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CERTIFIED WEIGHT REPORT

Part Number: 30006 Solvent(s): Lot#
Lot Number: 041322 Toluene 28508 (50%)
Description: EPA Method 525.2 Pesticide Mix #1 Hexane 273615 (50%) 041322
21 components Formulated By: Benson Chan DATE
Expiration Date: 041327
Recommended Storage: Refrigerate (4 ºC)
Nominal Concentration (µg/mL): 100 041322
NIST Test ID#: 6UTB 5E-05 Balance Uncertainty Reviewed By: Pedro L. Rentas DATE
Weight(s) shown below were combined and diluted to (mL): 100.1 0.001 Flask Uncertainty
Expanded SDS Information
(RM#) Lot Dil. Initial Initial Nominal Purity Uncertainty Uncertainty Target Actual Actual Uncertainty (Solvent Safety Info. On Attached pg.)
Compound Part Number Number Factor Vol. (mL) Conc.(ug/mL) Conc (µg/mL) (%) Purity (%) Pipette (mL) Weight(g) Weight(g) Conc (µg/mL) (+/-) (µg/mL) CAS# OSHA PEL (TWA) LD50

1. cis-Chlordane (0064) ER062410-01 NA NA NA 100 99.6 0.2 NA 0.01005 0.01008 100.3 1.1 5103-71-9 0.5mg/m3 (skin) orl-rat 500mg/kg
2. trans-Chlordane (0065) 090197 NA NA NA 100 99 0.2 NA 0.01011 0.01013 100.2 1.1 5103-74-2 0.5mg/m3 (skin) orl-rat 500mg/kg
3. trans-Nonachlor (0235) LRAB7486 NA NA NA 100 99 0.2 NA 0.01011 0.01012 100.1 1.1 39765-80-5 0.5mg/m3 (skin) orl-rat 500mg/kg
4. Aldrin 10013 052521 0.05 5.00 2000.5 100 NA NA 0.017 NA NA 100.0 0.8 309-00-2 0.25mg/m3 (skin) orl-rat 39mg/kg
5. a-BHC 10013 052521 0.05 5.00 2000.5 100 NA NA 0.017 NA NA 100.0 1.2 319-84-6 N/A orl-rat 88-270mg/kg
6. b-BHC 10013 052521 0.05 5.00 2000.8 100 NA NA 0.017 NA NA 100.0 1.2 319-85-7 N/A orl-rat 6000mg/kg
7. d-BHC 10013 052521 0.05 5.00 2000.8 100 NA NA 0.017 NA NA 100.0 1.2 319-86-8 N/A orl-rat 1000mg/kg
8. g-BHC (Lindane) 10013 052521 0.05 5.00 2000.9 100 NA NA 0.017 NA NA 100.0 0.8 58-89-9 0.5mg/m3 (skin) orl-rat 76mg/kg
9. 4,4'-DDD 10013 052521 0.05 5.00 2000.8 100 NA NA 0.017 NA NA 100.0 1.2 72-54-8 N/A orl-rat 113mg/kg
10. 4,4'-DDE 10013 052521 0.05 5.00 2000.5 100 NA NA 0.017 NA NA 100.0 1.2 72-55-9 N/A orl-rat 880mg/kg
11. 4,4'-DDT 10013 052521 0.05 5.00 2001.0 100 NA NA 0.017 NA NA 100.0 0.8 50-29-3 N/A orl-rat 87mg/kg
12. Dieldrin 10013 052521 0.05 5.00 2001.0 100 NA NA 0.017 NA NA 100.0 0.8 60-57-1 0.25mg/m3 (skin) orl-rat 38300ug/kg
13. Endosulfan I 10013 052521 0.05 5.00 2000.6 100 NA NA 0.017 NA NA 100.0 0.8 959-98-8 0.1mg/m3 (skin) orl-rat 18mg/kg
14. Endosulfan II 10013 052521 0.05 5.00 2000.6 100 NA NA 0.017 NA NA 100.0 1.2 33213-65-9 0.1mg/m3 (skin) orl-rat 18mg/kg
15. Endosulfan sulfate 10013 052521 0.05 5.00 2000.9 100 NA NA 0.017 NA NA 100.0 1.2 1031-07-8 N/A orl-rat 18mg/kg
16. Endrin 10013 052521 0.05 5.00 2000.9 100 NA NA 0.017 NA NA 100.0 1.2 72-20-8 0.1mg/m3 (skin) orl-rat 7mg/kg
17. Endrin aldehyde 10013 052521 0.05 5.00 2004.2 100 NA NA 0.017 NA NA 100.1 0.8 7421-93-4 N/A orl-rat 500mg/kg
18. Endrin ketone 10013 052521 0.05 5.00 2000.9 100 NA NA 0.017 NA NA 100.0 0.8 53494-70-5 N/A N/A
19. Heptachlor 10013 052521 0.05 5.00 2000.6 100 NA NA 0.017 NA NA 100.0 0.8 76-44-8 0.5mg/m3 (skin) orl-rat 40mg/kg
20. Heptachlor epoxide (isomer B) 10013 052521 0.05 5.00 2001.0 100 NA NA 0.017 NA NA 100.0 0.8 1024-57-3 N/A orl-rat 47mg/kg
21. 4,4'-Methoxychlor 10013 052521 0.05 5.00 2001.0 100 NA NA 0.017 NA NA 100.0 0.8 72-43-5 10mg/m3 orl-rat 6000mg/kg

