 2.99 %
0.03 + 0.03 x¯ 0.05 + 0.05 x¯
Na2O 0.14 – 7.15% Na2O 0.14 – 7.15%
0.06 + 0.03 x 0.04 + 0.18 x
Analysis of ash BS ISO 13605 ISO/TS 13605:2012 ISO : Not Applicable ISO : Not Applicable
(WDXRF method)
Chlorine method
- Oxygen bomb 352:1981(withdrawn) D4208-13 ASTM (DB) : ASTM (DB):
method ISO/TS 18806:2014 220 to 2100 µg/g 220 to 2100 µg/g
48.4 + 0.13XA 200 + 0.23XA

- Combustion/ BS 587:1997 D2361-95 ISO : ISO :

Eschka method 1016.106.6.1:1997 (Withdrawn 0.03 % 0.06 %
ISO 587:1997 2008)
Chlorine
Oxid.Hydrolysis
Microcoulometry
Phosphorus BS ISO 622:2016 622:2016 D2795 ISO : ISO :
(Withdrawn < 0.02 % : 0.002 < 0.02 % : 0.005
2001) ≥ 0.02 % : 10 % the mean ≥ 0.02 % : 25 % the mean
of results of results
Arsenic, selenium BS ISO 601:1981(withdrawn) D4606- 15 ASTM (DB): ASTM (DB):
11723:2016 11723:2016 Arsenic 0.7 – 12.2 µg/g Arsenic 0.7 – 12.2 µg/g
0.3 + 0.7 XA 0.6 + 0.1 XA
Selenium 0.6 – 5.0 Selenium 0.6 – 5.0
0.31 + 0.2XA 0.1 + 0.3XA
Mercury, acid BS ISO 15237:2016 D6414-14 ASTM : (db) ASTM : (db)
extr/wet 15237:2016 Hg 0.032–0.585 ppm Hg 0.032–0.585 ppm
oxidation/AA 0.012+ 0.11xA 0.003 + 0.25xA

ISO: (same moisture ISO: (same moisture

content) content)
0.14ω + 8 ng/g 0.25ω + 20 ng/g

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Fluorine BS ISO 1174:2016 11724:2016 ISO: ISO:
≤ 200 : 10 µg/g ≤ 200 : 20 µg/g
> 200 : 20 µg/g > 200 : 15%XA
- Oxygen D3761-10 ASTM : ASTM :
bomb/Ion < 15 μg/g (ppm) < 15 μg/g (ppm)
selective
electrode
- Prohydrolytic D5987-96 (2015) ASTM: ASTM:
20-120 μg/g 20-120 μg/g
<10 μg/g <20 μg/g
Trace element BS ISO 23380:2013 D3683-11 ASTM (in coal adb): ASTM (in coal adb):
AAS 23380:2013 (Cadmium, Lead –GF Be 0.2 ppm (0.5 to Be 0.5 ppm (0.5 to 5
AAS) 5ppm) ppm)
Cr 3 ppm (5 to 50 ppm) Cr 5 ppm (5 to 50 ppm)
Cu 2 ppm (5 to 50 ppm) Cu 3 ppm (5 to 50 ppm)
Mn 3 ppm (10 to 300 Mn 6 ppm (<50 ppm)
ppm) Mn 20 ppm (50 to 500
Ni 1 ppm (<5 pm) ppm)
Ni 3 ppm (5 to 30 ppm) Ni 3 ppm ( <5 ppm)
Pb 2 ppm (10 to 100 Ni 9 ppm (9 to 30 ppm)
ppm) Pb 9 ppm (10 to 100
V 5 ppm (10 to 100 ppm) ppm)
Zn 3 ppm (<50 ppm) V 9 ppm (10 to 50 ppm)
Zn 8 ppm (50 to 100 V 20 ppm (50 to 100
ppm) ppm)
Zn 4 ppm (<50 ppm)
Zn 17 ppm (50 to 100
ppm)
Trace element 23380:2013 D6357-11 ASTM ASTM
ICP AES (As, Be, Bi, Cd, Cr, Sb 0.17–5.71 Sb 0.17–5.71
Co., Cu, Pb, Mn, Mo, -0.06 +0.29 x¯A 0.08 +0.44 x¯A
Ni, Sb, Tl, V, Zn, Th, U As 0.56–138.79 0 As 0.56–138.79 0
– ICP-MS) 0.42 + 0.13 x¯A 1.73 + 0.23 x¯A
(Be, Cr, Co, Cu, Mn, Be 0.42–13.11 0 Be 0.42–13.11 0
Mo, Ni, V, Zn – ICP- 0.08 + 0.08 x¯A 0.14 + 0.30 x¯A
Hal 8 dari 14 hal
 AES) Cd 0.02–0.84 Cd 0.02–0.84
0.03 + 0.16 x¯A 0.04 + 0.43 x¯A
Co 0.76–47.18 Co 0.76–47.18
0.28 + 0.11 x¯A 1.26 + 0.18 x¯A
Cr 2.37–221 Cr 2.37–221
1.03 + 0.09 x¯A 1.50 + 0.18 x¯A
Cu 3.43–107.06 Cu 3.43–107.06
0.62 + 0.10 x¯A −0.31 + 0.28 x¯A
Mn 11.69–419.61 Mn 11.69–419.61
0.98 + 0.10 x¯A 8.12 + 0.15 x¯A
Mo 0.40–20.52 Mo 0.40–20.52
0.23 + 0.11 x¯A 0.80 + 0.18 x¯A
Ni 2.00–113.32 Ni 2.00–113.32
0.35 + 0.13 x¯A 1.26 + 0.19 x¯A
Pb 1.57–66.99 Pb 1.57–66.99
0.26 + 0.16 x¯A 0.13 + 0.30 x¯A
Zn 3.76–202.31 Zn 3.76–202.31
0.70 + 0.10 x¯A 2.98 + 0.18 x¯A
V 4.50–293.17 V 4.50–293.17
0.75 + 0.13 x¯A 2.02 + 0.21 x¯A
Form of sulphur BS 157:1996 D2492-02 (2012) ASTM (in db) : ASTM (in db) :
1016.106.5:1996 Sulfate Sulfur Sulfate Sulfur
ISO 157:1996 0.02 % by weight 0.04 % by weight
Pyritic Sulfur 0.1 to 12 Pyritic Sulfur 0.1 to 12
Referee Method Referee Method
0.08+0.09X¯ A 0.15+0.27X¯ A
Alternatif method Alternatif method
0.06+0.11X¯ A 0.07+0.19X¯ A

