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Thin-Walled Structures 187 (2023) 110721

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Thin-Walled Structures
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The compressive responses and failure behaviors of composite graded


auxetic re-entrant honeycomb structure
Sheng Yu a , Zhikang Liu a , Xiaoming Cao c , Jiayi Liu a,b ,∗, Wei Huang a , Yangwei Wang d
a
School of Naval Architecture and Ocean Engineering, Huazhong University of Science and Technology, Wuhan 430074, China
b
Hubei Key Laboratory of Naval Architecture and Ocean Engineering Hydrodynamics (HUST), Wuhan 430074, China
c
Wuhan Second Ship Design and Research Institute, Wuhan 430064, China
d
National Key Laboratory of Science and Technology on Materials under Shock and Impact, Beijing 100081, China

ARTICLE INFO ABSTRACT


Keywords: This paper investigated the quasi-static compressive performances and failure behaviors of composite auxetic
Re-entrant honeycomb core re-entrant honeycomb sandwich structure. Three types of auxetic re-entrant honeycomb structures with
Quasi-static compression different gradient configurations were manufactured and tested. The carbon/epoxy prepreg was used to
Energy absorption
fabricated the auxetic re-entrant honeycomb sandwich structure. The reaction force and displacement of the
Negative Poisson’s ratio effect
test fixture were collected by the transducer of the universal testing machine. The compressive processes of
specimens were recorded by high-resolution camera. Combined with the stress–strain curves and deformation
processes of composite structures, the compressive responses and deformation mechanisms was analyzed.
The Poisson’s ratio, energy efficiency and plateau stress of re-entrant honeycomb sandwich structures were
defined and utilized to study the auxetic performance and energy absorption ability. Furthermore, a high-
fidelity numerical model was established and finite element software ABAQUS was used to analyzed the
compressive performances and failure behaviors of composite graded auxetic re-entrant honeycomb structure.
The compressive failure modes of the numerical simulation results were compared with that of the experimental
results, and the numerical simulation results agreed well with the experimental results. The results indicated
that average structure exhibited best energy absorption performance and bidirectionally graded auxetic
honeycomb structure had the best negative Poisson’s ratio performance.

1. Introduction
of sandwich structure drawn more attention in aerospace industry, ma-
rine structure and auto industry. Among them, hexagonal honeycomb
Due to the better specific modulus compared with metallic mate-
sandwich structure was inspired by the honeycomb and exhibited large
rial, composite was extensively used in various industries. Meanwhile, in-plane and out-of-plane stiffness under compressive loads, which
sandwich structure was favored by many scholars owing to its better meant low energy dissipation ability. Based on the geometric features
load-bearing capacity and energy absorption ability compared with of hexagonal honeycomb unit cell, re-entrant honeycomb unit cell
monolithic plate. Therefore, composite sandwich structure was bound was generated by folding the four opposite sides of the hexagonal
to become an irresistible choice for special purpose. Sandwich structure honeycomb inward and utilized to absorb more energy compared with
is a multi-layer structure composed of two high strength outer plates conventional hexagonal honeycomb unit cell.
and a light-weight core [1], and its diversity mainly depends on the Deformation and damage mode, negative Poisson’s ratio (NPR)
variety of material types of panels and cores and the wide range of effect and energy characteristic of auxetic re-entrant honeycomb struc-
structural forms of cores. Sandwich structure showed similar mechani- ture were extensively studied by researchers. Xiao et al. [13] theo-
cal characteristics with I-beam when bearing bending and shear loads, retically and numerically studied the dynamic compression behavior
and it could excessively reduce the weight of the structure. Lattice [2– of the metallic re-entrant honeycomb structure under low and high
4], hexagonal honeycomb [5,6], X-shaped [7–9], Y-shaped [10,11], compressive velocities. The result demonstrated that the stress–strain
double-arrowed corrugated [12] and other cores sandwich structure curve underestimated the effect of the structural NPR effect on the
had been proposed and researched by researchers, and these types of crush stress. Shao et al. [14] studied the compressive performance of
sandwich structures had its own advantages in terms of mechanical metallic gradient auxetic re-entrant honeycomb structure under quasi-
properties. Recently, mechanical performance and energy absorption static and different compressive velocity. Meanwhile, the calculation

∗ Corresponding author at: School of Naval Architecture and Ocean Engineering, Huazhong University of Science and Technology, Wuhan 430074, China.
E-mail address: liujiayi@hust.edu.cn (J. Liu).

