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Construction and Building Materials 170 (2018) 366–377

Contents lists available at ScienceDirect

Construction and Building Materials


journal homepage: www.elsevier.com/locate/conbuildmat

Virtual Sliding Pipe Rheometer for estimating pumpability of concrete


Venkatesh Naidu Nerella, Viktor Mechtcherine ⇑
Technische Universität Dresden, Institute of Construction Materials, Dresden, Germany

h i g h l i g h t s

 A single-phase CFD model was developed for simulating pumpability tests with Sliper.
 Models without a lubricating layer (LL) are not generally applicable to concrete.
 The lubricating layer was implemented in the pipe flow CFD model.
 Influences of rheological parameters and thickness of LL were demonstrated.
 Particle-concentration-based models were suggested to estimate LL properties.

a r t i c l e i n f o a b s t r a c t

Article history: Predicting the pumping pressure needed to ensure a consistent flow rate of concrete is crucial to the
Received 1 September 2017 success of current construction processes and newly introduced, but fast-growing 3D-concrete print-
Received in revised form 26 February 2018 ing techniques. The Sliding Pipe Rheometer (Sliper) has recently proved to be a reliable experimental
Accepted 1 March 2018
tool in predicting pumping pressure. Building on the experimental results of an earlier investigation
Available online 23 March 2018
by means of Sliper, a single-fluid numerical model for simulating Sliper tests (virtual Sliper) was
developed using Computational Fluid Dynamics (CFD). Various observations as well as numerical lim-
Keywords:
itations of the model and their physical origins were analysed. It was demonstrated that lubricating
Pumpability
Computational Fluid Dynamics
layer has vital influence on concrete pumping and that single phase numerical models, not consider-
Lubricating layer ing the lubricating layer are only applicable to some specific concrete compositions. Hence, the initial
Sliding Pipe Rheometer single-phase model was improved by implementing a separate lubricating layer; its properties were
calculated using Chateau-Ovarlez-Trung and Krieger-Dougherty models. Experimental and numerical
comparative analyses confirm the validity of the above-mentioned approach in calculating lubricating
layer properties. Parameter sensitivity analysis showed that the plastic viscosity and thickness of the
lubricating exert the dominant influences on pumping pressure. The virtual pumpability testing tool
as developed should enable a more purposeful material design of pumpable concrete and
pre-estimation of pumping processes.
Ó 2018 Elsevier Ltd. All rights reserved.

1. Introduction blockages or circuit breakdowns over longer time durations


(see Fig. 1).
Concrete pumping has emerged as one of the most important
processing technologies in the construction industry. It often 1.1. Testing pumpability of concrete
makes possible the reduction of construction costs and consider-
ably speeds up the construction process. Concrete pumping is also Concrete pumping occurs by pushing concrete using high pres-
crucial to many advancements in construction-related processes sure into pipelines made of either flexible, abrasive resistant mate-
such as Digital Construction (DC), often called 3D-printing with rial or steel. In other words, the force of the applied pressure causes
concrete. In the case of onsite DC techniques, concrete must be the concrete material to deform in the direction of the force
transported or pumped over longer distances, periodically applied and so to transmit the force further. The pressure required
stopping after having pumped each layer, but without any to pump concrete depends on its composition as well as on the
pumping specifications such as distance, height to pump, pipe
diameter, and discharge rate. Any changes in the composition of
⇑ Corresponding author. concrete such as water-to-binder ratio, aggregate size distributions
E-mail address: mechtcherine@tu-dresden.de (V. Mechtcherine). (grading), and admixtures can exert a pronounced influence on its

https://doi.org/10.1016/j.conbuildmat.2018.03.003
0950-0618/Ó 2018 Elsevier Ltd. All rights reserved.
V.N. Nerella, V. Mechtcherine / Construction and Building Materials 170 (2018) 366–377 367

Fig. 1. Examples of concrete printing technologies: a) a CONPrint3D: concrete boom pump is depicted pumping and precision-placing fresh concrete (source: TU Dresden), b)
Contour Crafting: a concrete pump is depicted pumping concrete to a rail-mounted robotic printhead (source: University of Southern California).

rheological properties, indeed its behaviour during pumping. ifications of pumping circuit, one can estimate the discharge pres-
Hence, predicting the discharge pressure needed to pump a partic- sure P required for a pumping circuit under field conditions using
ular concrete mixture over a given distance or height at a specific Eq. (1) (considering plug/slip flow with no deformation in the plug
rate is not trivial. Much research has been conducted on this topic, [10,11]):
especially during the last two decades, which has led in turn to dif-
4L 16  L  Q
ferent prediction models and test approaches [1–7]. Convention- P¼ aþ bþqgH ð1Þ
ally, this crucial task has been accomplished using methods
D p  D3
based on empirical test methods [6] or experience [8]. However, where L is the length, D is the diameter of the pipeline, q is the den-
such empirical approaches have proven unreliable because of dif- sity of concrete, H is the pumping height, and Q is the desired flow
ferences in laboratory testing conditions and the corresponding rate.
actual situation during pumping [4,6,9]. Not so in the case of the Assuming a linear relationship between P and Q, see [4,10] and
Sliding Pipe Rheometer (Sliper, see Fig. 2) which is a relatively Fig. 2c, according to Eq. (2),
new device developed to overcome the conventional problems in
P ¼ A þ B  Q þ PH ð2Þ
testing the pumpability of concrete and estimating discharge pres-
sures for various concrete types [4]. where PH = pressure induced by deadweight of concrete in the Sli-
As the first part of this research, extensive laboratory investiga- per pipe, parameters a and b can be calculated from the P-Q plot
tions [6] were conducted using Sliper. Using the rheological of Sliper experiments using Eq. (3) which is derived by combining
parameters a and b obtained from Sliper experiments and the spec- Eqs. (1) and (2):

Pressure
sensor
Upper pipe
(on the top of
the piston)
Handles

(b)
Lower pipe
Pressure P

(inside the pipe)

Piston B
(inside the
lower pipe)
A
PH

Flow rate Q
(a) (c)