Hal 9 dari 14 hal

 ISO (same moisture ISO (same moisture
content) : content) :
Pyritic Sulfur Pyritic Sulfur
<0.5 : 0.05% <0.5 : 0.10%
0.5 to 1.5 : 0.07% 0.5 to 1.5 : 0.15%
>1.5 : 5% >1.5 : 10%
Sulfat Sulfur: Sulfat Sulfur:
<0.02 % <0.03 %

Sulphur in ash
- High temp D5016-16 ASTM : ASTM :
Range (0.7-3.8 %) Range (0.7-3.8 %)
0.06X ¯ + 0.06 0.2X ¯ + 0.2
- Eschka Method
Moisture holding BS 1016.21:1981 1018:1975 D1412-17a ASTM : ASTM :
capacity (ISO) ISO 1018:1975 0.035 X EQM +0.216 0.057 x EQM +0.398
Equlibrium
Moisture (ASTM)
ISO : ISO :
0.5% 1.2%
Carbonate D6316-09be1 ASTM : ASTM :
carbon content D6316-17 Total carbon Total carbon
(CO2) in solid 0.34–15.12 % 0.34–15.12 %
residues from 0.14 + 0.04X ¯ B 0.07 + 0.12X ¯ B
coal and coke Combustible carbon Combustible carbon
0.14–14.00 % 0.14–14.00 %
0.25 + 0.06X ¯ B 0.82 + 0.14X ¯ B
Carbonate carbon Carbonate carbon
0.01–2.75 % 0.01–2.75 %
0.01 + 0.08X ¯ B 0.04 + 0.13X ¯ B

