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201541511 i (19)? #RAGEUAR A; Vo (12) AREA A (ly amaee : TW 201541511 A al = (43)2012 PAE RBI 104 (2015) #11 AOL a (21) P 3 FAR | 104109219 (22) 358 = RRB 104 (2015) #03 B23 8 (S1)Int. Cl. + HOIL21/306 (2006.01) HOIL21/3065 (2006.01) (30) 4% : 2014/03/31 x8 61/973,077 2014/09/15 xa 14/486,105 (71) aA SARA ELAR GA FR 3] (8B) APPLIED MATERIALS, INC. (US) xB (72)8€88 A + de ait KIM, SUNG JE (KR) + £41848 347K KALITA, LAKSHESWAR (IN) ; 8 4) RAH PAREEK, YOGITA (IN) i -¢/ KADAM, ANKUR (IN) + i 438 45 AABN 3 HEA] ge GORADIA, PRERNA SONTHALIA (IN) + 3 #2 THAKUR, BIPIN (IN) ; #848 @ 3% Jkib ok 4} LUBOMIRSKY, DMITRY (US) (TARE A: Rpt BE PREREE SR PUPA MRK 14 HAKIS HSA (54) 4% 58 TMM LE RR Ca GENERATION OF COMPACT ALUMINA PASSIVATION LAYERS ON ALUMINUM PLASMA EQUIPMENT COMPONENTS (57,482 FSR SE EEL AE BCBG AE de: ART OR RAMEE ED 1 OE He RAE ED 1 GPA + SAAR 10°C 2 TR AEF ESTE IR EAS RN me PAE | B30 SAR + FAL HL PALI | EMT RAED 1 SE HORAEPER 1 SB > A LIES Aa NHJOH PEL BEL PR: RNR —F Ots AAT OREM ED 1 aR ASEH EES Ds ERIE RODEN OAS: ARETE > LAST EH A RES F AlyOy SQ > BLAPIE AlyOy 14 BAY Gi tai HLA AAT Al\Oy SOREL ARSE AY A AL So WE 0.05 fH © A process for generating a compact alumina passivation layer on an aluminum component includes rinsing the component in deionized water for at least one minute, drying it for at least one minute, and exposing it to concentrated nitric acid, at a temperature below 10°C, for one to 30 minutes. The process also includes rinsing the component in deionized water for at least one minute, drying it for at least one minute, and exposing it to NHyOH for one second to one minute. The process further includes rinsing the component in deionized water for at least one minute and drying it for at least one minute. A component for use in a plasma processing system includes an aluminum component coated with an AlyOy film having a thickness of 4 to Sim and a surface roughness less than 0.05j1m greater than a surface roughness of the component without the Al,Oy film 201541511 110 (BOR 155 TW 201541511 A ae BI i ts 120 KS 2 fl Bw enme RA io Sar ‘Rm #1 el 100+ + + ERRB A 10+ + + AGRE 11S + + + hill #a 120+ + + RRA 130+ + + RARE e 135+ ++ Bee 137+ + + eA 139+ + + AE *HRAES 201541511 201541511 mo oe FA fia Be 3K