Absolute Standards, Inc.

ANAB ISO 17034 Accredited

800-368-1131 Certified
CommentsReference Material CRM AR-1539 Certificate Number
www.absolutestandards.com https://Absolutestandards.com

CERTIFIED WEIGHT REPORT

Part Number: 91807 Solvent(s): Lot#
Lot Number: 102721 Methanol EA899-US
Description: Semi-Volatile Mix #2 102721
17 components Formulated By: Eli Aliaga DATE
Expiration Date: 102726
Recommended Storage: Refrigerate (4 ºC)
Nominal Concentration (µg/mL): 2000 102721
NIST Test ID#: 6UTB 5E-05 Balance Uncertainty Reviewed By: Pedro L. Rentas DATE
Weight(s) shown below were combined and diluted to (mL): 100.0 0.012 Flask Uncertainty
Expanded SDS Information
Lot Nominal Purity Uncertainty Target Actual Actual Uncertainty (Solvent Safety Info. On Attached pg.)
Compound RM# Number Conc (µg/mL) (%) Purity Weight (g) Weight (g) Conc(µg/mL) (+/-) (µg/mL) CAS# OSHA PEL (TWA) LD50

1. Benzoic acid 34 11930AW 2000 99 0.2 0.20203 0.20213 2001.0 8.2 65-85-0 N/A orl-rat 1700mg/kg
2. 4-Chloro-3-methylphenol 66 06209PV 2000 99 0.2 0.20203 0.20228 2002.5 8.2 59-50-7 N/A orl-rat 1830mg/kg
3. 2-Chlorophenol 83 MKBF1910V 2000 99 0.2 0.20203 0.20230 2002.7 8.2 95-57-8 N/A orl-rat 670mg/kg
4. o-Cresol (2-Methylphenol) 93 SHBC5581V 2000 99 0.2 0.20203 0.20232 2002.9 8.2 95-48-7 5 ppm (22mg/m3/8H)(skin) orl-rat 121mg/kg
5. p-Cresol (4-Methylphenol) 216 05412TV 2000 99 0.2 0.20203 0.20227 2002.4 8.2 106-44-5 5 ppm (22mg/m3/8H)(skin) orl-rat 207mg/kg
6. 2,4-Dichlorophenol 142 BCBH1617V 2000 99 0.2 0.20203 0.20215 2001.2 8.2 120-83-2 N/A orl-rat 580mg/kg
7. 2,6-Dichlorophenol 143 00501HW 2000 99 0.2 0.20203 0.20233 2003.0 8.2 87-65-0 N/A orl-rat 5940mg/kg
8. 2,4-Dimethylphenol 463 04319MT 2000 97 0.2 0.20620 0.20638 2001.8 8.3 105-67-9 N/A orl-rat 3200mg/kg
9. 2,4-Dinitrophenol 159 032516 2000 98 0.2 0.20409 0.20429 2001.9 8.2 51-28-5 N/A orl-rat 30mg/kg
10. 4,6-Dinitro-2-methylphenol 158 LC25844V 2000 99 0.2 0.20203 0.20229 2002.6 8.2 534-52-1 N/A N/A
11. 2-Nitrophenol 230 051897 2000 98 0.2 0.20409 0.20412 2000.3 8.2 88-75-5 N/A orl-rat 334mg/kg
12. 4-Nitrophenol 231 FGM01 2000 99 0.2 0.20203 0.20233 2003.0 8.2 100-02-7 N/A orl-rat 250mg/kg
13. Pentachlorophenol 243 06324ED 2000 98 0.2 0.20409 0.20439 2002.9 8.2 87-86-5 0.5mg/m3/8H (skin) orl-rat 27mg/kg
14. Phenol 250 SHBF1351V 2000 99 0.2 0.20203 0.20209 2000.6 8.2 108-95-2 5 ppm (19mg/m3/8H)(skin) orl-rat 317mg/kg
15. 2,4,5-Trichlorophenol 295 05714MV 2000 99 0.2 0.20203 0.20233 2003.0 8.2 95-95-4 N/A orl-rat 820mg/kg
16. 2,4,6-Trichlorophenol 296 051597 2000 99 0.2 0.20203 0.20206 2000.3 8.2 88-06-2 N/A orl-rat 820mg/kg
17. 2,3,4,6-Tetrachlorophenol 477 100317 2000 99.3 0.2 0.20142 0.20152 2001.0 8.1 58-90-2 N/A orl-rat 140mg/kg

• The certified value is the concentration calculated from gravimetric and volumetric measurements unless otherwise stated.
• Standards are prepared gravimetrically using balances that are calibrated with weights traceable to NIST (see above).
• Standards are certifed (+/-) 0.5% of the stated value, unless otherwise stated.
• All Standards, after opening ampule, should be stored with caps tight and under appropriate laboratory conditions.
• Uncertainty Reference: Taylor, B.N. and Kuyat, C.E., "Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Result,"
NIST Technical Note 1297, U.S. Government Printing Office, Washington, DC, (1994).

