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Journal of Magnetism and Magnetic Materials 421 (2017) 225–229

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Journal of Magnetism and Magnetic Materials


journal homepage: www.elsevier.com/locate/jmmm

Analysis of domain wall dynamics based on skewness of magnetic


Barkhausen noise for applied stress determination
Song Ding a,b, GuiYun Tian b,c,n, Gerd Dobmann b, Ping Wang b
a
College of Electrical Engineering and Control Science, Nanjing Tech University, Nanjing, Jiangsu 211816, China
b
School of Automation Engineering, Nanjing University of Aeronautics and Astronautics, Nanjing, Jiangsu 210016, China
c
School of Electrical and Electronic Engineering, Merz Court, University of Newcastle upon Tyne, Newcastle NE1 7RU, UK

art ic l e i nf o a b s t r a c t

Article history: Skewness of Magnetic Barkhausen Noise (MBN) signal is used as a new feature for applied stress de-
Received 16 December 2015 termination. After experimental studies, skewness presents its ability for measuring applied tensile stress
Received in revised form compared with conventional feature, meanwhile, a non-linear behavior of this new feature and an in-
29 July 2016
dependence of the excitation conditions under compressive stress are found and discussed. Effective
Accepted 8 August 2016
damping during domain wall motion influencing the asymmetric shape of the MBN statistical dis-
Available online 8 August 2016
tribution function is discussed under compressive and tensile stress variation. Domain wall (DW) energy
Keywords: and distance between pinning edges of the DW are considered altering the characteristic relaxation time,
Applied stress which is the reason for the non-linear phenomenon of skewness.
Magnetic Barkhausen Noise
& 2016 Elsevier B.V. All rights reserved.
Skewness
Domain wall motion

1. Introduction memory [7], logic devices [8,9] and DW dynamics, including ef-
fective mass and eddy current-damping effect [10–12]. For ex-
Magnetic Barkhausen Noise (MBN) has been proved as an ef- ample, behavior of DW dynamics are considered as responses to
fective technique to measure residual stress (RS) as well as applied its characteristic relaxation. Zapperi [12] et al. have studied ma-
stress (AS) on ferromagnetic materials. Micro-magnetic structure terial characteristic relaxation time and verified that it is a sig-
of material decides the shape and size of magnetic domains, and nature of negative effective mass of the DW in a ferromagnetic
then dominates the behavior of domain wall (DW) motion, i.e. its slice (thin sheet). Skewness of the shape of magnetic Barkhausen
dynamics, which influences Barkhausen noise significantly, thus jump distribution was proposed to track the characteristic of DW
MBN method attracts numerous researchers. In a dynamical dynamics behavior in an applied field. This method reveals a re-
changing (time-varying) magnetic field, DW movement is affected lationship between the electromagnetic signal on the macro-scale
by the structure of the domains itself and by lattice defects in and material relaxation time on the micro-scale for sheet speci-
material microstructure, such as inclusions, dislocations, grain men. It is well known that all magnetic moment are exchange-
boundaries, second phase precipitates and applied or residual coupled to their neighbors. Hence any change in the wall position
stress [1–5]. MBN signal are therefore widely utilized for the by motion will be dampened by the adjacent domain. Previous
characterization of material microstructure under applied field. study has shown that damping mechanisms in the adiabatic re-
Furthermore, in many published research works, the root mean gime was affected by applied stress [11]. Therefore, skewness of
square (RMS) value of MBN signals is considered as a function of the MBN signal distribution was proposed as a new feature for
the applied magnetic field, residual and applied stress, surface microstructure characterization and applied stress determination
hardness and hardening-depth, etc. [1–5]. However, this feature of carburized En36 steel, which had case-depth and double peak
depends on excitation parameters obviously, such as applied MBN shapes, and was demonstrated more sensitive than RMS and
magnetic field amplitude and frequency [3–6]. peak position [13].
Recent research on magnetic domains focus on nano-scale In the here presented paper, skewness is proposed as a sig-
mechanisms and their potential consequences on magnetic nature for applied stress detection on soft steel. Q235 steel spe-
cimens (Chemical composition see Table 1) were investigated
n under compressive and tensile applied-stress of variable ampli-
Corresponding author at: School of Electrical and Electronic Engineering, Merz
Court, University of Newcastle upon Tyne, Newcastle NE1 7RU, UK. tude to evaluate the effectiveness of this new feature for soft steel
E-mail address: tian280@hotmail.com (G. Tian). with single peak MBN shape. Subsequently, non-linear behavior

http://dx.doi.org/10.1016/j.jmmm.2016.08.030
0304-8853/& 2016 Elsevier B.V. All rights reserved.
226 S. Ding et al. / Journal of Magnetism and Magnetic Materials 421 (2017) 225–229