Hal 10 dari 14 hal

Carbonate BS 925:1997 ISO (same moisture ISO (same moisture
carbon content 1016.106.7:1997 content) : content) :
(CO2) in coal ISO 925:1997 Carbonate Carbon Carbonate Carbon
<0.4%: 0.02% <0.4%: 0.04%
≥ 0.4% : 5% ≥ 0.4% : 10%
Carbon dioxide Carbon dioxide
<1 % : 0.05% <1 % : 0.1%
≥ 1 % : 5% ≥ 1 % : 10%
Crucible Swelling BS ISO 501:2012 501:2012 D720/ D720M- ASTM : ASTM :
Number (ISO) 15e1 1 2
Free-Swelling
Index (ASTM) ISO : ISO :
(3 determination) :½ (5 determination) : 1
(5 determination) : 1
Swelling 1016.107.3:2012 8264:1989 D5515-17 ASTM : ASTM :
properties D5515/D5515M- T1 360-440°C 6 T1 360-440°C 20
dilatometer 17a T2 415-475°C 6 T2 415-475°C 20
T3 465–495°C 6 T3 465–495°C 20
%D2.50 <100 % 7 %D2.50 <100 % 17
%D2.50 100–200 % 16 %D2.50 100–200 % 35
Abrasion index 1016.111:1998 12900:2015
Mineral matter BS ISO 602:2015 602:2015 ISO: ISO:
0.4% Not Applicable
Float and sink BS 7067:1990 7936:1992 D4371-06 (2012) ASTM : ASTM :
characteristic Specific Gravity Fraction Specific Gravity Fraction
Repeatability, g Reproducibility, g
under 1.40 273 under 1.40 490
1.40 to1.65 0.247(W)A + 1.40 to1.65 0.296(W)A +
59 17
over 1.65 0.168(W)A − over 1.65 0.181(W)A −
49 16
Methods for BS 7530-1:1992 8858.1 : 1990 D5114-90 (2010)
froth flotation 8858.2 : 2004
testing of hard

Hal 11 dari 14 hal

coal. Laboratory
procedure
Methods for BS 7530-2:1992 8858.3:2004
froth flotation
testing of hard
coal. Evaluation
of flotation
characteristics
Magnetite for use 8833:1989
in coal
preparation --
Test methods
Methods for BS 1016-
analysis and 107.2:1991
testing of coal
and coke. Caking
and swelling
properties of
coal. Assessment
of caking power
by Gray-King coke
test
Methods for BS 1016-
analysis and 108.5:1992
testing of coal
and coke. Tests
special to coke.
Determination of
density and
porosity
Standard Test D2639/
Method for D2639M- 16
Plastic Properties
of Coal by the
Constant-Torque
Hal 12 dari 14 hal
Gieseler
Plastometer
Collecting D4596-09 (2015)
channel sample
Solid mineral 14180:1998
fuels -- Guidance
on the sampling
of coal seams
Collection of coal D5192-09 (2015)
sample from core
Tumbler test for D441-07 (2012)
coal
Cubic foot weight D291-07 (2012) ASTM: ASTM : Not Applicable
(two results) : <1.0 lb/ft3
(1.60 kg/m3), if differ,
two additional test shall
be made
(four results) : <1.3 lb/ft3
(2.10 kg/m3)
Drop Shatter test D440-07 (2012)
Standard ISO 1213-1:1993 D121- 15
terminology / ISO 1213-2:2016
Vocabulary
Standard guide 17025:2005
for quality
management
General info & BS 1016-100:1994 1170: 2013 D3180-15
reporting
Expression and ISO 923:2000
presentation of
result of coal
cleaning test
Testing, sampling 3323 : 1992 1213.2:1992
analysis (terms)

Hal 13 dari 14 hal

Coal and coke - AS 1038.21.1.1- AS: AS:
Analysis and 2008 RD<1.6: 0.03 RD<1.6: 0.08
testing - Higher RD>1.6: 0.03 RD>1.6: 0.08
rank coal and
coke - Relative
density - Analysis
sample/density
bottle method
Coal and coke - AS 1038.10.3- AS: AS:
Analysis and 1998 Boron< 50 mg/kg: 5 Boron< 50 mg/kg: 10
testing Boron> 50 mg/kg: 10% of Boron> 50 mg/kg: 20% of
Determination of mean mean
trace element-
coal and coke –
Determination of
Boron content –
ICP-AES method
Standard D388-17
Classification of D388-18
Coals by Rank
Determination of D8010-16
Water Soluble
Alkali Content in
Coal
Standard D1193-06(2018)
Specification for
Reagent Water
Standard E11-17
Specification for
Woven Wire Test
Sieve Cloth and
Test Sieves
Standard E323-11(2016)
Specification for

Hal 14 dari 14 hal

Perforated-Plate
Sieves for Testing
Purposes
Standard E832-81(2013)
Specification for
Laboratory Filter
Papers

Disusun oleh : A. Ikhsan P. tgl : 07 Desember 2018

Diperiksa oleh : Dedi Gunawan tgl : 07 Desember 2018

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