Fig. 2. a) Sliding Pipe Rheometer, courtesy of Schleibinger Geräte T. u. G. GmbH; b) pressure sensor (in dotted circle); c) schematic view of P-Q plot (A = parameter related to
yield stress, B = parameter related to plastic viscosity, PH = deadweight pressure of concrete).
368 V.N. Nerella, V. Mechtcherine / Construction and Building Materials 170 (2018) 366–377

Bpd
3
dA rheological properties of concrete in a phase are constant through-
a¼ ; b¼ ð3Þ out the modelled geometry. Numerical solution for fresh concrete’s
4l 16  l
rheological behaviour is then made possible by adding apparent
where A is the P-intercept of the P-Q curve, B is the slope of P-Q viscosity, commonly following the Bingham or Herschel-Bulkley
curve, and l and d are the length and diameter of Sliper pipe, 0.5 models, to the Navier-Stokes equations [13,17,18]. This method
m and 0.126 m, respectively. excludes the interactions among solid particles from the simula-
tion and, hence, is not appropriate to simulate heterogeneous phe-
1.2. Research significance nomena such as segregation and blocking directly [12].
Nevertheless, CFD has proven to be a useful tool for simulating
Today’s very broad spectrum of concrete compositions, which fresh concrete flows where macroscopic phenomena such as pres-
certainly become even broader in the future, makes it necessary sure vs. flowrate relationships during pumping are the focus [9]. It
to perform numerous experiments to characterise their rheological is worthy of note that it is possible to couple CFD calculations, rep-
properties and subsequently determine their pumpability. More- resenting the fluid phase, with DEM, which represents the particle
over, considering on the one hand that concrete properties are phase, but such calculation procedures are very complex, very
time- and thixotropy- (resting time) dependent and that on the time-consuming, and still in the early stages of their development
other hand pumping in the case of modern processes such as DC [14].
demands pumpability for longer durations, extensive experimental It is possible to simulate large volume concrete flows such as
studies are needed to assure the pumpability of concrete, even if its castings [13] and full scale pumping [19] using CFD. Thrane et al.
composition is unaltered. Therefore, a purely experimental [20] simulated mould-filling process of SCC as well as slump flow
approach for assessing pumpability does not seem feasible in all simulations with a phenomenological micro-mechanical CFD
the cases, since extensive experimental tests demand a great deal model. Tichko et al. [21] developed a CFD model for computing
of time and economic investment. formwork pressures by simulating form filling through bottom-
As in many other fields, numerical simulations present a up concrete pumping. Further literature presents various CFD
promising tool in complementing experimental studies [12] since modelling using single-phase flow and multi-phase approaches;
they may not only save time and costs but also increase the accu- see [12,13,22–27]. Jo et al. [9] developed a computational approach
racy of the predictions, enable better insight into material beha- to estimate lubricating layer (hereinafter LL) in concrete pumping.
viour, and support material design as well. With this in mind the They emphasized the inadequacy of conventional pumping pres-
experimental research on the pumpability of concrete [6,11] has sure prediction methods with the help of field measurements
been extended by developing a numerical model which simulates and a mock full-scale pumping test. Tan et al. [28] developed a
the Sliper experiment and in this way enables the estimation of multi-phase numerical model to investigate wear mechanisms of
the discharge pressure numerically. These numerically determined concrete piping wall. They combined DEM and CFD approaches:
pressures from the virtual Sliper can thereafter be utilized to pre- DEM to model concrete aggregates as discrete particles and CFD
dict the pumping pressure for pumping circuits of various lengths to model the continuous fluid phase. Choi et al. [19] simulated
and configurations. The virtual Sliper also makes it possible to fresh concrete flow in a 170 m long pumping circuit using a
investigate numerous concrete types with wide variations in their single-fluid CFD approach. The best fitting thickness for LL was
rheological properties without conducting physical experiments. determined by comparing calculated pressure with the experimen-
Thus, virtual Sliper can play an important role in establishing intel- tally measured values at a flow rate of 50 m3/h. Furthermore, they
ligent material design approaches for pumpable concretes. In addi- analysed pressure profiles comparatively along the circuit geome-
tion, virtual Sliper becomes an inherent part of DC approaches, try with the pressure profiles measured experimentally and
where minimal involvement of human labour is envisioned with observed that the deviations between the CFD-calculated results
enhanced machine-material integration (autonomous in the lines and experimental data were below 7% [19]. Choi et al. [5] also
of Industry 4.0). Fresh concrete properties can be determined investigated the formation of the lubrication layer and simulated
online or ‘in the process’ during transporting and the printing pro- the mechanism of shear-induced particle migration (SIPM) during
cess, these properties could then be sent to virtual Sliper. Virtual concrete pumping. Influences of particle shapes were indirectly
Sliper predicts the pumping pressures needed to ensure consistent modelled by solving SIPM equations, implementing a User-
pumping flow-rates considering the ‘change’ in rheological proper- Defined Scalar into ANSYS Fluent [5]. It was concluded that the
ties as well as in target structure geometry. Thus, a numerical LL was the dominant aspect in defining the flow of concrete during
model to simulate Sliper experiments or another adequate tech- pumping and found numerical simulations in considering particle
nique to predict pumping behaviour is indispensable. shape to correlate well with experimentally measured velocity
profiles using an Ultrasonic Velocity Profiler. Chen et al. [29] per-
1.3. Numerical modelling of fresh concrete formed CFD simulations of wet shotcrete flow in a pipe, including
modelling of LL. In addition to finding the best fitting thickness of
The common numerical approaches in simulating the behaviour the LL, the authors also compared numerically determined LL
of fresh concrete are Computational Fluid Dynamics (CFD) thicknesses with experimentally measured LL thicknesses and
[9,13,14] and the Discrete Element Method (DEM) [15,16]. In the found that LL for tested shotcrete compositions varied from 1.5
DEM concrete is modelled by a collection of interacting distinct mm to 3.5 mm.
particles, which can establish and break contacts dynamically. The approach presented in the article at hand is significantly
The method enables modelling of large strain and stress phenom- different to those previous to it. In all the above listed literature,
ena of heterogeneous materials. However, its applicability to large numerical models were primarily developed to study concrete flow
scale simulations (concrete volume of more than 10’s of litres) is characteristics, and that of LL, in a long pumping circuit. So far no
strongly hindered by the requirement that millions of particles numerical model is available to link the resulting rheological prop-
be simulated and subsequently demanding substantial computa- erties as observed in the Sliper tests to any other more commonly
tional resources. used experimental procedure such as the use of a rheometer or vis-
In CFD, concrete is modelled as a single continuum phase or as cometer. This is a rather significant knowledge deficiency that
multiple continuum phases, while the modelled domain is dis- should be overcome with the utmost urgency, considering the pro-
cretized as interconnected mesh elements. This means that the ven applicability of Sliper for pumping pressure prediction and its
V.N. Nerella, V. Mechtcherine / Construction and Building Materials 170 (2018) 366–377 369

