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N. Norhadi et al./MJCET Vol. 3 (2) (2020) 51–59
the drying and evaporation rate increase (Akoy, 2014; 2.0 Methodology
Shahari et al., 2015; Dereje and Abera, 2020).
Roughly, a thin-layer describes the condition of the 2.1 Material
samples that are sliced or cut thin according to the
Ripe mangoes used in this experiment were
appropriate size used in an experiment. In an
purchased from a local supermarket in Shah Alam,
engineering context, many thin-layer drying models
Malaysia. It has an average weight of 250 g while the
consist of different formulas. Therefore, the
average weight of each sample was approximately 5 g,
quantitative analysis can be compared to find the best
which was measured using an analytical balance. The
model representing the relevant process (Khodiry et al.,
mangoes were peeled, sliced, and kept in a plastic
2015).
container before being brought to the laboratory. The
Hence, these models can help in scaling up or
sliced sample had an average size of
optimizing the process and controlling the operating
25 mm × 30 mm × 5 mm.
condition of a process (Afolabi et al., 2015) to remain
economical and better quality of products. Thus, it is 2.2 Experimental devices
essential to determine the most suitable condition for
drying. Experimental devices used were laboratory-scale
Tray dryers were composed of more than one tray tray dryer (G.U.N.T. Hamburg CE 130), also known as
while oven only used one tray per time. The food will cabinet dryer and a conventional oven (Misha et al.,
be spread out on the trays and heating medium (hot air) 2013). The tray dryer was composed of compartments
will pass through across them. All the trays must fit for drying chambers, control panel, air heating system,
into the chamber, so there is no 'leaking' in air and electrical supply. The drying chamber has 4 trays
distribution. As the heating medium cross the trays, it with 5 cm spacing between them. The trays have a 30
will set off the conduction process from the heated cm × 40 cm dimension by mean 12 m2 as their surface
trays or surfaces and continue to move uniformly. area. The conventional oven (Memmert UF450)
Uniform airflow distribution over the trays resulted in consists of a control panel, electrical supply, a drying
the drying process excellent efficiency, which ensures chamber with one tray only, and a radiation heating
the desired moisture content of the product is achieved system. The tray dimension is 20 cm × 30 cm resulted
consistently. in the surface area of 6 m2.
The concept of oven dryer is similar to the tray dryer The weight loss of the sample was measured using
in which the sample is spread out on the tray but using an analytical balance (KERN 440-45N) with precision
radiation as its heating medium. It lacks an air velocity of ±0.1 g. The temperature probe and thermometer
controller; thus, the air velocity cannot be controlled were used to measure the surface temperature of the
nor measured. The radiation application formed when product conditions. Anemometer (Extech AN300) was
power is supplied and triggered the source of radiation used to measure the drying air velocity as well as to
to serve the heating medium in the chambers (Rihana determine the relative humidity. A stopwatch was used
et al., 2019). to measure the time set to record the required
Moreover, it is used for low moisture content parameters. These parameters would be recorded every
products to prevent overheating of the particles. This 15 minutes for the effect of drying time and 20 minutes
can happen if it is prolonged even at a temperature near for others.
60°C and resulting in degradation quality of the
2.3 Methods
material. The heat is transferred to the product by
convection and water evaporation is also moved to the 2.3.1 Calibration curve
surrounding by convection way (Guiné, 2018; Rihana
et al., 2019). A calibration curve test was conducted before the
In this current study, tray and oven drying were drying experiment to ensure the precision and accuracy
used to achieve these objectives: (i) to study the effect of the collected data. The main power was switched on,
of drying time, (ii) temperature and air velocity the fan and heater were turned on, then the power
towards drying of mango fruit, to compare the controller was set to Level 1. After 15 minutes,
characteristic of the sample after drying, and (iii) to temperature data at Level 1 was collected.
determine the best drying kinetics model fitted to tray Power was then set to Level 2 for 15 minutes to
and oven dryers by calculation. collect another temperature data. These steps were
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N. Norhadi et al./MJCET Vol. 3 (2) (2020) 51–59
repeated until power of Level 7. Then, the calibration can be described as the ratio of the weight of the water
curve was plotted using temperature against the power content to the weight of dry material. The dry basis is
level (Ismail et al., 2019). chosen for the calculation because the moisture content
percentage is calculated relative to the dry weight of
2.3.2 Effect of drying time the sample. The graph of the moisture content versus
drying time was plotted for each experiment.