FREGAGHE : 104109219 ries (zo ley 3 FREW : 2015 4 03 A 23 A IPC SNE: vt Lg + (BEAR) (208832) CEREBRAL EE EAC GENERATION OF COMPACT ALUMINA PASSIVATION LAYERS ON ALUMINUM PLASMA EQUIPMENT COMPONENTS, (3c) FO LAE SB BE be EE RR ie: DERT KBE BED 1 PM RRB BEY 1 Sy ME CA BERS 10°C ZIRE Fie BB + SE HS YE Ba TR HS 1 B30 Fe PM NBA: LAM kw FEED IADR RRR BED 1 DM? URGE SB NOP S 1 PE IDS HiuaNRBE-S ais: DKRRFKBREDERED 1 PM URGRDESS e@ D1 5) Sit > FA a a BE BE RO Sit 92 20 2 iE 4 ROK 8 ROK Z ALO, AR A AT sul ALO, i AE AY) 2 TH HE REEL AR AK ALO, MHZ KB fF 69 Ze TB 4H BS BEE DY HS 0.05 TOK ° (0) ‘A process for generating a compact alumina passivation layer on an aluminum component includes rinsing the component in deionized water for at least one minute, drying it for at least one minute, and exposing it to concentrated nitric acid, at a temperature below 10°C, for one to 30 PI-21601 1 201541511 minutes. The process also includes rinsing the component in deionized water for at least one minute, drying it for at least one minute, and exposing it to NH,OH for one second to one minute. The process further includes rinsing the component in deionized water for at least one minute and drying it for at least one minute. A component for use in a plasma processing system includes an aluminum component coated with an Al,Oy film having a thickness of 4 to 8nm and a surface roughness less than 0.05pm greater than a surface roughness of the component without the Al,O, film. (Rem) UBRERRM)] ° 50 1 +) Be (ARREARS) 50 Tf 100 18 i ba BR we 110 FRA 11S EB 120 HAE 130 RAZ ie = 135 #HGE 137 BRR AR 139 QE 140 $2 fill 2 150 Bim GE RE aE 155 A 160 2M 165 Sf 38 He 170 i (ARSE TRE RANA): PI-21601 2 201541511 eS FHS CARB. NUE ERED) CBB) (308E2z) FERRE ES ED LE RE SSE CE GENERATION OF COMPACT ALUMINA PASSIVATION LAYERS ON ALUMINUM PLASMA EQUIPMENT COMPONENTS CABBR FREE SEAISEN [FA] [0001] AMF RARER 2014 9A 1S BRB FE EG OS HF] RHE 14/486,105 WBE RBIS SS Fl) a HE 14/486,105 Al EHH 2014 3 Al Bae z FERRE 61/973,077 MAES bike A RRASKLAAKRS AHWS® - (Bear) [0002] ABBA ABE ME ee A BI A 5 EY BG OAR ERR ME LEER BR FB > LAR AR oe EF WS i eB 8 Yl 3 « (enter) (0003) 4? aS fs oe EA 8 A A +L Bah RELL RFRHNRRRBSRITRETAME PRR RARE HBRENEPMBERHR RRA KEKRTUSPMERRENREE: HME BEB RMARRPRRENM HARARE DRERR Sh PI-21601 1 201541511 ATM BANE PRERBK AES A AR EH Be Be a FB HS HE YB BE + ee AT AE PMRENHREE- LRA: RORGSRALKS- ATMS MRE MMEKRANHHAENAES bRE HRS RANGA SANRARERERNRRE ER (BHAA) [0004] MM — RAG HE OP > LES A LE HL SE (CE Z2NEE EER lOCCHBET HRRERERKRA ABD 30% BE 69 18 BR (HNO3) HE 1 5} GB 30 4) ZH ° (0005) MM — AAG SG Ol op RE ER ER (4B fi AAO, RAY 88 BB E> Ata ALO, MARR 4 KE SRAKZER? A Ara Al.O, SRN RM MEK RA eX Al,O, TAR Z $B BB A BY Ze TH BS BESO HS 0.05 HK © 0006] R—-AM RHO P ALLER ME LEE REAL BALE CREE: CLEFT KPRRBMBEED 17> POM GRAF BD 1B REM 10°C ZU Pie 88 BE RBRR ER BY 30% 2 RM (HNOs) PE 1 B 30 5 > WEE hABEAR FT RKP RRR ED-DM: MRR EE D1 SS Sal DA Be ie $B BB AP RE BE A fe SH (NH,OH) PE 1 HE 1 ft - RES OBERT KP RRBMEED 1 > LAR ACRE BR BE BD 1 5 ae (0007) Hk Hh HS BE HG Oi Be AF Be HS eA OR SAS A AR 2 FD AR ARR EH TS P1-21601 2 201541511 RAAB ABR ZHAR RMT RG SAS FR: MSURAERKERRES - CSR RAA) (0008) ABRRYTSRUS RAPA MRAM BET R- RPRTAARAPHAUN BE RAM UNAS BH: BE BME BT WPBM BAP HRA RE WA EE KIB @n- Rk RTS ASMAAeTRHA—De > ep Se ON ET Rm [0009] #81 A@nRRR-AMR HEM ZCERRERRHE Batt « (0010) 5 2 Gil a Stk FR Ze OE SA ER ER $8 O0 1h FR AS aR HG HE AZ (0011) S3AMRAIBAREMMT STM RARET A $$ (SEM) FR Fr > FW EEL 3} ll SAE — A HP HL BLAS te EE DA is OB US TR BR (HNO) Be BE HY 8 T° [0012] #$4AMRS4BHRENI SR TOPARETA MA(TEM RA MAS MRE R RS DARE AZKEAKARANHBRA ZAHRA HieMe AZ Re AK AB ORR HNO; REURK SIRF LRA HNO; Re [0013] 5A MR 5B Bl ME — A Bi BI He AB Tel BE Be Beg PN A eR AH (69%) HINO Bi BE AY $8 Se HB — FR SEM FAK (0014) $ 6A BS OH MSMR SEW SEM RK SH PI-21601 3 201541511 ARESARBA PS: KERRY) RKR: ARERR Fe RE] FS > DAR Ma St HR AR HNO, Bt 3B AY SA Re (0015) B7HRORE-REREH PD BRERARE ZReRAW RAMEE RBRORARA RARE RAH A AR fit BHT (0016) #% 8AM RH BM AMT S ORM Wi IP > 5 LA Hi HNO; BAe HNO: BBR BBE CREAR EE GR ZER (Sits) (0017) 8 1 MMR T RR -ABA HZ RRBR {100 WERTH AR 100 KHMCRREARS RRA BRERA PNARMMRMA RMS: KAM ZR ‘it Be Uk Rl BA Bt a A PERE BP AS WE) 2 A Ee ELH MH 100 WIR MAS 110> PLAS 110 A AL 11S + ASSP 120. ES 130~ HIE 140 LR MS A Se ES 150 A > BE 130 @i-RSBRAAE 135’ ANH 115 TRC 50me BREA SHURE HAUMHL A) BRERA 13525 DET RB > (SB)RB 155 BRS 139 DRA 137 Thi #5] A SAS EE 130 > BSS E+ BE(RF Gen) 165 HEH WRU S 130 PERE: GAGE 135 HRA - RBS 130 HMR ARMM 137 FRTRARVER 100 CREPE KA HHEMMR 137 TU RRS FL BRM 137° UPS