• The certified value is the concentration calculated from gravimetric and volumetric measurements unless otherwise stated.
• Standards are prepared gravimetrically using balances that are calibrated with weights traceable to NIST (see above).
• Standards are certifed (+/-) 0.5% of the stated value, unless otherwise stated.
• All Standards, after opening ampule, should be stored with caps tight and under appropriate laboratory conditions.
• Uncertainty Reference: Taylor, B.N. and Kuyat, C.E., "Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Result,"
NIST Technical Note 1297, U.S. Government Printing Office, Washington, DC, (1994).

Part # 30006 Lot # 041322 1 of 2 Printed: 4/14/2022, 11:20:03 PM

TIC: [BSB1]30006.D
Abundance
 NIST Technical Note 1297, U.S. Government Printing Office, Washington, DC, (1994).

Absolute Standards, Inc. ANAB ISO 17034 Accredited

800-368-1131 Certified
CommentsReference Material CRM AR-1539 Certificate Number
www.absolutestandards.com https://Absolutestandards.com

TIC: [BSB1]30006.D
Abundance

200000
15.79
Method GC7MSD-1.M: Column: SPB-608 (30m X 0.25mm ID X 0.25µm
190000 film thickness) Temp 1 = 150°C (4min.), Temp 2 = 290°C (13.5 min.),
Rate = 8°C/min., Injector B= 200°C, Detector B = 290°C. Split Ratio =
50:1, Scan Rate = 2. Analysis performed by Candice Warren.
180000

170000 18.47

15.15 17.19
160000

20.16
MSD RT
150000
Name (min.)
a-BHC 9.46
140000
g-BHC (Lindane) 10.68
14.90
17.94 19.91 b-BHC 11.02
130000 14.75
Heptachlor 11.77
d-BHC 12.00
120000 17.31
Aldrin 12.68
Heptachlor epoxide 14.22
110000
trans-Chlordane 14.75

100000
trans-Nonachlor 14.90
15.96 cis-Chlordane 15.15

90000 Endosulfan I 15.17

14.23 4,4'-DDE 15.78
80000 Dieldrin 15.95
16.81
Endrin 16.80
11.02 12.01 4,4'-DDD 17.19
70000
12.69
10.68 Endosulfan II 17.30
60000 4,4'-DDT 17.95
9.47
11.78 Endrin aldehyde 18.06
50000 Endosulfan sulfate 18.47
Methoxychlor 19.91
18.06
40000 Endrine ketone 20.16

30000

20000

10000

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Part # 30006 Lot # 041322 2 of 2 Printed: 4/14/2022, 11:20:03 PM