(fly 407 - 07" TABLE 2 Continued eae Cemooaten Preceaare sw 20 mb aoa ace Use a cetid an testes Mood. mere wih gone agiaton 5-30 3g pote aca 50 mi shanol 85%) oF mtranol (95%) 128 anne Use a cetiod an testes hood. Inmrse wih gone agiaton 5-15 Sm HNO, 200 mL water 120 some ‘Swab 10-20 &. Vary H to netease or docranse ati 60m lacte acid 190 25 mLHC! Caution Keop boon 24°C (75°F. Elec at 30 V or 30s 78m mete! 31 SmLH,50, Use a certties and tated hood, Elect at 6-60 V for 10-20 meee 100 mano! (05 10m HNO, (a) Saab win nea praseute or S10 Water ane, aohol ns, ay than tn wh 0 ml laste ald No. de. (0) Swab for 5-90 0 mL acetic acid cherscally posh wit longer times. Sutdized grin boundaries etched before normal grain oundaries. Do not toe 108 70m My POs lecrolti 6-10 V for 5-608. (Pasha a high curets) 138 s0mLHNO, Use a corttied and tested hood, Wam specimen in bling water pr to immersion for 10 amLHe ‘1205 v9 109NaN0, Bloctolyi, 02 Nem, t min 00 rs water 198 59 FeCly ‘we 10-60 5 2m HC 100 ml ethanol (85%) oF methanol (85 199 5aKon Use a certod ana testes hood~Can give of extremely potonous hyeogan cyanide 400 ms water Precauton—Aso pasonous by ingestion as wall as sh corse. mre 10-100 05m HO. (3%) 40 50 mL acetic aes Use a certo’ and tesod hood. De not sire. Decomposes wth posible exploson on SD ml HNO. Staring. Inmsre 10-30 WT S3RH.Cr Ti a aria and sind Hod nab 5-306 Do TS 3900, ve SnLAF eave a ESV IAS 1omt gor a5 nl water oo * Tecra W SOU K epoaen@ ean, TOV, 510s Then SOV W SoR 109 sodium tosutate ‘Br specimen ls anode, 10V, e108 100 mt water us 2 mbH, 50, dtl at $10 V for 5-185. Use platinum wires He SO, may 8 ncroases 0 20 ml. 100 rs water Yor cooper atack 1eomL HNO, wr 20mLHNO, Immerse 5-90 ‘Copyiht by ASTM inal sights reserved); Th Sep 201021459 EDT 2012. g owloaéedpined by MC MASTER UNIVER:(fly 407 - 07" TABLE 2 Continued eae Cemooaten Preceaare 9 50 mLHC! Immerse 10-90 & De not store, 2 mH, 0, (0%) 180 eo mL! Use a carted and estes ood. De not sore, Swab fe seconds fo a mouse Properly 20mL HNO, ‘scar when sluton tame dar yolow. 40 mk geo! 25m PND, 160 mt water 182 85 mL Ni OF Use cated and tested hood, meres 5-15 8, De not slareDecompases, 15mLH, 0,(80%) 19 10mLHNOS Use acento’ and tested hood. Do nt store, Ads HNO. ne. Property scars when sre SoU HCl ‘yolon, immerse 10-60 s. Proteating specten in bong water Rastns reaction, 60m ghewot 1st so mLHC! Immerse 10-100 , 50 mL thanol (85%) oF methanol (95%) 185 mi selec aid Use a cetitod an tested hod. immerse 1-15 min, (Up 1630 lo HCI may be uted fo tem Ho! mote vigotous ion} Stable fo 3-90 dys, dapanding on HC concentaons. Use appro 100 mL thanal (05%) oF methanol (95 fate goves. 