CN 104046968 B (19) he A ROR ARAL g “p (12) ABSA . * (10) BALA CN 104046968 B (45) $8424 A 2016.06.01 (21) HFS 201410311676. 2 (22) BIKA 2014.07.02 (3) SAULA Ep MAE edit 4130079 HAG Ae ADL TEN Dx 152 SPE AE (72) SARA SAL BE (74) SARA ALL A Ee ACE ‘si 42102 RBA TE (61) Int. cl 6230 18/36(2006..01) 0230 18/44(2006. 01) 6236 18/18(2006..01) FER Lo BARAT OAT ARTE G4) BABAR RP EA ER Se A GE ABS BAG TIS Ay BEBE Wik, HT PMC oP a, ‘BCLENS (i, AS A SE IE TA FEMME AE SD BR FFA ER RAL HESSD E) CE EA PY EAT BS AF BH ATE, A SBR TFL BH fs SLAY BAF TE = TR A ABRAM E a SAE th 2 PRS SRT GIRS UE RR. PE fy BL ED WPT BAS EE RF PETE (AL BRE ATES 9 FEL ERE MA HE PE He. ARES IRR TE . 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SHAR s AR 2 AD HE LIB RCL BB AT ABs AN KAS HELO ~30 g/L PQANI~20 g/L Ue TE RAE NDF e/L EFUB ~ 6 mL/L, ANE Fk. 2 AEA BEAR LIARS Fa SERIA EA AY BE eB TT TE: SORE TE Fs RAP RL HOFF Rh AV200 ~300 WERENT fe] ANS—LOmin. 3 ARAB BE AR LITA Fi DEBTS EA A BEBE SH» TURE Ts IR OY 2 25 YES FEE REISE A NTA REI 4 HC BR RA BR AB EE EPI EEE ME AE BIS AE — i 5 Be BY LR ERE» 94 — i TO EA BALE A ITO Fa LB AR FA S70 HE SOA HE EE HE 5 A ARAB ARAL BEAR LSA Fa BEBE A =E A AY GE eB TT HE: SORE LE Ts PBA RD) WOSPPRARDLL.5 ~ 1.7 mL © min MRA EMNES ~ 5 ming 5 ARAB AU BEAR LIPASE Fi PEE EA PN BEE Se 7 Hd: OIE LET? « PR EDD SHAE PPR TELIZL0 ~~ 15 mine 6 RAE LAU BEAR LIT SAR TS Fa SEE EA AY BEE eH FV TE: SORE LE Fs BA RS PEER EAB 12 ~ 14 nme 7 ARAB BEAR LIPASE Fi SE BRE EY BE eB 7 HS ONE AE: PBA BR (OFFTENIA3 ~5 mine BARE BAU BER LTA NY Fa DEST EA FA BEE TT TS HORI T> «FTG A RS) HOD AIZ. OTA TE) AVS~5 min 8 PERM TA) 10 ~ 15minCN 104046968 B hk WB 14K HARRIE REAPS NTE RAT Coon] Az AH] fat Fa SE ETE AES RU» ES BE Dk — SEE AS DS A SEH ihe WRK [0002] PE RBI FS UA BTL PEAS UAL ik PHA Oh OE a SEARED DRONE OR RTS STU HET REO RES SAS HPA SP PT IE AREAIT » BA TTA A ISSR Bs TAT I AR Oe aS RP aS, PAR SERA AEF (STN OG TAG A PIER AY AS EE HBP A AAs SCS HL CARR Te CHT RN 93 — RE Coos] EL Bi» St BRT AYP de AU (PY St AF A & PLP OI RU A HI BY 5 GX a DE ARSE AR 2 EAR eT PH TET Bd TT GB (Oi 45 9S BPE A GS» MEA SUL RT AGP A 5 RL 2 MT A A FALE AVA RTF NAA WD AB DFA Fak a Pe BAT TE SEB RY A SR th CB [0004] LAF SOWA i EAN A OE RT DRS aS BA RT PALI,» SEL LSE fs» Ls