HOI KHOA HOC KY THUAT PHAN TicH HOA, LY VA SINH HOC VIET NAM VIETNAM ANALYTICAL SCIENCES SOCIETY ISSN - 0868 - 3224 Tap chi a Ra LU RAS Pee oy mV ier Lel ape} T-23 HA NOLHOI KHKT PHAN TICH HOA, LY VA SINH HQC VIRT NAM TAP CHi PHAN TICH HOA, LY VA SINH HQC - TAP 23, SO 5 (DAC BIET)/2018, Myc Lyc CONTENTS Xe dinh him Iugng Ascorbyl Palmitate trong thy phim chite ning bing phuong phip sic ki ling higu nang cao Determination of Ascorbyl Pamitate in functional food by chromatogephy performance liquid Lieu Thi Huyén Trang, Vit Thi Trang, Lé Thi Thy, Vii Thi Kim Oanh, Lé Thi Hong Héo ‘éc dinh mot s6 chat tgo ngot nhém polyols trong thye phim bing phuong phap dign di mao quan sir dung detector do 46 din khéng tiép xiie (CE-C'D) Determination of polyol sweeteners in food samples by capillary electrophoresis with capacitively coupled contactless conductivity detection (CE-C'D) Pham Thi Thu Phuong, Neuyén Thi Anh Huéng, Lé Thi Hing Hao, Vii Thj Trang, Lé Thj Hong Hao, Nguyén Thi Thanh Bink Xiy dung phuong php xéc dinh céc chat tre ché Phosphodiesterase-5 trén tréi phép trong ché phim dong duge bing sic ky lop mong higu ning cao (HPTLC) Study on determination of synthetic phosphodiesterase-S inhibitors illegal adulterated in herbal products by high performance thin layer chromatography (HPTLC) Dao Thi Cam Minh, Nguyn Thi Thanh Huyén, Pham Thi Thanh Ha, Neuén Thi Kidw Anh Ung dung phuong php sic ky long dinh gid ty 1é cdc thinh phin Flavonoids trong cic ché phim thude va thy phim bio vé ste khée ¢6 chira cao ld bach qua Application of high performance liquid chromatography for the determination of flavonoids components in drugs and supplements consisting of gingko biloba leaft extract Nguyén Thanh Dat, Nguyén Thi Hing Hanh, Bim Thi Th Duong Thé Bic, Hoang Thi Nucong, Lai Thi Phurgng Nghién cru tgo doc t6 rugt ty chu Jogi Cl (secl) tdi 16 hgp trong Escherichia coli Generation of recombinant staphylococcal enterotoxin type CI (sect) in Escherichia col Trén Thi Sao Mai, Pham Tién Diing, Lé Quang Héa Khio sit kha nang dmg dung cia bp kit thir nhanh kiém tra dur Ingng Clenbuterol, Ractopamine vi Salbutamo! trong tht heo ‘Validation of commercial rapid test kits for B-Agonists residues detection in pork Neuyén Hicomg Giang, Ngé Thi Lu, Huinh Khdnh Duy, Lé Hujnh Long, ‘Xe dinh tinh chéng oxy héa ciia m6t sé Anthocyanin va Anthocyanidin bang phyong php do quang sit dung phan img v6i 2,2'-diphenyl-1-picrylhydrazyl (DPPH) Determination of antioxidant activity of Anthocyanidins and Anthocyanins by uv-vis using reaction with 2,2”-diphenyl-I-pierylhydrazyl (DPPH) Va Thi Trang, Lé Thi Héng Hiio, Neuyén Bite Ho, [Nguyen Hai Th, Lé Hoang Ditc, Nguyen Xuan Trung Trang 7 2 28 3317, Pht hign eu vet dng vét trong thye phim chay bing phuong php PCR vi real-time POR 89 Detection of animal traces in vegetarian food using PCR and real-time PCR Nguyén Thi MP Linh, Hé Hujnh Thiey Duong, Ta Diing Khoa 16 Hujnh Thivy Duong 18, ‘Thim dinh phuong phip dinh Iugng Coenzyme Q10 trong thye phim bio vé strc khoe 94 biing she ky long higu ning cao sir dung detector UV-VIS Method validation for quantification of coenzyme QL0 in dietary supplements by high performance liquid chromatography with UV-VIS detection Mac Thi Thanh Hoa, Nguyén Thi Hong Ngoc, Cao Cong Khinh, Lé Thy Héng Héo 19, Phit hign nhanh hin the trong thye phim bing gidy Curcumin 98 Rapid detection