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    The document provides NMR spectral data for the analysis of several compounds, including 4-hydroxy propiophenone, flurbiprofen, indomethacin, and 5 unknown compounds labeled A through 9. Key proton signals are reported for characteristic functional groups including methyl, methylene, methoxy, and hydroxyl groups, along with the corresponding peak locations in ppm.

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    Chem.633

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    The document provides NMR spectral data for the analysis of several compounds, including 4-hydroxy propiophenone, flurbiprofen, indomethacin, and 5 unknown compounds labeled A through 9. Key proton signals are reported for characteristic functional groups including methyl, methylene, methoxy, and hydroxyl groups, along with the corresponding peak locations in ppm.

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    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
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    8 views10 pages

    Chem 633

    Uploaded by

    nadaelbeltagy4
    The document provides NMR spectral data for the analysis of several compounds, including 4-hydroxy propiophenone, flurbiprofen, indomethacin, and 5 unknown compounds labeled A through 9. Key proton signals are reported for characteristic functional groups including methyl, methylene, methoxy, and hydroxyl groups, along with the corresponding peak locations in ppm.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    of 10

    ‫نورهان ساىم محمد جنينة‬

    ‫‪Chem.633‬‬
    4-hydroxy propiophenone

    No 4: CH3 appear triplet at 1.1ppm

    No3: CH2 appear quartet 2.9ppm more deshilded than CH3

    No5: OH appear broad signal singlet at about 10.3 ppm

    1
    Flurbiprofen

    No11: CH3 appear douplet at about 1.4ppm

    No 1: OH appear broad singlet at about 12.4ppm

    2
    Indomethacin

    No 1: OH appear broad at about 12.4ppm

    No 11: CH3 appear singlet at about 2.3ppm

    No 9: CH3 appear singlet at about 3.9ppm

    3
    A: CH3 appear triplet at about 1.5ppm

    B: CH2 appear quartet at about 2.6ppm

    4
    CH3 appear triplet at about 1.3ppm

    CH2 appear quartet at about 2.9ppm

    CH3O appear singlet at about 3.8ppm

    5
    CH3 appear triplet at about 1.4ppm

    CH2 appear quartet at about 4ppm deshilded

    6
    CH3 appear singlet of 6 protons at about 2.2ppm

    7
    .

    CH3 appear singlet at about 2.2ppm of 6 protons

    OH appear broad singlet at about 12.6ppm

    8
    .

    CH3 appear triple at about 1.2ppm

    CH2 appear quartet at about 2.5ppm

    OH appear broad singlet at about 6 ppm

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