\ \ \. INSTRUCTION MANUAL TO. KK Industrial sensor with refillable internal solution electrode IMMERSION TYPE pH/ORP SENSOR MODEL HC-763, etc. (Models HC-763/703C/703F/7031/753/753C/753F/753T), (Models SHC-763/703) @ Please keep this instruction manual close a hand of the persons who are in charge ot the operation of this product @ Before operating this product, please read this instruction manual carefully fr is correct handling No. HC7-1849700EModel: WC-163 Introduction (2) Thank you very much for your purchase of our product. The Immersion Type pH/ORP Sensor (hereafter called the product or sensor) can measure pH or ORP (Oxygen Reduction Potential) of a solution when the sensor is connected to an industrial pH meter transmitter or ORP meter transmitter (®)This product is an immersion type sensor combined with a refillable internal solution electrode, This manual describes about this sensor, For transmitter to combine with the sensor, refer to the instruction manual attached fo the transmitter (c)There is a possibility that the product indicates or outputs an erroneous measured value by the following causes, Prepare a backup system so that no damage occurs to the related facilities even in the case like these. ‘= Any problem of the product such as deterioration or damage of the detecting section or inappropriate insulation of cables. «+ Improper setting of operating conditions or calibration operation. + Electrical interference such as noise in the vicinity or improper grounding * Other unpredictable phenomena (@)Since important items are described in “Safety Information,” read the contents carefully. (©) The product should be handled by persons who have received proper training. In addition, for technical services such as repairs, ask a specialist to do who is qualified for the technical certification system in our company oF a person who hnas technical skills equivalent to that certification system,Mode HC-763 cre Stery information Safety Information (1) Meaning of markings Meaning of symbols such as the ones used in notations of warning in the instruction manval is described below. In addition, the alert symbol (4\: General caution symbol) used on a product label, etc. is meant to notify the existence of hazard/loss and it also means “Refer to the Instruction Manual” A\warnines: Indicates the degree of hazard which can lead to death ot serious injury if you fail to operate the product properly. Serious injury means an injury such as loss of sight, burns (high temperature or low temperature), electric shock, bone fracture and poisoning, and the aftereffects of the injury remains or the injury requires hospitatization or long periods of outpatient treatment. A\GAUTION: Indicates the degree of hazard/loss which can result in minor injury or property damage if you fail 10 operate the product properly. Minor injury means an injury not requiring hospitalization or long periods of outpatient treatment. Property damage refers to damage that affects property around the product such as equipment and buildings (wide-ranging damage). [IMPORTANT] Indicates important matters such as to prevent damage to the product main body, prevent data destruction, prevent wasting time, and maintain performance: (NOTE) Indicates comments, reasons, background information, a case example and other items to help the reader understand the meaning [= Indicates reference items, ®, ®, ® -ndicates item numbers such as the ones used in operations (2) Safety compliance items Z\WARNING Fall Injury @ When you work near the measurement reservoir, take fall prevention measures such as wearing safety belt. In addition, to prevent injury, wear a hetmet, life jacket, safety shoes, etc,Softy tora Mode! HC-763 ae (3) A\GAUTION Disassembly and Modification @ Do not disassemble or modify the sections of the product that are not described in the instruction manual. The product can be damaged Warning Label Lost @ if any warning label affixed to this product becomes too difficult to read or lost, please order a new one through your local sales agent or our sales office and affix it fo its original position Disposal @ In case you dispose of this product or any part of this product, handle it as industrial waste as specified by law. Notes on use of the instruction manual Important items such as “Safety compliance items” are described in this manual. Handle the manual as follows: (@)The instruction manual is required not only at the start of operation but also required when maintenance is performed or in case a fire occurs. Please Keep the manual at hand all the time 50 that the operator who actually operates the product can read the manual at any time, (yIF the manual is lost or too smeared to read, please order a new copy through your focal sales agent or directly from our sales office. (©)Some of the diagrams used in the manual or on product labels may be modified with part of their shapes or displays omitted or they may be described in abstract form. In addition, numbers etc. shown on the screen example are just examples for such cases. (The contents of the manual may be changed without prior notice for reasons such as to improve performance. (Intellectual property right of the manual belongs to DKK-TOA. All or part of the manual must not be reproduced without permission,Model 10-763 Warranty Warranty (1) Warranty Coverage DKK-TOA Corporation (DKK-TOA) warrants its produets against defective material or workmanship forthe warranty period, (@) The warranty period is one year from the date of delivery to the original user. the date of delivery eannot be specified, the waranty period is 24 months from the month following the date of manufacture shown on the product nameplate () Specitie written agreements with DKK-TOA, if any, shall take precedence over this warranty. (©) The limitation of warranty described herein may not apply where applicable laws do not allow such limitation, 2 Limited Warranty This warranty does not cover the cass listed below. (9) Direct o° indirect failure or damage caused by the use of the product for a purpose or in a manner not prescribed by the specifications or the instruction manual for the product (b) Director indirect feilure ot damage caused by force majeure, including but not limited to an act of God, natural disaster such as earthquake, storm and flood damage, and lightning, fire, accideat, abnormal voltage, salt damage, 225 damage, Inbor unrest, acts of war (declared or undeclared), terrorism, civil strife, or acts of any governmental jurisdiction () Failure or damage