Part # 91807 Lot # 102721 1 of 3 Printed: 11/11/2021, 11:15:04 PM

Method GC8MSD-3.M: Column:SPB-5 (30m X 0.25mm ID X 0.25µm film thickness) Temp 1 = 50°C (1min.), Temp 2 = 300°C (9min.), Rate = 10°C/min., Injector B= 200°C, Detector B =
275°C, Split Ratio = 100:1, Scan Rate = 2. Analysis performed by Melissa Stonier.
 • The certified value is the concentration calculated from gravimetric and volumetric measurements unless otherwise stated.
• Standards are prepared gravimetrically using balances that are calibrated with weights traceable to NIST (see above).
• Standards are certifed (+/-) 0.5% of the stated value, unless otherwise stated.
• All Standards, after opening ampule, should be stored with caps tight and under appropriate laboratory conditions.
Absolute Standards, Inc. • Uncertainty Reference: Taylor, B.N. and Kuyat, C.E., "Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Result," ANAB ISO 17034 Accredited
800-368-1131 NIST Technical Note 1297, U.S. Government Printing Office, Certified
Comments
Washington, Reference
DC, (1994). Material CRM AR-1539 Certificate Number
www.absolutestandards.com https://Absolutestandards.com

Method GC8MSD-3.M: Column:SPB-5 (30m X 0.25mm ID X 0.25µm film thickness) Temp 1 = 50°C (1min.), Temp 2 = 300°C (9min.), Rate = 10°C/min., Injector B= 200°C, Detector B =
275°C, Split Ratio = 100:1, Scan Rate = 2. Analysis performed by Melissa Stonier.

TIC: 91807.D
Abundance

8000000 7.18
8.73
9.10
10.90
9.65
7.52 14.71
7500000 6.17 12.01
11.92
17.20 Peak MSD RT
7000000 No. Name (min)
1 Phenol 5.98
6500000 8.55
2 2-Chlorophenol 6.17
5.98
6000000 3 o-Cresol (2-Methylphenol) 7.18
15.43 4 p-Cresol (4-Methylphenol) 7.52
5500000 14.01 5 2-Nitrophenol 8.55
6 2,4-Dimethylphenol 8.73
5000000 7 2,4-Dichlorophenol 9.10
8 Benzoic acid 9.38
4500000
9 2,6-Dichlorophenol 9.66
14.29
4000000 10 4-Chloro-3-methylphenol 10.90
11 2,4,6-Trichlorophenol 11.92
3500000 12 2,4,5-Trichlorophenol 12.01
13 2,4-Dinitrophenol 14.01
3000000 14 4-Nitrophenol 14.29
15 2,3,4,6-Tetrachlorophenol 14.71
2500000
16 4,6-Dinitro-2-methylphenol 15.43

2000000 17 Pentachlorophenol 17.20

1500000
9.38
1000000

500000

0
Time--> 5.00 10.00 15.00 20.00 25.00 30.00

Part # 91807 Lot # 102721 2 of 3 Printed: 11/11/2021, 11:15:04 PM

Absolute Standards, Inc. ANAB ISO 17034 Accredited
800-368-1131 Certified
CommentsReference Material CRM AR-1539 Certificate Number
www.absolutestandards.com https://Absolutestandards.com

Peak FID RT
No. Name (min)
1 Phenol 7.62
2 2-Chlorophenol 7.92
3 o-Cresol 8.82
4 p-Cresol 9.12
5 2-Nitrophenol 10.21
6 2,4-Dimethylphenol 10.27
7 2,4-Dichlorophenol 10.51
8 Benzoic acid 10.71
9 2,6-Dichlorophenol 11.22
10 4-Chloro-3-methylphenol 12.30
11 2,4,6-Trichlorophenol 13.32
12 2,4,5-Trichlorophenol 13.41
13 2,4-Dinitrophenol 15.24
14 4-Nitrophenol 15.42
15 2,3,4,6-Tetrachlorophenol 15.90
16 4,6-Dinitro-2-methylphenol 16.55
17 Pentachlorophenol 18.22

Part # 91807 Lot # 102721 3 of 3 Printed: 11/11/2021, 11:15:04 PM