188 1 gthiowea ctl 0.005-0001 Nem, 1-2 min sr 2530:05 Use a cenit and testo hood. Immerse 5-20 sm HOI 188 lomL HF ‘Swab 5-15 Do no store Property discard air use Suton decomposes on standing, 10m HNO, 20m geo! 20 mL HNO, Som ace acis ssi He 50, SmUHNO, 50 mt water TE * ‘Swab 1-5 inh SSN Ais as GR SGA. Tech, Swab wh Souion BTS Repeat # necessary. The HF may be vari © give rare ot es ectng. Do net Soe. 50 mt ace aces 20 mL lace ace Om -NO, idm HE Te Brn, 50, Tmerse 5-80 , Use We Sakon Tor aerate Gh and pon 35 dope HO, (50%) 30 mt vaio Ter SOL NO: TSH BAT A OST HE, SAE TTT 50 g ammonium bitworde 165 tom He! (@) Becrotyic at 10 for 20s, Uso carbon eatnode and platinum wie connect to (0) Eerie at 6 Vor 10s Use stiles sie! cathode and pata or Nome wie contacto specimen ‘Copyriht by ASTM intl sighs reserved) Thu Sep 20101489 EDT 2012. owloaéedpined by MC MASTER UNIVER:(fly 407 - 07" TABLE 2 Continued eae Cemooaten Preceaare 108 a Uso a certios ana totes hood~Can give of exvemely posonous hyetogen evan. 209 ammonium pots Precauson—Aso posonous by ingestion 2s wal as skin contact Max + rato of Sc ‘90 me water ton AandB ust before use. (A muro of § drops of each wil over he surface ot an 3 ‘is mount} Innere tosoveral mints, 209KoN 187 S9Nacn Use a corte ans tested hood Can giv of extremely ptonaus ystegen cyanide 100 rs water Precaution Alo poisonous by gest as wok 8s sk conc! Elec at 1-8 Va 168 20 LHC! CCemposton given wil state the soliton wh NaCl, Electrteat 16 V a for ¥ min, {59 Naci 0 mk water 169 SmLHNO, Eleevoye a 0.05 Ae? or 2 min. Use sarass sea cathode 50 mL eyene aol 20 mi shanal 65%) or maranol (95%) 170 tLe (a) Swab 5-00 «Follow wih water sie lehal nse dy ‘som. HNO, (0) Swab for 10 interval inrease HF to exaggerate gran boundaries. ‘0 ml lace ald ™ conconted HCI Use a cored and tested hood, Elctroti tS V ac fr 1-2 min. Fos ech polishing, use ‘shorter tee Plow wih water fea, lehol nee, andy sr a Use a comtied ana testea hood—Can gh of exvemaly poisonous rystogen cyan. Saqsmmonmperatte __Pracavton Also posonaus by ngeton as wel as kn contact Prepare = more ot S00 mt weier Solitons A and But Boor use Ursa drops ofeach wl cove hosts of 8 2 "na mount) immerse 1-2 min 5 gKON 100 ml water w 50 mLNMy OF Immerse ow seconds fo 9 minule. to-admLH, 0, (50%) v4 a Use a conte and tested hood, Prepare 1 +1 mbcure ot Solitons Aand 8 Apt with camel's hai brush Nonacharent imo siver chromate should ‘rm. i fim adheres, 260 19 Ks Gr Oy 1000 mL water 3 409.010, 3gNs, 50, 18 9c, Use acenties and tested hood, Immerse to 1 min, time S0. 000 mt water 178 29 FeCl, Inmerse 5-90» ” 10g NaOH ‘swab or immerse 5-185 20m HNO, 0 mt laste ald 173 a Use a cortiod and tested hood—Mix Sluson 8 very slowly Soaion Ais used a8 a chemiaipolsn, tough some staring wil occur Swab 2 of more minus for deste Su Taco. eutace ls meufioenty etched uso Souton B elecrolicaly at 5-1 Al.® of -spocimen. Use carbon cafheds an pathum wre cornecton to spose. Properly 1oMLENO, 0m lacie abe 8 tom ‘Copyriht by ASTM inal sighs reserved) Thu Sep 201021459 EDT 2012 1g owloaéedpined by MC MASTER UNIVER:(fly 407 - 07" TABLE 2 Continued eae Cemooaten Preceaare 100 10mLHNO, Use a certed and testo hood, Immerse for Ye—10 min at 96 to 42°C (100-108"F. Do ‘om aca eit not tre Property card alr ute. Saluton composes on slang. sO mb gvesrol TT Ba HCl Sab eT 100 than (95%) oF methanol (85% 182 10mLHNO, Use a cetied and tested hood. Immerse for Yo —10 mina 36 to 42°C (100-108"F. Do ‘so ml acate ace ot Sore Propory discard alaruse. Soon decomposes on stanang 80m gyeorl 189 2 dors HF Immert or + min, Oo nt sor. Propaty aca afer ue, Soliton decomposes 1 trop rN sanding. 