‘5g ot unpre acetanilide sampe *09 wegned and placed im @ 250 mL {hase Then, flows was Jabeied, & Flosk A Tne reaidual (iguid wes pressed Out of the mat ot trysals Using @ cean rubber stopper. Tne ucHion wes conned fer another 2-3 mined ‘The suction NASK was dreconnecied trom the aspirarer: A} Purification of sond acetomilige by Kecrys torizarion FHM of aismtd woret ana smon amoum of Gece ieurizing cnarceat ‘yare agoed to ask A-6O Then, Fiesk & wos neaied eat Sot t RES Utton sond d5s At the same nme,2ome ef wattr was heartd no be! e029 arenes) Soignon in 125K B was stirred te wrtte op GNSS ) The uppermost guid wis transferred ince Buchner funmer ro Sittred fargt ten, the remaning srry of erystalS poured ints. the fumersy Then, me cryStais cre waned wath fresin, cold water trem on ‘ee both. A tiated (00 paper wan prepa The funnel with furea futer pa wag pinced on antiner Erienmeye Fase wnich was iapaied Fa BY est,me friter paper was, neid wn piace wGing stringy 109, 16 quidt het HQuid, het solunon was poured ve minimize Crysrom ra an in fer paper 1@SK A wag rigsed with FOML aes of tana eet Ine Fong in BOTneN, fritrate was aiawed te a acawee uo disturbing, WNL) Negt, the seiutuer wOS placed nan Ke pam for furtmer cooling (3)Determination of punty by aging melting gaint method p—mopuaty tube i => Tne Crystals were pricktd mio me capillarg qube and made sure The crystals faus off the closed part of the copilary - Mmeiting pont tool made - 4 aaund?rmanly, ¢ne finn, eating of meinng parm vias recorded