Table 1
Chemical composition (wt%) of the Q235 steel used in this study. 40

C Si Mn S P Cr Ni Cu
30
r0.22 r 0.3 0.30–0.70 r0.045 r 0.045 r0.30 r 0.30 r 0.30
20

and excitation independence are presented and discussed. Domain 10

Voltage (mV)
wall energy and pinning edges distance, influenced by applied
0
stress, affect the characteristic relaxation frequency, which is
considered the dominant variable to govern skewness of MBN -10
signal distribution.
-20

-30
L
2. Experimental setup
-40

In this experiment, Q235 steel is selected as a sample to eval- 650 700 750 800 850 900 950 1000
uate how applied stress affects MBN signal feature. This soft ma- time (ms)
terial can provide significant Barkhausen noise under low applied Fig. 2. Example of MBN signal. The red cure is excitation and the blue one is MBN
stress, which contributes to remarkable changes in the MBN signal signal. L describes the period of one MBN signal in time domain. The start point is
distribution. The chemical composition of the Q235 steel is illu- selected when MBN signal profile over a certain threshold, and the cutoff point is
selected when MBN signal profile less than the same threshold. (For interpretation
strated in Table 1. of the references to color in this figure legend, the reader is referred to the web
As shown in Fig. 1, a Q235 steel bar (660 mm  30 mm  5 mm, version of this article.)
L  W  D) is subjected to four-point bending. The vertical press
makes compressive stress on the top surface of the specimen and 3. Results and discussion
tensile stress on the opposite surface. On the basis of structural
mechanics the compressive stress can be expressed as σmax =
3Fd
, As mentioned previously, skewness of MBN profile shape is
S
influenced by damping mechanisms. To calculate the MBN signal
where s is the cross sectional area of the bar, and F is the applied
skewness, equation according to the method mentioned by Zap-
force. The applied stress was limited to be within the range 0–
peri et al. [12] was applied as follows:
150 MPa to avoid macro-plastic deformation (the yielding point of
1 L 3
Q235 is about 200 MPa and influenced by the specimen ∫0 dt v( t , L ) ( t − t¯ )
L
dimension). sk( L)= 3/2
1 L 2⎤
To obtain MBN signals, the Agilent 33,250 A provided low fre- [ L ∫ dt v( t , L ) ( t − t¯ ) ⎥⎦
0 (1)
quency excitation which is amplified by a bi-polar power amplifier,
Newtons 4th LPA05B. The output of the power amplifier is fed to L is the length of a time-window in which the distribution of
the coil wound the magnetic yoke (made of ferrite core) to drives events ν (here the BN distribution) in amplitude is larger than a
the applied field. The frequencies of the magnetic excitation are certain threshold which is normally given by the electronic noise
selected variable from 2 to 10 Hz, and the current was about 0.8 A in the receiver circuit.
in its peak maximum (corresponding to a maximum tangential L

magnetic field Hmax ¼7000 A/m). The MBN signal, as show in


t¯=1/L ∫0 dt v( t , L ) t

Fig. 2, was detected using a pick-up air-coil (with 1500 turns of is the so called first moment of the distribution function and de-
0.07 mm diameter wire) on. fines the mean value at which the distribution is maximal. sk
the surface of the bar sample. The MBN signals were amplified (L) characterizes how skew the distribution is, skew means – the
(gain has been fixed at 30 dB), band pass filtered (2–40 kHz), and distribution is not symmetric to the mean value. This window
sampled at a 200 kHz frequency by 14-bit data acquisition length L is clearly influenced by the excitation frequency. For ex-
(DAQ2010) analog-to-digital converter. Synchronously, the excita- ample, with 2 Hz excitation, L is about 200 ms, less than a quarter
tion voltage was acquired using the second channel [13]. of the driving period. However, L changes to 35 ms, near half of the
driving period, when the excitation frequency increases to 10 Hz.
With different compressive and tensile stress values, the
skewness and the RMS1 value of MBN signal are calculated and
compared for estimating the effect of domain wall dynamics and
excitation parameters. All these features are normalized by di-
viding the values with the one obtained from 0 MPa stress.