newness and unavailability in most concrete laboratories and 3. Single-phase numerical model
ready-mix concrete practitioners. This paper addresses this chal-
lenge by presenting virtual Sliper – a CFD model able to predict Sli- In the first step of the Sliper modelling experiments, concrete
per experimental results using rheological input parameters was assumed to be a continuous Bingham fluid, and the approach
according to the Bingham model as obtained from viscometer tests. is termed as ‘Initial single-phase model (ISPM). The numerical
From this point on, this paper is organised into the following model and the corresponding simulation results are presented in
segments: Experimental background (Section 2), Single-phase the following sections.
numerical model (Section 3), and User-defined, single-phase model
(Section 4), followed by the summary and conclusions (Section 5). 3.1. Modelling schema
In both numerical model sections, the modelling schema is pre-
sented in detail, followed by results and discussion. In the initial Concrete flow was modelled by the conservation equations for
single-phase model, Sliper simulations were carried out without mass and momentum of steady-state, incompressible flow. The
considering the LL. It was demonstrated that single-phase numer- continuity equation for the conservation of mass is [30]:
ical models which do not consider the LL are applicable only to
some specific concrete compositions. With that in mind, an initial r ~
u ¼ 0: ð4Þ
single-phase model was improved by implementing a separate LL !
where u is the velocity, r is the divergence in a tensor notation,
using a user-defined function; its properties were calculated using
and r  ~
u is the time rate of change of the volume of a moving fluid
Chateau-Ovarlez-Trung and Krieger-Dougherty models. Finally, the
element in an infinitesimally small cell [17]. The divergence of the
applicability of user-defined single-phase model for predicting
velocity characterizes the volume density of the velocity flux arriv-
pressured measured with Sliper is demonstrated for all concrete
ing and leaving a finite volume.
compositions under investigation.
The momentum in the numerical model is conserved according
to Eq. (5):
2. Experimental background
r  ðq~uÞ ¼ r  r þ q~
u~ g ð5Þ
As the first part of this research, extensive laboratory investiga- where ~ g is the gravitational acceleration, q is the density and r is
tions of the pumpability of fresh concrete were conducted using the stress tensor.
Sliper [6]. Measurement of the pipe velocity representing concrete r can be subdivided into normal stresses rii and the shear stres-
discharge rate (Q) and the pressure acting at the piston head (P) ses sij as:
yielded Sliper parameter a, which is related to the yield stress of 0 1 0 1 0 1
the LL and parameter b related to the plastic viscosity of the LL.
rxx sxy sxz p 0 0 rxx þ p sxy sxz
B C B C B
Twelve different concrete mixtures were systematically investi- r ¼ @ syx ryy syz A ¼ @ 0 p 0 A þ @ syx ryy þ p syz C A
gated, with the major focus on the influence of various constituents szx szy rzz 0 0 p szx szy rzz þ p
of concrete on its rheological properties and pumpability. The r ¼ pI þ s
results obtained clearly demonstrated the links between such mix- ð6Þ
ture parameters as water-to-binder ratio, aggregate shape, use of
admixtures, and consistency class on the one hand and the pumpa- where p is an isotropic pressure term, rp is the pressure gradient,
bility of concrete on the other. Fig. 3 gives an overview of the mix- I is the unit dyadic, and s is the shear stress tensor [31] as reported
tures under investigation. All these concretes were also tested in [12] .
using a ConTec Viscometer 5 and the flow table. The evaluation From Eqs. (5) and (6) we obtain Eq. (7):
of the results emphasised the advantages of using Sliper to charac- r  ðq~uÞ ¼ r  s  rp þ q~
u~ g ð7Þ
terise the pumping behaviour of concrete, while a positive correla-
tion was found between the Sliper viscosity parameter b and the For incompressible flow, shear stress can be expressed as:
plastic viscosity m as obtained from the viscometer tests. Finally, r  s ¼ gD~
u ð8Þ
the predicting capability of Sliper was validated under field condi-
tions by measuring full-scale pumping pressure. The details of the
q~ uÞ ¼ rp þ gD~
u  ðr  ~ u þ q~
g ð9Þ
mixtures tested, testing procedures, and the results obtained are
presented and discussed in the previous article [6]. Here g is the dynamic viscosity; see also Section 3.2.

Fig. 3. Overview of concretes investigated experimentally by Mechtcherine et al. [6].


