| Laksh Finechem Pvt. Ltd... 4801/02 & 1801/03 Phase - IV, G.L0.C.| Email || Vithal Udyog Nagar - 388121, Dist - Anand.Gujarat - India.| web site |, Plot No. Coll No: + 91- 99799 22293, + 91- 99785 22233 + 91 2692 - 23322 4 info@lakehfinechom.com ‘wwwelakshfinechem.com (SELLERS TITLE Cilnidipine (WS) License No G/25/2046 ‘CAS NO [132203-70-4] Batch No LF-WS/CILN/012023/001 Molecular Formula CyHasN207 Batch Size 250 kg. Molecular Weight 492.52 g/mol Mfg. Date’ JAN 2023 HSN CODE 29333990 ‘Analysis Date | JAN 2023 Grade In-house : Retest Date DEC 2025) Sr.No Test Parameter Specifications "Results 01 _| Description Light yellow, crystalline powder. Light yellow, erystalline powder. 02 | Solubility Very soluble in N-N-Dimethyl acetamide; freely soluble in acetone; sparingly soluble in methanol; practically insoluble in water. Complies Identification a. By IR b. By HPLC The transmission minima (absorption maxima) in the spectrum obtained with the substance to be examined correspond in position and relative size to those in the spectrum obtained with the Cilnidipine working standard The retention time of the major peak | in the chromatogram of the sample ‘Complies | Complies Prepared by QC Officer Signature eat Date 20)0112023Gel No : + 91- 99799 22299 + 91- 99785 22203 ! 0 | tele + 91 - 2692 - 233224 aw MIplll, Plot_Ne, 190102 & 190109 Phase «WV, SLD.C.| Emall | info@iaksninecnom om if sh, Fae ee ea: eanand Gujerat inca: | Website: ww lokentinesnem com uh \ pecererserens srs canna RS CRC Ca CERTIFICATE OF ANALYSIS TITLE Cilnidipine (WS) Ticense No | G/25/2046 Pca CAS NO [132203-70-4] Batch No LF-WS/CILN/012023/001 Molecular Formula | CavHzsNzO> Batch Size | 250 kg Molecular Weight 492.52 g/mol | Mfg. Date JAN 2023 | HSN CODE 29333990 ‘Analysis Date | JAN 2023 Grade In-house Retest Date z | [Sr.No Test Parameter ~ Specifications Results. ~T chromatogram of the standard preparation, as obtained in Assay by HPLC. Melting Range 108°C to 113°C 109°C Loss on drying Not more than 0.5% 0.20 % wiw Heavy Metals ‘Not more than 20 ppm 12 ppm ‘Sulphated Ash ‘Noi more than 0.2% wiw 0.13 %wiw Related Substances by HPLC Cilnidipine Impurity A | Not more than 0.15 % 0.07% Any other impurity Not more than 0.10 % 0.06 % Total impurity Not more than 0.3 % 0.19% 09 [ Assay (on the dry basis) | Not less than 98.0% to 102.0%. 99.81 % wiw Remarks: The Batch is Complies / Boes-not complies as per above specific CHE, #3 ] Prepared by | Checked by: QC Officer QC Head ~ ‘Signature si | i; Hy ) Das Bolotl2022 | 2oler!2o2