AER/MERKRELS PL-21601 4 201541511 130 oP > ii 3 He Ay FL AB BE AY Fe Hl te Be AE YE HY - (0018) LAS Hl ASTM EB AG 100 HOR AN TEE (Bae JR aF HH 5 LAT A ee PT RRA a SH th OE AO 7 fF ih RAR > GAO HD B/C it BH a S| RS HE WS RIK HR FM A RIE fh OM BO BE ke CPR REF RWS: 2B Be HE ft Le a eS als BAe a th FF BV IR (access port) FST RE R ABE 100 PR EA te fe A AMA Po RT HEE 165 RRM 155 ZH Hh RE HM A 160 R/T A AY BM 170 aS AiG 100° MM AG 100 AMAR ZI > a EK 100 BY Be Hii AS ask 85 1 A 1 SE lS SF + ft HY He tT EE EA Ge 100> HM MA Ris MH BSR RAED BA REARS GERTRERA ARARERREP - B Chih: BS LMRRBRR BRK S 130 PREM F BC at i Bil AY DR SE 4m BY SE Sh ES AT A" Fife (downstream) , Be" lia(remote) ; BH AM > MB — fe se BH eH KERR RERLKEMEHEA-URUETNE - [0019] KHBBNEN DAR SAHRA RRA RE SRREOKRE HRERELARHTEHRREMS TEA AS 3 A aK A HA BB BR SS DOT O° BT ER RA ‘CE (rT AGE SS (A+ ae He Bl ) OR RRARABLE MPRRRARRERRERRL EH RRP ETRONBRRE BA SK TRH NB E PL-21601 5 201541511 Bike (00200) HRERAKRIERRKEHBRNA2Z-BRUER 16 & (NF3) & A(t Hi (N20) MG KZ BRA (SiN) Bs DRE SRA HMRI BCAA 135: ee 130 89 Gl BF ER ARM 137° RR: Be 1698 SE (— ALA ALO, RR HB HSE ALLO; BABB AS ZEB LTRS RAKES BEAR) HAD 8H BB (4 FY eH OR B52 2 BY (HNO) RAY ee (6 98 FB te BR TT DA Wik Te SB ELA Be AS SE HNO; Piz AFi#R- Be HN AKAM NBR BT RE RIEB Bo BE GH RRM - [0021] KAA AI AO EP > AR RAE HNO; fi JE i ME HNO,» 3K EEE EH A AZ ' 7 AR (highly concentrated) ; HNO; K#HA 60 SB%VE 100 RA%*ZBREW HNO, MARA AZ " WB (concentrated) , HNO; (@ @ MiB fa HNO: )AARAA 30BS YE 100 BH %Z i REA HNO; « SABRE YR AE HNO; BRAN Eth (AER HS HNO, ABZ Bie AT AAR fi HNOs WS $8 88 (4 He BH BDL A ALO, > SE ae Rt ES Oh Se) ASE AT Rk OR RR He 38 BB fr 22 Ha 8 YG HNO; iii FF OE RIG HNO, HBA MKD > TRURKERBYW Al RH QEEAS - FWSAZ Al RA)LELRS - Pe A Oey ALO, Be th BA HNO, LHERR/IMA LMR RS BPI REE AT P1-21601 6 201541511 sit HE RBS (bY HO H2O. + HCl» HF » HNO;+HF + H2S80, - HCI+HNO; & NH.OH + [0022] hm T EG HNO, RBS BF fil 5) BR il] HNO 89 8% BE(AD 4HNO; => 2H2O + 4NO2 + O2)> SRAM LOSRMBARANHKRRRERS AM: B SR) ASR FLAY AlxOy FB > BEM ZEA BE Ag WY Ee SP YS Al, Oy ff PE I RKBAS(S B6RKEEW AIO, BH) Lh Wi HNO; RH ZBRATRRE MRNAS HEE BE FE MLA AS HNO, Be i HB AY See fe’ RNLRABBE LAME RR ZRH RB COMB ABRAM RE ALO, MPRA ie HAGTARBRNRBLA KAHAN BARRE Bit MM: Ze HE Hy BK TBR AL Oy HZ 9) Be Pag