https://doi.org/10.1016/j.tws.2023.110721
Received 5 December 2022; Received in revised form 19 February 2023; Accepted 19 March 2023
Available online 31 March 2023
0263-8231/© 2023 Elsevier Ltd. All rights reserved.
S. Yu, Z. Liu, X. Cao et al. Thin-Walled Structures 187 (2023) 110721

method of structural Poisson’s ratio was defined. The result demon- Table 1
Geometric parameters of the re-entrant honeycomb unit cell.
strated that the graded configuration had an apparent effect on the
energy dissipation capacity of the re-entrant honeycomb structure. Xiao Category Value

et al. [15] researched the compressive behaviors of the unidirectionally- Overall height h 16 mm
Half the length of connecting bar l 12 mm
graded and bidirectionally-graded re-entrant honeycomb structures
Inclined angle of inclined bar 𝜃 45◦
under quasi-static compression load. The result indicated that the Length of the horizontal bar b 24 mm
horizontal shrink deformation and gradient distribution had a great
influence on the crush stress and Poisson’s ratio. Dong et al. [16]
researched the effect of the thickness of cell wall on the quasi-static
compressive response by experiment and numerical simulation. The
results demonstrated that deformation modes were highly affected by
the wall thickness. Usta et al. [17] studied the energy absorption
performance and failure modes of polyurethane foam core sandwich
structure and 3D printing auxetic re-entrant honeycomb cores sandwich
structure. The results demonstrated that the re-entrant honeycomb
structure had better resistance to bending deformation due to its NPR
deformation feature. Zhao et al. [18] experimentally and numeri-
cally discussed the compressive performance of aluminum-foam-filled
re-entrant honeycomb structures at different loading directions. The
results indicated that loading direction had a great impact on the
energy absorption of re-entrant honeycomb structures. Usta et al. [19]
studied the anti-impact performance of composite sandwich structure
with auxetic and no-auxetic core. The results indicated that auxetic
configuration had obvious advantages to resist large deformation.
Due to the great designability of re-entrant honeycomb core, the
geometric optimization design of re-entrant honeycomb core was uti-
lized to strengthen the mechanical properties and energy absorption
capacity of the structure by researchers. On the basis of the research
of Xiao et al. [13], Jiang et al. [20] proposed novel concentric aux-
etic re-entrant honeycomb. Due to the existence of plastic hinge and
enhancement of the deformation coupling, this novel structure ex-
Fig. 1. Geometric feature and configuration of composite auxetic re-entrant honeycomb
hibited higher plateau stress and energy absorption compared with
sandwich structure: (a) Geometric feature of unit cell, (b) Configuration of composite
traditional auxetic re-entrant honeycomb structure. Tan et al. [21] auxetic re-entrant honeycomb structure.
studied the energy absorption performance of regular-arranged and
cross-arranged auxetic re-entrant honeycomb structure under quasi-
static and different compressive velocities. The results indicated that
feature of three types of composite re-entrant honeycomb structures
the regular triangle configuration had the better energy dissipation
under quasi-static compressive loads were studied and discussed. Com-
performance due to more plastic hinge compared with hexagon con-
bined with the experiment and numerical calculation, the effect of the
figuration. Tatlier et al. [22] proposed a circle-embedded re-entrant
gradient configuration on the compressive performance of composite
core unit cell and studied the effect of the angle and thickness of
re-entrant honeycomb structure was demonstrated under quasi-static
cell wall on the improvement of the in-plane stiffness. The results
compression.
proved that embedded circle had a positive effect on the bearing
capacity and energy dissipation capacity. Qi et al. [23] theoretically
and numerically researched the compressive performance of 3D re- 2. Model and methodology
entrant honeycomb structure under different compression velocities.
The results indicated that geometric parameter had a great influence 2.1. Structure feature
on the structure performance at different compression velocities. Zhan
et al. [24] manufactured novel re-entrant honeycombs by 3D-printed The unit cell of auxetic re-entrant honeycomb core is presented as
technology and studied their mechanical performances. By refining the shown in Fig. 1(a). The geometric parameter of the auxetic re-entrant
geometric configuration of re-entrant honeycomb unit cell, the defor- honeycomb unit cell are listed in Table 1. The relative density of this
mation mechanism of whole structure was overturned. In addition, the unit cell is able to be calculated by following equation [25].
mechanical performance including strength, stiffness and stability had 2𝑡 𝑏 sin 𝜃
( ℎ + 1)
been extensively improved. 𝜌= ℎ
(1)
In conclude, a great deal of scholars researched the quasi-static 2𝑏 sin 𝜃

− cos 𝜃
and dynamic mechanical performances of metallic auxetic re-entrant
where 𝑡 represents the thickness of the unit cell wall, 𝑏 represents the
honeycomb structure. Moreover, the geometric optimization and para-
length of the platform, ℎ represents the height of the unit cell, and 𝜃
metric design were also applied to enhance the mechanical perfor-
represents the inclined angle.
mance and energy characteristic of metallic auxetic re-entrant honey-
comb structure. Considering the excellent specific strength and specific
modulus of carbon/epoxy and outstanding energy absorption perfor- 2.2. Fabrication processes
mance of re-entrant honeycomb structure, this structure had profound
potential to resist the dynamic loads, such as projectile impact, un- In this paper, the auxetic re-entrant honeycomb structures includes
derwater blast and others. In order to better analyze the dynamic two face sheets and six layer cores as shown in Fig. 1(b). The material
performance of composite re-entrant honeycomb structure, it was nec- used to fabricate the sandwich structure is carbon/epoxy T700 prepreg.
essary to study the quasi-static compression properties of structures. In The material properties of carbon/epoxy prepreg are listed in Table 2.
this paper, the deformation behaviors, energy characteristics and NPR The epoxy resin adhesive was used to bond the re-entrant honeycomb