370 V.N. Nerella, V. Mechtcherine / Construction and Building Materials 170 (2018) 366–377

The concrete flow was considered isothermal in accordance To complete the implementation, the critical shear rate c_ c was
with [12,21,24]. assumed to be close to zero, thus prompting the solver to examine
a second case in Eq. (13) immediately after flow initiates, i.e., even
3.2. Implementation of Bingham model at very low shear rates. Low c_ c implies a very high dynamic viscos-
ity g0 as long as c_ 6 c_ c .
Fresh concrete is a heterogeneous material with constituents of
various sizes and shapes. Its rheological behaviour is that of a yield
stress fluid, i.e., it yields non-zero shear stress at a shear rate of 3.3. Geometry, boundary conditions and model parameters
zero. With increasing shear rates, the shear stress increases often
non-linearly, thus accounting for shear thickening or thinning The numerical discretization of the computational domain plays
effects. Hence, concrete can be classified as a non-Newtonian fluid a vital role in the overall performance of the model. The accuracy of
with yield stress. The Hershel-Bulkley model represents this shear the model significantly increases with more detailed, finer dis-
stress-shear rate (s  c_ ) relationship (Eq. (10), Fig. 4a) using three cretization but leads also to drastic increases in computational
parameters: yield stress s0 , plastic viscosity lpl , and power law time. Hence, an optimum is to be strived for, which would repre-
index n. For the sake of simplicity, the description of concrete as sent the physical phenomena sufficiently while being cost effec-
a Newtonian fluid with yield stress is often applied alternatively, tive. The Sliper pipe is axi-symmetric; see Fig. 2. The flow of the
the so-called Bingham plastic model (Eq. (11), Fig. 4b). This model concrete can be assumed to be axi-symmetric in a macroscopic
was proven to represent concrete’s rheological behaviour with perspective. Therefore, instead of the whole pipe geometry, a quar-
adequate accuracy [16,32,33]. ter of it was modelled using the meshing tool ICEM CFD; see Fig. 5.
The modelled geometry is created as an assembly of four surfaces:
s ¼ s0 þ lpl c_ n ð10Þ pipe wall (Sliper pipe), top (top surface of filled concrete), bottom
(piston head of Sliper, where the pressure sensor is located) and
s ¼ s0 þ lpl c_ ð11Þ internal walls, the inner boundaries of the Sliper quadrant under
consideration.
In the present research, the Bingham model was implemented
The boundary conditions applied are a no-slip moving wall for
by adopting the built-in Herschel-Bulkley model, also called the
the pipe wall, symmetry for the internal walls, and a fixed wall for
bi-viscous model [24] of commercial CFD solver ANSYS Fluent
the top and bottom walls. Because of this relatively simple geom-
(Eq. (12)). The bi-viscous model emulates two viscous fluids: one
etry, the use of the single-phase material model, and a structured
with a very high, constant dynamic viscosity g0 and one with grad-
grid, the computational time is relatively low. The boundary layer
ually decreasing dynamic viscosity gi . The change from one beha-
close to the pipe wall is important in investigating the lubricating
viour to another occurs coincidently with the passing of the
layer phenomenon. The fineness of discretization (dimensions of
critical shear rate c_ c : finite elements) plays significant role in numerical simulations.
8   h i
> s c_ c_ Considering this, a numerical refinement near the wall surface
< g0 ¼ c_ 0c 2  c_ c þ k ð2  nÞ þ ðn  1Þ c_ c c_ 6 c_ c
g¼ ð12Þ was employed; see Fig. 5. Instead of creating fine mesh throughout
h in1
>
: g ¼ s0 þ k c_
i c_ c_ c c_ > c_ c the entire modelled domain, which would increase the computa-
tional time drastically, the region close to the pipe wall were mod-
Assigning the power law index n equal to 1, the above equation elled using a finer mesh. Since the observed thickness of
result in Bingham model as long as shear rate is higher than critical lubrication layer Varies between 1 mm and 5 mm (see details in
shear rate, i.e. c_ > c_ c . Section 4.1), the elements size close to the pipe boundary was cho-
8   sen as 0.84 mm. This resulted in the total number of 58,460 ele-
< g ¼ s0 2  c_ þ k c_ 6 c_ c ments in the model.
c_ c c_ c
g¼ 0
ð13Þ
: g ¼ s0 þ k c_ > c_ c Table 1 gives a conceptual physical description of the numerical
i c_ model and experiments. Input and output parameters of the

Fig. 4. Shear stress vs. shear rate curves f, or the a) bi-viscous and b) Bingham models.
V.N. Nerella, V. Mechtcherine / Construction and Building Materials 170 (2018) 366–377 371

Fig. 5. a) Discretization of a Sliper quadrant with b) a detailed view of the optimized mesh.

Table 1
Experimental and numerical model parameters.

Parameters Experiments Numerical Model


Input 1) Concrete composition 1) Rheological properties (from viscometer tests)
2) Velocity of pipe (varies with weights added) 2) Velocity of pipe (wall velocity parameter)
Output 1) Pressure measured with the sensor 1) Pressure as ‘‘measured” by virtual pressure sensor
2) Pumpability curves (Excel) 2) Pumpability curves (Excel)

numerical model were chosen to reflect the corresponding experi- mixtures with low water-binder ratio of 0.3, i.e., Mixtures 5, 7,
mental parameters closely. 10 and 11. The representative results are shown in Fig. 6a on the
Concrete composition and pipe velocity V are the varying example of Mixture 10. In contrast, for mixtures with high
parameters in the Sliper experiments. In other words, different water-binder ratios of 0.45 and 0.6, especially for Mixtures 2 and
rheological properties were attained by mix design, and different 3 (see Fig. 6b), the calculated results showed little agreement with
pipe velocities were obtained by changing the weights attached experimental findings. Correspondingly, the P-Q diagram can be
to the pipe [6]. Similarly, the rheological parameters of the con- roughly subdivided in two areas as showed in Fig. 7.
cretes under investigation, yield stress s0 and plastic viscosity l; The primary reason for the poor agreement between the calcu-
as measured using viscometer and pipe velocity from Sliper tests, lated and measured P-Q curves for concretes with relatively high
were used as input parameters for the numerical model. The out- w/b appears to be the effect of the lubricating layer, which forms
put parameter from the experiments was pressure P measured at the pipe wall and has immense influence on the discharge pres-
by a sensor at the bottom of the Sliper pipe for different discharge sures according to [4,6,10,11,19,34,35]. Since ISPM does not con-
rates Q, so that pumpability P-Q curves could be plotted [6]. In the sider the LL, i.e., constant material properties are assigned
numerical model, pressure acting at the bottom wall was ‘‘mea- throughout the model domain (Sliper pipe), the pumping beha-
sured” by means of a virtual sensor, which calculates it as area- viour of mixtures with relatively high water-to-binder ratios can-
weighted averages. not be predicted well because the rheological properties of the LL
in such mixtures differ very pronouncedly from those of bulk con-
3.4. Results and discussion crete and the thickness of the LL is relatively high in comparison to
concretes with lower w/b. This conclusion is supported by the
Seven concrete mixtures, namely 1, 2, 3, 5, 7, 10 and 11, were results reported by Jo et al. [9], who reported a decrease of LL thick-
chosen from experimental study [6] based on availability of the ness from 5 mm to 1 mm with decreasing water-to-binder ratio.
viscometer results, but for a better overview the notations are used Furthermore, Choi et al. [35] measured increases in LL thickness
unaltered in this paper. Fig. 6 shows measured pressures from Sli- with increasing w/c. Thus, neglecting LL in the ISPM makes the
per experiments and calculated pressures from ISPM simulations model only applicable to concrete with a low w/b.
over corresponding flow rates. Still further, from the fundamentals of the numerical model
Both experimental and numerical results confirm the consensus developed, it can be deduced that the larger the discrepancies in
that with an increase in flow rate the discharge pressure becomes Sliper and viscometer measurements for a concrete mixture,
higher as well, showing a nearly linear P-Q relationship. The pres- the poorer the experimental and numerical correlation (ENC) is.
sure values calculated with ISPM showed good agreement with the Table 2 shows that mixtures with high w/b, i.e., Mixtures 1, 2
Sliper measurements, both qualitatively and quantitatively, for and 3, yielded very low values of Sliper viscosity parameter b,
372 V.N. Nerella, V. Mechtcherine / Construction and Building Materials 170 (2018) 366–377