BB B/E BAY BRR AA: BBW AO, BBNEVRRKEE ME: ARH HHO AA ARM ERR LAHORE (surface finish)» JREN > BASE Al,O, WA > BRB AlxOy BRA RANPRAARRLRBRM ER zw eM DiS 0.05 ARK > HIG HS BE AL UR AR HNO, B42 BH Al,O, 89 RS Hol RRGREH AES Bo A BB BB Sti He BB HF aS RI FZ FB ER LA AG HNO; 38 77 BLE ER EF ALLO, HF (0023) 5 2 Ail Hi St Aa 2 7 9 HE SE BS OB Eb 35 24 (tA AY 7R EAE 200° WEE 200 RAE HIM HAY KOREN BRA BH ZBL ME 200 HRB PI-21601 7 201541511 4 WY SE 7 WG HE BEAL 200 Fir BR ah aD eS AB i A RA A qT MB-—PFMMRPR: (0024) WZ 200 RUA F (DI HERA SE SF (210) > eB HS 92 FAY HZ EA (clean dry air » CDA)+H #7 #2 $8 BB (5 M215) > BHR 210 R 215 HAH: KR-MTRE Be BR 220 oh > HR ek Ae Be ER HNO; 4 AE IS (GIA {GHS 10°C)> R-B ABBE ARMA ARES 60% BY HNO3> LAd§ H.0 HW RZ ALLO, PHBE Rik: RR Rie B ii Pl b> ATU AF hs AI SCI ARAN Al,O, BHRHHRE AMER HARROP HNO CHa BUD RAN ER a HNO; BZ fi RK BR OB i ( Be BBE St HNO, RS 1 B30 (225) BRA HWEH 18 15 PM BBO A-AMF(DDKHEE 1 B30 58 (230) BRAN EAH SHS: PRENSA PERS 1 B 30 8 (235)> BAR M EAA 5S Bt ¢ HNO; BET Rei 4B BRAKE AY Al, Oy? HRM A SB 6 ARK BF 7 @ (65 98 8 89 Ze TH HR BG BE LE BB SB 0.05 HH HK AK > SB EB HF Be BB HS A (BE (NH.OH)E 1 HE 1 5} Bi (240) RANE 1 BS > Lip AE ARAN HNO; > REK NHOW RRSURBHKEF (DDKAKE 1 B 30 (245) RAIN EAH SPH UREN REARER 3 1 B 30 4} 81 (250) RAF M EAM 5S DH [0025] HBMKBHAM A > NE 200HSMERREME AMAAMW HELSARBAHTRRBBAKERAA PL-21601 8 201541511 HMA FRR R BAN -BAIF RB ROM AMT (DI) 2k 38 BE BR BZ HF BY Bz 2E (CDA) HZ BR GR 210 #2 2153 LAR SR (N2) 5G FE th 48 BA G9 1 HE SA FS A 1K zs 1B BY Bz ESR (CDA) 1F fE — Bg 8 HY Be 2 $A (CDA) 82 AR BE 215 » 235 > 250; LAWNS BY 92 18 Wo Bz 2H (CDA)( Be HE fth 48 BA AD 1B TE Se AB) OO DS BR BZ IP BY Bz Ze (CDA) RZ AR BE 215 RIK 235° HS AS & BEF (DI) HEA ZR BHR 225 BK 240> Be 3K HE HL BR On Se HE BEE (DI) 2k Be BK IP AY Be 2B RA (CDA) 8G LUBE HNO; MUL RE ALO, KEY [0026] AF #5 2 8 HE RE HE IMB RAT BE URRAN HNO; C7 RBH OIF > [0027] B3ABRSIBEREMASR TORRES 6 BE (SEM) #8 Fr + DWBA RR TUBB R WG HNO; ba HR AY Al RA 3A AAA LA HNO, Be Hy Al Ze AA BB He LE IR AR HNO; BREA Al RBC 3B i) 3 HB [0028] #4AHRH BARE R SBA aT BA TEM RA RAS NARA EM CREB K AS LW HNO, RE )ARARZ ALRAOA AWA 4A)? 