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Table 2 Table 3
Mechanical properties of carbon/epoxy T700 unidirectional lamina. The ply stacking sequence for different thickness core layers and face sheet.
Mechanical properties Symbol Value Category Stacking sequence Lay-up diagram
Longitudinal modulus (MPa) 𝐸11 100000
Transverse modulus (MPa) 𝐸22 8000
Out-of-plane modulus (MPa) 𝐸33 8000
Poisson’s ratio 𝑣12 , 𝑣13 , 𝑣23 0.21, 0.21, 0.3
Shear modulus (MPa) 𝐺12 , 𝐺13 , 𝐺23 4000, 4000, 3000
Shear strength (MPa) 𝑆12 , 𝑆13 , 𝑆23 104, 104, 86
Longitudinal tensile strength (MPa) 𝑋𝑇 2100
Longitudinal compressive strength (MPa) 𝑋𝐶 700
Transverse tensile strength (MPa) 𝑌𝑇 42
Face sheet [0◦ ∕90◦ ∕0◦ ]𝑠
Transverse compressive strength (MPa) 𝑌𝐶 160
Out-of-plane tensile strength (MPa) 𝑍𝑇 42
Out-of-plane compressive strength (MPa) 𝑍𝐶 160
Density (kg/m3 ) 𝜌 1500

core layers. For the selection of the adhesive, the effect of the thick-
ness, adhesion strength and curing temperature of the adhesive on the
mechanical performance of the structure will be considered. Unlike Thin core layer [0◦ ∕90◦ ]𝑠
the forming method of metal structure, the structure forming in this
paper adopted the hot-pressing mold forming method. The fabrication
processes of composite auxetic re-entrant honeycomb structure were
divided into the following three stages as shown in Fig. 2. (I) The
manufacture processes of core layers were demonstrated as Fig. 2(a).
Above all, on the basis of the designed stack sequence, the prepreg
was cut into strips with certain size and assembled into the moulds
according to the sequence of the mould assembly. The end of the strips Medium thickness core layer [0◦ ∕90◦ ∕0◦ ]𝑠
was embedded into the face sheets during the preparation of the top
and bottom core layers. More elaborate procedures of mould assembly
and prepreg laying were able to obtain from previous literature [26].
Subsequently, the prepreg in the mould was heated and cured at curing
temperature. After curing, the moulds were removed from the re-
entrant core layer. (II) The size of the specimen fabricated from stage
(I) was slightly larger than the design size, and excess part of the
specimen would be cut off along the cutting lines by CNC as shown
in Fig. 2(b). After cutting the redundant part, the rough surface was
polished using the abrasive papers. (III) Due to the complexity of this Thick core layer [(0◦ ∕90◦ )2 ]𝑠
multi-layer sandwich structure, the entire re-entrant honeycomb struc-
ture was manufactured by the secondary forming technique as shown
in Fig. 2(c). The auxetic re-entrant honeycomb core layers were bonded
layer with different graded configuration were listed in Table 3. The
using epoxy resin adhesive and then cured. In this experiment, there are
schematic diagram of the compression experiment was demonstrated
five re-entrant honeycomb cores in each core layer and the surface size
in Fig. 4(d). Considering the quasi-static condition and height of the
of the face sheet is 160 mm × 160 mm. The compressive experiments
specimen, the loading rate of the indenter was set to 1 mm/min, which
are implemented under the guidance of ASTM C365. The compressive
met the requirements of quasi-static loading.
specimens of composite auxetic re-entrant honeycomb structure are
shown in Fig. 3.
2.4. Finite element analysis
2.3. Compression experiment
The compressive responses and failure behaviors of composite aux-
In order to compare the effect of the gradient forms on the mechan- etic re-entrant honeycomb structure were simulated by commercial
ical performance, three types of composite auxetic re-entrant honey- finite element analysis software Abaqus/Explicit. The numerical model
comb sandwich structure were tested as shown in Fig. 4(a)–(c), and of composite auxetic re-entrant honeycomb structure under compres-
they are respectively named as average auxetic honeycomb (AAH), sive loads was created as shown in Fig. 5. In consideration of the
unidirectionally graded auxetic honeycomb (UGAH) and bidirectionally symmetric geometry features and boundary conditions (BCs), symmet-
graded auxetic honeycomb (BGAH). For core layers, the differences rical model of half structure was established and symmetric boundary
among them were stacking sequence, stacking angle and quantity of conditions was applied in the cross profile of the fixtures and re-
stacking layers. Three colors were used to distinguish different cell entrant honeycomb structure. The upper and lower fixtures were set
wall thicknesses in Fig. 4. The thicknesses of cell walls from low to as rigid bodies during analysis. The motion of the upper fixture was
high were respectively 4 plies (green), 6 plies (pink) and 8 plies (gray). consistent with the upper reference point and the lower fixture was
For entire re-entrant honeycomb sandwich structures, UGAH and BGAH constrained in all degree of freedom. Due to the requirement of quasi-
had the same quantity of corresponding core layers with same stacking static simulation, the smooth amplitude load curve was utilized to
sequence, and the difference between them was that the assembly control the displacement of the upper fixture. The constitution model
sequence of the same core layers was diverse. In addition, in order of carbon/epoxy uni-directional fiber-reinforced material was described
to compare the mechanical performance between graded configuration by engineering constant in ABAQUS. Hashin criteria and Yeh criterion
and average configuration, AAH was set as a contrast and researched at were respectively utilized to judge the in-plane material failure be-
approximately the same relative density. The stacking sequences of core havior and interlaminar failure behavior. As the compression process

