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International Communications in Heat and Mass Transfer 148 (2023) 107079

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International Communications in Heat and Mass Transfer


journal homepage: www.elsevier.com/locate/ichmt

Temperature variation and influence on local mechanical properties


assessed by nanoindentation in AA6061-AA7075 dissimilar FSW
Madhav Raturi , Anirban Bhattacharya *
Department of Mechanical Engineering, Indian Institute of Technology Patna, Bihar 801106, India

A R T I C L E I N F O A B S T R A C T

Keywords: The present study aims to elucidate the temperature advancement along and transverse to the weld direction
Dissimilar FSW during dissimilar friction stir welding (FSW) between AA6061-T6 and AA7075-T651 with two different tools.
Aluminum alloys Temperature measurements by thermocouples near surface and inside the plates exhibited faster rise in tem­
Temperature
perature for the threaded with intermittent flat faces pin. Experimental measurements and finite element
Nanoindentation
Local properties
simulation shows asymmetric temperature distribution in-and-near the stir zone (SZ) with high temperature
towards retreating side (AA7075) whereas at distant, temperature is slightly higher on advancing side (AA6061)
owing to its higher thermal diffusivity. Additionally, asymmetricity is also noted under shoulder influence re­
gion, as well along the weld line with higher temperature towards the trailing side. The electron back scatter
diffraction analysis shows regions experienced high temperature yielded high angle grain boundaries. Higher
modulus and hardness for AA6061 in the recrystallized region is noted from nanoindentation tests as grain
refinement along with the intense strain and dislocation pileup at grain boundaries prevailed the other
strengthening mechanism. Recrystallized AA7075 within SZ demonstrated reduction in hardness with respect to
base metal due to the dissolution of strengthening precipitates.

1. Introduction modes is often difficult except for predicting it using numerical


modeling. Lambrakos et al. [5] used an inverse problem approach where
Friction stir welding (FSW) in last three decades emerged and thermal fields were experimentally obtained using thermocouples and
established itself as a joining process working below melting tempera­ the same information was used as a constraint to model the problem.
ture of materials to be joined. The process reduces the spread of heat The approach put the constraints on the simulated solutions based on the
affected zone controlling the change in the maiden structure and prop­ values obtained from experiments, improving the correlation of degree
erties of the material to be welded. The FSW technique initially of deformation and actual temperature during FSW. The better accord
employed to join Al alloys is gradually adopted for other materials [1]. between the model and the experimental observations may be improved
For executing FSW, a non-consumable rotating tool with a pin is plunged using volumetric distribution of the heat sources. Amount of the heat
into the workpiece and once the pin is completely plunged and shoulder generation and temperature distribution can also be reasonably esti­
surface touches the workpiece top surface, the tool is allowed to travel mated using process parameters and tool dimensions. Such model can be
along the abutting line in order to obtain the joint [2]. The rotational useful in optimizing the process parameters like rotational speed, tool
motion of the tool along with the traverse movement allows thermally dimensions etc. Also, it helps in improving the temperature field pre­
softened plasticized material to flow around the pin to form the joint. dicting capabilities of the known material and for given weld parameters
The thermal softening occurs due to the combined effect of two heat [6]. Analytical study also helps in identifying the approximate amount
generation mechanisms i.e., by friction and plastic deformation [3]. of heat generated by the different portions (shoulder surface or pin
Further, at the tool-work interface the contact condition could be surface) of the tool. Schmidt et al. [4] presented the analytical modeling
different e.g., sliding, sticking, combined sliding/sticking, and accord­ of heat generation in FSW for cylindrical tool pin with horizontal and
ingly the heat generation varies [4]. However, the exact method to conical shoulder surfaces considering different contact conditions at
derive the proportionality of heat produced by various mechanisms/ tool-workpiece interface. Gadakh and Adepu [7] proposed analytical

* Corresponding author.
E-mail address: abhatta@iitp.ac.in (A. Bhattacharya).

https://doi.org/10.1016/j.icheatmasstransfer.2023.107079

Available online 6 October 2023


0735-1933/© 2023 Elsevier Ltd. All rights reserved.
M. Raturi and A. Bhattacharya International Communications in Heat and Mass Transfer 148 (2023) 107079

