Rama Caesar Dwi W

5008201174

ekstraksi single stage dilakukan larutan 400 kg yang mengandung 35% berat asam asetat sisanya air. Larutan
tersebut dikontakkan dengan 400 kg isopropyl ether murni. Hitung jumlah dan komposisi fase ekstrak dan fase
rafinat dengan menggunakan cara perhitungan dan cara grafik. berapa asam asetat yang tereksttak?

water layer (wt %) isopropyl ether layer (wt %)

acetic acid water isopropyl ether acetic acid water isopropyl ether 1
0 0.988 0.012 0 0.6 0.994
0.9
0.0069 0.981 0.012 0.0018 0.5 0.993
0.0141 0.971 0.015 0.0037 0.7 0.989 0.8
0.0289 0.955 0.016 0.0079 0.8 0.984 0.7
0.0642 0.917 0.019 0.0193 1 0.971 0.6
0.133 0.844 0.023 0.0482 1.9 0.933
0.5
0.255 0.711 0.034 0.114 3.9 0.847
0.367 0.589 0.044 0.216 6.9 0.715 0.4
0.443 0.451 0.106 0.311 10.8 0.581 0.3
0.464 0.371 0.165 0.362 15.1 0.487
0.2

0.1
V2
0
0 0.1 0.2 0.3 0.

1
L0
XA0 0.9
XB0 0.8

0.7
Grafik
0.6
diket XA1 0.25
L0 400 kg XC1 0.03 0.5

Xa0 0.35 XB1 0.72 0.4

V2 400 kg 0.3
Ya2 0 YA1 0.12
0.2
yc2 1 YC1 0.865
YB1 0.015 0.1

0
L0 + V2 = M 0 0.1 0.2 0.3 0.
M 800

L0.Xa0 + V2.ya2 = M.Xam

M.Xam 140
Xam 0.175
Xcm 0.5

Mencari L1 dan V1
L1.XA1 + V1.YA1 = M.Xam
L1.XA1 + V1.YA1 = 140

L1.XC1 + V1.YC1 = M.Xcm

L1.XC1 + V1.YC1 = 400

pers. L1 V2 M
1 0.25 0.12 140
2 0.03 0.865 400

0.03 0.0144 16.8

0.03 0.865 400
----------------------------------------------------
-0.8506 -383.2

V1 450.505525511 kg
L1 343.757347755 kg
0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1

0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1

diketahui dari grafik 1
L0 200 kg/h Xan 0.03 0.9
XA0 0.25 Xbn 0.96
0.8
XB0 0.75 Xcn 0.01
XC0 0 0.7
Vn+1 600 kg/h YA1 0.07 0.6
Yan+1 0 YB1 0.012
0.5
Ycn+1 1 YC1 0.918
Xan 0.03 0.4

0.3

0.2
Neraca massa
L0 + Vn+1 = M 0.1
M 800 kg 0
0 0.1 0.2 0.3 0.4 0.5 0.6

Nerca komponen A 1
L0.XA0 + Vn+1.Yan+1 = M.XAM 0.9
M.Xam 50
0.8
Xam 0.0625
0.7
neraca komponen c 0.6
L0.XC0 + Vn+1.Ycn+1 = M.XCm
0.5
M.XCm 600
XCm 0.75 0.4

0.3

0.2
Mencari Ln dan V1
Ln + V1 = M 0.1
Ln = M - V1 0
0 0.1 0.2 0.3 0.4 0.5 0.6

Ln.XCn + V1.YC1 = M.Xcm

(M-V1)XCn + V1.YC1 = M.XCm
V1.YC1 - V1.XCn = M.XCm - M.XCn mencari jumlah plate
V1(YC1 - XCn) = M(XCm - XCn)
V1 = (M(XCm - XCn)) / (YC1 - XCn)
V1= 651.9824 kg/h
D
Ln= 148.0176 kg/h

1
V5
V4V
3

0.9

0.8
 1
V5
V4V
3
V2 V1
0.9

0.8 M
0.7

0.6

0.5

0.4

0.3

0.2

0.1 L4 L3 L2 L1 L0

0
0 0.1 0.2 0.3 0.4 0.5 0.6

0.9

0.8

0.7

0.6

0.5

0.4

0.3

0.2

0.1

0
0 0.1 0.2 0.3 0.4 0.5 0.6
 L0
XA0
XB0

water layer (wt %) isopropyl ether layer (wt %

acetic acid water isopropyl eacetic acid
0 0.988 0.012 0
0.0069 0.981 0.012 0.0018
0.0141 0.971 0.015 0.0037
0.0289 0.955 0.016 0.0079
0.0642 0.917 0.019 0.0193
0.133 0.844 0.023 0.0482
0.255 0.711 0.034 0.114
0.367 0.589 0.044 0.216
0.443 0.451 0.106 0.311
0.464 0.371 0.165 0.362

0.3 0.4 0.5 0.6 0.7 0.8 0.9 1

0.3 0.4 0.5 0.6 0.7 0.8 0.9 1

 Jumlah stage = 4

0.3 0.4 0.5 0.6 0.7 0.8 0.9 1

0.3 0.4 0.5 0.6 0.7 0.8 0.9 1

 VN+1

XAN

isopropyl ether layer (wt %)

water isopropyl ether
0.6 0.994
0.5 0.993
0.7 0.989
0.8 0.984
1 0.971
1.9 0.933
3.9 0.847
6.9 0.715
10.8 0.581
15.1 0.487