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Fig. 2. Fabrication processes of composite auxetic re-entrant honeycomb structure: (a) Initial fabrication stage, (b) Precise cutting stage, (c) Secondary curing stage.

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Fig. 3. The compressive specimens of composite auxetic re-entrant honeycomb structure: (a) Outer core layer and face sheet, (b) Middle core layer, (c) Assembly of face sheets
and core layers, (d) Specimens with different graded configuration.

Fig. 4. Schematic diagram for different graded configuration: (a) AAH, (b) UGAH, (c) BGAH, (d) Experimental equipment and compressive test.

went on, the material points of finite element model were progressively define the contact model between core layers and face sheets due to
failure. In this paper, a failure criterion based on the dimensionless there was no debonding failure mode in the experiment. In addition, in
failure strain was applied to assess the material point status. Once order to avoid the result distortion caused by sliding between the face
the failure criterion was satisfied, the stiffness matrix of elements was sheets and fixture, penalty was applied to define the contact behavior
progressively degraded and stress distribution of elements was updated between them. The mesh independence of the numerical model was
at each increment. The running process of user subroutine VUMAT in verified by the convergence of the load–displacement curve in ABAQUS
this simulation was depicted as Fig. 6. Tie constrain was applied to and the mesh size was finally set to 4 mm.

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Fig. 5. Finite element model of composite auxetic re-entrant honeycomb structure under compressive loads.

3. Results and discussion Local densification of the weakest core layers occurred at the nominal
strain of 0.34 and 0.41. As the nominal strain continued to increase
3.1. Deformation and failure modes to 0.49, the four core layers in the middle were almost completely
compacted, and only the thickest core layers continued to deform, and
The deformation modes of composite auxetic re-entrant honeycomb the overall NPR effect were gradually limited. The reasons for these
structures are generally divided into three stages: linear elastic defor- deformation processes were that the deformation capacity of the core
mation stage, plateau stress stage and entire densification stage. The layers connected to the face sheets was limited by the face sheets,
experimental and numerical deformation modes of composite auxetic and the failure and densification of the weaker core layers may lead
re-entrant honeycomb structures under quasi-static compressive loads to the shrinkage deformation of the stronger core layers. When the
were demonstrated in Figs. 7–9. nominal compressive strain reached 0.64, the thickest core layer began
The deformation and failure modes of UGAH were demonstrated as to collapse. The whole core layers were densified at the nominal strain
Fig. 7. At the beginning of compression, an approximately symmetric of 0.74. Due to the geometrical symmetry of BGAH, the experimental
deformation mode was observed for the weakest core layers at the results were in good agreement with the numerical simulation results.
nominal strain of 0.09. Due to NPR effect of re-entrant honeycomb unit The deformation and failure modes of AAH were depicted in Fig. 9.
cells, the first two core layers of UGAH tended to shrink towards the At the beginning of compression, double ‘‘V’’ mode was observed in the
middle at the nominal strain of 0.19. After the collapse and densifica- middle core layers at the nominal strain of 0.09. As the compression
tion of the weakest core layers, the structure showed the deformation process continued, the cells on the left side of the sample showed
mode of double ‘‘V’’ mode at the nominal strain of 0.33. After the overall shrinkage deformation to the middle, while the shrinkage of
compaction of the weakest core layers, the relative thick core layers and the core layer on the right side was not obvious. When the nominal
thickest core layers exhibited the global deformation when the nominal compressive strain reached 0.41, the second and fourth core layers
compressive strain was 0.41. Local densifications of middle core layers showed obvious local compaction of single cells, and the right end of
were observed at the nominal strain of 0.49. As the compression process the middle core layer also showed a tendency to collapse. When the
continued, most of re-entrant honeycomb cores were compacted at the compressive nominal strain reached 0.49, the two middle core layers
nominal strain of 0.63. The reason for these deformation processes were almost completely compacted, and the second and fifth core layers
was that the relative thick core layers (6 plies) was liable to deform were mostly compacted. When the nominal compressive strain reached
compared with the thickness core layers (8 plies) after the densification 0.63, the middle four core layers were almost completely compacted,
of the weakest core layers. The whole structure was almost densified and the auxetic properties of the structure were almost limited. The
at the nominal strain of 0.71. There existed discrepancies between reasons for this deformation process were that the mechanical property
the experimental results and numerical results. The reasons for these of the core layers was same and the shrinkage deformation of the end
phenomenon were that the fiber continuity at the corner would be core layer connected to the panel was limited by the panel compared
inevitably destroyed in the process of sample preparation and failure with the middle core layers. The whole core layers were densified at the
of the weakest core layer had a great influence on the subsequent nominal strain of 0.69. There were some differences in the deformation
deformation mode. process between experiment and simulation due to the inconsistencies
The deformation and failure modes of BGAH were demonstrated as in damage to the left and right cores during compressive experiment.
Fig. 8. The middle core layers deformed symmetrically at the nomi- According to the deformation processes of UGAH, BGAH and AAH
nal strain of 0.13. The middle cells of the thinnest two core layers in Figs. 7–9, the similarity and difference of the deformation mech-
collapsed, and the edge cells contracted and piled up towards the anism of these structure were explicitly observed and summarized.
middle, while the other core layers had no obvious changes. Local Compared with the deformation processes of graded structures and
deformation with ‘X’ mode was presented at the nominal strain of average structure, the deformation mechanism of graded structure was
0.19, and the overall structure began to show an obvious NPR effect. mainly affected by the strength of the core layers, and that of average