expressions for cylindrical taper tool pin and reported less temperature formability and improved corrosion resistance make the alloy favorable
compared to straight cylindrical tool pin. Computational fluid dynamics in aerospace and marine applications with fuel-efficient structural de­
based thermo-mechanical model is also used to predict heat generation signs. Precipitation hardened 7xxx alloy with better high strength and
and distribution during FSW [8,9]. There have been efforts to establish scratch resistance make it suitable for stringer and spars in aerospace
analytical relations to correlate torque to temperature based on nu­ industries with minimal repair. Dissimilar joining of different alloys
merical results. The influence of the tool dimensions, rotational speed, appeared as a need to fabricate hybrid structures for weight reduction
weld speed and base material thickness on the stirring volume, welding and tailored properties [29,30]. During the dissimilar FSW, for an
heat input and torque were taken into account. The influence on torque effective material mixing and better joint quality, the AA6061-T6 is
was noticeable when large shoulder tools were used and/or in thick placed on the advancing side (AS) and AA7075-T561 on the retreating
plates welding [10]. side (RS), as noted in reported literatures [18,19,31–33]. Constant
The amount of heat produced and degree of deformation influences process parameters i.e., 1200 rpm tool rotational speed and 98 mm/min
the metallurgy and structure of the obtained joint. Thus, many studies weld speed are maintained to perform the dissimilar FSW of AA6061 and
focused on finite element analysis adopting various approaches to pre­ AA7075 following the arrangement as schematically shown in Fig. 1(a).
dict the temperature during similar FSW of aluminum alloys e.g. The tools used are made from H13 die steel of shoulder diameter of
AA6061 alloy [8,9,11–16], AA7075 [17]. As well, some of these studies 20 mm and pin having profile of threaded with intermittent flat faces
also conducted experimental measurements of temperatures (TIF) or plain cylindrical. TIF pin profile contains alternate threaded and
[9,11–14,17] for the purpose of validation of predicted temperatures flat faces, prepared first by a right-hand metric thread (major diameter 6
during similar FSW. However, there are less literature [6,18,19] avail­ mm) profile of 1 mm pitch followed by milling to generate three equally
able that focused on temperature measurements during dissimilar FSW. spaced flat faces (see Fig. 1(b)). However, for the sake of comparison in
Various temperature measurement methods during FSW includes temperature and behavior, another dissimilar FSW joint is also prepared,
workpiece thermocouple, tool thermocouple on shoulder/pin/probe, keeping all other parameters unchanged, using the simplest tool pin
tool-work thermocouple, thermal cameras etc.; however, embedded profile i.e., plain cylindrical (CYL) (Fig. 1(c)) of same pin length (5.9
thermocouple on workpiece possibly the most common method of mm) and diameter (Φ6 mm) as that of TIF tool pin.
temperature measurement adopted for FSW [20]. Such studies have Temperatures during the dissimilar FSW process are recorded by
immensely helped the thermal behavior of the FSW process neverthe­ deploying the K type thermocouples of 0.09 mm element size (in
less, the subsequent influence of temperature variations on local/zone- stainless steel SS316 sheath of Φ0.5 mm) near the plate top surface as
wise properties especially for dissimilar FSW remains as the avenue of well as at the inside of plates through drilled holes. Thermocouples are
profound investigation. To quantify the change in mechanical behavior placed in two different configurations hereafter referring as Config-1
of various regions in and around the weld nugget, advanced character­ (see Fig. 2(a)) and Config-2 (see Fig. 2(b)) for recording the history of
ization techniques like nanoindentation can work effectively, in partic­ temperature variation along the weld direction, and transverse to weld
ular where the material under consideration is present in small volumes. direction, respectively.
Implementing nanoindentation can help to determine elastic modulus, In Config-1, total eight thermocouples are placed, four each on AS,
hardness, stiffness, yield stress, creep etc. [21,22]. During the FSW of and RS aligned along the weld direction. Among these, three thermo­
dissimilar materials certainly there will be a formation of inhomoge­ couples on AS (1AS, 2AS and 3AS) and three on RS (1RS, 2RS and 3RS)
neous microstructural zones and the possibility of any intermediate are placed near the start, middle and end of the weld length equidistant
structure. For evaluating the mechanical behavior of different recrys­ on both the sides from the faying line and 0.5 mm below the top surface
tallized phases in such a close proximity, researchers have used nano­ of the plates, as marked on Fig. 2(a). Micro-holes are made by die
indentation technique for local characterization of similar FSW joints sinking electric discharge machining (EDM) operation and the thermo­
like AA6082 [23], AA6061 [24], brass [25], as well as dissimilar joints couples are fixed at the desired locations. Inclined holes are further
such as AA6061-AA5A06 [26], AA6061-AISI304 [27]. made by EDM and the thermocouples 4AS and 4RS are placed at the mid
It is evident that the local properties at various zones differ in a FSW of the plate thickness to record the thermal history inside the plates. To
joint due to intense deformation and heat generation. Further, the avoid any loosening, the thermocouples are placed in the taper holes
temperature field observed in FSW is asymmetric [28]. As a consequence with thermal pasting to ensure thermal contact throughout the process.
of variation in mechanical and thermal properties of the base materials, In Config-2, total six thermocouples are placed along the line
the nature of material flow, mixing and temperature distribution on perpendicular to the weld line (transverse direction) nearly at the mid
either side of the weld line and local mechanical properties is rather span of the weld length. Two thermocouples on AS (1AS and 2AS) and
complex for dissimilar FSW joints. The objective of the present study is two on RS (1RS and 2RS) are placed equidistant from the faying line
firstly to appraise the variation in temperature along the weld and aligning in traverse direction. The thermocouples 3AS and 3RS are
transverse to the weld direction. In order to accomplish, thermocouples placed at mid thickness and as near as possible to the stir zone (SZ). The
are mounted at various positions in two different configurations (along positions and detailed dimensions of thermocouple locations are
the and traverse to, weld line) during dissimilar welding of AA6061-T6 mentioned in Fig. 2(a), (b) for the two configurations. All the thermo­
and AA7075-T6. For further insight of heat distribution and asymme­ couples are connected to LabVIEW via National Instruments (NI) data
tricity in the temperature field, attempt has been made to simulate the acquisition system (cDAQ-9181, Module 9213) and the temperature
dissimilar FSW by finite element using coupled Eulerian-Lagrangian data are recorded at 10 Hz sampling rate. The experimental arrangement
approach and thus acknowledge the temperature distribution over the is shown in Fig. 2(c).
workpiece. The local mechanical properties at various zones are In order to unravel the heat flow and temperature distribution
assessed through nanoindentation tests and the behavior is correlated pattern, a finite element (FE) analysis is performed for the dissimilar
with the microstructure and texture. FSW taking into account the difference in mechanical and thermal
properties of the base material. The model geometry for dissimilar
2. Methodology combination wherein AA6061 is kept on AS and AA7075 on RS is
created by partitioning the workpiece (see Fig. 3) and assigning their
Aluminum alloys AA6061-T6 and AA7075-T651 of 6 mm thick plates respective material properties. The dimensions of the plate for the model
are joined by FSW in the square butt configuration for detailed mea­ 142 mm × 70 mm × 6 mm are kept in butt welding configuration alike
surement of temperature during the process by mounting thermocouples the experiment. The tool used for the simulation is the plain cylindrical
at various locations. Mg and Si based 6xxx series alloys find wide (CYL) with shoulder diameter, pin diameter and pin length of 20 mm, 6
application in automotive industries as external body panels. The high mm and 5.9 mm, respectively.

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M. Raturi and A. Bhattacharya International Communications in Heat and Mass Transfer 148 (2023) 107079

Fig. 1. Schematic illustration of (a) dissimilar FSW in square butt configuration, (b) TIF and (c) CYL pin profile.

Fig. 2. Thermocouples positions in (a) Config-1, (b) Config-2, and (c) experimental arrangement.

The material properties for AA6061-T6 and AA7075-T651 are capacity (Cp) as Cp = 794.58 + 0.5051T − 0.00004T2 J/kg-K are used
referred from the existing literature [11,12,17,34,35]. For AA6061-T6, [11,12]. Also, temperature dependent mechanical properties of AA6061
the temperature (T in K) dependent thermal conductivity (K) of is are referred from Roy et al. [34]. Similarly, temperature-dependent
used as K = 96.442 + 0.2466T − 0.00009T2 W/m-K, and specific heat thermal properties, mechanical and physical (density) properties of

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M. Raturi and A. Bhattacharya International Communications in Heat and Mass Transfer 148 (2023) 107079

Fig. 3. Schematic view of the (a) base plates placed for obtaining dissimilar butt weld and (b) cylindrical tool for finite element simulation (All dimensions are
in mm).