Fig. 6. a) Comparison of experimental results and corresponding numerical simulations for Mixture 10 (w/b = 0.3) and b) Mixtures 1 and 3 (both with w/b = 0.45).

Fig. 7. Correlation of the results of the simulation comparing ISPM with experimental results; the base figure is adopted from [6]. Note: correlation for Mixture 1 is better
than that for Mixture 2 or Mixture 3; see Discussion.

Table 2
Experimental results from Sliper and viscometer tests, adopted from [6] showing relative viscosities and discrepancy.

Mixture-Nr Sliper Viscometer Sliper Viscometer Discrepancy


b l Rb Rl D
Pas/mm Pas Pas/mm Pas %
Mixture 1 0.59 76 0.51 0.60 17.57
Mixture 2 0.14 38 0.12 0.30 147.73
Mixture 3 0.81 230 0.70 1.83 159.16
Mixture 5 2.3 236 2.00 1.87 6.35
Mixture 7 1.74 164 1.51 1.30 13.98
Mixture 10 1.15 126 1.00 1.00 0.00
Mixture 11 3.1 291 2.70 2.31 14.32

0.59 Pas/mm, 0.14 Pas/mm and 0.81 Pas/mm, respectively, while relative plastic viscosity to compare measurements from various
the corresponding plastic viscosities measured by viscometer were rheometers [36]. By dividing Sliper and viscometer measurements
76 Pas, 38 Pas and 230 Pas, respectively. To understand the rela- of viscosity viz. bn and ln of any composition n with the same of a
tive sensitivity of both Sliper and viscometer to mixture variation, reference composition r, relative viscosities were calculated. In this
a value denoted as ‘discrepancy’ D (Eq. (14)) was calculated. When research, Mixture 10 was chosen as reference considering in the
comparing measurements from different instruments, to avoid the measured spectrum of viscosities its closeness to the medium vis-
common variables such as geometrical factors and test conditions, cosity measurements as well as the low influence of the lubricating
a ‘relative parameter’ can be calculated. Ferraris et al. calculated layer; see also Section 4.2. In the next step, the discrepancy is
V.N. Nerella, V. Mechtcherine / Construction and Building Materials 170 (2018) 366–377 373

quantified by dividing the difference in relative viscosities as region near the pipe wall and assign the corresponding properties.
obtained from Sliper and viscometer measurements with relative This task was accomplished by implementing ‘user defined func-
viscosity obtained by using Sliper Rb. tions’ (UDF) in ANSYS Fluent controlling s0 and l values of the
‘fluid elements’ based on their distance from the pipe wall.
D ¼ ½ðbn =br Þ  ðln =lr Þ=Rb: ð14Þ The UDF approach improves model performance by adding four
The calculated discrepancy values are presented in Table 2 parameters to the initial model: layer thickness TLL, yield stress fac-
as percentages. Very high discrepancies in cases of Mixtures 2 tor sf , viscosity factor lf and gradient factor; see Fig. 8. The yield
and 3 indicate very poor ENC. The negative sign in the discrep- stress and viscosity factors are the ratios of yield stress and plastic
ancy indicates that Sliper relative viscosity parameter showed viscosities of mortar to the same values for concrete. Note that in
higher reduction than that of relative plastic viscosity from the literature the terms ‘dimensionless viscosity’ and ‘dimension-
viscometer. less yield stresses’ or ‘relative viscosity’ and ‘relative yield stress’
It is noteworthy here that Sliper measurements catch the have been used previously [36,38]. However, these terms were
influence of the LL much better than does the viscometer, which introduced as the ratio of higher viscous material to the lower vis-
originates from the devices’ respective geometries and function- cous material, while the present case is the inverse, hence the
ing principles in both experiments. In the viscometer, the whole choice of the new terms. TLL defines the region in which the prop-
concrete is sheared with the help of special ribs designed to pre- erties of fine mortar should be applied. Defining two different sets
vent slippage. Although in Sliper varying from mixture to mix- of material properties in the LL domain on one hand and plug
ture, primarily the material in the vicinity of the pipe wall is domain on the other implies an abrupt local variation of the model
deformed. The discrepancy of mixtures with poor ENC, i.e., 2, 3 parameters, causing numerical instability. Hence, the rheological
and 1 all are negative and high, thus showing higher reductions properties over the TLL are varied with a gradient, having a lower
in relative viscosities measured with Sliper than those with vis- limit at the pipe wall and an upper limit (equal to plug properties)
cometer. Thus, it is evident that among the concretes under con- at the inner boundary of the LL. Feys et al. [39] observed that the
sideration, the behaviours of Mixtures 2 and 3 followed by flow of SCC during pumping can be described as plug flow with a
Mixture 1 were significantly influenced by a prominent LL. Mix- uniform velocity profile and a LL with large velocity gradient. In
ture 1 showed a somewhat better ENC than Mixture 3 even addition, the results from Jo et al. [9] and Choi et al. [40] affirmed
though it had the same w/b. This can be explained by the fact the existence of a large velocity gradient in the vicinity of the pipe
that the yield stress of M1 was with 245 Pa among the lowest wall, thus substantiating the approach chosen for UDFM. It possi-
of all tested concretes, and much lower than 450 Pa and 533 Pa ble to vary properties within the LL using linear, exponential or
measured for M2 and M3, respectively. The low yield stress of any other mathematical function. For the current model, a linear
M1 appears to have resulted in the partial shearing of the plug function was chosen.
during Sliper testing; see [10,37]. In other words, here the shear Determining the thickness and rheological properties of the LL
of the plug affects the measured pressure in addition to the defor- is not trivial. Experimental investigation of LL requires special
mation of the LL. Thus, since ISPM considers only the shear of equipment such as Ultrasonic Velocity Profiler [19] and/or tri-
concrete bulk, M1 yielded better ENC in comparison to M2 and bometer [37]. Such an examination has not been a part of the pre-
M3. This view is also supported by the best-fit results presented ceding experimental work [6]. Therefore, a theoretical approach for
in Section 4.2. estimation of UDFM model parameters sf and lf was followed.
Obviously, the applicability of ISPM is strongly limited due to its There are numerous investigations on predicting yield stress and
not considering the LL. To overcome this limitation, ISPM was plastic viscosity of a suspension based on the corresponding values
improved by implementing a user-defined function as described of the suspending fluid [41–47]. Mahaut et al. [38,45] reported that
in the next section. the yield stress of suspensions depends only on coarse particle con-
centration (suspending phase) and yield stress of the carrying fluid
and is independent of physicochemical interactions. They observed
4. User-defined single-phase model
that elastic modulus-to-concentration relationship followed the
Krieger-Dougherty Law and was in agreement with Chateau et al.
A single-phase model with user-defined functions, hereinafter
[44], deriving the following model:
UDFM, enables the incorporation of the LL’s influence into the ini-
tial single-phase model. Even though it is possible to model the LL vffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi
sc ð/Þ u 1/
and plug as separate phases using a multi-phase model, such an ¼u ð15Þ
approach demands relatively large amounts of computational sc ð0Þ t1  / 2:5/m
/m
resources, and so it increases model complexity and, accordingly,
computational time. In contrast, the single-phase model calcula- According to Krieger-Dougherty [41], the viscosity of suspen-
tion with UDF took approximately the same time as the simula- sions can be related to the coarse particle concentration and vis-
tions using the initial single-phase model. cosity of fluid matrix as:

lc ð/Þ 1
¼ ð16Þ
lc ð0Þ 1  / ½g/m
4.1. Modelling schema
/m
The LL forming during the flow of concrete in a pipe is assumed
to be composed of cement, water, admixtures and fine aggregates; In the above models, sc ð/Þ, lc ð/Þ are the yield stress and viscosity of
therefore, it can be broadly considered to be fine mortar. The the suspension with particle concentration (packing fraction) of /.
absence of coarse aggregates in the fine mortar layer reduces its sc ð0Þ and lc ð0Þ are the yield stress and plastic viscosity of the sus-
yield stress s0 and plastic viscosity l dramatically. From the per- pension with particle concentration of zero; thus, the plastic viscos-
spective of numerical modelling, this means that the fluid elements ity of the fluid matrix, /m is the maximum possible packing fraction
(cells) near the wall have lower yield stress s0 and plastic viscosity and ½g is the intrinsic viscosity [40,48].
l than more distant elements. To assign varying rheological prop- Eqs. (15) and (16) are valid for monodisperse suspensions. For
erties appropriately across the cross-section of Sliper, the numeri- multidisperse suspensions such as concretes, as reported in [40],
cal model must identify the positions of all elements in a specified the Farris [42] model should be employed:
374 V.N. Nerella, V. Mechtcherine / Construction and Building Materials 170 (2018) 366–377

Fig. 8. Sketch of modelled plug and lubricating layers in UDFM including model parameters.

 ½ga /a;m  ½gb /b;m


lc ð/Þ / / and properties of this layer as well as flow characteristics, i.e. plug
¼ 1 a 1 b ð17Þ
lc ð0Þ /a;m /b;m flow or plug-plus-shear flow. Kaplan et al. [10] suggested that con-
crete flows as slip-plus-shear flow after the interface shear stress si
where indices a and b indicate two phases in the suspension, e.g., exceeds the yield stress s0 of concrete. Even in case of low w/b,
fine sand and coarse sand in concrete. common for SCC, presence of LL with partial shearing of plug
Following the above models, Jo et al. [2] deduced for concrete region is apparent. Feys et al. [39] suggested that due to very low
Eqs. (18) and (19): yield stress part of bulk concrete is partially sheared during the
vffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffivffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi pumping of SCC. Research carried out at the TU Dresden [11,37]
sco ð/Þ u 1  /cement u 1  /sand
¼u u independent of this work ascertained this phenomenon very
si ð0Þ t1  /cement 2:5/cement;m t1  /sand 2:5/sand;m clearly with SCC compositions having w/b = 0.29 (w/(c + 0.4fa))
/cement;m /sand;m
vffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi or 0.39 (w/(c + fa)) and resulting in the complete shear of bulk con-
u
u 1  /gravel crete. Nonetheless, if the thickness of the layer is small for the
u
t 2:5/gravel;m ð18Þ tested mixture or the difference in plug and LL properties is rela-
/
1  / gravel tively low, then the simulation results obtained without imple-
gravel;m