PARE RUA» DG Td 9 HA» BO BE DAR EF A tr BB Ze SB ABE A BE FD Se RI BS PA RAL SH ME UAB (He) Be SALE UU (On RF) ZZ SHORE EAE HE OF EVE RUA si PHL,» AG SRY BEB A) A BES PB SOB AE ACE RI 0 FE FE BLS RE Sa HF PE BT AR A BR PE A A +5 BEX RBA [ooos] A Ae 8) PTE ARIA HEE TE fil i Se BE ° Coos) Ay SI HIB 5 Ba AR a aE, AS AR BR ASG SE [0007] SEAL ANE ALE BE RAAT LILA Bae (000s) 1) SERRA Ae IG Ee oe I EO EL BT FE AEA EAE OT IS AL (looos] 2) Aen RAE A = ZEA kB (OE FP PA SEL Sk ES BEAT SE A A MS TB RR WEAEAL RAN LAO.32~ 0.34 mL « min" 3 BE TELE EAM AE Lh GE Is 12h Ht SEE AT EE Ae,» EEA ie Se EA PA DR SA Be TE A Sk 28S HORE EHC RRA yoWes ~ Lawenify3-B. SURE TEASE FP PETER « (ooo) 3) FE AKIRA: HELIA RELLO.32~ 0.34 mL © min HIRE FG BE SW RD Whi AL-2h; ATE] EAE BYE EDIE HN ES A OBE SA IVI: ITI:CN 104046968 B hk WB 2A Coors] af RR HLF RE BEUAL.28 ~ 1.36 mL + min ii. ZE70~80 °C% AEE RAGAN B30 min fii 430-6Omin, MBA LIF ARB Cora] 5 4k RS HEE ULL 28 ~ 1.36 mL + min “HSER. ALTO ~ 80 “CATE Fi CAVE >20 min tis 920 ~ 30 min, AHMAD Fok AZ, TE Be FI BATH Coors) RAT SEH, TRAP EL DH HY FFA DI 200 ~ 300 W, A BANE Th Ay5— 10min. Coon] Eady SEN POTS YA RS eH TD SE PS eee iF PEE PA A, SPAR SLT DUB Ie TLE i SES EM «AA SE RTE Oh 5 FL CEE» 733 BH AE ALLY AES ES TEL A LR ARTA YF FE, SEAL SLA EAMES PATE)» Coors) RAR TRA IRD) A FEET. ~ 1.7 mL + min AYER EAS. ~ 5 mine Coorg) iB Ar ae PARE RRZ) I Ae CRRA TA) ILO ~ 15 mine Coor7] RAT SEH TRA RS NY FEL er RRR P12 ~ 14 nm, Coors) LR AF FRAP , TLR A BRS) HUY SELES RT ts BRAS RR AA 1: il #4 « SEU DGG PF RRR AMT ah I AO eA SE 22 HY BR A CP (NHa)2C14)0.08 ~ 0.09. g/L AP ERARY NasCet07)0.35 ~ 0.4 g/L. ARIF AEC NILOH + HCL) 0.08 ~ 0.09 g/L. Wa T90+2 °C, RMA 20 Sh AREA. 5-LNN AEH. Coors) EB Ar SEH , TRAE SRD he GB AT A RACH 2 FF Rel a Ak ABE FREECNISOs + 6HLO) 20 ~30 g/L.REGRHYCCHsCOONa) 15~20 g/L. TET AY(NaH2PO2) 25~ 30 g/LFLARCCaHG05)4 ~ 6 mL/L HAA SEEK. (0020) iB SEH PAR AES iA BEMT TE] 93 ~ 5 mine [0021] RF Reh AAAS) A EAA IZ, BENE N85 min EH AMF TA Ag10 ~ 15 min. (0022) ERT SH AR ERA EN KE AP 25 OK. AEA 300 BOK. Coo) ESR AF EP, ITAA BR eH Sk FS TS ER eR IT ATURE ARMIMID HEPES HR LIE ASR Fk. [0024] [0025] Coz) Axe HY) aL iL Aa Ws FARA A BBB A EA SLI Ti) ig BE OSS BL Ta SE el EAE A 3 Oe BS EY SD EEE WAY REEL AT BS