AA7075-T651 are referred from Salloomi et al. [17] and used for the electron back scatter diffraction (EBSD, Ametek) detector are used for
present FE simulation. The weld plates are thermo-mechanically microstructural and texture studies. EBSD analysis is performed over the
coupled and material is kept deformable and meshing is done using region of interest selecting step size 0.8 μm, aperture size 60 μm, voltage
eight node thermally coupled brick element (C3D8RT). The meshing 20 kV followed by analysis using TSL OIM Analysis™ v8 software.
near weld line (covering shoulder regions) is selected with fine element
(1 × 1 × 1 mm3), whereas the remaining portions are coarse (1 × 2 × 1 3. Results and analysis
mm3), while the tool and the backing plate are modeled as rigid surfaces
without thermal degrees of freedom. Johnson-Cook (J-C) hardening 3.1. Temperature variation
model is used for temperature, strain rate dependent flow stress
modeling for both AA7075 and AA6061 material. The J-C model pa­ The variations of temperature during dissimilar FSW of AA6061-
rameters are selected from literature for AA6061-T6 [13,36] and AA7075 measured by thermocouples near the top surfaces of the
AA7075-T651 [17,35]. The J-C parameters and melting temperature workpiece as per Config-1 are shown in Fig. 4. Out of six locations near
(Tmelt) used for the present FE simulation are provided in Table 1. Room plate top surface, three each are mounted on AS and RS of the weld, and
temperature for the model is selected as 25 ◦ C. their recorded temperature variations are shown side-by-side for an easy
Coupled Eulerian-Lagrangian (CEL) approach is used for the work­ comparison. During each welding, the temperature data are recorded
piece [37,38]. A CEL approach is used to take advantage of both from the beginning of the tool plunging and continued till the end of the
Eulerian and Lagrangian method. The workpiece is first defined as a welding. At point 1AS and 1RS the temperature sharply increases during
Lagrangian part which is being used as a frame of reference when the plunging as the thermocouples are placed near the start of the weld on
workpiece is again defined as a Eulerian part with same co-ordinates and both the sides. During plunging slightly delayed rise in temperature
dimensions. Temperature prediction is sensitive to the coefficient of profile for joint with the TIF tool can be observed on both the sides as
friction (μ) and in many analytical, numerical models of FSW the value compared to that of the CYL tool. The rise in temperature during
of μ is taken as 0.3 [11,12,14–16,39]. For the present FE analysis also μ plunging is majorly due to the frictional heat as the plunging is slow and
= 0.3 is selected to model friction between the tool and the workpiece. plastic deformation is not severe during the weld traverse. More fric­
Inelastic heat fraction for the present model is selected as 0.9 [40]. tional heat for cylindrical as compared to pin profile having flats is re­
For the appraisal of mechanical and microstructural variations with ported in literature [41]. Gradually, the heat generation due to plastic
local temperature at various regions, metallurgical studies and nano­ deformation induced by the rotating shoulder and pin, becomes influ­
indentation tests are performed for the weld specimen. The transverse ential along with the friction induced heat. Thus, as the pin is fully
sections of the welded samples are mechanically polished successively plunged and the shoulder effectually comes in contact with the plates, a
by various grades of emery papers (up to 2000 grit size) followed by quick rise in temperature as well as higher temperature is noted for the
diamond suspension (3 μm, 2 μm and 1 μm) and finally with the colloidal joint with TIF pin profile. Point 2AS and 2RS positioned near the mid of
suspension of up to 0.02 μm. Nano indentation tests are performed on the weld length initially shows a plateau during tool plunging, indi­
Hysitron TI 950 TriboIndenter (Germany) with motorized stage. A cating the rise in temperature due to the conduction. Later, when the
Berkovich indenter (half angle 65.27◦ , total included angle 142.3◦ ) of FSW tool approaches the thermocouple location, temperature increases
diamond, calibrated against fused quartz, is used for the test applying rapidly.
maximum load of 50 mN. The standard trapezoidal function is used with Thermocouples placed at point 3AS and 3RS show the smooth rise in
loading time of 30 s followed by hold for 10 s finally unloading time of temperature while the tool reaches near the respective thermocouple
30 s. The test and the analysis of the acquired data are performed using locations. It would be important to note that the schedule of peak
TriboScan9.8.1.3 software provided with the instrument. The optical temperature at locations 1, 2, and 3 are consistent to the tool passing the
microscope (AxioImager.M2m, Zeiss) and field emission scanning elec­ respective locations; however, the amplitude of the peak temperature is
tron microscope (FESEM) (Gemini500, Zeiss, Germany) equipped with almost in same order, as the thermocouples are placed equidistant on
both sides from the weld line. Thus, it may be concluded that the
maximum temperature cease to increase continuously due to steady
Table 1 state heat generation during the process, and do not noticeably influ­
J-C parameters for AA6061, AA7075 and Tmelt used for the present FE model. enced by the weld traverse. Similar observation was reported during
Material A (MPa) B (MPa) n C m Tmelt (◦ C)
fully-coupled thermo-mechanical analysis of AA6061 similar FSW [15].
It may be also easily noted from Fig. 4(b), (c) that the instant when the
AA6061- T6 289 203 0.35 0.011 1.34 655
maximum temperature (above 300 ◦ C) is noted at mid weld length
AA7075-T651 520 420 0.52 0.001 1.61 620

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M. Raturi and A. Bhattacharya International Communications in Heat and Mass Transfer 148 (2023) 107079

T emper atur e ( C )
T emper atur e ( C )

)
(C Tp
ratu
m
e

T emper atur e ( C )
T emper atur e ( C )

)
(C
ratu
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Te
T emper atur e ( C )
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Fig. 4. Variation of measured temperature near the workpiece top surface on AS and RS at three positions (a) start, (b) middle and (c) end of weld length, as per
Config-1 (refer Fig. 2(a)) during AA6061-AA7075 dissimilar FSW.