caused by any repair or modification not authorized by DKK-TOA. (@) Failure or damage caused by the transport, moving, or dropping of the product after the purchase that is not attributable to DKK-TOA. (©) Electrodes and consumables (The warranty period for each part has priority when the period is shorter than that for the main unit of the product. Ifthe customer requires any part after more than six months from the date of manufacture, consult DKK-TOA oF its distributer.) { £) Failure or damage caused by the use of consumables, parts, or software not supplied by DKK-TOA. (g) Malfunctions or damage caused by the use of connecting equipment not supplied by DKK-TOA. {h) Loss of data, settings, programs, or software stored on the product not attributable to DKK-TOA, (4) Any product other than DKK-TOA'S, if specified by the purchaser or user, that incorporates or is incorporated into ‘or combined with DKK-TOA’s products (#1). In such cases, this warranty covers DKK-TOA's produets only. (J) Any product net under proper maintenance in accordance with the instruction manual furnished by DKK-TOA, (0) Products without a nameplate (excluding products proved to have been delivered by DKK-TOA). EXCEPT AS EXPRESSLY SET FORTH IN THE PRECEDING SENTENCES, DKK-TOA MAKES NO WARRANTY OF ANY KIND WHATSOEVER WITH RESPECT TO ANY PRODUCT. DKK-TOA EXPRESSLY DISCLAIMS ANY WARANTY IMPLIED BY LAW, INCLUDING BUT NOT LIMITED TO ANY WARRANTY OF MERCHANTABILITY OR FITNESS FOR A PARTICULAR PURPOSE. LIMITATION OF REMEDIES: In the evont that a defect is discovered within the warranty period, DKK-TOA or its authorized distributor will tits option, repair or replace the defective product or its part, or will refund the purchase price ofthe product. THIS 1S THE EXCLUSIVE REMEDY FOR ANY BREACH OF WARRANTY. LIMITATION OF DAMAGES: IN NO EVENT SHALL DKK-TOA BE LIABLE FOR ANY INCIDENTAL OR CONSEQUENTIAL DAMAGES OF ANY KIND FOR BREACH OF ANY WARRANTY, NEGLIGENCE, ON THE BASIS OF STRICT LIABILITY, OR OTHERWISE. (3) Others (a) Produet parts for maintenance (#2) will normally be supplied for five years (*3) from the date manufacturing and sales are discontinued () The cause of any malfunction or damage shall be determined by a DKK-TOA technician (c} For repairs, contact a local distributor in your country or state "1: Warranties for products from other companies must be maintained by the user. "2: Maintenance parts refers to parts that are required to maintain operation of the produet. 3: This five-year period is subject to availability of parts or their replacement,Dowel, HO-765 ot eating ike Reading Guide Refer to the necessary sections of this instruction manual depending on your purposes such as understanding the outline of this product or starting the product as shown below. The numbers in circles indicate sections to be referred to in sequential order Purpose |} Start Maintenance (startup) _} | and inspection, ‘and troubleshooting Check installation, piping and wiring Understand the outline of this product Section Introduction © Safety Information 1. Configuration and Names of Each Part 2. Preparation before Operation 3. Stopping the Operation }4, Maintenance Spee 2 5, Troubleshooting 3 6. Specifications — 7. Installation NEModel: C763 ot Table of Contents Table of Contents _ @ Introduction 1 @Safety Information 2 (1) Meaning of markings “= 2 (2) Safety compliance items 2 (3) Notes on use of the instruction manual =~ 3 @Warranty . See ; cd @Reading Guide _ . " 5 1. Configuration and Names of Each Part Sete 1.1 Configuration Example and Specification Check 9 1.2 Names of Each Part for Main Sensors resem 10 1.3. Installation Example and Names of Each Part~ n 2. Preparation before Operation Suannenenelc 2.1 Procedure of preparation before operation- 7 eee meee 12. 2.2. Installing Electrode- zs eer Perret . eer ae (1) Key points of electrode installation ~~ 16 (2) Installing electrode for head pressure type sensor ~~ 16 G) Installing electrode for pressurized type sensor ~~ 17 2.3. Filling Internal Solution rns z eee 30) (1) Key points of how to fill internal solution -~- 20 (2) Filling internal solution for head pressure type sensor ~~ 20 (3) Filling internal solution for pressurized type sensor -~ 21 (4) Preparation of internal solution = 21 2.4 Pressurizing the Internal Solution. “ 23 (1) Key points of pressurization «= 23 (2) Guideline for pressurization 25 (3) Pressurization using instrument air ~~ 23 (4) Pressurization using a manual pressurization pump ~~ 24 3. Stopping the Operation a 5 res BS 3.1. Stopping the Operation for a Short Period of Time: rereareee 2S, 3.2. Stopping the Operation for a Long Period of Times--~-~ sree 5 4. Maintenance a 4.1 Maintenance List a a 27 4.2. Accessories, Kits and Spare Parts for One Year: 29 -6-Monit HOH (1) Accessories 29 (2) pl calibration kit and ORP check hit -~ 30 (3) Spare parts for one year = 32 4.3 Mounting/Removing the Sensor- 33 (1) Key points of mounting/removing the sensor -- 33 (2) How to remove the sensor =~ 33, (3) How to mount the sensor --- 35 4.4 Replenishing Internal Solution - : ” (1) Key points of replenishing internal solution += 37 (2) Replenishing internal solution for head pressure type sensor -»-38 (2) Replenishing internal solution for pressurized type sensor ~~ 38 4.5 Cleaning the electrode 39 (1) Procedures for cleaning the electrode and inspection of liquid junetion (2) Cleaning the pH electrode with tough dirt --- 40 (3) Cleaning the ORP electrode with tough dirt 41 4.6 Replacing the Electrode: 42, (1) Replacing the electrode for head pressure type sensor ---- 42, (2) Replacing the electrode for pressurized type sensor ~~ 23, 5. Troubleshooting~~-~---~ oon 45 5.1 Determining the location of failure eeeens sea oS 5.2 Cause of Fallure and Necessary Action . se 46 6. Specifications wm pitt eeaetag 6.1 Sensor Specifications: : 48 (1) Common specifications ~~ 48 2) Modet HC-763 and Model SHC-763 specifications «48 (3) Model HC-703C and Model SHC-703 (PVC) specifications -~ 49 (A) Model HC-703F and Model SHC-703 (PDF) specifications ~~ 49 (5) Model HC-703T and Model SHC-703 (PFA) specifications -~- 50 (6) Model HC-753 specifications --- 51 (7) Model HC-753C specifications »-- 51 (8) Model HC-753F specifications =~ 52 (9) Model HC-753T specifications --- 53 6.2 Electrode Specifications z “ 54 (1) Specifications of main pH electrodes ~- 54 (2) Specifications of main ORP electrodes «$5 (3) Checking items for selection of pl electrode -~- 56 7. Installation 7 Z 57 7.1 Key Points of Installation Conditions and Mounting co $7 (1) Conditions