3.1. Effect of compressive stress on skewness

With different applied compressive stress, skewness of MBN


distributions and RMS are obtained by calculation and compared.
The normalized features with scatter-bars, representing the

Fig. 1. Schematic for compressive stress loading and MBN signal detection. F is T
applied at B and C to produce compressive applied stress on the top surface and RMS(x(t)) ¼ ∫ x 2( t )dt )/T , where T is an apropriate choosen integration
1

tensile applied stress on the bottom surface. interval. 0


S. Ding et al. / Journal of Magnetism and Magnetic Materials 421 (2017) 225–229 227

100 100
RMS data
Skewness data
95 95
RMS fitting curve
Normalized MBN Features (%)

Normalized MBN features (%)


Skewness fitting curve
90 90

85 85

80 80

75 75

RMS data
70 70 Skewness data
RMS fitting curve
Skewness fitting curve
65 65
0 50 100 150 0 50 100 150
Compressive Stress (MPa) Tensile Stress (MPa)

Fig. 3. Normalized skewness and Root Mean Square (RMS) of MBN signal dis- Fig. 4. Normalized RMS and Skewness depend on applied tensile stress.
tributions. Both these features are normalized by dividing the maximum respec-
tively. The uncertainty of the features is calculated from 20 periods MBN signal.

energy, which make the Barkhausen jump easy to be performed.


repeatability, are presented in Fig. 3. In fact, both of these features So the MBN profile peak becomes higher and left-shifted [1,2]. As
have been averaged taking into account the MBN information re- main result we see:
ceived in 20 individual excitation periods. Fig. 3 reveals three facts:
● The normalized skewness shows better sensitivity to applied
● Normalized skewness has better sensitivity than RMS when the tensile stress compared with the normalized RMS value.
compressive stress is below 75 MPa. ● The fitting curve of the RMS values remains linear from 0 to 150
● Normalized RMS decreases linearly with compressive stress, MPa, while the skewness curve keep this characteristic below
whereas skewness has an ambiguous behavior, which will be 120 MPa only. Distinct nonlinearity and scatter appears when
discussed in Section 3.4. the applied tensile stress above 120 MPa for skewness curve.
● The scatter in the RMS curve becomes larger above 90 MPa
According the basic understanding of stress interaction with applied stress.
DW [1,2], compressive stress aligns the magnetic domains per-
pendicular to stress direction and makes the magnetization pro- 3.3. Effect of domain wall energy and pinning edges distance on
cess difficult, when excitation is in stress direction. In our ex- skewness
periment we have observed too the well-known fact, that the peak
position in the time scale of the MBN distribution increased In Fig. 3, skewness presents its sensitivity and linearity to
monotonously with increasing compressive stress; the same is compressive stress below 75 MPa, and then rises reversely with
with the peak position in RMS. It is also in line with the standard
the applied compressive stress increasing up to 150 MPa. The in-
inertia theory describing the resistance of material mass when
crease of domain wall energy, which has been mentioned in Sec-
movement start or when movement temporarily is stopped and
tion 3.1, can be used to explain the decrease of skewness with low
has to start again; a slightly higher driving force has to be applied,
compressive stress. However, it cannot explain the reverse in-
to overcome the effect [12]. As a whole, applied compressive stress
crease of skewness when compressive stress is above 75 MPa in
does not only delay the peak position, but also decrease the peak
this experiment. The same phenomenon has been presented in
value of MBN signal, which both make the MBN profile tend to a
Beck's [11] study, where the effective damping reversed when the
negative skewness. Thus, it is easy to accept that skewness shows
applied stress was above 50 MPa.
better sensitivity than RMS on measuring applied compressive
To find an interpretation for these experimental results, we
stress.
consider a simple model that describes the Barkhausen effect in
3.2. Effect of tensile stress on skewness soft ferromagnetic materials on the basis of dynamics of a domain
wall according the differential Eq. (2) [14]
The MBN signal were measured also to understand the effect of d2x dx
applied tensile stress. The relationship between MBN signal fea- m +β + αx=2MsH0e jωt
dx2 dt (2)
tures and tensile stress is presented in Fig. 4. Skewness and RMS
again were normalized on the maximum value. Both features were where m is the effective mass of domain wall, β is a viscous
averaged after collecting individual BN distributions in 20 different damping parameter, α is spring constant, Ms is saturation mag-
exciting periods. The symbol positions in Fig. 4 indicate the aver- netization, H0 is amplitude of applied field, ω is angular frequency,
age value. and x is the domain wall displacement. Considering that domain
From Fig. 4, skewness rises with the increase of tensile stress. wall velocity (dx/dt) is proportional to the recorded v( t ), and the
RMS is calculated for comparison which shows the same tendency mass of domain wall m is considered as 0, Eq. (2) can be solved.
as skewness. Obviously, skewness curve is more sensitive – i.e. has The relaxation frequency ω0 is expressed as ω0=α /β . Taking into
a higher dynamic - to the applied tensile stress than RMS curve, account a simple model that domain wall is pinned along two
which has been also presented in previous research [13]. It is edges, the spring constant and domain wall energy are related by
known that applied tensile stress not only decreases exchange α = 18σw /d2. The relaxation frequency ω0 is written
228 S. Ding et al. / Journal of Magnetism and Magnetic Materials 421 (2017) 225–229