(location 2, Fig. 4(b)), the temperature at position 3 (3AS or 3RS) reads compared to CYL. This is due to the fact that measurement location 4 is
nearly one third (~ 100 ◦ C). Further, just prior to the sharp rise of sufficiently away from the shoulder affected region and thus the region
temperature at location 2 (time 100–125 s) or 3 (time 125–150 s), the experiences heat generation more by the pin and less by the shoulder.
temperature gradient is slightly higher at AS than RS (refer highlighted The shoulder is mainly controlling the amount of heat being generated
boxes in Fig. 4(b), (c)). during weld and is mostly experienced by top layer or layer beneath.
The temperature variations inside the plate (half of the thickness) at Comparing the results in Figs. 4 and 5, it may be noted that a little
the mid weld length (position 4) on both AS and RS for the FSW with TIF higher temperature is detected on the AS and for the TIF tool pin,
and CYL tool pin are shown in Fig. 5. It may be referred from Fig. 2(a) especially at locations 2, 3 or 4. The three intermittent flat surfaces in
that the position of thermocouples 4AS or 4RS is 20 mm away from weld the TIF tool pin somewhat reduces the contact area for friction with the
center line on either side (along mid thickness of plates, with less than a workpiece; however, they create a pulsating action and rigorous defor­
mm deviation during taper hole making), that is around 17 mm away mation and stirring of the material. Thus, at the beginning of welding i.
from the boundary of the SZ. Thus, the peak temperature recorded at e., plunging and initial travel, the CYL tool exhibited little higher tem­
location 4AS and 4RS are slightly higher than temperature at location 2, perature, but gradually a steady state heat generation reaches, and
and comparatively higher temperature is observed for joint with TIF tool temperature rise due to combined friction and deformation is recorded

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M. Raturi and A. Bhattacharya International Communications in Heat and Mass Transfer 148 (2023) 107079

T emper atur e ( C )
T emper atur e ( C )

Fig. 5. Measured temperature at location 4 (depth of 3 mm from top surface, at middle of weld length) as per Config-1.

to be little more for TIF tool pin. Further, it is also important to note that marked by dotted lines. From Fig. 7 the asymmetric temperature field
the temperature rise in AS is slightly higher than RS, mostly at all can be clearly noted. Within the pin marked region, that essentially
thermocouple positions. While in similar FSW, a higher material indicates the SZ or nugget zone, the high heat accumulation and high
deformation, plastic strain, higher temperature on the AS has been re­ temperature (red color field) towards the RS of the joint is observed due
ported [11,12,15,17], the situation is rather complex and additionally to the high specific heat capacity of AA7075. It is also interesting to note
dependent on the thermal properties of the two different materials that beyond high temperature region (in SZ), the surrounding regions of
placed on the AS and RS. In a dissimilar AA6061-AA7075 FSW joint, the successive lower temperatures (orange, dark and light-yellow color
material AA6061-T6 possess a higher value of K; however, Cp is lower field) are comparatively narrow in RS due to the low thermal conduc­
than the material AA7075-T6, although their densities are nearly equal. tivity as well as thermal diffusivity of AA7075. The same behavior
Thus, the material kept at the AS (AA6061) has higher thermal diffu­ persists from the top of the plate (shoulder affected region) till the
sivity compared to material placed on the RS. This could also be influ­ bottom (only pin influenced region) on the RS of the dissimilar joint.
ential behind the temperature distribution, and to appraise the nature of Thus, it is conclusive that during dissimilar AA6061-AA7075 FSW joint,
thermal distribution on AS and RS during the dissimilar FSW, the FE the thermal energy in the SZ is stored majorly on RS (AA7075) leading to
predicted temperature at the sectional view of the plates are analyzed. high temperature rise in and around the SZ towards RS; however,
The temperature distribution on the AS and RS while the tool is at the beyond this region the effect is decayed very quickly within a narrow
location 1 (start of weld traverse) and location 2 (mid of weld length) for zone. The high thermal energy towards the RS within the SZ is also
the joint with CYL tool are shown in Fig. 6(a) and (b), respectively. The expectedly alter the material flow, nature and associated local me­
asymmetric heat distribution between AS and RS can be noted from chanical properties of the material present in RS.
Fig. 6(a) and (b) whereas asymmetricity in leading and trailing side During numerical simulation of similar FSW, asymmetric distribu­
becomes noticeable at location 2 with higher temperature at the back­ tion and higher temperature has been reported under the tool shoulder
side of the tool. A steep temperature gradient on RS due to higher heat [11,14,16] that induces higher deformation towards the workpiece top
capacity of the material (AA7075), and towards the leading edge of the surface [15]. From the enlarged view of the upper region shown in
tool is also observed from the FE simulations. Higher temperature Fig. 7, it may be clearly noted that the high temperature region is
gradient on the leading side has earlier been reported for similar FSW extended over a comparatively larger region near the workpiece top
[15]. surface below the shoulder than plate bottom region. Higher region of
To further appraise the asymmetric temperature field of dissimilar contact between the shoulder and workpiece top surface, and associated
AA6061-AA7075 joint, FE predicted temperature variations at location friction causes higher temperature near the shoulder-plate interface.
2 (mid weld length) is further studied in detail. Fig. 7 shows the tem­ However, due to higher effective velocity and material flow, the defor­
perature field at the weld transverse section with the magnified views of mation is more on the AS. This effect in combination with the higher
shoulder influenced and pin influenced regions. The regions of shoulder thermal conductivity and diffusivity of the AA6061 placed on the AS of
diameter (20 mm) and pin diameter (6 mm) from the weld center are the joint, a wider region with moderate-to-high temperature (green,

Fig. 6. FE predicted temperature variation corresponding to tool position at (a) location 1, (b) location 2 for dissimilar AA6061-AA7075 FSW with CYL tool pin.