of installation location «$7 (2) Key points of mounting the sensor ~~ $7 SageMode: 10-763 ee Table of Contens 7.2. Mounting the Sensor: 39 (1) Mounting the sensor to foundation bolts =~: 59 (2) Mounting the sensor to a pole using Model ZC-1B / ZC-1C bracket ~~ 60 (3) Mounting the sensor to a pole using Model ZC-2 bracket = 61 (4) Mounting the sensor using Model ZCD- bracket ~~ 63 (S) Mounting the sensor using loose flanges“ 64 7.3. Instrument Air Piping: 66 (1) Connecting to the piping system of instrument air -- 66 (2) Installing the air set» 66 (Last page -~- 68)Mosel: HO-763 oe | Configuration Example and Specification Creek 1. Configuration and Names of Each Part — ] 1.1. Configuration Example and Specification Check ‘When sensor cable is used oe ble (an | Connector box eee fy Centodeeodwies l — Li oH Meter Transmitter o Receiving stent ORP Meter Transmitter (ecorderete} Sensor Configuration Example of Main Devices (@) When you install pH electrode in this sensor (or itis already installed), use an industrial pH meter transmitter to combined with this sensor. When you install ORP electrode in this sensor (or it is already installed), use an industrial ORP meter transmitter to combined with this sensor. (b)By operation, this sensor can be separated into two main types: pressurized type and head pressure (atmospheric pressure) type. Check the model name of the sensor for operation and read the corresponding item in this instruction manual (©) The sample pressure range differs depending on the model name and the operating temperature range differs depending on the electrode combined. For example, the operating temperature range of the sensor is ~5 to 80°C: but the operating temperature range of the electrode may be ~5 to 50°C. Check the model name of the sensor and use it in a condition conforming to its specification (>> 6.1 “Sensor Specifications", 6.2 “Electrode Specifications” (a) The electrode of DKK-TOA to be installed in this sensor, except for a special case, contains a temperature element of 10k(2/25°C. Use a DKK-TOA transmitter containing a corresponding temperature circuit (10kQ at 25°C) to combine with this sensor. (@)IF it is not possible to connect the electrode lead wires directly to the transmitter when this sensor is installed away from the transmitter, a sensor cable and a connector box are required, [>> Instruction manual of the transmitter.Model HC.763 6 2 Names of ach Par for Min Sensors 1.2 Names of Each Part for Main Sensors Electrode lead Pressure gauge _— Blectiode lead wires Halder cap wires (010 02MPa) [o}-—nirsatton pssscatoninn kp Hiorson sina se filing hele Instrument ai E specication: Ret/ Manval pressurization pump specification: — Holder Holder Equipped with LJ (made of PP material, ete) (made ot PP material, pressurization inlet rit ete.) 4 BHIORE electrode "1 roteton piping PH/ORP elestode "1 — actecton pining ~=Preseurized Type> (Mode's HC-763, HO-7030, HC-703F, HC-7031) (Models HC-783, HC-7530, HC-753F, HO-7531 (Models SHC-763, SHC-703) Names of Each Part for Main Sensors (a) The measurement object of this sensor is for a sample solution of atmospheric pressure such as water in a reservoir. (b)Difference of model names depends mainly on the material of the holder used. However, “S” at the start of the model name indicates the sensor is an explosion-protection type and itis used when combined with an explosion-protection type transmitter. The shape, structure and handling instructions are the same as those of the normal type and the model name only differs. (©) The head pressure type (also called atmospheric pressure type) sensor uses the head pressure between the liquid surfaces of sample solution and internal solution in the sensor for internal solution to seep out and leaving the inside of the sensor open to atmosphere. The pressurized type sensor uses instrument air or a manual pressurization pump to pressurize the inside of the sensor. ~10-Model C263 13° tnsiion Ssnpe an Names of eh Pat 1.3 Installation Exampie and Names of Each Part Pole stand (Model 28-1, 508 stee! pipe) (Option) 7 Electrode lead wires Holder mounting (bracket Hodercamp.__ (Pi. (Mode! 20-18) eo ‘ \ Air sot (Madel PAS-10) pq @ption) ;pport bar wweasi zn) /| | Stop vane /' Wot provided as accessory) _— Instrument air Holder guide. Protection piping ~ i Installation Example and Names of Each Part (2)'The minimum configuration of the sensor consists of the sensor main body (holder, protection piping, electrode, etc.) and other parts, such as a holder guide, support bar, holder mounting brackei, air set and a pole stand) will be added depending on the ordered specification. (b)Parts such as a valve on the supply side of the air set shown in the diagram above are not included in the supplied products. (©)For names of each part for mounting bracket or air set, refer to the corresponding items. (>> 7.2 “Mounting the Sensor”, 7.3(2) “Installing the air set” SatModel HC-763 ee 21 Procedure of preparation bere wperaion = 2 _ Preparation before Operation (@)This scetion explains about preparation required before starting the operation. Since the description of preparation items differs partly depending on the head pressure type or pressurized type, refer to the corresponding items to operate the sensor, (b)This sensor does not need procedure to make it operational (operation starting procedure after power is supplied to the transmitter). When this preparation before operation is completed and making the transmitter ready for operation, this sensor also becomes ready for operation automatically 2.1 Procedure of preparation before operation Follow the procedure below for sensor to prepare before operation. A\WARNING Fall Injury ® When you work near the measurement reservoir, take fall prevention measures such as wearing safety belt. In addition, to prevent injury, wear a helmet, life jacket, safety shoes, etc. @Cheeck the installation. Check that the necessary work regarding installation is completed. [= 7. “Installation” @Remove the sensor. ---- if the sensor is mounted by support fixtures, etc., remove the sensor. + If the measurement system is in operation, remove it safely by following the reference items. (= 4.32) “How to remove the sensor” Electrode lead wires _- Suppo ba (Model ZN-7) Clamp —~ ee Section A oe (Press here to untesten the hook) | Hook-— Sensor Opening / Closing the Holder Clamp install the electrode. If the electrode is not installed in the sensor, install it by following the reference items, [= 2.2 “Installing Electrode” @Fill internal