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during the compressive processes due to the differences in strength and


buckling stress between core layers with different cell wall thickness.
The stress–strain curve and plateau stress were discussed as follows by
combining the deformation and failure processes.
The relationship between the nominal strain and nominal stress
of UGAH was revealed in Fig. 10. There existed four plateau stresses
during the compressive process and each plateau stress was accom-
panied by stable deformation modes, densification of core layer and
local damage. The corresponding compression situation around the
plateau stresses of UGAH and corresponding compressive strain were
indicated in Fig. 10(i)–(iv). The first plateau stress occurred at the
stable deformation of the weakest core layers. The second plateau stress
emerged at the stable NPR deformation after the local failure of several
re-entrant honeycomb cores. The third plateau stress appeared after
the densification of the weakest core layers, and other core layers
demonstrated a deformation trend towards the center re-entrant hon-
eycomb core of UGAH. The fourth plateau stress occurred in the local
compaction of the relative thick and thickest core layers. The thickest
core layers fractured at the nominal strain of 0.69 and stress–strain
curve experienced obvious downward trend, as shown in Fig. 10(v).
Among them, the first plateau stress of UGAH was approximately 0.07
MPa due to local buckling deformation and material failure after linear
elastic stage. The fluctuation near the plateau stress in the stress–strain
curve was mainly due to the continuous failure of the material. The
maximum of crushing stress was 1.24 MPa with the fracture of the
middle thickest core layer before overall densification. The core layers
of UGAH was densified at the nominal strain of 0.71, as shown in
Fig. 10(vi).
The stress–strain curve and plateau stress of BGAH were demon-
strated, as shown in Fig. 11. The corresponding compression situation
around the plateau stresses of BGAH was indicated in Fig. 11(i)–(v).
There were more plateau stresses compared with that of UGAH. The
first plateau stress of BGAH occurred after the fracture of the middle
weakest core layers. The value of the first plateau stress of BGAH was
0.11 MPa due to the stable deformation of the weakest core layers.
The second plateau stress appeared after densification of the middle
re-entrant honeycomb core and buckling of the re-entrant honeycomb
cores at either end of the weakest core layers. After the densification
of the weakest core layers, the third plateau stress and fourth plateau
Fig. 6. Damage evolution of composite material in Abaqus/Explicit user subroutine stress emerged at the stable deformation of relative thick core layers.
VUMAT. The fifth plateau stress arose at the densification of the relative thick
core layers. The fluctuation around the fifth plateau stress was mainly
due to the fracture of the relative thick core layers. The thickest core
structure was related to the deformation of distal and middle core layer of UGAH fractured at the nominal strain of 0.70 and densified at
layers. For example, the core layers shrank towards the weakest core the nominal strain of 0.74, as shown in Fig. 11(vi).
layers for UGAH and BGAH, and the core layers connected with the face The relationship between the nominal stress and nominal strain of
sheets deformed after the global deformation of middle core layers. AAH were exhibited, as shown in Fig. 12. The corresponding com-
pression situation around the plateau stresses of AAH was indicated in
3.2. Stress–strain curve and plateau stress Fig. 12(i)–(iv). Compared with UGAH and BGAH, the first plateau stress
of AAH underwent a longer nominal strain range due to the identical
Plateau stress generally occurs in the following three deformation mechanical properties of the relative thick core layers. The value of the
circumstances [27]: (I) stable deformation of entire structure after first plateau stress of AAH was approximately 0.36 MPa. The second
elastic phase, (II) stable deformation of entire structure after global plateau stress occurred after densification of the core layers except the
buckling deformation and (III) stable deformation of local substructure core layers that connecting the front face sheets. The fluctuation of the
with slightly large stress fluctuations. The value of the plateau stress stress–strain curve at the second plateau stress attributed to the fracture
and width of the plateau region are utilized to characterize the sta- of the middle core layers. All core layers of AAH were compacted at the
ble load-bearing capacity and energy absorption ability [28–30]. The nominal strain of 0.69, as shown in Fig. 12(iv).
plateau stress can be calculated by the following expression. The comparison of the relationship between the nominal stress and
𝜀 nominal strain of AAH, UGAH and BGAH was demonstrated in Fig. 13.
∫0 𝐷 𝜎(𝜀)𝑑𝜀
𝜎𝑝 = (2) At the stage of the linear elastic stage, AAH had a larger scope in the
𝜀𝐷 stress–strain curve compared with UGAH and BGAH. The reason for this
The stress–strain curve of UGAH, BGAH and AAH sandwich struc- phenomenon was that the fracture and local buckling deformation of
tures were demonstrated as Figs. 10–12. On the basis of the initial the weakest core layers occurred at the initial elastic stage of UGAH and
linear stage of stress–strain curve, Young’s modulus, first plateau stress BGAH. After the linear elastic stage, the stress–strain curves of UGAH,
and densification strain were listed in Table 4. In terms of multi-layer BGAH and AAH all presented a plateau stage. The reasons for this trend
graded structure, several stress plateau regions were explicitly existed was stable deformation of the weakest core layers for UGAH and BGAH.