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M. Raturi and A. Bhattacharya International Communications in Heat and Mass Transfer 148 (2023) 107079

Fig. 7. FE predicted temperature field at the transverse section near the mid weld length of AA6061-AA7075 FSW joint.

yellow, orange and some portion of red color regions, see Fig. 7) are AS and RS during similar FSW with CYL and TIF tool pin along with the
observed on the AS. Thus, FE results and the preceding discussion in­ thermocouple locations are shown in Fig. 9. Following the preceding
dicates the asymmetric temperature field during AA6061-AA7075 dis­ discussions, since there is no variation in the thermal properties of the
similar FSW joints are obvious with higher temperature on shoulder base materials on AS and RS (similar FSW), slightly higher peak tem­
influenced region, and wider spread towards the AS (material having perature is noted on the AS (Fig. 9(a)) due to higher material defor­
high K, α and low Cp). Additionally, within and surrounding the SZ, the mation on the AS. However, the difference in peak temperature is
material on RS (having high Cp and low K, α) reserves the higher tem­ considerably less than observed during dissimilar FSW exhibiting more
perature region making the temperature field further asymmetric. temperature on RS. Thus, it can be concluded that, moreover the nature
The observations on asymmetric nature presented in Fig. 7 is of deformation of AS and RS, the difference in thermal properties of the
attempted to validate by measuring the temperature along the weld base materials imparts crucial influence on the asymmetric heat accu­
transverse direction mounting the thermocouples close to the SZ at the mulation and thermal field during dissimilar FSW. This asymmetricity,
same time ensuring that they are not damaged and temperatures are therefore, would be decisive factor behind the nature of deformation,
recorded uninterruptedly. The thermocouple arrangement and their metallurgical behavior and subsequent local mechanical properties of
locations can be referred from Config-2, shown in Fig. 2(b). The the joint.
measured temperature variations by the thermocouples at 1, 2, 3 on AS
and RS as per Config-2 are presented in Fig. 8. The thermocouples at
point 1 (1AS and 1RS) and Point 2 (2AS and 2RS) are close to the 3.2. Microstructure and local mechanical properties by nanoindentation
workpiece top surface just outside the shoulder region, and the
measured temperature variation shows a slightly higher temperature on The optical micrograph of the transverse cross-section of the
the AS compared to the RS due to the higher deformation on AS as well AA6061-AA7075 FSW joint prepared with TIF tool is shown in Fig. 10
as the relatively higher thermal conductivity and diffusivity of the (a). The upend bell-shaped SZ with light and dark shades can be
AA6061 material placed on the AS of the joint. Since the thermocouple observed towards the center of the joint. The dissimilar materials with
locations at 2 is further away from location 1, expectedly lower peak the light and dark color contrast after etching can be identified as
temperature is observed at location 2 (Fig. 8(b)). Please note that the AA6061 (AS) on the left and AA7075 (RS) on the right as shown in
irregularity in temperature profile near the peak for CYL tool at location Fig. 10(a). The characteristic SZ showing the intermixing of two dis­
1RS (Fig. 8(a)) is due to the glitch with the thermal sealing and a one-off similar materials with light and dark sites reveals the heterogeneous
case of loosening of the thermocouple. The thermocouples at location 3 mixing of two materials. Also, the region separates itself from the other
on AS and RS are located inside the plate thickness and reasonably close regions with a very fair boundary highlighted using dashed line. The
to the SZ. Thus, considerably higher temperature is noted at 3AS and different regions with varying microstructure and mechanical properties
3RS, and higher peak temperature is recorded at the RS (AA7075), refer identified over the weld cross section is the result of occurrence of the
Fig. 8(c). The experimentally measured temperature shows approxi­ series of events like plastic deformation and friction. These events lead
mately 24 ◦ C higher temperature on the RS for CYL tool whereas, for the to acute thermal variations, mixing of plasticized materials, subsequent
joint with TIF tool around 50 ◦ C higher temperature is noticed on RS, recrystallization and other associated metallurgical phenomena result­
thus corroborates the previously presented FE results and discussions. ing in the formation of characteristic zones. Fig. 10(a) is marked with
The temperature variations predicted from the FE simulation for CYL 1–7 different regions where the nanoindentation tests are carried out to
tool are observed to be in close proximity to the experimentally identify localized mechanical properties.
measured temperatures. The weld center region (nugget zone), known as the stir zone (SZ),
To further confirm the behavior, temperature at the middle of the experiences intense heat and deformation and is characterized by fine
plate thickness near the SZ is also measured on both AS and RS during a recrystallized grains. Surrounding the SZ, the narrow thermo-
similar FSW of AA6061-AA6061, wherein the thermal properties of the mechanically affected zone (TMAZ) with relatively coarser and elon­
base material on both sides are identical. The temperature variation on gated grains is observed that undergoes moderate heat and deformation.
The heat affected zone (HAZ) experiences much less heat with no strain

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M. Raturi and A. Bhattacharya International Communications in Heat and Mass Transfer 148 (2023) 107079

T emper atur e ( C )
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(TC )
ratu
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T emper atur e ( C )

T emper atur e ( C )

Fig. 8. Measured temperature variation on AS and RS at various positions along the weld transverse direction, as per Config-2 (refer Fig. 2(b)) during dissimilar
AA6061-AA7075 FSW.

or deformation, and coarser grains (than SZ, TMAZ) are observed. These far apart from the SZ of joint and referring as HAZ-AS and HAZ-RS (near
regions and the locations of nanoindentation at various zones each on AS thermocouple) as these locations are near the placement location of
and RS are annotated on Fig. 10(a). Fig. 10(b) represents the magnified thermocouples inside the plate (3AS, 3RS in Config-2).
images from the core of the SZ (Region 1), showing layers of AA6061 The load versus displacement plots obtained from the nano­
and AA7075 material stirred and heterogeneous mixing of two alloys. indentation test performed at the various locations marked in Fig. 10(a)
The nanoindentation tests are carried out to mechanically characterize are presented in Fig. 11. At each specified region, two indents at the
them at two specific locations, hereafter denoted as AA6061-(SZ) and nearing vicinity have been chosen for the reading, and the corre­
AA7075-(SZ). Magnified views of Region 2 and Region 3 shown in sponding load v/s displacement graphs for such two readings are pro­
Fig. 10(c) represents TMAZ and HAZ (near SZ) are considered from the vided in each plot.
AS of the joint (AA6061) and locations of nanoindentation. Alike, in The reduced Young’s modulus (Er) or local elastic modulus, and
Fig. 10(d) Region 4 and Region 5 represents the TMAZ-RS and HAZ-RS hardness (H) obtained from the nanoindentation tests at various zones
(near SZ) with figurative location of nano-indents. The nanoindentation are provided in Fig. 12. The bar plot for the purpose of comparison
data is also collected over Region 6 and Region 7 on the HAZ regions but provided in Fig. 12(a) and (b) is the average of two readings specified in

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M. Raturi and A. Bhattacharya International Communications in Heat and Mass Transfer 148 (2023) 107079

500
450
400 AS-CYL
AS-TIF
350 RS-CYL
Temperature (°C)

300
RS-TIF CYL
Tool
250
200
150 Dimensions in mm
AS
100
50 (b) RS
0
0 25 50 75 100 125 150 175 200
Time (s)
(a)

Fig. 9. (a) Measured temperature variation at middle of the plate on AS and RS close to SZ during AA6061-AA6061 similar FSW with CYL and TIF tool, (b) the
thermocouple location details.