solution. --~ If the sensor is not fitled with internal solution, fill internal solution by following the reference items. C= 2.3 “Filling Internal Solution” -12-Mode 10-953 ee 1 Proesdme of prepaaton before oprainy @Set the internat solution under atmospheric pressure or apply pressure. follows: -oceed as Lin the case of head pressure type) If the holder cap is fixed by a tie band, eur the bend using pliers, et, Then rotate the holder eap 10 ‘open the internal solution filling hole to about Imm. The pressure in the sensor becomes : atmospheric pressure. oe eon Holder cap Open to about vm, ~ internal solution filing hole “Tie band (Cutthe band) - Holder Cap UIMPORTANT] + When the internal solution filing hole of the sensor is opened, hold the sensor nearly in upright position. IFit is laid down or put it upside down, the internal solution comes out from the internal solution filling hole. [In the case of pressurized type] Apply pressure to the internal solution with instrument air or by using a manual pressurization pump. [2.4 “Pressurizing the Internal Solution” @Check that the rubber cap is removed. ---- Check that the rubber cap is not attached to the tip of the electrode. If it is attached, remove it. * Proceed quickly to the next operation so that the tip of the electrode does not dry. u _Rubber Cap Removing the Rubber Cap @Prevent drying electrode. --~ If there is time when the sensor cannot be immersed to a sample solution, immerse the tip of the sensor body in pure water (city water can also be used). =13-Mods: 0-76 21 Proce oF preparation before operation UIMPORTANT] © If the tip of the electrode is left in the air for a long time, the liquid junction and pH glass membrane (for pH electrode) dries up and its ay characteristic temporarily deteriorates, Luguid junctién It the tip of the electrode is dried, 7 PH ass membrane immerse it in internal solution for Temperature (or sensing metal) several hours and use it when the __sempersation element characteristic is restored. ‘An Example of Electrode Tip Pure water (City water can also be used) immersing the Tip of the Sensor in Pure Water @®Lower the sensor to the support bar. .-.-.. Lower the sensor to the holder guide support by putting the holder guide attached to the sensor along the support ber. C= 7.2 “Mounting the Sensor” + Ifother type of holder mounting fixture used, fix the sensor by its appropriate method. -14-sod WOT e 2 te of preparation before operation __Support bar Holder guide ~ passpieaat TITTTT? Holder guide support Mounting the Sensor Fix i with holder clamp. «=~» Open the clamp while pushing the section A of the holder clamp and push the upper part ofthe sensor to the center of the holder clamp and then close the clamp. |_— Electrode lead wires ‘Support tar (Model ZN-7) Clamp Holder camp (Press here to unfasten the hook) L— Hook— Sensor ~ Opening / Closing the Holder Clamp @Connect the electrode lead wires. Refer to the instruction manual of the transmitter to connect the electrode lead wires to the transmitter or connector box. Preparation before operation for sensor is completed. Then set the transmitter to operating condition by referring to the instruction manual of the transmitter. This sensor becomes operational together with the transmitter, ee eeHEI ee 22 tnsaing Hlectoe 2.2 Installing Electrode (1) Key points of electrode installation (@)if electrode is already installed inthe sensor, this operation is not needed (b)Hendle the electrode carefully not to damage it and not to soil the tip of the electrode. UIMPORTANT) «Do not apply strong shock to the electrode such as hitting It or dropping it to the ground. The electrode made of glass may be damaged Do not allow the tip of the electrode contaminated by fats and oils or do not touch it by dirty hand. Deterioration of the characteristic may occur. + Do not allow the crimped terminals on the end of the electrode lead wires get humidified, contaminated by fats and oils or touched by dirty hand Insulation problem may occur (2) Installing electrode for head pressure type sensor (a) In the case of head pressure type sensor, install electrode in the procedure below. (b)If electrod already installed in the sensor, this operation is not needed. isp _-Flectiode lead wires ler sotiton ting Hot Etecroge pecking \ wester | Pater Protection png \ \ sy Electrode Installing Electrode for Head Pressure Type Sensor Remove the protection piping, etc. ~~ Unscrew the protection piping to remove it and remove the washer and then extract the electrode packing from the holder. @Put through the holder. «-~- Insert the electrode from the top of the holder (on the end where internal solution filling hole exists) and take it out from the bottom of the holder. @Remove the tape and rubber cap. ---- Remove the blue tape and rubber cap from the electrode —16-—Model HC-765 at 22 Installing Eeerode Blue tape Breciode Sa ‘sre << Y name go CO Aecrode Bua oley ebvodo pack Biue Tape and Rubber Cap Installing Electrode Packing ®install the electrode packing. ---- Install the electrode packing to the position 4Smm from the tip of the electrode and install the washer also (o the electrode. ®Screw in the protection piping. --- Screw in the protection piping with electrode inserted, to the holder. install the holder cap. -»~ Put the holder cap onto the top of the holder ‘Then, fill internal solution. C= 2.3 “Filling Internal Solution” (3) Installing electrode for pressurized type sensor (a)In the case of pressurized type sensor, install electrode in the procedure below. (b)Attach a crimping terminal to each end of electrode lead wires after putting the wires through the cap and others @Remove the protection piping, eto. Unscrew the protection piping to remove it and remove the washer and then extract the electrode packing from the holder. @Remove the cage, etc. ---~ Loosen the lock nut to remove the cage from the holder and remove the cap, washer (for lead wires) and taper packing from the cage. Electrode lead wires \ Core wire Crimping terminal (Accessories for electrode) oe “bps Washer (Aocessory for electrode) Taper packing A (Accessory for elector Cage Coring (P28 oF P26) \ {installation can be mace without removing this Electrode packing coca | Holder Prseton pg ( a tod Washer Installing Electrode for Pressurized Type Sensor @Put through the holder. .- Insert the electrode from the top (on the end of lock nut) of the holder and take it out from the bottom. Sy ieModel 10-763 et 22 waling Flecwe @ Remove the tape and rubber cap. -- Remove the blue tape and rubber cap from the electrode: Blue tape i Blectiode Washer d Blue Tape and Rubber Cap Installing Electrode Packing Rubber cap Electrode \, Elestode packing Install the electrode packing. ---- Install the electrode packing to the position 45mm from the tip of the electrode and install the washer also to the electrode. ®Screw in the protection piping. ---- Screw in the protection piping with electrode inserted, to the holder. {IMPORTANT] «If the protection piping is loosened, internal solution may leak out or sample solution may flow backward to the inside of the sensor @Put through the cage. ----- Insert the electrode lead wires from the bottom of the cage and put them through the cage, and then put them through taper packing, washer and cap. install the cage.» Serew in the cage to the holder and fix it with lock nut @Fix the electrode lead wires. Allow extra length for electrode lead wires in the sensor and pull them out tothe top ofthe cage and then fix them with ap. [IMPORTANT] «If the cap is loosened, air in the sensor leaks out and pressurized air cannot be maintained @Attach crimping terminals, ---- Attach a crimping terminal to each end of the electrode lead wires as described below. Core wite 3 (Rea) [Core wire 2 Core wire 4 (Black) Bloctioce lead wires Core wite 1 (semi-transparent) Cove wite E (gray) 9.510 1mm osm Crimping terminal {accessory for electrode} \, Marker tuse \ ene ticdaces 7 [ead wires ray) crimping temminal Mather tube Remove the coating of core wire and Cote wie of electrode lead wires Couble up the conductor atthe end cross Section atter Being Crimped> Attaching Crimping Terminals to Electrode Lead Wires -18—Move HO-768 0 22 Italing Plewod {a] Put wire through marker tube, --~ As shown in the diagram “Attaching Crimping Terminals to Electrode Lead Wires,” put wire through marker tube (accessory for electrode) of the number (1 to E) corresponding to the color of the wire. [b] Put core wire through crimping terminal. Double up the conductor at the end of the core wire and insert it to the cylinder section of the crimping terminal, as shown in the diagram, UMPORTANT] « Fold back the conductor of the core wire to double it up at the end. This is to prevent improper connection * Avoid pulling out the coatings of core wire 2 (white) and core wire E (gray) with too much force. If strong force is applied, the coating may be pulled out and may result in insulation problem. + Use an appropriate size of tool for crimping and make sure that the crimped terminals do not come off and there are no wires stick out from the terminal {[c] Crimp the terminal, «-~- Fix the core wire to the cylinder section of the crimping terminal using a crimping tool [4] Wrap the crimped section with tube. ~~~ After the terminal is crimped, move the marker tube to the crimped section to wrap it up. Then, fill internal solution, [= 2.3 “Filling Internal Solution” ~19-Mose ICI we 23 fi ern Soiion 2.3 Filling Internal Solution (1) Key points of how to fill internal solution (@)Electtode is so structured that a small amount of internal solution seeps out from the liquid Junetion to sample solution. Therefore, ifthe sensor is not filled with internal solution, fill it at the time of preparation before operation and itis necessary to fil it periodically (b)If'a powder type “KCI powder for non-leak silver chloride electrode internal solution” (hereafter called powder reagent for internal solution) is used instead of a solution type non-leak silver chloride electrode internal solution (3 mol/L potassium chloride solution, hereafter called internal solution), itis necessary to prepare the internal solution beforehand, [=> 2.3(4) “Preparation of internal solution” (2) Filling internal solution for head pressure type sensor In the case of head pressure (ype sensor, fill internal solution in the procedure below. Internal solution fing hole / Holder cap \ % Internal solution filing hte Piastic beaker (containing interna solution) Upper level indication Tor Internal solution Filling Internal Solution for Head Pressure Type Sensor OPrepare internal solution. ..- Prepare internal solution in a container such as a plastic beaker. [> 2.3(4) “Preparation of internal solution” ‘The internal solution filling hole for this sensor is relatively large, a plastic beaker, instead of a wash boitle, can be used to fill internal solution Plastic beaker> Plastic wash bottle> Preparation of Internat solution @Open the internal solution filling hole, --- Rotate the holder cap to fully open the internal solution filling hole. @Fill internat solution. -.--. Fill internal solution from the internal solution filling hole, ‘If there is an upper level indication for internal solution, fill internal solution up to that level and if there is no indication, fill it to the level about SOmm below the internal solution filling hole. —20-Model HC-763 ee 2.3 hing femal Siar [IMPORTANT « For the senor filled with internal solution, hold it nearly in upright position IF itis laid down or put it upside down, the internal solution comes out from the internal solution filling hole. ‘Then, set the pressure of internal solution 10 atmospheric pressure, (=> 2.1 “Procedure of preparation before operation” G)*Check that the rubber cap is removed.” (3) Filling internal solution for pressurized type sensor In the case of pressurized type sensor, fill internal solution in the procedure below. Plastic wash bottle (containing internal sutton) Internal solution Ailing hole Pressurization oa © Upper ever incision inet |, forimema soon Cap for interna internal sotaion Salton fling hola thing hole Internal scltion Filling Internal Solution for Pressurized Type Sensor @Prepare internal solution. ---- Prepare internal solution in a container such as a plastic wash bottle Open the internat solution filing hole, ~-- Remove the cap for intemal solution filling hole @Fill internal solution. -.-- Fill internal solution from the internal solution filling hole. * If there is an upper level indication for internal solution, fill internal solution up to that level and if there is no indication, fill it to the level about 10mm below the pressurization inlet @Close the internal solution filing hole, --- Put on the cap for internal solution filling hole securely. [IMPORTANT] « If the cap for internal solution filling hole is loosened, air in the sensor leaks out and pressurized air cannot be maintained. + For the senor filled with internal solution, hold it nearly in upright position IF itis faid down or put it upside down, the internal solution comes out and may cause a feilure of the pressure gauge. Then, apply pressure to the internal solution. C= 2.1 “Procedure of preparation before operation” © Set the internal solution under atmospheric pressure or apply pressure.” (4) Preparation of internal solution (a)1f you want to use powder reagent for internal solution (KCI powder for non-leak silver chloride internal solution), prepare internal solution in the procedure below. ‘if a solution type of internal solution (non-leak silver chloride electrode internal solution) is used, this operation is not needed. —21-Mase 110-768 23 illing interna Sutin (b)Powder reagent for internal solution is available from DKK-TOA. You can also use GR grade potassiuin chloride. In either case, proceed as follows: Preparation «.. Prepare the following items » Power reagent “1 bag (112g) or 112g of GR grade potassium chloride (KCI, molec: 74.56) Pure water =~" S00mL, # Measuring flask (500mL) 1 piece @Prepare to dissolve reagent. --- Put one bag of power reagent (or 112g of GR grade potassium chloride) in a measuring flask of 500ml. Powder reagent or GA eee, i : oe os Measuring flask | —}+— Marker GoomL Preparation of Internal Solution @Make it dissolve in pure water. ~~ Add pure water until water reaches the level slightly below the marker (500mL) and stir the solution thoroughly (NOTE) «When potassium chloride dissolves, the temperature lowers @Adjust the volume at room temperature. ----- Leave it for a while and add pure water when the temperature of the measuring flask returns to nearly the room temperature Internal solution of 500mL is now ready. {NOTE} loformal preparation method Put one bag of powder reagent for internal solution in a ‘container such as beaker, and add pure water of 460ml (not SOOmL) and stir it thoroughly. This method uses the reduced volume of pure water considering the volume increase afterward -22-Moet HO-763 es 24 Pressing the interna Soutony 2.4 Pressurizing the Internal Solution (1) Key points of pressurization (a)For pressurized type sensor, the pressure of internal solution can be set higher than that of sample solution so that a small amount of internal solution flows out from the liquid junction of the electrode head ssure type sensor, pressurization by air cannot be made. (b)Pressurization method differs depending on the selection of the specification for pressurization method, ‘When the internal pressurization method is “Instrument ai”: (=> 2.4(3) “Pressurization using instrurnent air” ‘When the internal pressurization method is “Manual pressurization pump method”: => 2.4(4) “Pressurization using a manual pressurization pump” (c)The internal pressure can be checked by the pressure gauge of the sensor or by a pressure gauge of air set (option), (@Continuation of pressurization is required during measurement and also required during calibration oF when ORP standard solution is used for performance check. In addition, even when measurement is stopped, if the pressure of the sample solution is higher than the atmospheric pressure, continue the pressurization, (@)IE the sensor is in a location difficult to perform necessary work, set the transmitter to maintenance mode and remove the sensor and then move it to a location where it is easy to perform necessary work (© After operation is started and if the pressure gauge indicates a pressure lower than that of the sample solution, sample solution may be flowing back to the inside of the electrode, Pressurize the sensor correctly and perform pH calibration or use ORP standard solution for performance check, and if itis not possible to do this operation correcily, replace the electrode. (2) Guideline for pressurization (a) The pressure range of sample solution (withstand pressure), limitation of pressurization, and the scale range of pressure gauge are shown below: Pressure range of sample solution ===" Atmospheric pressure Guideline and limitation for pressurization-~-~ 0.05 to 0.1MPa Scale range of pressure gauge vere 010 0.2MPa (b)If the internal solution is pressurized to a higher value, consumption of internal solution increases and if itis less pressurized, unstable indication may occur. (3) Pressurization using instrument air (a) When the ordered specification for internal solution pressurization is “Instrument air”, the specification for pressurization inlet is as follows: ‘* Pressurization inlet ~-+ Female taper pipe thread (Re!1/8) (®)Apply instrument air to the piping connected to the pressurization inlet of a pressure value corresponding to that of the sample solution, [== 2.4(2) “Guideline for pressurization” (©)For piping work to the pressurization inlet, refer to 7.3 “Instrument Air Piping”. —~23-Mosel: WC-764 ere 24 Passurizing the lena Sotion (4) Pressurization using a manual pressurization pump Pedal Thread for bicycle use / pee ee t Pressurization inlet unit (Check valve for bicycle use) Prossute gauge Ar pressure meter (Option) Pressurization using Manual Pressurization Pump (@)If the selected specification for internal solution pressurization is “Manual pressurization pump, method”, a pressurization inet unit (check valve for bicycle) is provided at the pressurization inlet of the sensor. (b)Pressurization can be performed while measurement is continued. However, if it is difficult to perform pressurizing work, set the transmitter to maintenance mode and remove the sensor, and move it to a location where itis easy to perform necessary work. ‘Connect a manual pressurization pump. --- Install the manual pressurization pump (foot pump) by referring to its instruction manuial for operation, and connect the threaded end of the hose (for bieycle use) to the pressurization inlet. @Apply prossure, .... While checking the indication of pressure gage, step on the pedal of the ‘manual pressurization pump repeatedly and stop when the pressure gauge indicates the specified pressure, + Ifthe pressure decreases soon after it is pressurized, itis probable that the tube (62 $3 x 30mm) for pressurization inlet check valve in the pressurization inlet unit is deteriorated to work properly as a check valve. In this case, replace the tube A Pressurization inet unit ~. (Check valve for bieyote use) Ppa oxing ? Sh, Caprut ieee of inlot check valve Qa) (62x63%30mm) Pressurization Inlet Unit @Remove the manual pressurization pump. ~-- Remove the hose of the manual pressurization pump from the pressurization inlet. ‘+ If the sensor is removed for pressurization work, reinstall the sensor in the same way as before. -24-Mode: 1-763 ae 3.1. Stepping the