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1. Scope* 3. Terminology
1.1 This test method covers the determination of the expan- 3.1 For definitions of terms relating to aggregates used in
sion of a specimen of carbonate rock while immersed in a this test method, refer to Descriptive Nomenclature C294.
solution of sodium hydroxide (NaOH) at room temperature.
The length changes occurring during such immersion indicate 4. Summary of Test Method
the general level of reactivity of the rock and whether tests 4.1 Small rock cylinders are immersed in a solution of
should be made to determine the effect of aggregate prepared NaOH except when removed for determination of length
from the rock upon the volume change in concrete. change. The length change of each specimen is periodically
1.2 The values stated in SI units are to be regarded as determined.
standard. No other units of measurement are included in this
5. Significance and Use
standard.
5.1 This test method is intended to give a relatively rapid
1.3 This standard does not purport to address all of the
indication of the potential expansive reactivity of certain
safety concerns, if any, associated with its use. It is the
carbonate rocks that may be used as concrete aggregates. The
responsibility of the user of this standard to establish appro-
test method has been successfully used in (1) research and (2)
priate safety and health practices and determine the applica-
preliminary screening of aggregate sources to indicate the
bility of regulatory limitations prior to use.
presence of material with a potential for deleterious expansion
when used in concrete.
2. Referenced Documents
5.2 The test method is intended as a research and screening
2.1 ASTM Standards:2
method rather than as the basis of a specification requirement.
C294 Descriptive Nomenclature for Constituents of Con-
It is intended to supplement data from field service records,
crete Aggregates
petrographic examinations according to Guide C295, and tests
C295 Guide for Petrographic Examination of Aggregates for
of aggregate in concrete according to Test Method C1105.
Concrete
C1105 Test Method for Length Change of Concrete Due to 5.3 Alkalies participating in the expansive reactions with
Alkali-Carbonate Rock Reaction aggregate constituents in concrete usually are derived from the
D75 Practice for Sampling Aggregates hydraulic cement; under certain circumstances they may be
D1248 Specification for Polyethylene Plastics Extrusion derived from other constituents of concrete or from external
Materials for Wire and Cable sources. Two types of alkali reactivity of aggregates are
E177 Practice for Use of the Terms Precision and Bias in recognized: (1) alkali-silica reaction involving certain siliceous
ASTM Test Methods rocks, minerals, and artificial glasses, and (2) alkali carbonate
reaction involving dolomite in certain calcitic dolomites, do-
lomitic limestones, and dolostones. This test method is not
1
This test method is under the jurisdiction of ASTM Committee C09 on
suitable as a means to detect alkali-silica reaction.
Concrete and Concrete Aggregatesand is the direct responsibility of Subcommittee
C09.26 on Chemical Reactions. 6. Apparatus and Reagents
Current edition approved Oct. 1, 2011. Published November 2011. Originally
6.1 1 N Sodium Hydroxide Solution—Dissolve 40 6 1 g of
approved in 1966. Last previous edition approved in 2005 as C586 – 05. DOI:
10.1520/C0586-11. reagent-grade sodium hydroxide (NaOH) in distilled water,
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or dilute to 1 L and store in a polyethylene bottle.
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on 6.2 Sawing, Drilling, and Grinding Equipment, suitable for
the ASTM website. preparing test specimens of the dimensions given in Section 8.
APPENDIX
(Nonmandatory Information)
X1.1 Since the expansion caused by reactions between tive of the variability of the production of the source is a
cement alkalies and carbonate aggregates is sensitive to subtle difficult task and requires the efforts of an individual trained to
changes in aggregate lithology, the results of measurements distinguish differences in lithology.
should be interpreted with full recognition of the variables
which would affect the results obtained. The acceptance or X1.2 The relationship of the test results to the behavior of
rejection of aggregate sources based solely on the results of this large quantities of rock from a given source will depend upon
test is not recommended since, in commercial production, the degree to which the petrographic and chemical properties
expansive and nonexpansive materials may occur in close of the rock vary within the source.
proximity and the securing of samples adequately representa-
SUMMARY OF CHANGES
Committee C09 has identified the location of selected changes to this test method since the last issue, C586
– 05, that may impact the use of this test method. (Approved October 1, 2011.)
(1) Revised 1.2 to delete comment regarding informational (3) Revised 7.3 regarding the testing of specimens of rock in
units. which discontinuities exist or bedding cannot be discovered.
(2) Deleted informational inch-pound units throughout.
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