Fig. 10. (a) Optical micrograph image of AA6061-AA7075 FSW joint (prepared with TIF tool), and magnified images of (b) Region 1 in SZ, (c) Region 2, 3 on AS and
(d) Region 4, 5 on RS of the joint.

Table 2. In the SZ, a higher depth of penetration (displacement) for the SZ; however, nearly uniform over different zones i.e. TMAZ, HAZ on AS
recrystallized grains of AA7075 compared to AA6061 can be noted from of the joint.
Fig. 11(a). This indicates less hardness of AA7075 in the SZ than AA6061 The Er and H obtained from the nanoindentation tests along the line
(see Fig. 12(b)) even though their Er are nearly equal (Fig. 12(a)). The 1 mm below the top surface to access the behavior affected typically by
load-displacement plots of other regions, namely TMAZ, HAZ nearing SZ the shoulder induced heat is given in Fig. 13(a) and (b), respectively.
and far apart (near thermocouple location) shows higher hardness and The graph shows parent material reading on the both extremities of all
lower indentation depth on RS (AA7075) than AS (see Fig. 11(b)-(d)). It the graphs. The modulus and hardness values for AA7075 parent ma­
is therefore important to note that even though the parent AA7075 terial is higher than AA6061. The higher heating rate shows an increase
material has higher H, in the SZ of dissimilar FSW, the recrystallized in modulus values for AA7075 side within the SZ but for AA6061side the
AA7075 showed softening with lower hardness due to the metallurgical values are not as high. The hardness values depreciated for the AA6061
changes associated with the asymmetric temperature field with higher except for the points with fine grains, although it has been reduced for
temperature towards RS (AA7075), as discussed in the preceding sec­ the recrystallized AA7075 from the parent material. An appreciable
tion. Beyond the SZ, where the temperature influence is reduced, higher reduction in hardness of AA7075 within the SZ due to the local heat
hardness at the TMAZ, HAZ nearing SZ as well as far apart are noted accumulation in RS due to slow cooling with an annealing-like effect can
higher for AA7075 than AA6061 (see Fig. 12(b)). The variation of Er at be beneficial for achieving higher elongation of the joint.
various local zones indicates a slight decrease in RS as moved away from To appraise the local property variation in the SZ of the joint, EBSD

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M. Raturi and A. Bhattacharya International Communications in Heat and Mass Transfer 148 (2023) 107079

Fig. 11. Load-displacement graph of nanoindentation test on (a) AA6061 and AA7075 within SZ, (b) TMAZ (AS and RS), (c) HAZ (AS and RS) near SZ and (d) HAZ
near thermocouple (AS and RS) (refer Fig. 10(a) for locations).

analysis of the SZ at a selected location (Region-1 marked in Fig. 10(a)) movement and thus stimulates the strengthening mechanism [25]. The
is performed and the inverse pole figure (IPF) of the region is shown in plastic displacement for AA7075 is higher than AA6061 (refer nano­
Fig. 14(a). Further analysis in terms of IPF, grain boundary (GB) map, indentation load-displacement plot in Fig. 11(a)) for the same load
kernel average misorientation (KAM) separately for AA6061 and application. In contrast, the magnitude of elastic displacement is the
AA7075 within this region of SZ are presented. In the IPF map, two same for both cases, and thus, the hardness is higher for AA6061 while
optically separable recrystallized alloys with fine grains of AA6061 the modulus (Er) is same for both. The fraction of HAGBs for both alloys
(Fig.14(b)) and comparatively coarse grains of AA7075 (Fig.14(d)) can within the SZ is significantly high. This is associated with the continuous
be identified. While joining the dissimilar materials, due to their rotation of LAGBs due to the stirring action caused during the FSW
inherent material properties, both materials experiences differing ab­ process leading to the formation of a higher fraction of HAGBs within
solute shear strain against the same loading condition [26] and thus the SZ [42]. Fig. 15(a) and (b) shows the local strain distributions within
result in different grain sizes. The grain refinement within the SZ is the the SZ using KAM map at locations mentioned in Fig. 14(b) and (d),
result of dynamic recrystallization, during which the severe plastic respectively for AA6061 and AA7075. KAM helps in studying the strain
deformation tends to elongate or flatten the large grain. distribution in lattice structures by calculating average misorientation at
The low angle GBs (LAGBs) of 5◦ -15◦ and high angle GBs (HAGBs) of a point with respect to neighboring points. The local misorientation
15◦ -65◦ for both AA6061 and AA7075 regions available within the SZ angle of grains predicted through KAM is manifested as the accumula­
are shown in Fig. 14(c) and (e), respectively. The hardness of AA6061 tion of dislocations [27].
within the SZ is significantly higher than AA7075 (Fig. 12(b)) and can be Fig. 15(a) and (b) shows the strain accumulation at two different
apprehended to the fine grain structure of AA6061. The fine grain regions of AA6061 and AA7075 material within the SZ using KAM map.
structure with a higher fraction of HAGBs impedes the dislocation Recrystallized AA6061 within the SZ reveals higher intensity points near

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M. Raturi and A. Bhattacharya International Communications in Heat and Mass Transfer 148 (2023) 107079

Fig. 12. Variation of (a) Er and (b) H values obtained using nanoindentation at different locations (zones) over the AA6061-AA7075 FSW on AS and RS.