Opsaton for a Shon Pera of Tune 32 Stopping dhe Opermion fora Lame Peo ef Ti 3. Stopping the Operation 3.1 Stopping the Operation for a Short Period of Time Iis not needed to do the necessary work if you stop the operation for a short period (2 weeks) for which there is no fear of electrode being contaminated. However, if there is a possibility of electrode getting ditty or the electrode tip exposed to open air and dries up, take action of 3.2 “Stopping the Operation for @ Long Period of Tite” 3.2 Stopping the Operation for a Long Period of Time If there is a fear of electrode getting dirty or if the period of operation stop is expected to go beyond the short period (2 weeks), stop the operation of the transmitter and proceed as follows (Remove the sensor, » Remove the sensor from the holder mounting bracket [= 4.3(2) "How to remove the sensor” ZA\WaARNING Fall Injury ® When you work near the measurement reservoir, take fall prevention measures such as wearing safety belt. In addition, to prevent injury, wear a helmet, life jacket, safety shoes, etc. @Close the internal solution filling hole or stop the pressurization. - Proceed as follows [In the case of head pressure type sensor] Close the internal solution filling hole by rotating the holder cap. -25-Model HC-763 ot, 32. Stop ie Opection fra Long Pee oF Fine Oc Internal solution filing Pole Closing the Internal Solution Filling Hole [In the case of pressurized type sensor] Ifthe sensor is pressurized by instrument air, stop the supply of instrument air. [7.3 “Instrument Air Piping” @wash the tip of the sensor, »-» Wash the periphery of liquid contact area for sensor using clean water. @Remove the electrode lead wires. «... Refer to the instruction manual of the transmitter to remove the terminals of the electrode lead wires from the transmitter or from the connector box ®Remove the instrument air piping. If it is necessary to remove the instrument air piping, remove it from the pressurization inlet of the sensor. @Take measures to prevent electrode being dried and store it. .--- Immerse the tip of the sensor to pure water (city water can also be used) and store it in a place where direct sunlight does not strike. Pure water {City water con also be used) Storing the Sensor by immersing the Tip of Sensor in Pure Water [IMPORTANT] «if the tip of the electrode is left in the air for a long time, the liquid junction and pH glass membrane (for pH electrode) dries up and its characteristic temporarily deteriorates. IF the tip of the electrode is dried, immerse it in internal solution for several hours and use it when the characteristic is restored, To start the operation again, refer to 2.1 “Procedure of preparation before operation”. BaeMove HC-263 ae 41 Maimenanee Lis 4, Maintenance 4.1 Maintenance List (@)'To operate the product correctly and maintain the specified performance, itis necessary for you to thoroughily understand its functions and perform maintenance periodically. [IMPORTANT] «If periodical maintenance is not performed, equipment failure may occur. (b)The “Maintenance cycle” described in the following table is based on the standard condition of installation location (conditional state that satisfies the items in 7.1(1) “Condition of installation location”). Since the maintenance cycle differs depending on the installation condition, modify the cycle depending on the operation results of more than several months. (©)For technical services such as repairs, please call a sales representative in your area or directly contact our company, A specialist who has attended a technical training course in our company or a person who has technical skills equivalent to that course must perform technical services. (€)"O"indicates the guideline maintenance cycles to manage the measurement system under the supervision of maintenance standard (repeatability #0.1pH) of Water Works Law. This marking is indicated only for items where the cycle differs from general maintenance method Maintenance List Wancanes oye Hem] Target Deseription ale le] [E| exccuion metnoa ee slElEE\2 2 (ER (2 H\= |e] |S |e | [2/5 Sear sang ecco] T [Internal solution Replenishment Oo Oo = 4.4 “Replenishing era oon F |Pressure gauge [Cheek the pressure with | © o [== 2.42) “Guideline for [Pressurization using Oo [== 2.4(4) “Pressurization fn pp feign inane [raat ressoraton restoration pr lpump type) 7 ota tautd—foeaing OT] esse ihe aon vay omc ston tits din. ash hen wae ros Canine te ies [[Electrode] 4 [Glass surface, Cleaning O/e > 4.5 “Cleaning the roa srac n sro: gid uncon 5 [Liquid junction [Check that it is not @ oO E> 4.5(1) “Procedures for [trprecrces [ogee isang te clesrode ane bee) aspen o i © [Electrode in [Replacement OO] [O[e=46 “Replacing the eens iccroue (To be continued) oyManel C765 a L Msimtenance Last (Continued fom previows page) Niintenance ele a tiem] Target Description alee | |e | exccmionmethod, ee gle VEE (2 [2 | (ELE B= |e ie lade je [212 Overall measurement system) 7 [iransmiterand [Calibration Calibration [O] [© = nsiaetion manual oF sensor jorcheck for pH meter the transmit [GRPmeer [OT [O check (Ov in the case of general maintenance © ~-Cyele for maintensnce standard based on the Water Works Law and the eyele differs from generat maintenance method, —28-Mosel C7636 12 Acsussoves, Kis aa Spare Pats or One Yess 4.2 Accessories, Kits and Spare Parts for One Year Examples of accessories, pH calibration kit, ORP check kit snd spare parts for one year are shown below. These items differ depending on the ordered specification and may change without prior q) notice Accessories The instruction manual contained jn the accessories may be sent separately from the product depending on the ordered specification, Example of Accessories Geamiity Item | Code No. | Part name (Code name) Sketch view g 3 Remarks 8lé 7 instruction manual ia a [1434252 [internat sotation "TF rovided when holder (intemal solution of z length is 3m or more fhon-leak silver eoride 2 One botte per tm oF electrode) 2 holder length 3 + For non-leak silver 7 chloride electrode (3M z potassium chloride 5 olution) a +5001. 