Moreover, Fig. 5 shows that skewness value of MBN shape is


nearly independent to excitation frequency and wave-shape. As a
3rd order statistical parameter, skewness reflects variation of do-
main wall relaxation frequency, which is mainly decided by the
material microstructure and modified by applied stress in this
experiment. According to Zapperi’ research [12] the relaxation
time of a DW is about dozens of nanosecond, we believe that is
why skewness is especially insensitive against excitation para-
meter influences at low frequency applied field.

4. Conclusion

In conclusion, this paper presents the result that skewness of


the MBN distribution is affected by applied compressive and ten-
sile stress on Q235 steel. Compared to RMS, the most popular
Fig. 5. Normalized skewness with different frequency and wave-shape excitation. feature to utilize MBN signal for stress measurement, skewness
The excitation frequency changes from 2 Hz (L ¼ 200 ms) to 10 Hz (L ¼ 35 ms), and shows better sensitivity when the applied stress from  75 MPa to
at each frequency, triangular and sinusoidal wave are used as excitations to pro- þ120 MPa. The applied compressive stress decrease the peak of
duce the applied magnetic field. The applied stress is unloaded and increase from
MBN signal, and delay the peak position of MBN profile synchro-
0 MPa to 150 MPa when the excitation wave or frequency is changed.
nously. On the contrary, the applied tensile stress shifts the peak
position to the opposite direction. By considering the definition of
skewness, this 3rd statistic feature includes more information of
ω0=18σw/[d2 × β ] (3)
the random process realization. Thus, better sensitivity of this
where σw is domain wall energy, and d is the distance between indicator is acceptable.
pinning edges [14,15]. Furthermore, this paper discusses the ambiguity phenomenon
According to current models of damping mechanisms, the main when compressive stress above 75 MPa amplitude is applied. The
damping sources are associated to an eddy current effect βE and same behavior were presented in Beck's research results. Further
spin relaxation βR [16,17]. Beck [11] has discussed that until a discussion based on domain wall energy and distance between
critical stress is attained, both the eddy current and spin relaxation pinning edges are carried out. These two factors are considered as
contribute to the stress dependence of the domain wall damping. the reason for the reverse increase of skewness curve when the
Above the critical stress, as the eddy current damping is stress applied compressive stress is higher than 75 MPa for this kind of
independent, the main modification of the damping mechanisms material.
is due to spin relaxation. The viscous damping is nearly propor- Finally, different frequency and waveform excitations are used
tional to applied stress. Our experimental results show that to estimate the effect of excitation parameters on skewness. Due to
skewness decreases linearly with increase in compressive stress skewness has been proved mainly associated with the character-
up to 75 MPa. It is mainly due to the increasing of viscous damping istic relaxation time, an inherent micro-magnetic property of
under compressive stress. When the compressive stress increases material, the applied fields with different frequencies and wave-
above 75 MPa, skewness increases, but is not proportional to the forms can hardly alter skewness curve. Thus, skewness shows an
applied stress. insensitivity against excitation variation, especially in the low
Compressive stress has been proved to impede the domain wall frequency range.
motion [5], in other words, it increases the pinning energy of DW.
Considering the increase of wall energy, the distance between
pinning edges and damping, they affect skewness of MBN shape. Acknowledgments
Experimental results indicate that the material has elastic de-
formation below 75 MPa. Low applied compressive stress cannot This work is supported by “Health Monitoring of Offshore Wind
change the distance between pinning edges much. However, this Farm (HEMOW)” (FP7-PEOPLE-2010-IRSES, Grant No. 269202)
distance can decrease with the increase in the density of disloca- project, National Natural Science Foundation of China (Grant No.
tions when the compressive stress is large enough [5]. In spite of E070104) and Jiangsu Graduate Student Innovation Found
the increase of viscous damping, from Eq. (3), we consider that the (CXLX11_0184).
rise of the domain wall energy and reduction of the distance be-
tween the pinning edges can cause the domain wall relaxation
frequency increases conversely. As a result, skewness presents its References
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