Table 2
Values of Er, H, force and depth during nanoindentation tests on various zones of AA6061-AA7075 dissimilar FSW joint.
Weld zones→ HAZ-AS HAZ-AS TMAZ AA6061 AA7075 TMAZ HAZ-RS HAZ-RS
(near thermocouple) (near SZ) (AS) (in SZ) (in SZ) (RS) (near SZ) (near thermocouple)

Trial 1 74.51 70.64 72.67 90.55 103.3 97.52 85.22 69.25


Er (GPa)
Trial 2 77.02 73.66 68.95 94.46 96.90 90.76 86.58 72.57
Trial 1 0.779 1.09 1.18 1.88 1.62 2.22 1.99 1.84
H (GPa)
Trial 2 0.757 1.13 1.07 1.88 1.45 1.88 1.92 1.99
Trial 1 50,017 49,529 49,348 49,751 49,630 49,910 49,843 49,913
Max Force (μN)
Trial 2 49,633 49,538 49,545 49,717 49,998 49,586 49,750 49,697
Trial 1 1558.9 1336.1 1285.4 1043.6 1102.7 970 1025.3 1076.6
Max Depth (nm)
Trial 2 1571 1313.2 1347.8 1039.9 1164.4 1042.6 1037.1 1036.3

Fig. 13. Variation pattern of (a) Er and (b) H using nanoindentation on a straight line 1 mm below the top surface over the AA6061-AA7075 FSW joint along with the
parent material values (bars at the extremities).

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M. Raturi and A. Bhattacharya International Communications in Heat and Mass Transfer 148 (2023) 107079

Fig. 14. EBSD analysis of Region 1 (marked over Fig. 10(a)) within SZ showing the (a) IPF of the region, and separately IPF and GB map for (b), (c) AA6061 and (d),
(e) AA7075 regions.

Fig. 15. KAM plot of two different regions in SZ (a) AA6061 and (b) AA7075 of the AA6061-AA7075 FSW joint (refer Fig. 14 for regions).

grain boundaries that signify the piling up of dislocations. This leads to of its equiaxed shape and comparatively small size, can dissolve easily
the increase in strain hardening effect and thus increasing material’s causing over-aging of the alloy [24] leading to a reduction in Er and
ability to resist plastic deformation or increasing hardness [27]. hardness in HAZ.
Generally, the higher strain rates lead to the formation of dislocations in
the form of lattice defects, which further accumulates and on annihila­ 4. Discussion
tion, creates sub-grain boundary. Later this sub-grain boundary changes
to LAGB or HAGB depending upon the amount of energy (heat or strain) The temperature distribution measured at various locations on AS
being supplied. This is a general course of action that takes place during and RS for AA6061-AA7075 dissimilar FSW joints with two different
the dynamic recrystallization of grains during stirring of the material tool pin profiles (TIF and CYL), and the FE analysis by CEL approach
taking place within the SZ. The modulus and hardness values of TMAZ- detailed in the previous sections represents an asymmetric nature. The
RS and HAZ-RS nearing SZ are relatively tending towards its BM prop­ FSW process and the transient temperature distribution is analogues to
erties i.e., AA7075-T6. The AA7075 is a precipitate-hardened alloy with 3D heat conduction problem with heat generation, expressed by the
a higher percentage of alloying elements like zinc and of reasonably governing equation:
large size precipitates [43]. During FSW, the asymmetric thermal field ( ) ( ) ( )
with higher temperature is noted on the RS (AA7075) over AS (AA6061) ∂ ∂T ∂ ∂T ∂ ∂T ∂T
k + k + k + Qv = ρCp (1)
in-and-close around the SZ. The peak temperatures noted during mea­ ∂x ∂x ∂y ∂y ∂z ∂z ∂t
surement and simulation are high enough to cause metallurgical With simplification, considering no spatial variation of K in x, y, or z,
changes like precipitate coarsening, shrinkage, and dissolution. Though the equation can be written as
the temperature is high enough on both sides, the size and properties of
the strengthening precipitate will determine the consequences. The very ∂2 T ∂2 T ∂2 T Qv 1 ∂T
+ + + = . (2)
common and densely populated Mg2Si precipitate in AA6061, because ∂x2 ∂y2 ∂z2 K α ∂t

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M. Raturi and A. Bhattacharya International Communications in Heat and Mass Transfer 148 (2023) 107079

Where, Qv is the heat generation per unit volume (W/m3), K is shows the schedule of peak temperatures measured at thermocouple
thermal conductivity (W/m-K), Cp is specific heat capacity (J/kg-K), ρ is locations 1, 2, and 3 (all at same height, along weld traverse line, refer to
density (kg/m3), and α is thermal diffusivity (m2/s) defined as α = ρKCp . Fig. 2(a), Config-1), and the peak temperatures at the corresponding
The amount of heat generation during FSW can be expressed in terms of locations are recorded at 114 s, 158 s, 200 s, respectively. The interval of
the tool dimensions and process parameters. Considering the contribu­ peak temperature is nearly uniform (44 s and 42 s, deviation of 2 s) as
tion in heat generation from the shoulder bottom surface and pin pe­ the thermocouple 1, 2, 3 are equidistant (50 mm apart). The tool tra­
ripheral and bottom surface, the total heat generation (Qt ) is the sum of verse time between these locations can be calculated as
Q1 , Q2 and Q3 (as shown in Fig. 16(a)), and for a cylindrical tool pin distance between thermocouple locations
(Fig. 16(b)) can be expressed as [4]. tool traverse time = (6)
weld speed
{( }
2π )
QCYL = ωτc rs 3 − rp 3 (1 + tanδ) + rp3 + 3rp 2 h (3) The traverse time by the tool to reach from location 1 to 2 or from
3 location 2 to location 3 is therefore calculated as 9850mm/min
mm
= 30.6 s. The
Where rs and rp are shoulder and pin radius, h is pin height, ω is tool tool passes the location in 30.6 s, whereas the peak temperature reaches
rotational speed, and τc is contact shear stress. It may be noted that for a about 42–44 s (~ 40% delay in time), thus corroborating the fact that
sticking condition, τc can be taken as the maximum shear stress the higher temperature is at the trailing side and asymmetry exists be­
considering von Mises criterion i.e., τc = √y̅̅3, when σ y is the workpiece tween the leading and trailing edge of the tool.
σ