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A RRRA BRERA APOS 1 ME (69%) 89 HNO; HZ SBR HB SA MAME S°C Be) 60°C Hk B WG BA se 77 me SAA SEM RR BP hie bi SERB ROR ER A Al,Oy A ° SEM #8 Fy (KAR IR BS FE (G (visual evaluation) it RR HNO; BHR ERE AMPS RRRRBRZAAL 89 GED We AR AK AR EL BR Ge i > SS SB BAA LL 5 5} Mt B 400 4} SiH A WG AB AN PE TT AL RAY SEM FR > ep TY it iS bh Se RR ee Al, Oy Jif ° SEM §8 fr 4h AR 98 BY OE BE AY ie Of ath ARR HNO] Be BMA A Kih > MSRM RSE ZAG LAH Bi we RAR AR LE BRE ft [0030] % 6A B38 6H SWATH SEM & ioe HS B YB BY BU (BI A HS 10°C) - GE RERA(BIMD S B 25 4 SHH YC He ARF FA (RO 90 150 5} GH)» LA LAIR AG BR 7 YA AE HINO, BBR AAG RA 6AMER OX ATR ZCRHBR Sp + Dk Se Bee FA) Be HE a Be NB th bd FP ZED ROR EP SEAS OR AK RS UT Be BK EF aR AR ‘A Ba BS HR BE HS >t Lk HINO Be BY BR A aR AE HINOs iS FF 68 AR EN oe B89 HR BH BE ° (0031) SS 7 GB GR aa is EF Et OR P1-21601 10 201541511 HZ ARAN RAAB ARM RK Pit 7 a ik RR SEL HNO; ER (PIATRA 10°C) FT RE DR HNO; & HW RAW RHR RT AR 8H > Ti LAY AE HNO; & Fi AE HNO Be Hi a 28 be AR AY eT BS BED th By LE ME HNO; RR A HNOs Be 8 89 oR RA BS) Se Bi HB BS BE bE OR Bk HY Be AA eT HBS BE HS 0.05 Ke Bis KAMA PT RIEHRAHSRKERZ ALOR: A Bk Al,Oy Ji 89 2 Hi #8 BS BE LL Re BE oz BB eT EH DHE 0.05 fh K BY 8B ABE [0032] # 8A BRS 8B KM AF BLL HNO; Rie HNO; HE 2 BME CREB ER BRA ° RB BA HS RRAMRAETREN ARERR RK ELS BR Be EA AY PS EHS All (side), A > BBE HOW BR RBA CREAR KEASER UMAR 8 HARZAA: RE-HRSRAWLA-WEShwWAS BY at > Be Ah SS) SB ew oh EB #9 3000 RMA ERB it HSREKARMWRNT RA BAMA RABIN AZ 200 IBA ALAM RRRKER SERRE RRO RERZA RS BBAHHS AAMT OAH ACNE ‘GF AGE ACE E> FW SU Ze 18 YR WHAKWN SR BES BARR ZAK EMH 25 KB RERRET AD RAAN REA REY BH Se — Bl th BA BEE HY MY BH fl WL Be (side-to-side matching) > (0033) AT LRNS MAM Ol Bakes oe 0B P1-21601 u 201541511 ER MMAR ACHAT ASHEE SRAAU RSD FRR It REMC RAMA NBR UREA Wy SE Sh HEE AR BAA ° RL + DAE Rah a eS eR ‘HZ BR Hil © (0034) a HE — 6 AY BC + RSE BC AR Op OG OF i AR RESON BSB om Tb PR Se a BP RBBMH +A Z— > BT Ar Be ae Be fe ae BR ot ae “OZ WE Pa A A Be Sk A PE A — BR ee EP aj aS SE BL BBE 7} HG KS S| 6 HAY L BR BF IR AY He ASRHERRKRHP SRA (RP CRR)REN QSE-AERE CAMARA RKSGRE) SK 7B Se BP Fir Rt HU +R EE RZ EAR ZHAORER ENS eZ RB LHD LERKPE-SRGSKAAHER {a 9 #6 A (0035) A BWA a A A PR RE A SAE e+ BRB —(a)y » (an), R&T R(the), BREMIETRM: Ah OM SBR’ -RE, Aen LERB ASR REG, GHSR-RSMRAREA REAAMZY-RSPRBZLERM: SS- wa LR BA SR AD