ANALYSIS CERTIFICATION METHOD OF PREPARATION : GRAVIMETRIC / PRESSURE TRANSFILLING METHOD OF ANALYSIS : GC (FID) ACCURACY : + 2% RELATIVE Ma LOT NO. COMP. 1 COMP. 2. COMP. 3. COMP. 4 COMP. 5 COMP. 6 Exp Date P/N & Ory. Cyl AIR 804532 898052(7) 0.75% BALANCE 02/01/21, (This lot contains 0.1% He) Gas mixtures manufactured with balances calibrated by an ISO 17025 accredited Company using NIST traceable weights and meets or exceeds the requirements of NIST Handbook 44. Calibration test CG/01/03/17/MC01, CG/01/03/17/MC02, CG/01/03/17/MCO3, or CG/01/03/17/Mco4 dated, 3rd January 2017 applies. WEIGHT SETS USED: Kit# 92231, Test# 2403472, Kit# 03610, Test# VA-16-10240F 13 Test# VA-16-10240B No affecting environmental conditions during analysis. REQUESTED BY : MSA DO BRASIL CUSTOMER PURCHASE ORDER NUMBER : 4502278852 PACKING LIST NUMBER : 8973380 CERTIFICATION DATE : January 30, 2018 ANALYSIS BY : Quality Representative "We certify that all the cylinders for the Lot numbers identified herein are manufactured and tested within the requirements of CFR 49 part 178.65 and that physical and chemical test reports are on file and copies will be furnished upon request." CALGAZ, a division of Airgas USA LLC 821 Chesapeake Drive, Cambridge, MD 21613-0149 Phone: (410)228-6400 Fax: (410)228-4251CERTIFICATE OF COMPLIANCE COMPANY NAME : MSA DO BRASIL PURCHASE ORDER NUMBER : 4502278852 PACKING LIST NUMBER : 8973380 LOT NUMBERS OF MATERIAL SUPPLIED : 898051(7) QUANTITY OF MATERIAL COVERED BY THIS CERTIFICATION: 7 CYLS. ACTUAL TEST AND INSPECTION RESULTS SUPPORTING THIS CERTIFICATE ARE AVAILABLE FOR REVIEW We hereby certify that the materials supplied meet all require- ments of the above purchase order including the requirements of applicable drawings, specifications and standards referenced by this purchase order. Further we certify that Calgaz makes every effort to select suppliers and materials that minimize environmental impact. Base chemicals for the majority of our mixtures are nitrogen and oxygen, the main elements in ambient air. Calgaz products in DOT 39 cylinders do not contain toxic levels of any requested compound. This is prohibited by US regulations. Calgaz products are routinely used to protect the environment by providing an accurate source of calibration gases for monitoring instrumentation deployed worldwide. IMPORTANT NOTE: ONE COPY OF THE CERTIFICATION MUST ACCOMPANY SHIPMENT OF MATERIAL. CERTIFYING OFFICIAL (Quality Representative) DATE OF CERTIFICATION : January 30, 2018 CALGAZ, a division of Airgas USA LLC 821 Chesapeake Drive, Cambridge, MD 21613-0149 Phone: (410)228-6400 Fax: (410) 228-4251