material yield stress. Similarly, for sliding condition τc = μp, when μ is To further illustrate the asymmetry on AS with RS, and leading side
the frictional coefficient, and p is contact pressure. Further, considering with trailing side, the temperature history of some nodes neighboring
the tool shoulder face as flat (i.e. δ = 0), Eq. (3) can be simplified as: the tool location is considered. The temperature history of nodal points
1–27 on AB along the transverse to weld direction, and nodal points
2π { }
QCYL = ωτc rs 3 + 3rp 2 h (4) 1–16 on CD along the weld direction are shown in Fig. 18. The nodal
3 positions along the weld direction (line CD) and transverse direction
Similarly, for TIF tool pin with alternate flat and threaded regions (line AB) are marked on the top view as shown in Fig. 18(a), and the
(with dimensions shown in Fig. 16(c), (d)), the total heat generation intersection of AB, CD indicated the tool position (×). The temperature
considering flat shoulder can be expressed as [44]: history of nodes 1–16 on CD is shown in Fig. 18(b) with the tool position
( ) 17 indicated. Corresponding to the tool location (vertical green dotted
π 2π
QTIF = ωτh r1 2 + r1 2 + r1 r2 + ωτha2 + ωτrs 3 (5) line), the temperature at the trailing side (node 8, 7, 6, 5; blue asterisk)
6 10 3
are higher than at leading side (node 9, 10; red circle). In fact, the dif­
It may be noted that the amount of heat generation is dependent on ference in temperature between node 8 and 9 near the tool center is
the tool pin geometry and dimensions; however, the heat propagation small; however, the difference is quite significant with the higher tem­
and temperature distribution is influenced by the thermal properties e. peratures at nodes 7, 6, 5 (on the trailing side) compared to node 10
g., K, ρ, Cp of the materials. In order to realize the comparative influence, (leading side). Fig. 18(c) and Fig. 18(d) represent the temperature
from the relevant properties at room temperature (25 ◦ C) it may be mapping on the RS and AS, respectively.
noted that K of AA6061-T6 (169 W/m-K) is about 1.3 times higher than On the RS, close to the tool position the temperature at point 9 or 8
AA7075 (130 W/m-K), whereas for AA 7075 the value of Cp (870 J/kg- (on RS) is noticeably lower than the nodal position 10–15 (at the tool
K) is nearly 1.36 times higher than AA6061 (640 J/kg-K), however, central region) with high thermal gradient. However, the temperature at
density (ρ) of AA6061 (2700 kg/m3) is nearly equal to that of AA7075 nodal position 16 or 17 is close to that of 10–15 with a smooth tem­
(2810 kg/m3). Therefore, the thermal diffusivity (α) of AA 6061 (9.78 × perature gradient. Additionally, at distant, the temperature on RS (node
10− 5 m2/s) becomes 1.83 times higher than AA7075 (5.317 × 10− 5 m2/ 1 or 2 on AB) is somewhat lower than nodal points 25, 26 on AS due to
s). The net effect will be a higher amount of heat retention capacity or the higher thermal diffusivity of AA6061 than AA7075. It may also be
thermal bulk by the AA7075 material placed on the RS of the joint. important to note that the simulated temperature is somewhat higher
On the contrary, the AA6061 material placed on AS of the joint ex­ than the measured values near the SZ (refer Fig. 8) and gradually be­
hibits higher heat transfer with faster conduction of thermal energy with comes low as moved outward from the SZ. However, this deviation
less tendency to store. This difference in thermal behavior along with the could be noticeable in core of SZ due to the hindrance in heat transfer
variation in the amount of generated heat and material mixing/distri­ through the tool and can be corrected by adjusting the tool thermal
bution by the tool in the dissimilar FSW joint, influences the asymmetric properties in the model.
heat and temperature distribution in the FSW joint. Moreover the The consequences of asymmetric temperature field with higher
asymmetric temperature distribution at AS and RS of the joint, the FE temperature on RS within the SZ is observed in grain size and texture
simulation result also showed unsymmetric temperature variation at the variation, as discussed in previous sections. The EBSD analysis of
leading and trailing side of the tool in weld direction. The same can also AA6061 and AA7075 within the SZ showed finer grains with HAGBs,
be validated from the measured temperature distributions also. Fig. 17 intense strain and dislocation pileup at GBs of AA6061 compared to

Fig. 16. Schematic to show geometry of CYL and TIF tool pin for heat generation estimation.

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M. Raturi and A. Bhattacharya International Communications in Heat and Mass Transfer 148 (2023) 107079

Fig. 17. Schedule of peak temperature at different thermocouple locations of Config-1 with respect to tool traverse.

Fig. 18. FE predicted temperature variation on the plate top surface in the direction of welding and traverse direction during dissimilar AA6061-AA7075 FSW with
CYL pin.

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M. Raturi and A. Bhattacharya International Communications in Heat and Mass Transfer 148 (2023) 107079

Fig. 19. IPF and pole figures of (a) AA6061 and (b) AA7075 within the SZ with ideal shear texture, (c) fcc simple shear texture components and (d) ideally
superimposed over (001), (101) and (111) pole figures [45,46].

7075. The pole figures of the same regions within the SZ shown in precipitates also altered in AA6061 and AA7075 within the SZ, which in
Fig. 19 shows texture evolution faced by both the alloys in the severely turn influenced the local characteristics and properties like hardness.
deformed region. Both the alloys are lying adjacent and almost experi­ Large-size precipitates in parent AA7075 material are shattered and
encing equal amount of heat and almost close strain rates as both the redistributed predominantly along the boundaries of the recrystallized
locations lies close to each other and within the SZ. Only a slight vari­ grains, as can be seen in Fig. 20(a). Due to comparatively larger grain
ation can be observed due to the material’s inherent property. There­ size in the SZ and precipitates at the GBs, much less hard substances are
fore, the slight increase in B/B texture in recrystallized grains of AA7075 noted under the impression of the nano-indent on AA7075 (Fig. 20(b))
can be observed with respect to A/A in AA6061. thus exhibits comparatively lower hardness. Whereas many precipitates
Moreover, the grain size and texture, the distribution of the along the boundary of the fine grains in AA6061 can be noticed under
the nano-indent on AA6061 within the SZ of the joint.

Fig. 20. FESEM images showing (a) fine precipitates along the GBs in AA7075 within SZ, nano-indents taken on (b) AA7075 and (c) AA6061 within the SZ of
AA6061-AA7075 dissimilar FSW joint.

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M. Raturi and A. Bhattacharya International Communications in Heat and Mass Transfer 148 (2023) 107079

5. Conclusions References

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