ME UTODH Aa 5 7S Sh BEE» PALE LO mL min) AES (AEE SE FRET] CfA 204) ASL eI «TT ELAS S AT LP RHE HD RE MA EE ET AEE STP SAGE A HD SRE) SB a 8 WD AE RWC FG PREY BB) AS AS ES HP ELA (0027) RTE RRL FCS HE FT ESE HIE (0028) FINE A (EAL ANN FIT AB BE PT SE» BE SE RAT (SCR eR pL AL Ss A, AER IST IBA BB A TE AE HE RB 4CN 104046968 B hk WB BAT PEEL (0020) 1 WHREMT AEST STN. 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[0039] sie 2 (0040) ERP FE300 MK M28 ROKK ES PEALE min, #R We PESE— SSE AS EERE , CO 5 AG RHE 5 ST EH EE n a 5CN 10404 hk WB WAT BBE FP Sea AAG DR » A FS Rv * A 7 « FS AR ARTA RF ARE, DUANE APR SE PLLA L.GmL © min HARE EAS min REGAL LAO. 33 mL * min’ HORE RE ELE EAM oh, FEPUBRDAL SmL © min OER EAMES min, PEAY ESCA IATA | 20 CHEN) 3 BUE ES SESE EAR, PAW He SHE AE LS SPARES min ARSEAETS FAW EEL 1.36 mL «min RE PACA S30min KAMAL ALAS min, CM omin ETERS min, HATE Bete Ay | 2 tO 3 SAE A AE = A SEE ct FES (041) bSAB FLYER REAR FATS Aa 38 lB «FS RP EAT BHAA GB SE s HAL SP A Ag SE A We CP CNH) 2C 140.09 g/L ATER ARAN (NasCslls0700.34 g/L, ihe Me (NHOOH © HC1)0.09¢/L, RRA F9O+ 2 °C, REMI NTH BEE TERR ALTER HL 12 ~ 1dnme Loose] ie PBR RAR IA LPC AT CA BS «77k CHEE ERCN SOs * 6120) 30 a/ LIRA (CHsCOONa )20 g/L 2K TERRE ANCNaH2PO2) 30 g/L BCFLARCCsHeOs)6mL./L Je HE Bk. [loos] 824 SEE WY RE eA RGIS, Bee EY 120m K FLAG BBR SHEA LS Ta AEE AEE Bh EN OGTR TIE. ATU Oe SAS HT LTE ZB Se SE FA i SES To ERE eA VF CE AE BAS 8 TY BA A EL BE 79500. [0044] zie gals (0045) BURA E300 ALIS BKK ARES ASP ALEES min, YS FATES MASS LEEK, AE SAR REE SLB 2 AB OP ES TT BRL FP Sea AAG I 5 A FN 2 w™ AY 70 «FR ARTA FR EL, aH 5 HH FP PRA. TL. « min "fy HEHE LS EAN min, ERT ALARTAIELO 34 ink © min SSRIS EAS hy SEPAAEDAL .SmL © min HERTS EATS min. ERAN EIEAL TATA LOw t 001) 323 1 ESA AE Ho SP JE AAR ARE AL PALA PERIL FAME BE 2-1 An FE EE ETAL LAO 34 mL © min AS THLEES SEIT Lh AR AEAERO °° PERLE RL ECE BELL 1.300 mL + min PAE, 30min ASF AGES min REE ALBO °F SMI LAE BG CA HELL 1.300 mL © min 5 SAH ZE EAN 20min 5 Bk FI SS SFR AT, ES» PR SPR (loose) LAR LAMAR BRMLHANA LL FRCS AT AC Hl Bs AK Ar BRA ERNE SOs © 6120) 25 2/ Ls REAGAN (CHsCOONa)15. g/L 2K TEBRERENCNaHePO2) 25 g/LXFLARCCaH6Os)5mL/L FEAL BP. 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