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Fig. 7. Deformation and failure modes of UGAH at special nominal strains.

However, the reason for this trend was that the stable deformation of 𝜀𝑦 and axial strain 𝜀𝑥 .
the relative thick core layers was observed for AAH. With the gradual 𝜀𝑦
failure and densification of the weakest core layers, the stress level 𝜈=− (3)
𝜀𝑥
of graded structure gradually increased to the same level as that of
For a common material, a shrink deformation tendency along the
AAH. Due to the fracture and densification of the relative thick core
transverse direction will arise if the standard sample under axial tensile
layers, the relationship of the nominal stress and nominal strain of force. This phenomenon is widely known and called as Poisson’s ratio
UGAH, BGAH and AAH had similar changing trends at the nominal effect. According to the definition of Poisson’s ratio in above equation,
strain from 0.35 to 0.6. At the later stages of the compression processes, the value of Poisson’s ratio will remain positive value for conventional
the trend of the stress–strain curve depended on the deformation mode material. However, based on the macroscopic definition of Poisson’s
and thickness of the core layer. In a word, more strain energy was ratio, negative Poisson’s ratio performance can be achieved by special
absorbed by AAH during the quasi-static compression process due to structural design, such as auxetic re-entrant honeycomb structure [30,
the stress–strain curve enclosed a larger area with the 𝑥-axis. 32].
In this study, seven pairs of measuring points of each specimen
with UGAH, BGAH and AAH configuration are adopted in Fig. 7(a)–
3.3. Poisson’s ratio
(c). The horizontal strain and vertical strain of 𝑖th(𝑖 = 1, 2, … , 7) pair of
measuring points are calculated by Eqs. (4)–(5) [13,14].
In general, Poisson’s ratio [31] is originally utilized to characterize
𝜀𝑥𝑖 = (𝐴0 𝐵0 − 𝐴𝑖 𝐵𝑖 )∕𝐴0 𝐵0 (4)
the deformation behavior of a material when the standard samples
under uniaxial force and defined as the ratio of the transverse strain 𝜀𝑦𝑖 = 𝜀𝑛𝑜 min 𝑎𝑙𝑠𝑡𝑟𝑎𝑖𝑛 (5)

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Fig. 8. Deformation and failure modes of BGAH at special nominal strains.

where 𝐴0 𝐵0 represents the original length between two measuring strain of each core layer were depicted, as shown in Fig. 15(a)–(c).
points, and 𝐴𝑖 𝐵𝑖 denotes the distance between two measuring points. Moreover, the results of Poisson’s ratio of core layers with same stack-
The horizontal strain of each core layer is determined by four ing sequences were exhibited, as shown in Fig. 15(d). The gradient
measuring points of distal re-entrant cores of each core layer as shown layer 1, gradient layer 2 and gradient layer 3 represented the weakest
in Fig. 14. The calculation method of horizontal strain of each core core layers, relative thick core layers and the thickest core layers,
layer is defined in Eq. (6). The Poisson’s ratio of a core layer can be respectively.
calculated by averaging the sum of Poisson’s ratios of cores with same The results of the horizontal strain of UGAH were demonstrated in
thickness in Eq. (7) [15]. Fig. 15(a). The horizontal strain of the first two core layers showed
𝜀 an obvious trend of increasing first and then decreasing, and remained
𝑣𝑖 = − 𝑥𝑖 (6)
𝜀𝑦𝑖 unchanged at last. The reason for this phenomenon was that the
weakest core layers were compressed and densified, then these core
1∑ 1∑ 1∑
3 5 7
𝑣𝑈 𝐺−1 = 𝑣𝑖 , 𝑣𝑈 𝐺−2 = 𝑣𝑖 , 𝑣𝑈 𝐺−3 = 𝑣 layers did not deform significantly. The amplitude of the horizontal
3 𝑖=1 3 𝑖=3 3 𝑖=5 𝑖
strain of the second core layer was larger than that of the first core
1∑ 1∑ 1∑
3 5 7
layer due to the core deformation limitation by face sheet and the
𝑣𝐵𝐺−1 = 𝑣𝑖 , 𝑣𝐵𝐺−2 = 𝑣𝑖 , 𝑣𝐵𝐺−3 = 𝑣 (7)
3 𝑖=1 4 𝑖=2 4 𝑖=4 𝑖 coupled deformation between the second core layer and third core
layer. The middle two core layers mainly experienced the trend of
1∑
7
𝑣𝐴𝐴 = 𝑣 first increasing, then decreasing, and finally continuing to increase. The
7 𝑖=1 𝑖 reason for this phenomenon was that the deformation of the second
where the subscript numbers 1, 2, and 3 of Poisson’s ratio v repre- core layer affected the horizontal deformation of the third core layer in
sent respectively the thinnest core layer, relative thick core layer and the early deformation stage. The remain two core layers showed a trend
thickest core layer. of gradual increase with fluctuations. The reason for this phenomenon
In these compressive experiments, the deformation processes of was that the remaining two core layers were the strongest core layers,
UGAH, BGAH and AAH were recorded, and the horizontal strain of each and other core layers could hardly deform horizontally because they
core layer could be calculated by Eq. (5). The curves of the horizontal were compacted entirely.