The drying processes were conducted at a constant
airflow rate of 1.3 m/s and were tested at temperatures 𝑋𝑋𝑜𝑜 −𝑋𝑋𝑓𝑓
40, 50 and 60°C to investigate the effect of drying time 𝑋𝑋 = (1)
𝑋𝑋𝑓𝑓
on the weight loss of mango samples. The air velocity
where X = moisture content, Xo = initial moisture
was regularly monitored using an anemometer to
content and Xf = final moisture content.
ensure that it is maintained at 1.3 m/s. The sliced
From the moisture content value, the drying rate, V
mango samples were distributed uniformly on the tray
(min-1), can be calculated using Eq. (2). The graph of
and placed in the drying devices to dry. Weight losses
drying rate versus moisture content was plotted for
of the samples were measured every 15 minutes for 3
each experiment to describe the drying curves of this
hours. These steps were repeated at different
process.
temperatures. All experiments were done in triplicate
to get more accurate data. The drying curve was plotted 𝑋𝑋 (𝑡𝑡1 )−𝑋𝑋 (𝑡𝑡2 )
using the drying times against weight loss. The 𝑉𝑉 = (2)
𝑡𝑡1 −𝑡𝑡2
moisture content of the samples was calculated.
where V = drying rate, X = moisture content, t1 = initial
2.3.3 Effect of temperature time and t2 = t1 + ∆ t
Careful measurements were taken to ensure that the These obtained experimental data were then used to
mass of the sample must be constant in all tests and air calculate the dimensionless moisture ratio (MR), which
velocity was maintained at 1.3 m/s. Tests were done at is required by the thin-layer drying models (Shahari
temperatures of 40, 45, 50, 55 and 60 °C. The sample and Hibberd, 2014). The data gained then were fitted
was distributed evenly on the tray and placed into the into three models named Page, Logarithmic and,
devices. The sample weights were measured after Henderson and Pabis models. The thin-layer drying
20 minutes of drying, and the weight losses were models used are shown in Table 3, including the
calculated. All tests were repeated three times for data corresponding constants. The moisture ratio can be
accuracy. A curve was then plotted using temperature calculated using Eq. (3).
against weight loss to determine the effect of
temperature towards the drying process of mango fruit. 𝑀𝑀𝑀𝑀 =
𝑋𝑋𝑡𝑡 −𝑋𝑋𝑒𝑒
(3)
𝑋𝑋𝑜𝑜 −𝑋𝑋𝑒𝑒
2.3.4 Effect of air velocity
where MR = moisture ratio, Xt = moisture content at
The temperature was held constant at 60°C while any time, Xe = equilibrium moisture content and Xo =
varying the air velocities at 0.5, 0.8, 1.0, 1.3 and 1.5 initial moisture content.
m/s to investigate the effect of air velocity to the drying The correlation coefficient (R2) and root mean
of mango samples. Drying time was 20 minutes. A square error (RMSE) are the criteria required to select
curve was plotted using air velocity against weight loss the best model for this process (Shahari et al., 2014;
to determine the effect of air velocity towards the Ismail et al., 2019). The highest R2 and lowest RMSE
drying process of mango fruit. showed the best model to describe the drying curve and
determine the fit's consistency. The higher the value of
2.3.5 Data analysis
R2 and the lower the value of RMSE, the better the
All data obtained from experiments were analysed accuracy of the fit (Chukwunonye et al., 2016; Hada
to obtain drying rate curve. The curve consists of Masayu et al., 2017). R2 and RMSE can be calculated
moisture content as manipulated variable and time as using Eq. (4) and (5), respectively.
the responding variable. The moisture content, X, of the
∑𝑁𝑁 (𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀−𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀)2
sample can be calculated using Equation (1) where X 𝑅𝑅2 = 1 − � ∑𝑖𝑖=1
𝑁𝑁 (𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀−𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀) � (4)
𝑖𝑖=1
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N. Norhadi et al./MJCET Vol. 3 (2) (2020) 51–59
1
1
𝑅𝑅𝑅𝑅𝑅𝑅𝑅𝑅 = [ ∑𝑁𝑁
𝑖𝑖=1(𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀 − 𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀𝑀)]2 (5)
𝑁𝑁
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N. Norhadi et al./MJCET Vol. 3 (2) (2020) 51–59
Fig. 2 Drying curve of mango in tray dryer Fig. 3 Drying curve of mango in oven dryer
Fig. 4 Drying rate curve of mango in tray dryer Fig. 5 Drying rate curve in oven dryer
Fig. 6 Weight loss against temperature in tray dryer and Fig. 7 Weight loss against air velocity in tray dryer
oven dryer
temperatures required a shorter time to dry the sample, oven dryer, and it proposed a better efficiency (Rihana
resulting in a significant extension of drying capacity et al., 2019).
