ortai2t, 6:55 eM OiLBased Drling Fluid Test Procedures AQ sHn0K 0 Home oducts “Figs Systems Mudiad-— Mud@lont— aboutus 8. Fluid Alkalinity Description ‘ne alkalinity velue is used to calculate tne concentration of non-reacted “excess” lime in ol-based dling fluid, xcoss alkaline material © limo, hop to stabilize the emulsion and also neutralize acidic carlson dioxide or hydrogon sutfce gases. The alkalinity of an oll mud is otermnines by breaking the emulsion and titrating the mirure rapidly to the frst color change or endpoint. The number of mlof 0] N sul ‘cid used in the titration por ml of ruc! is reported as the alkalinity of the mud or POM. Apparatus Solvent, consisting of propylene glycol normal-propyl ether (PNA) (CAS No. 1568-01-3) Titration vessel pint jor oF 400 cm? gloss beaker Phenolphthateinindicotor solution: gfl00 em? of 50% IPA/water solution Standardized 0. (N/Id) sulfuric acid solution iver nitrate reagent 0282N, containing 47.1 git, stored in amber oF opaque bottle Distiled or deionized water Disposable syringe: two 5 om® Graduated cyinder (70): one 25 om? 10._ Serological (graduated) pipettes (TD): two lems andl two 19 ems 1. Magnets stiror with 15-inch string bor (coated) 12. Calcium buffer solution: IN sodium hydroxide, kept a closed, sealed bottle to minimize absorption of C03 trom air i 2 3 4 5. Potassium chromate indicator solution: 5 gfi00 em? water 6 7 8 8 13, Colcium ingizotor.Colverilor hydroxy naphthol blue 14, EDTA solution (Versenate or equivaten’): 0) Mole, cisocium (ethylenediamine) tetraacetate aihydrate, stondarcized (Iem® = 19000 CoCOz 1em3 = 4000 malt calcium) Note: Ths FDTAIs ten times more concentrated thon that used in water-base lid testing Procedure |. Adal 100 em PNP to a 400 m3 beaker or pint jar (titration vessel) 2. Fila S.em syringe with whole fluid post the 3 em? mark 3. Displace 20 m3 of whole fluid into the titration vessel 4. Swit the mixture until itis homogeneous. ©. Add 200 em? distiled water 6. Add 18 drops of phenolphthalein indicator solution. hitpslwwn.sharkol.com.cn/portaatleindexiciia/966.him| 1ortai2t, 6:55 eM AQ sHn0K 0 OiLBased Drling Fluid Test Procedures. Home Products volume of aci¢ used for all three titrations the endl point 9. Calculate the whole fluid alkalinity. Calculation Fluids systems Mud to Mud ont aboutus Q or retuins, titrate with acid a second time. Ifa pink color returns after the second titration, titrate with acid a third time and call the tot To convert this value to 51 Co(OH)2 (time), mukoly by 1285.1 Cao (quicklime) is used to activate the emulsitor, the conversion facto Iofbblis 098, Alkalinity Control Agents Biocides Ccorrasion inhibitors Datoarners Detergents & mules ana wessng surfactants Agents Fitration Control agents Los eons Ppe-Frecing Agents sors Shoe iniorors Thinners ond Viscostfors & susponsion Dispersants Agen Weighting agents 91-858 6202 SHARE OLFELD BLACK SunRe® HTWOM HvPcRORL~ sak Ruces hitps ww sharkol.com cn/portaVatleindexici/d/966.him| Mud Plan rus Mud ont sane erond IC20200007075-1 Powered oy! 2