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S. Yu, Z. Liu, X. Cao et al. Thin-Walled Structures 187 (2023) 110721

Fig. 9. Deformation and failure modes of AAH at special nominal strains.

The horizontal strain versus nominal strain of BGAH were depicted, of UGAH, BGAH and AAH, the third and fourth core layer maintained
as shown in Fig. 15(b). An increasing trend was observed in the larger horizontal strain compared with other core layers.
horizontal strain of whole six core layers and the horizontal strain of In order to compare the NPR feature of core layers with same stack
two core layers with the same cell wall thickness had similar values sequences, the mean values of the Poisson’s ratio of the core layers were
and changing trends. This phenomenon was mainly attributed to the calculated by Eq. (7) and depicted as Fig. 15(d). For composite auxetic
following two reasons. On the one hand, it was due to the symme- re-entrant honeycomb sandwich structure with graded core layers, the
try of the core layer configuration in BGAH as shown in Fig. 4(c). gradient layer 1 with the weakest cell wall exhibited the best NPR effect
Furthermore, the structure exhibited a symmetric deformation during regardless of their structural configuration, and the gradient layer 3
with the thickest cell wall demonstrated the worst. In addition, the
the compressive process. Moreover, the value of the horizontal strain
gradient layer 2 of BGAH revealed the best NPR effect in all gradient
decreased as the increase of the strength of the core layers, which
layers of UGAH, BGAH and AAH.
meant that the weakest core layers had the best NPR performance and
the thickest had the worst one. 3.4. Energy characteristic
The relationship between the horizontal strain and nominal strain
of AAH was depicted, as shown in Fig. 15(c). The horizontal strain Comparing with common structural form, the outstanding advan-
of six core layers of AAH increased first and then decreased. Base tage of NPR structural form lies in the energy absorption during the
on the results of the horizontal strain of core layers of AAH, there deformation process [33,34]. For the sake of characterizing the energy
existed an apparent discrepancy between the middle core layers and absorption mechanism of re-entrant honeycomb structure during the
distal core layers during the compressive process. The horizontal strain quasi-static compressive process, the energy efficiency is defined as the
curves of the two core layers connected to the panel and the four core ratio of the strain energy at specific nominal strain 𝜀 and corresponding
layers in the middle showed coincidence respectively. The reason for nominal stress 𝜎(𝜀) in Eq. (8) [35].
this phenomenon was that the deformation of the end core layers was 𝜀
∫0 𝜎(𝜀)𝑑𝜀
limited by the face sheets. Combined with the horizontal strain curves 𝜂 (𝜀) = (8)
𝜎(𝜀)

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S. Yu, Z. Liu, X. Cao et al. Thin-Walled Structures 187 (2023) 110721

Fig. 10. The stress–strain curve and core densification processes of UGAH.

