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800-368-1131 Certified
CommentsReference Material CRM AR-1539 Certificate Number
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CERTIFIED WEIGHT REPORT

Part Number: 20001
Lot Number: 091520
Description: Hexadecane Extraction Volatiles Mix #1 091520
CLP July '91 6 components Formulated By: Benson Chan DATE
Expiration Date: 091525 Solvent(s): Lot#
Recommended Storage: Refrigerate (4 ºC) Methanol DX932-US
Nominal Concentration (µg/mL): 2000 091520
NIST Test ID#: 23060 5E-05 Balance Uncertainty Reviewed By: Pedro L. Rentas DATE
Volume(s) shown below were combined and diluted to (mL): 100.0 0.012 Flask Uncertainty
Expanded SDS Information
Part Lot Dilution Initial Uncertainty Initial Final Uncertainty (Solvent Safety Info. On Attached pg.)
Compound Number Number Factor Vol. (mL) Pipette (mL) Conc.(µg/mL) Conc.(µg/mL) (+/-) µg/mL CAS# OSHA PEL (TWA) LD50

1. Benzene 21001 012819 0.10 10.00 0.042 20000.5 2000.0 18.7 71-43-2 1 ppm orl-rat 4894mg/kg
2. Toluene 21001 012819 0.10 10.00 0.042 20000.7 2000.0 18.7 108-88-3 200 ppm orl-rat 5000mg/kg
3. Ethyl benzene 21001 012819 0.10 10.00 0.042 20001.0 2000.0 18.7 100-41-4 100 ppm (435mg/m3/8H) orl-rat >2000mg/kg
4. o-Xylene 21001 012819 0.10 10.00 0.042 20001.1 2000.0 18.7 95-47-6 100 ppm (435mg/m3/8H) ipr-mus 1364mg/kg
5. m-Xylene 21001 012819 0.10 10.00 0.042 20000.8 2000.0 18.7 108-38-3 100 ppm (435mg/m3/8H) orl-rat 5g/kg
6. p-Xylene 21001 012819 0.10 10.00 0.042 20000.3 1999.9 18.7 106-42-3 100 ppm (435mg/m3/8H) orl-rat 5g/kg
• The certified value is the concentration calculated from gravimetric and volumetric measurements unless otherwise stated.
TIC: 20001.D • Standards are prepared gravimetrically using balances that are calibrated with weights traceable to NIST (see above).
Abundance • Standards are certifed (+/-) 0.5% of the stated value, unless otherwise stated.
• All Standards, after opening ampule, should be stored with caps tight and under appropriate laboratory conditions.
1600000 • Uncertainty Reference: Taylor, B.N. and Kuyat, C.E., "Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Result,"
36.13 NIST Technical Note 1297, U.S. Government Printing Office, Washington, DC, (1994).
1500000

1400000

1300000

1200000 Method: GC6MSD-1. Detector: MSD (Scan mode).

Column: Vocol (60m X 0.25mm ID X 1.5µm film
1100000
thickness). Oven Profile: Temp. 1 = 35°C (Time
1000000 1=10min.), Temp. 2 = 200°C (Time 2=8.75 min.), Rate
= 4°C/min., Injector Temp.= 200°C, Detector Temp. =
35.85 37.93
900000 29.85 220°C. Analyst:Candice Warren.

800000

700000
MSD RT
22.47
600000 Name (min.)
Benzene 22.44
500000
Toluene 29.87
400000 Ethylbenzene 35.87
m-Xylene 36.15
300000
p-Xylene 36.15
200000 o-Xylene 37.92

100000

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Part # 20001 Lot # 091520 1 of 2 Printed: 9/22/2020, 11:15:30 PM

 200000 o-Xylene 37.92

100000
Absolute Standards, Inc. ANAB ISO 17034 Accredited
800-368-1131 Time--> 0 Certified
CommentsReference Material CRM AR-1539 Certificate Number
10.00
www.absolutestandards.com 15.00 20.00 25.00 30.00 35.00 40.00 45.00 50.00 55.00 60.00
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FID RT
Name (min.)
Benzene 18.41
Toluene 25.08
Ethylbenzene 30.41
m-Xylene/p-Xylene 30.68
o-Xylene 32.20

Part # 20001 Lot # 091520 2 of 2 Printed: 9/22/2020, 11:15:30 PM