menting LL (ISPM) correlate reasonably well with the measured


 2:5/cement;m  2:5/sand;m !2:5/grav el;m results.
lco ð/Þ / /sand /grav el
Disregarding the good correlation of a few mixtures in cases of
¼ 1  cement 1 1
li ð0Þ /cement;m /sand;m /grav el;m
ISPM, all the mixtures under investigation were simulated using
ð19Þ UDFM. In the first step, a sensitivity analysis for the model param-
eters was conducted, documenting the high influence of lf on the
where /cement , /sand and /grav el are the concentrations of cement, sand
calculated pressure. Fig. 9a illustrates the comparative results for
and gravel in cement paste, mortar, and fresh concrete, respec-
the calculated pressure with viscosity factors varying from 0.001
tively; /cement;m , /sand;m and /grav el;m are the corresponding maximum
to 0.2, while layer thickness and yield stress factor were kept con-
concentrations; sco ð0Þ and lco ð0Þ are the plastic viscosity and yield
stant at 5 mm and 0.2, respectively. It was also observed that the
stress of concrete with solid particle concentration /; si ð0Þ and increment in viscosity factor can cause drastic drops of the pres-
li ð0Þ are the plastic viscosity and yield stress of concrete with zero sure at higher discharge rates Q and lower pressure drops at lower
solid particle concentration. discharge rates Q. Similarly, layer thickness TLL also showed consid-
Within the constraints of the work at hand, upon implementa- erable influence on the calculated results. Fig. 9b gives the compar-
tion of LL through UDF, a parametric study was carried out by vary- ative results of measured and calculated pressure values for layer
ing one model parameter while the other two were kept constant. thicknesses of 3, 4 and 5 mm.
The thickness of the LL (TLL) was varied from 1 mm to 5 mm based In contrast, sf variation yielded minimal influence on calculated
on literature and reported expert opinions [9,40]. The viscosity fac-
pressures. Fig. 10 shows the comparative results for yield stress
tor lf was varied from 0.001 to 0.8, while yield stress factor sf was
factors of 0.08, 0.2 and 0.8 with layer thickness of 5 mm and viscos-
varied for a few mixtures from 0.08 to 0.8 and kept constant at ity factors of 0.001 (Fig. 10a) and 0.02 (Fig. 10b). Similar low influ-
sf ¼ 0:2 for the other mixtures; see Section 4.2. Finally, the lf val- ences of yield stress on rheological behaviour of concrete have
ues at which numerical simulations fitted the experimental results been generally reported, especially in cases of high shear flows
best were compared with lf values calculated using Eq. (16) and where the final shape of the fluid body is not of primary concern
considering the LL to be equivalent to the representative mortar. [9,14,24]. Here it may probably originate from the flow character-
It is noteworthy that the rheological properties of the lubrication istics of concrete in the pipe. Prior to a Sliper experiment the for-
layer in pipe flow may not be necessarily equal to those of consti- mation of the LL is ensured with help of pre-strokes [6]. During
tuting mortar belonging to the corresponding concrete. The valid- the progress of a Sliper experiment, due to the presence of LL
ity of this condition depends upon the concrete composition and and ever-increasing pipe velocity, shear rates in the vicinity of
flow characteristics. For flows with a very thin LL, the constituting the pipe wall are relatively high. From the fundamentals of the
of fine mortar consisting of cement paste and very fine sand is Bingham model, it is clear that at higher shear rates the influence
apparently realistic. However, in this first study, for sake of sim- of yield stress is relatively low since the plastic viscosity tends
plicity, the properties of the LL were assumed to be equivalent to towards dynamic viscosity; see also Fig. 4. Considering the low
those of constituting mortars. influence of sf on calculated pressures, its value was set constant
at 0.2 for all the subsequent simulations.
4.2. Results and discussion Table 3 presents the final best-fit parameters from the numeri-
cal simulations as well as lf values calculated using Eq. (16). It is
Though ISPM yielded good correlations for mixtures with low noteworthy that Mixtures 1 and 5 contained round natural quartz
w/b, it does not imply the absence of LL during the pumping of aggregates while all the other mixtures contained crushed basalt
these mixtures. In reality, the existence of LL for all mixtures is aggregates. The intrinsic viscosity ½g for the round and crushed
very probable. However, the crucial point to notice is the thickness aggregates was assumed, broadly based on [40], to be 2.5 and 5,
V.N. Nerella, V. Mechtcherine / Construction and Building Materials 170 (2018) 366–377 375

Fig. 9. Results of simulations using UDFM; comparison of results calculated a) with different viscosity factors (layer thickness 5 mm, yield stress factor 0.2), b) with different
layer thicknesses of 3, 4 and 5 mm (yield stress factor 0.2, viscosity factor 0.001).

Fig. 10. Results of UDFM simulations for different yield stress factors carried out with layer thickness 5 mm and viscosity factor a) 0.001 and b) 0.02.

Table 3
Viscosity factors lf calculated using Eq. (16) and best-fit values from simulations. LL remains constant throughout the pumping period [5,10,35,37]
and the dependency of TLL on concrete composition is becoming
Mixture Eq. (16) Best fit (simulation with experiments)
more and more clear [9,11,37,39,49]. Furthermore, the gradient
1 0.10 0.50/0.40/0.12 for TLL = 5/4/1 mm, respectively of LL properties and, as a consequence, velocity profiles in pipe
2 0.07 0.07 for TLL = 5 mm
flow could also be experimentally deduced or assumed based on
3 0.05 0.02 for TLL = 5 mm
5 0.11 0.07/0.10 for TLL = 1/2 mm, respectively the literature [9,19].
7 0.07 0.80 for TLL = 1 mm Nonetheless, the dependence of any suspension’s rheological
10 0.07 0.07 for TLL = 1 mm properties on their suspending fluid is influenced by the
11 0.07 0.07 for TLL = 1 mm

a) Maximum packing fraction of the particles;


b) Packing fraction of particles or paste volume in the concrete;
respectively. For Mixtures 2, 5, 10 and 11, best-fit values matched c) Particles, shape, size distribution and size range: minimum
positively with viscosity factors calculated/predicted using Eq. and maximum diameter;
(16); for Mixture 3 the match was very close. The only divergent d) Intrinsic viscosity of particles.
case in these results was Mixture 7 for reasons yet to be deter-
mined. Mixture 1 in a peculiar case showed a positive ENC for three In addition, in the case of applying particle concentration mod-
different TLL, viz. 5 mm, 4 mm and 1 mm, each with different lf , els for Sliper model, TLL has also to be considered. Considering the
viz. 0.50, 0.40 and 0.12. The ambiguous results are rather another complexity of this phenomenon, the findings presented in this
upshot of slip-plus-shear flow that occurs in case of low yield study should be taken as preliminary observations on the applica-
stress concrete; see Section 3.4. Nevertheless, acceptable agree- bility of particle concentration models for determining properties
ment of best-fit values and predicted viscosity factors make it pos- of the LL. Further studies are essential to explain how the parame-
sible to estimate lf parameters roughly for further studies, largely ters influence the applicability of such models in determining the
independent of empirical knowledge. In addition, by assigning cal- properties of the LL.
culated sf and lf values, one can determine TLL for a particular Fig. 11 brings together the results of experimental measure-
composition if experimental pressure and flow rate results are ments and of ISPM and UDFM simulations. The results of numerical
available. Also, input parameters of UDFM, that Eq. (16) does not simulation using the calibrated UDFM model showed very good
indicate, are the thickness of LL and the gradient of LL properties. agreement with experimental results for both mixtures. For other
However, as repeatedly proven, once formed, the thickness of the mixtures similar results were obtained as well.
376 V.N. Nerella, V. Mechtcherine / Construction and Building Materials 170 (2018) 366–377

Fig. 11. Experimental and numerical results for a) Mixture 10 having a low water content and b) Mixture 3 with high water content.

The layer thickness in the Sliper experiments appears to vary of Mixture 3, due to a potential experimental error in the viscome-
from 1 mm for mixtures with low water content (low w/b) to 5 ter tests, the torque-rotational speed curve T-N did not fit well with
mm for mixtures with high water content, in agreement with ear- the P-Q curves of the Sliper tests. While for all other mixtures T-N
lier research findings [4,9,10]. The yield stress of LL is 5 times lower curves correlated well with P-Q curves, the T-N curve measured for
than that of concrete based on assumed sf . The plastic viscosity Mixture 3 was very steep, leading to a much higher plastic viscos-
factor, which is the ratio of plastic viscosities of LL to the same of ity measurement from the viscometer [6]. Such a high plastic vis-
concrete, varied from 1/1.25 to 1/20. For Mixtures 1, 2, 10, and cosity, when used as input for numerical model, leads to the
11 the plastic viscosity of the LL is approximately 15 times lower prediction of overly high Sliper pressures. Consequently, best fit
than that of concrete; note the different TLL. values for TLL and lf have to be high and very low, respectively.
It is commonly understood that if a concrete mixture can
develop a thick LL, of which the yield stress and plastic viscosity
are always lower than those of concrete, then the pumping dis- 5. Summary and conclusions
charge pressures are lower in comparison to concrete with a thin
lubrication layer. It is also well known that paste-rich concretes A numerical tool to simulate Sliper tests is highly relevant in
and concretes with low yield stresses are prone to develop a predicting the pumping behaviour of concrete. Such a tool, a virtual
thicker LL. The numerical results and experimental measurements Sliper, was developed using the single fluid CFD method, short
clearly support the earlier knowledge. The mixtures with low ISPM. ISPM predicted the general trend of pressure variation with
water content (low w/b) which are also exhibit higher yield stress respect to the discharge rate correctly and provided acceptable
and plastic viscosity [6] had a best fit TLL of 1 mm indicating very agreement with experimental results in the case of concretes with
moderate LL formation. low water-to-binder ratios. However, since the lubrication layer LL
When looked more specifically, Mixture 2 with a w/b of 0.6 is was not considered, the applicability of ISPM was limited to the
very flowable even without superplasticizer [6], and its plastic vis- scenarios in which formation of LL was not pronounced.
cosity measured by means of viscometer is the lowest among all Thus, an improved single-phase model with User Defined Func-
the compositions tested. Consequently, the pressures P measured tion (UFD) was developed, which can model the lubricating layer.
as a function of flowrate Q for Mixture 2 are significantly lower This approach also makes possible the estimation of the thickness,
than all other tested compositions. The w/b of 0.6 and higher paste yield stress and plastic viscosity of the LL for different concrete
content of Mixture 2 ensured a thicker LL with low plastic viscosity compositions. In the framework of a parameter study performed
in the Sliper experiments, as demonstrated by viscosity parameter using the UDF model it was observed that both the thickness and
b, which was equal to 0.14 Pas/mm; see Table 3 in [6]. Thus, irre- plastic viscosity of the LL have pronounced influences on concrete
spective of the lower l for the plug, high TLL and lower plastic vis- pumpability, while the yield stress parameter showed a negligible
cosity are to be assigned to the LL for simulating high w/b effect. Additionally, the best-fit results suggest that the assumption
mixtures. of a yield stress factor parameter equal to 1/5 is appropriate, while
In contrast, mixtures with the lowest w/b of 0.3 seem to plastic viscosity factor and thickness parameters varied within the
develop a very thin LL. The mixtures 5, 7, 10 and 11, all with lower ranges from 1/1.25 to 1/20 and from 1 to 5 mm, respectively. The
w/b ratio (0.3) exhibited best-fit TLL values of 1 mm. For Mixture 5 parameter study and the subsequent empirical fitting of the calcu-
best-fit lf is 1/10 to 1/14, depending on layer thickness. Mixture 5 lated results indicate the validity of calculating the viscosity of the
has a w/b of 0.3 and is without any secondary cementitious mate- lubricating layer as a function of concrete viscosity using the
rials; it has the lowest water content among all mixtures having Krieger-Dougherty model.
W/B of 0.3. For Mixtures 1 and 5 the plastic viscosity of the LL is The virtual pumpability testing tool developed should enable
approximately 10 times lower than plastic viscosity of concrete. both a more purposeful material design of pumpable concrete
For the best fit of Mixture 3, a 50 times lower plastic viscosity of and estimation of pumping processes. In addition, virtual Sliper
the LL than that of the plug was determined. At first glance, this might become an inherent part of DC approaches where minimal
may lead to false conclusions about Mixture 3’s having a 5 mm involvement of human labour is envisioned with enhanced
thick LL of very low lf , lower than that of Mixture 2. However, machine-material integration. Virtual Sliper can predict the
in the experimental investigations it was observed that in the case required pumping pressures with help of supporting on-line
V.N. Nerella, V. Mechtcherine / Construction and Building Materials 170 (2018) 366–377 377

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