As the nominal strain increasing, the maximal energy efficiency will and BGAH, the energy efficiency of AAH was larger than that of UGAH
arise when the vertical strain of the specimen reaches the densification and BGAH before the nominal strain reached 0.55. In addition, the
strain 𝜀𝐷 , which is given by Eq. (9). The densification strain can be de- fluctuation of the energy efficiency of graded structures was observed
termined by the maximum of the energy efficiency in experiment [36]. before this nominal strain. The reason for this fluctuation was that
𝑑𝜂 (𝜀) | the sudden failure of the weakest core layers (4 plies) led to the
| =0 (9)
𝑑𝜀 |𝜀=𝜀𝐷 drop of the compressive stress. The maximums of energy efficiency of
Energy efficiency is utilized to compare the energy absorption be- UGAH, BGAH and AAH occurred around the compressive strain of 0.7,
tween different structures, whereas it does not consider the effect of which meant the core layers were densified. Among three structural
structure mass on its energy absorption capacity. In order to highlight configurations, BGAH had the highest energy efficiency with the value
the energy absorption advantage of lightweight material, the specific of 44%. Furthermore, the maximum of the SEA of three types of sand-
energy absorption (SEA) is presented to describe the energy absorption wich structure were listed in Table 4. The results indicated that AAH
performance with unit mass and defined as the ratio of the exter- had an excellent energy absorption capacity with unit mass compared
nal work and total mass [37]. The corresponding expression can be with graded structures. As the reference literature [38] proposed, the
demonstrated from the following equation: maximal plateau stress, densified strain and curve fluctuation were used
𝛿 to evaluate the energy absorption capacity of structures. Therefore, the
∫0 𝐹 (𝛿)𝑑𝛿 𝑊𝑉 fluctuation of the stress–strain curve caused by the failure of the core
𝑆𝐸𝐴(𝛿) = = (10)
𝑀 𝜌 layers may affected the energy absorption capacity of the structure to
where 𝛿 denotes the compressive displacement of the fixture, and 𝑀 a greater extent. In other words, although the graded structure UGAH
denotes the total mass of the specimen. 𝑊𝑉 represents the work of unit and BGAH had greater densification strain, AAH still had better energy
volume, and 𝜌 represents the material density. absorption capacity due to better stability of the stress–strain curve of
The results of the energy efficiency of UGAH, BGAH and AAH AAH. In addition, the ratio of the strain energy of face sheets and core
during compression were depicted in Fig. 16. Compared with UGAH layers at the densification strain were extracted in numerical results

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S. Yu, Z. Liu, X. Cao et al. Thin-Walled Structures 187 (2023) 110721

Fig. 11. The stress–strain curve and core densification processes of BGAH.

and demonstrated in Fig. 17. For graded structures, the increase of the Table 4
thickness of the cell wall would increase the ratio of strain energy under Young’s modulus, plateau stress, densification strain and SEA of UGAH, BGAH and AAH.

quasi-static compression. By observing the strain energy ratio of the UGAH BGAH AAH

face sheets, the face sheets of AAH occupied larger proportion com- Mass/g 653 674 675

pared with that of graded structures, which meant that the existence of Young’s modulus/MPa 3.78 4.08 9.07
weak core layer would limit the deformation of the face sheet. 𝜎P1 0.07 0.11 0.35
𝜎P2 0.14 0.24 1.09
Plateau stress/MPa 𝜎P3 0.38 0.40 –
4. Conclusion 𝜎P4 0.93 0.49 –
𝜎P5 – 0.95 –
Densification strain 0.71 0.74 0.69
In this paper, the quasi-static compression behaviors of composite
Maximal energy efficiency 0.42 0.44 0.38
auxetic re-entrant honeycomb structures were discussed experimentally
SEA/(J/g) 1.23 1.17 1.53
and numerically. The deformation and failure modes, Young’s modulus,
plateau stress, Poisson’s ratio and energy absorption characteristic of
UGAH, BGAH and AAH under compression load were analyzed and
discussed.

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S. Yu, Z. Liu, X. Cao et al. Thin-Walled Structures 187 (2023) 110721

Fig. 12. The stress–strain curve and core densification processes of AAH.

1. The structural configuration had a great effect on the deformation


and failure modes of composite auxetic re-entrant honeycomb struc-
ture. For graded structures UGAH, BGAH and average structure AAH,
the deformation and failure modes of whole structures were largely
affected by the deformation and failure modes of weakest core layers.
2. Combined with the deformation processes and stress–strain curves
of UGAH, BGAH and AAH, Young’s modulus mainly depended on
the performance and deformation mode of the weakest core layers.
The stress of UGAH and BGAH would decrease when the failure of
the weakest core layers occurred and stress of AAH did not decrease
significantly before the failure of core layers.
3. The first plateau stress depended on the mechanical properties of
the weakest core layers. For the graded structures, the second plateau
stress was approximately twice of the first plateau stress. The final
plateau stress of UGAH, BGAH was approximately similar due to the
similar core layer type. In addition, the final plateau stress of AAH
was larger than that of graded structure, which meant the final plateau
stress was related to the global configuration of the structure.
4. By comparing the results of the horizontal strain and Poisson’s
ratio of UGAH, BGAH and AAH, the weakest core layer of graded
structures had the most apparent NPR effect during the compression
Fig. 13. Comparison of the stress–strain curve of composite auxetic re-entrant processes. Among six core layers, the fourth core layer exhibited the
honeycomb structures.
most conspicuous NPR effect regardless of the structural configuration.

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S. Yu, Z. Liu, X. Cao et al. Thin-Walled Structures 187 (2023) 110721

Fig. 14. Distribution schematic diagram of measuring points for different graded configuration: (a) UGAH, (b) BGAH, (c) AAH.

Fig. 15. Horizontal strain: (a) UGAH, (b) BGAH, (c) AAH, (d) Poisson’s ratio.

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S. Yu, Z. Liu, X. Cao et al. Thin-Walled Structures 187 (2023) 110721

Acknowledgments

The present work are supported by National Natural Science Foun-


dation of China under Grant Nos. 12172140 and 12272147 and Na-
tional Key Laboratory Foundation of Science and Technology on Mate-
rials under Shock and Impact under Grant No. WDZC2022-11.

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