FH a SE Fl 8G Bh TAY © @ B(comprise) , H ' (include), SABRHREM Mit ZH RE BERS RR KS AGAR ERE MM — RSH Hh EA aR fF ER + Hh fe Re BE A + P1-21601 2 201541511 Cat] [0036] 50 Tf 100 1 ME He HEH BE 110 ae 11S ASH 120 AST 130 8 #2 135 BHAB 137 BAR 139 QE 140 42 fil 3 150 i GE RE Be 155 AS 160 REM 165 Stee 170 Gf 200 Mi 210 > 230 > 245 DI 2k Yh YE 215» 235 + 250 CDA #238 220 HNO; #4] 225 HNO; #8 240 NH,OH i 40A > 40B Al 42A + 42B Al,Oy 44A > 44B Ir 46A + 46B C Rt (EMR a] RSA (eS POE ABA SERIF EEC) > ESA + SIR REED) (PFI) GRR REM) P1-21601 13 201541511 ard Sl) #6 LAI A DLE — 98 8 a de HB UB gaa: GH 10°C HET HREM RR AGE 30% 62 i HE Z HB Be (HINO, ME 1M 30 BZ AM» 2. RK 1 Ak HR HN RABY ooviy WE ° 3. AUER 1 Ak 2 We ER HNO; AA SC RBG EE 4. MHRA Ak 2Ne RRRBHSRAS: eK SEB fF 2 EK HNO, PS 1 DMS 1S HZ 5. RR 1 AANA L-FAR: HRB ER Bw K HNO; Zl AK MEF (DIK BE HK BS BD a RB BBE 6. WR 1 Ak ZN E-SOS: ERR RER SRR HNO; ZR? KM (DIARRA E - 7. Ra RR 6 Arak NB - SAR) CMR RER SiR HNO; WU AMF (DIAM RBM ZR HK PL-21601 1 201541511 BS NH,OH PS 1 OS 1 DBZ 8. OGRA 7 Arak BAS» Hop ie SB BD fF HB BS NH,OH eS : HRB NHOH PE 13 102 - 9. —-MAR-BRRBAR CRE BS: Me HK 38 G0 (FB i AE 4 RK B 8 RK Z— Al,Oy BM BH Al,O, BRHRAABEMTD AAR Al.O, SRZKBRENKE AHS BEG DD HE 0.05 fK © 10. — #8 Fl LA Ze — $8 OB + b Ee — Be tk 98 SE te aa: RARFAPRRRBREBED IDS: ERASED 1 Be: ERR OCHRE T HMERERB KAA ED 30% i) 2 EZ ARE (HNO:) Ps 1 DME IOH MSH: RART KP RBRARBMABED 1S: SCR IRE SBD 1 hes RBBB NHOW PH IPEIAMZH: REETKPRREABMEBED 1 DM UR Sc RIAD BD 1 Be 11, EHR A 10 Arak ZR HbR HNO, RABY 60rv0y WE: PI-21601 2 201541511 12. MER 10 Arak ZN PR HNGAA SC REE AY i BE 13. 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ROG IR 10 fp at ZAR HS RY BB BD FSR NHWOH LS | i $8 HS NH,OH PS 1 B 10 Wizhi - PI-21601 3 201541511 [Et x G@ae 155 110 fe ee 115 120 Se a if tl BB 1a Alb He aw a ce 6 170 201541511 a 200 210 BRT bE = 1-305} | 218 FRE RI 220 A) 1308388 225 2 30% HNOs #27. 1-305}48 (1-155) 4 oe | Rae E ASR A) T1305 —Y 235 BPH Ze CR 305388 ss 3 2 il 240 NH4OH 332i | wes C-5e) | 248 ART SY 305388 | 250 ROVNZZESRRCIR ~y 1305328 201541511 oH 3A [el 26 3B fal 5B 4A [Bi 28 4B [el 201541511 ALO, fi (ES Et / MREEBIR) 255A fil Al,Oy (eS i / AMREEBIR) 5 5B ee 1 TELE CMREEBIR) FeFfe] 2 FFT CMREEBIR) 201541511 9 HNOs, 28h, RHEHNO:, 2238, ‘eagle Beles 86D