for borax in food by curcumin paper Thiiy Chau To, Lé Tht Hupnh Niue 20, Phin tich dur lugng thude tr siu cg clo (OCPs) trong ehé bing phuong phip sic ki 102 hi khdi phd GC/MS Analysis of organochlorine pesticides (OCPs) residues in tea samples by gas chromatography-mass spectroscopy GC/MS Lé Quang Hudng, Nguyén Thi Anh Hudng, Pham Thi Ngoe Mai, Pham Thj Phuong Thao, Vii Dite Nam, Nguyén Quang Trung 21. Nghién eiru xe dinh ham lugng Caffeine trong mau che biing phuong phip Von-ampe 107 hoa tan hap phy sir dung dién eye than guong bién tinh Nafion Determination of caffeine in tea samples by adsorptive stripping voltammetry method using nafion modified glassy carbon electrode Nguyén Thi Kim Thudng, Pham Tudn Anh, Tran Ngoe Minh, Tran Gia Khai 22, Ung dung phong phip ICP-MS nhim bude diu dinh gia mirc 49 6 nhiém mot s6 kim 112 Joai ming trong thye phim gin khu khai thée mé & Thai Neuyén Application of icp-ms to assess the level of heavy metals in food collected at the vicinity of mining areas in Thi Dinh Viet Chién, Lé Théi Binh, Pham Thi Ngoc Mai, Neuyén Thj Anh Hheing, Lé Hitu Tuyén, Nguyén Van Anh, Newyén Xudn Treng. 23, TY Ié nhiém Staphylococcus Aureus trong nhém sin phim thit sir dung trye tiép tai 117 thanh phé H6 Chi Minh nim 2017 ‘The rate of staphylococcus aureus contaimination in ready-to eat (rte) meat in ho chi ‘minh city in 2017 Nguyén Dé Phtic, Nguyén Thi Hoang Oanh 24. Xée dinh déng thoi 19 chit mau céim trong gia vi bing site ky long khdi phd hai lin 121 Simultaneous determination of 19 illegal dyes in spices by liquid chromatography tandem mass spectrometry Nguyén Thi Ha Binh, Trin Cao Son, Pham Thi Minh Hai, Neuyén Thi Kiéu Anh 25, Xie dinh polyphenol trong thye vat bing phuong phap quang hoc str dung thud thir Folin-ciocalteu Determination of polyphenol in plants by photometric method using flin-ciocalteu reagent 16 Thii Binh, Doan Thi Thanh Hicong, Nguyén Thi Anh Huéng, Pham Thi Ngoc Mai 26. Xée dinh ding thoi vitamin K, va vitamin Ko trong thye phim bing phuong phap sic ‘ky long khéi phd LC - MS/MS a Simultaneous determination of vitamin Ky and vitamin Ke in food, functional food. LC-MS/MS Lé Viét Ngdn, Dinh Viet Chién , Lé Thi Thity, Va Thj Trang, Lé Thi He365 (dae bigy/2018 © sinh hoc - Tap 23. Tap chi phim tich Ho, Livi cron nave TH THONG THUC PHAM EAT c PHA’ én toa sogn 1-8-2018 ‘Thiy Chau Téa Lé Thi Hujah Now Trvimg Bai hoc Thit Dau Mot SUMMARY RAPID DETECTION FOR BORAX IN FOOD BY CUR “rapid test for borax in food based on the complex reaction between borale aR ‘condition was manufactured. The rapid test paper for borax (curcumin paper) was; ‘paper sheet in 500 ppm curcumin solution. Detection time for borax of curcus range of 3~ 30 minutes. Detection limit for borax of curcumin paper in food test kit was applied to qualitative and semi-quantitative detection for borax in fo markets in Thu Dau Mot city Keywords: Borax. curcumin, kit, food L.BAT VAN DE Hin the (borax) o6 tic dung sit Khun nbe, Kim ic min ht, 5 ch, i Ia, ca, bi... wild ed biel etiai ace! a eae ete ee Jozi te pm. Hin the Ki vio co thé ngubi $2 ich mdm, phd, th, da iy... py raccdc ee Ee eee, Se cS ba dd yw dng me 3, 4} ré em Sé dong tye phim chia nhiéu hin the = chien phat tridn va anh Ing ti hogt cia tino 3,5} 6 Vitt Nam han ne 06 trong dan myc cée mie ne eg ae ke so 1 bee ong da tin hanh trong phon 8895:2012 [1]. Vige p higa trong. phong/ thicrbong. 