25m gyeerol 108 109 Foci, Immerse or Ye in 2m HCl 185 lomLuF ‘ab for fo scone 30m HNO, SmUHNO, fe mt water ser some Swab 3-20 50 mL water 108 imcHe Use a certios and tested hood, Swab ut stain removed, 2m HNOy so mL H, 0. (30%) SO mL water 169 somLue ‘Swab 3-20. Do not store Property discard aor use Sluton decomposes on standing 45 mi geo! 20 mi water 190 8 9KOH Saab 3-20 so mit, 0, (20°) 0 mi water 0 25 m1. HE Saab 3-20 18.9 banrkoniim cdorde "8 metal (5 0), 0 mt ghewol 192 tance ‘Swab 3-10 or mmerse 10-30 5. (HF atacks ana HNO, organs the suace of ta 26m. HNO, ‘lum. Wake concanraton changes on is basi) 100 rs water 193 2 dope HE ‘Swab 3-20 8. Do nat store Property card sir use luton decomposes on standng ‘atop HNO SmL HC 25 mL geet 0 2omLuF nmacss $-20 s.0e no tore Properly card ater use, Souon decomposes on tana 20mL HNO, ina 60 mt geo! 195 S0 mL Hy PO, lcd at 18-20 V (0.03 Nem or 5-15 mn ‘0 mL eye dhol Omi stnanl (8 5) 198 18960, Uso a corto’ and tested hood, Dissove C10 ot wale and coo bole asking ace ‘7 mb aos acid 20, Koop sluton Below °C (95°F) durag use, Elo at BDV for 5-90 min Do Mat ‘Zam water ‘ore 97 5 g oxalic acid Elect at 6 V for 5-20 100 rs water ‘Copyriht by ASTM intl sighs reserved) Thu Sep 201021459 EDT 2012. jg owloaéedpined by MC MASTER UNIVER:(fly 407 - 07" TABLE 2 Continued Cemooaten 198 199 203 207 208 200 a0 mie 0mL ayer} 2 mune 5 gA0NO, a 409.010, 39N2, 50, 409010, 200 mL water 499.010, 15g ap 80, 200 mL water 40900, a 10900, 1gNa, 50, 409010, 20m water 2060, 100 water 0 mL porchione ald TO mL gheeto| ‘om ethrcl (98 6) 2m AGNO, (5 %) 00 ms water 10 mL HNO, 100 mi gest 20mL HNO, Sok water 1 mLNH, OF 5. ammonium perstate 1SmLHNO, etd 50 mL wate (cls satrated with soca ‘hsuiste 1 a potassium metabisuio 3g potassum metabisute 10g sium tosuato ‘Swab or 60s, Do not store. Propo scat ater use, Solution decomposes on standing ‘su for S5 Use a certied and testes hood. Immerse in Solution A wih gene agtaton for several “otonde, Pines n Soluson 8 Use a certtied and tested hood, Imes in Soliton A wih gre again for several Use a carted and testehood, Inmet in Soon A for 2-5 ingen Sokiton Use a cat an teste hood. Eectroyic at 02 Alon for 8s. Use na wash dounprechori ated tune hood. Precautln—Keep coo when mbing end use. Elctoytc at 15-50 V for 15-80. ‘Swab vigrousty for 10-80, Wet clon Frequent. Prectuon—Properycectd ator uo, Soliton decemposes on sanding. Elecite at o12Viert-10min, ‘Sab lor 6-90 Deol store Immerse or swab fow seconde to 8 mine Immerse §-60 Fst greet in stock scion. Aad potassum metalslte before use. Soliton gon for ‘soveral days, or niger morse faco up, gonty aie unl eairaionbeghs allow fo ote. Sop eich when suraca'redlet Els na varios with male Cols matrix Use fresh soliton. Inmersa specimen face up gery agate solution ut clean beg, allow sete. Step oth when suraco Is rea-volt. Ech ime varos wih matoal ‘Copyriht by ASTM intl sighs reserved) Thu Sep 201021459 EDT 2012.99 owloaéedpined by MC MASTER UNIVER: