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Investigation on the laboratory performance of bitumen modified with SBS, Elvaloy and Lotader. A joint venture of Total Oil India Private Limited, Bitumen Division and
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Abstract. This paper investigates the variation of dynamic modulus and phase
lag with confinement pressure and rest period. In this investigation, bituminous
mixtures fabricated with unmodified VG30 binder were used and tested as per
AASHTO: TP-79 (2010) protocol incorporating confinement pressure and rest
period between successive frequencies. The analysis of the data showed that
there is a considerable change in the modulus of the material with the applica-
tion of confinement pressure. The phase lag at higher temperature exhibited de-
creasing values at lower frequencies similar to what is seen in test procedure
without any rest period.
1 Introduction
Since only dynamic modulus and the associated master curve are used in pave-
ment design, not much attention is focused on the variation of phase lag as a function
of frequency. Deepa et al. (2017) [3] has shown from a careful analysis of the dynam-
ic modulus data that a phase lag can decrease as the frequency decreases especially
for temperatures above 35°C. While this is considered as an ‘anomalous’ behavior in
many literatures [2 and 5], Deepa et al. (2017) have shown that it is indeed the charac-
teristic trait of a viscoelastic material when subjected to loading without rest periods.
It is expected that such variation of phase lag will influence the dynamic modulus
computed. Also, it is not clear how the application of confinement pressure during
testing can change the dynamic modulus and phase lag.
This paper aims at determining whether the inclusion of rest periods will lead to a
decrease of phase angle for a decrease in frequency. Also, in these test protocol, the
influence of confinement pressure during testing was investigated.
2 Experimental Investigation
The batching of aggregate was done as per the mid-gradation. The mixing and com-
paction temperature for the binder was determined using the viscosity-temperature
relationship. Based on this, the binder was heated to a temperature of 165°C. The
mixing of aggregate and binder was carried out in an automatic mixer machine. After
mixing, the mixture was short-term aged for 4 hours at 135°C and 0.5 hours at 155°C
for compaction. At the end of 4.5 hours, cylindrical samples were cast using a Super-
pave gyratory compactor. A vertical pressure of 600 kPa and 205 gyrations were ap-
plied to the sample at an angle of 1.25° to produce specimens of 165 mm height and
150 mm diameter. The samples were then cored and sliced to 150 mm height and 100
mm diameter specimen for testing. The samples used for carrying out the test had air
voids in the range of 4 ± 0.5 %.
The test specimens were then fixed with hexagonal studs to which the LVDT’s
were clamped before the test. The studs were glued to the specimens using a stud
fixing jig maintaining a gauge length of 70 ± 1mm. Three axial LVDT’s were
4
mounted on the specimen at an angle of 120°. Figure 2 shows the procedure followed
for the stud fixing.
Figure 3 depicts the load application with a rest period and confinement pressure. The
UTS006 software records the axial deformation using the three displacement trans-
ducers as a function of time for all the twenty cycles. This data is used to calculate the
dynamic modulus and phase lag.
The variation of dynamic modulus with frequency for three different temperatures is
shown in figure 4(a)-(c). It can be observed from the plots that the dynamic modulus
increases considerably with the application of confinement pressure, especially at
higher temperatures.
5
a) 5°C b) 35°C
c) 55°C
At low temperatures and high frequency (for instance 5°C and 25 Hz), the dynamic
modulus at confined conditions is almost 6% less than the unconfined conditions. At
intermediate conditions (for instance 35°C and 1 Hz), the dynamic modulus at con-
fined conditions is nearly 17% more than of the unconfined conditions. At the very
high temperature and low frequency (for instance 55°C and 0.01 Hz), the dynamic
modulus at confined conditions is 90% more than that at unconfined conditions.
6
4 Conclusion
This paper looked into modifying the existing AASHTO: TP-79 (2010) protocol to
determine the dynamic modulus and phase lag. From the analysis of the data, it was
seen that there is an appreciable increase in the dynamic modulus with the application
of the 200kPa confinement pressure at higher temperatures. This may be attributed to
the fact that the mastic in the bituminous mixtures exhibits considerable pressure
sensitive nature at high temperature (45, and 55°C) and all frequencies. One of the
possible reasons for the decrease in phase lag with decreasing frequency at high tem-
peratures even with the application of confinement and rest period may be due to the
increase in strain after the initial decrease in strain when the sample is subjected to a
hydrostatic state of stress.
Acknowledgements
The authors thank Department of Science and Technology, Govt. of India [grant
number DST/TSG/STS/2011/46] for the funding and IPC Global, Australia for the
technical support provided during the experimental investigation.
References
1. AASHTO: TP-79, 2010. Standard method of test for determining the dynamic modulus
and flow number for hot mix asphalt using the asphalt mixture performance tester
(AMPT). American Association of State Highway and Transportation Officials, Washing-
ton, DC (2010).
2. Bonaquist, R.: NCHRP Report – 629, ruggedness testing of the dynamic modulus and flow
number tests with the simple performance tester. Washington, DC: Transportation Re-
search Board (2008).
3. Deepa, S., Saravanan, U., and Murali Krishnan, J.: On measurement of dynamic modulus
for bituminous mixtures. International Journal of Pavement Engineering,
DOI:10.1080/10298436.2017.1380809 (2017).
4. IS: 73-13, 2013. Paving bitumen – specification, Bureau of Indian Standards, New Delhi,
India (2013).
5. Lee, K., et al.,: Dynamic modulus of asphalt mixtures for development of Korean pave-
ment design guide. Journal of Testing and evaluation, 35 (2), 143-150 (2007).
6. MORTH, 2013. Specification for roads and bridge works, 4th revision, Ministry of Ship-
ping, Road Transport and Highways, New Delhi, India (2013)
7. NCHRP: 1-37A, ed. Guidelines for the mechanistic-empirical design for new and rehabili-
tated pavement structures. Washington, DC: Transportation Research Board (2004).
8. UTS006, 2017. SPT dynamic modulus test software reference. Australia: IPC Global
(2017).