4 Pome pa Ph dp thu phan we (U pug pip OV V8 in ti cia dung, dich va curcumin i ll. Ph hip thy phim tie ‘curcumin ‘chuin bi dy dung dich euret pm (pha trong etanol) €6 pH idwing | ~ 14. Ghi phd hip thy dung dich trén trong khoding ‘om dén 700 nm voi mau dung dich so sinh. Két q Hinfareomg tinh) ccho két qua 1g 46 curcumin Ib 500 ppm. ee as hao sit thoi gian ig mat CH sidy chi thi Tim acid HCI Ken ‘sau dé ding dia thay 100 va 0 ppm (miu tring) len ‘miu cia gidy fly curcumin 500 ppm (iy chi thi), tinh chim hai the (borax) I ei chi thi. Quan sit thay chi thi theo thoi gian (Hin 3). ® Clg © 1 qeritit Hin 3. Sie hién miu cia gidy chi thi theo thot Miu si is pa chi thi 43 ko bein ng min gy chit ning a ‘0, mau sic d& quan sit va sy hign Fre en shank hon patie ma girehicning din Be pT gt sa ching ti chon khoing fan hich bop dé phi hign hin the tn s an pais inh tinh: 3 - 30 phat ee w hn the trong mi z sso EE u) va phan tich bin, 1.23. Xie dink 2 gun ie maga "§ Dhdt hién hin the Tim acid HCI Bing 2. 1h dag wink tay 4 orax 50; 20; 10 ppm th hign trong 20 lan th 100%): 5 ppm e6 19 25 pga Gareinh 4.Thang mau bdn dink lieong borax Tired két qué nghién ctu, ching t6i da ché ‘uo diege b6 kit thir nhank han the bao gém iithi curcumin, dung dich dém va ecmg. sirdung dé kiém tra nhanh ham the trong thwe phim (Hinh 5). Fala 1 hes nh Be een SSN ae oe ig gc om Uy a ch ft apn etn i Ab dung thye té te be kit ché tao dge BX: bin dinh Igng ham ¢ ‘hue phim (cha Iya, ch ‘anh ust) dang tw hanh think phd Thi Das MOt cho két qua & Bang 3. Két qua cho thay, ‘hin the duge phat hign trong 03 miu bin léy 6 chg Thi Dau Mét véi ham lugng (bin dinh lugng) trong khoang 50 — 100 ppm vi khong Phat hign han the trong cite mau thye phim. Khe (cha lua, cha ed, phd va banh ut). Bang 3. Kés qué phan tich dinh tinh hin the trong mét s6 mau thc phim Két qua phin sé tich dinh tinh ‘Noi iy miu lugng C— Khong miu hin 6 han the the: CMD ‘Mot 9 3 6 ‘Chg Vinh Son 2 0 3 Chg Phi MY 8 0 8 ‘Khu vue ‘TruimgDaihoc = 3 3 ‘curcumin sci Kt in oy 06 ng00g duge trong. ® ' Spm) hip omnis vice sn vigtgts vn cha. due qua IY 0 ; Fang ve ep dn cit en che vil ge con ngui gin tip db Liicim om hin citw nly cea bop phin | ng ce chit de trong thye PI \VASETD-TPO1/16-18) vi hop phn 2: “Pht trién phurong php nhin dang chit dée trong, thge phim” (MS: VAST.TD.TP02/16-18) thage dr én Khoa hoe vi Cong nghé Trong sm “Nghign ctu xic dinh cite chit de trong bao quin vi ché bién thye phim” (MS: VAST-TD.TP/G-18). Cée tie gid xin cdm on dyin di bd trg vé mt Ki thugt va kinh phi dé thyehign nghign ci ny. ‘TALLIEU THAM KHAO 1. BY Nong nghigp vi Pit tién ming thin (2011), Thing ne vé vige ban hank Dank muc TALLIEU THAM, KaAO 1.B9 Khoa hoe va hati eee aN 2012), Xie dn "ic - Phuong phip dink 95:2012), Ha PHAT HU A IEN NHANH HAN THE TRONG THY PHAM. shude bao ve Hnce vat ehé sie dung, cdm sit di 2, AOAC Official Me and Partitioning with 3, Beatriz Albero, Consuelo and José L. Tadeo (200 Pesticides in Honey by Soli and Gas Chromatog Spectrometry”, J. Agric, pp. 5828-5835. 4, Hanan Abd El-Gawad ( method of organochlorin in waterusing gas cht mass”, Water Science 30, 5. Ligang Chen, Lan Ding , Song, Huarong Zhang, Jian Yulang Wang, Hangi determination of based on. extraction coupled with extraction of high chromatography”, A 589, pp. 239-246, Of the Science of Fo SS.pp. 261.268, opt