Isl - Tens HNO, 218, RAG ffi HNOs, {ICIE, » (Sah, Sn Rah fa NOs, =A OHI Eal - i, aS S38 (i, SE 201541511 0.24 201541511 0 eee eee ee 0 500 1000 1500 2000 2500 3000 3500 Qe fa B 3B 8A [El R pet a | —_ K, t @ (it ae | (al m > wm fi)2 Oe 4 0 san 100 1500 201541511 5 104109219 sk 8-41 # HER 104-07 R21 AE t wh HE Me RR A {tb 7 WM H.02 + HCl+ HF » HNO3+HF + H2SO, + HCI+HNO; & NH,OH [0022] RM ERI Fe HNO; RH B—-BAA GH Fe 7] BR fii] HNOs 64 fF BE (AD 4HNO; => 2H2O + 4NO, + O2)> if —F REAM HONRBBRANKERRERE AM B SARI ALO, Ho PREG HH NR Mb eR Al, Oy FAY BE th ARO BAS (S B 6 RKB AO, HH) LA ihe HNO; RE ZBAA THRO BKRERS HR @ STF AOL PEE HINO, om Tis RB A AY GE + Fo RNLRAARE AMBRE RRCRRREHRER CHM ABRAM MRE ALO, PRAMS R Mist BPARGHDRNERA PARA BPRRAE Bit HM Fe TH EH BK MT BR ALO, PZ 9 fe Fe B/E BR] BRRAKA: BBW ALO, BEN EDMRAKEE > wis ARC ty BF ite Ol HE EE Fe AT Ze SB BB PbO He BY) eB (surface finish) > 7hB0 + #4: 98% Al,O, BM > BRE Al,O, PRA RAW RA BRAMMER 2 SBD ie DHS 0.05 GAR > BiG HS FB EAD YR ME HNO; GE & SE AI.Oy Ft A) AAG SHG). RR RR A AY SE HB Be XE 8H 1 BB FH RE BRA ABE BR > LUGAR HNO; if (7 Bt LTE Be EG ALO, HF (0023) 3% 2 (Hl ah FA 2K 7 9 RE I EE Rt $8 St 1b FE AY 7 WE PE FZ 200 > AZ 200 RAE > BIA HH KERR BT BRA ECHL Ni 200 HRA i PI-21601-A1 7 201541511 % 104109219 4-41 3H 104 07 A 21 aE BAR TEM AAR eR RS 2A 42B PMB 3B 5 RK EEA ALO, fH - [0029] SAM RS SBMA HAE 1 BSH FR he FAW — A5 SEM RA? BMRA AERA RE Le WR AE (69%) HNO; REZ SRM BSA MARKER SC a 60°C 09 Yeh BE HG Hl PY te 77 oe AY 88 AY SEM FR > eH TP TC LP ch SS HS AY Al,Oy & ° SEM §& Hr 4 #8 ie AB FE fei (visual evaluation) ith @ RM HNO, REBAR AMOS RERRBEL GAL AY BE Fl th OR A AR EL BR EAL BB OSB TRU 5 5 HB 400 4 Si) A ZEEE Al RAY SEM RA A HY ee BR SL BAP es Bl HO PL SS a Se eB AlxO, Fit © SEM [i fr (4 #8 oR SY SE GE BE AY ik OE fk te ARR HINOS AER R SEW | A: PERM RRR ZA LH Bil ah 7 Hk BR Lb BRE fit © [0030] 3 6A B38 6H BAAS FA SEM RH ial Sar WS UB BR (BU A BA 10°C) » RFRA (BIA 5S B25 5 BH) BG ER AF FY (Bl) MO 90 150 5} BE)» LA DAR a Be RE HNO, RHLNW ARH KH 6OAMES OH AMAR ZRAUR Ppl Dk Be Bap Pa) Bi HB Se AS te bP ET RAR HEE AHS > UP A RAR Eh BI PAR (Bie FB AY RAR AR BYR CHO Be HY RA EL i HNOs WA 68 OR EF oe BY RAAB H+ (0031) #8 7 MACHA EHARAM RN ERBRAR PI-21601-Al 10

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