(Akoy, 2014). It can be concluded that the drying rate
of the tray dryer is higher than the oven dryer. This 3.4 Effect of air velocity
matter could be because of the type of heating medium
The effect of air velocity is tested by exposing the
used, or efficiency of the heat transfer rate wherein the
sample to five different air velocities for 20 minutes
tray dryer is said to be transported uniformly through
each at which the mass of the sample is ensured to be
each tray. It is consistent with the results of the
constant. The air velocity is changed by controlling its
previous study that compared three types of dryers,
button at the control panel and measured using the
including tray and oven dryers. The results concluded
anemometer. In this context, it only involved the
that the drying rate of the tray dryer was higher than the
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N. Norhadi et al./MJCET Vol. 3 (2) (2020) 51–59
Table 1: Characteristics of dried mango in tray dryer and oven dryer
Characteristic Tray dryer Oven dryer
40 °C Watery 40 °C Watery
application of tray dryers. It has an open end, while It was found that the tray dryer successfully
oven dryers did not have the air velocity button and in maintained the colour of the mango while the oven
closed containers; thus, air velocity cannot be dryer showed the sign of getting burnt by having a
measured using an anemometer. This experiment is slightly dark colour around the edges of the sample. It
repeated three times for a better result. The results are showed that overheating occurred if drying was
shown in Fig. 7. prolonged at a temperature of about 60 °C and
An increase in air velocity would increase the rate degraded the quality of the material. Furthermore,
of weight loss. This is because higher air velocity observation of both samples’ dryness texture gave
would increase the drying rate and accelerate the results that the sample in the tray dryer was not
evaporation process, which in turn improve the
elimination of moisture content in the sample. Thus, Table 2: Equilibrium moisture content and ratio values
more weight loss obtained in high air velocity Tray dryer Oven dryer
Temp.
conditions over time. The result was consistent with the Time Time
past study and it can be strongly justified that one of (°C) at Xe Xe MR at Xe Xe MR
(min) (min)
the studies also found that high air velocity aid in faster
drying (Misha et al., 2013 ). 40 180 40.57 0.4560 180 57.31 0.6415
3.5 Product characteristics comparison 50 180 39.79 0.4232 180 47.46 0.6250
completely dry as some watery structure still exists in used for calculation of MR. Hence, the value of Xe and
the mango. Otherwise, the sample in the oven dryer is corresponding calculated MR is tabulated in Table 2.
almost dehydrated as no moisture structure detected The moisture ratio decreases as temperature
(Zulkifli et al., 2012). increases. It is affected by the value difference of the
The sample in both dryers shrunk, but the oven moisture content at a particular time. The predicted MR
dryer sample shrunk more when compared to the tray obtained then proceeded with the experimental MR
dryer. The size and shape of the sample changed as calculation. Then, RMSE and R2 were evaluated using
their moisture content faded away over time. The last Eq. (4) and (5), respectively. As the value obtained, the
criterion observed was the smell, which can only be drying process’s characteristics in the tray and oven
experienced during the experiment period. The sample dryer can be determined. For experimental MR, the
in the tray dryer did not encounter any burnt smell; value from mathematical kinetic models is used, and
however, the oven dryer’s sample does have a little previously three model kinetics were chosen. Thus, the
smell of burnt. The smell was probably coming from equations of these three models are listed in Table 3.
the part of the sample that has a slightly dark colour. These equations have some constant parameters;
Overall, the tray dryer is found to be better than the kinetic parameter, k (min-1), a, c and n are the empirical
oven dryer as the quality of the sample is still parameters (dimensionless) (Uribe et al., 2014). The
acceptable. In contrast, in the oven dryer, it degraded parameter values are different according to their
the sample’s quality and appearance only at 60 °C temperatures. As the temperatures were set to 40, 50
which is the highest temperature. and 60 °C, the parameter values were listed based on
those temperatures. Table 4 presents the estimated
3.6 Drying kinetics model parameters of these models at the required condition.
With the information gathered, the MR was
The drying data obtained was converted to a
calculated using those three models. The calculated
dimensionless unit of moisture ratio (MR). Predicted
values of MR, R2 and RMSE are shown in Table 5.
moisture ratio was calculated using Eq. (3) and the
A good model was decided according to the value of
notation required in the equation such as equilibrium
the correlation coefficient (R2) and root means square
moisture content, Xe, was determined using the drying
error (RMSE). The higher the value of R2 and the lower
curve for both dryer types, as previously shown in
the value of RMSE, the more accurate the fit would be.
Fig. 2 and Fig. 3.
The best fit model represents the mango drying
Equilibrium moisture content refers to the point
process's behaviour as well for its control processes. As
where the moisture content was neither gaining nor
calculated in Table 5, the selected model is highlighted
losing the moisture or in simple words the point where
at a specific temperature. For the tray dryer, it shows
the curve is getting constant. For consistency and to be
that the best fit model is Henderson and Pabis model at
sure on the completion of the drying process, the value
60 °C, while for the oven dryer, the best fit model is
of Xe is taken at 180 minutes and Xt at 60 minutes was
Page's model at 40 °C.
Table 4: Parameters of drying models according to temperature (Rayaguru and Routray, 2012)
40 0.004 - - 0.965
60 0.006 - - 0.928
40 0.0032 0.981 - -
60 0.004 0.967 - -
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N. Norhadi et al./MJCET Vol. 3 (2) (2020) 51–59
Table 5: Modelling of moisture ratio, R2 and RMSE values
MR R2 RMSE MR R2 RMSE
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