3 | 143A053 | Powder reagent for =e, [One bag per im of holder internal solution <> & | "rengn (KCI for internal & | eFornon-tcaksitver Si aie § | chloride electrode (for 3M silver chloride hd tassium chloride ecto) 3 | Sitiony | o112¢ for Soom, a 7] 3970030K [Tube assembly for 1) | eProvided when sensor 8 pressurization falet, manual pressurization heck valve pump type (option) 94243 30mm, containing 2 pieces 3 [1258971 | Manual pressurieation T [1] Provided when sensor a pump ‘(Pocket pump pedal inflation) ks> nee sae I ae —29-Mode: HC-763 ee 1.2 Accesories, Kits an Spe Pars For One Year (2) pH calibration kit and ORP check kit (a)Depending on the ordered specification, pH calibration kit or ORP check kit corresponding to the ‘model and specification of the sensor is added, (by The type of kits differs depending on whether itis for domestic use or for overseas use and also it depends on the measuring range. The detailed items are shown in the following table. The quantity shown is for one kit. (©)For operation of pH meter calibration and ORP meter check, refer to the instruction manual of the transmitter. pH Calibration Kit Quantity Domestic | Overseas em | Code No, | Part name (Code name) Skech view |Z |Z | 2/2 Remarks 32 [3 |e 1 [136C05s | Beaker T[2 [2 | 2 [ever som. Made of polyethylene 2 _[TBEIOI [pH Ot standard saltion TPT T= Paton (Phthalate pH standaré solution (pH4.01)) 3 |GET? [pH6 86 standard saltion TPT t= Fito {Neutral phosphate ptt Sandard solution (pH6.86)) 7 143FI93_[pH9.18 sendaed solution =PT [= |= psoat {Borate pH standard soltion (pH9.18)) 3 |TASESO7 — [Powder wagon for phar a ee standard solution + Container provided © | HSFS0E [Powder reagent for pHONS SPH PTT Por stmt stendardsoivtion +Container provided 7 |I4GESO9 | Powder reagent for pHi18 P= PR 17 For stm standard solution | +Comtainer provided 3 | 143F060 [Powder reagent for pHAOT T T= [1] |r Gontaining 5 baas for tanderd solution $00mi- 9 |WaarOsT [Powder reagent for pi6.BS T] TPL 1 |e Containing 5 bag for standard solution 500m 10" [TASFOGD [Powder reagent for pT TE TT [=] |[rGoncaining Sbaas for standard solution S00mL (Zo be continued) —30-SaunSETEES ‘Quantity Basic [Ovens um | Coden, | ror ome ode mane) | sternview {2 ]Z/Z [Z| tems iT [iscO19 a boats wah noe ; TP TTT] 1 san [avo Tremor TET TTP pte orET RC si 150,86, Sete mars 68 ORP Check Kit Temiy ; Bones [Overs tem | Code Wo Port ame steccn view [Domest [Ores Remarks Check i heck i ic ean 17 5eC055 eer 1) 1 [ar Sta tad of ptylene 7 GFTBS ORF santa sotaton A = [atom 3 PST [Power eagen or ORF = For S00 Sunda Slaton sComaier provides 7 [FORT — [Power eget or ORF Tammie bas or Sandndseaten Soon 3 YineCoIT | Weak bo wt vole 4 TT s500m -31-Markl C768 (3) Spare parts for one year (a) The parts shown in the table below are general spare parts for one year. These parts differ depending on the ordered specification and subject to change without prior notice. £2 Acoossories, Kits a Spare Pats for One Yea (b)For pH standard solution and ORP standard solution, refer to the instruction manual for preparation Spare Parts for One Year Spine pa or one ar teem | CodeNo, | Partname (Code name) | Sketch view oa Remarks Consunabies | 5 pare 1 @3AR52 Tera soho Bier ed] |p Forwomleak ver {internat soltion of wl chloride secede on-lesk iver chloride {Got potassion siosrods) chloride solution) 500i. 2 [WSA255 [Powder veagon for or naleak wer interna) solution PS chloride electrode {GCI Tor internal soaton 6 moi possum otnon-tak silver chloride solution) ehiorige electrode) rida we sean 7 [= Beara = 7 |-pH eeseods or ORF electrode Fogo iaMose: He 4 Mounting Removing the Sensor 4.3 Mounting/Removing the Sensor (1) Key points of mounting/removing the sensor (a) The procedure to remove the sensor when itis operated and the procedure to mount the sensor after maintenance work to make it ready for operation are described here. If mounting fixtures not described here are used, refer to the items such as 7.2 “Mounting the Sensor" or the drawings of the delivery specification to mount or remove the sensor: (b)Electiode lead wires and instrument air piping are normally not needed to remove. (Handle the sensor carefully so that the electrode installed inside will not be damaged or the tip of the electrode will not be contaminated, [IMPORTANT] «Do not apply strong shock to the electrode such as hitting it or dropping it to the ground, The electrode made of glass may be damaged + Do not allow the tip of the electrode contaminated by fats and oils or do not touch it by dirty hand, Deterioration of the characteristic may occur. + Do not allow the crimped terminals on the end of the electrode lead wires, get humidified, contaminated by fats and oils or touched by dirty hand. Insulation problem may occur. (2) How to remove the sensor ‘This is the procedure to remove the sensor from the mounting fixtures to perform maintenance work, ete, ZA\WARNING Fall injury @ When you work near the measurement reservoir, take fall prevention measures such ‘a5 wearing safely belt. In addition, to prevent injury, wear a helmet, life jacket, safety shoes, ete. DSolect the maintenance mode. ~~ ithe transmitter is in operating condition, set it to the maintenance mode, ‘* This is to prevent a sudden change in indication from maintenance work from affecting the contol system, @Open the holder clamp. ----. While pushing the section A of the holder clamp, open the clamp. * If other type of fixtures is used, unfasten the fixed sensor by its proper method. [== 7.2 “Mounting the Sensor” migMode HC-763 ee 4.3. MeuntingRemeving the Sensor 4_--Electiode lead wires ‘Support bar (Model ZN Section A (Pross here to unfasten the hook) Opening / Closing the Holder Clamp @Pull up the sensor. --~- Hold the upper part of the sensor and pull it up from the support bar [IMPORTANT] « Avoid pulling up the sensor using the electrode lead wires, If excessive force is applied to the electrode lead wires, wires may be broken, @Ciose the internal solution filing hole. ~--- In the case of head pressure type sensor, rotate the holder cap until the internal solution filling hole hides behind so that the internal solution does not leak out from the filling hole. ++ In the case of pressurized type sensor, this operation is not needed. _—Holder cap ~~intemel solution filing note Closing the Internal Solution Filling Hole @Cleaning -- If the liquid contact area of the sensor is dirty, wash the area with clean water. Prevent drying electrode. If there is time when the sensor cannot be immersed to a sample solution, immerse the tip of the sensor body in pure water (city water can also be used). ~34-Model HC-T63e 1.3 Mounting? emoving the Sensor Sensor. Pure water (City water can also be used) — immersing the Tip of the Sensor in Pure Water UIMPORTANT] « If the tip of the electrode is left in the air for a long time, the liquid junction and pH glass membrane (for pH electrode) dries up and its > characteristic temporarily deteriorates. Liquid junction If the tip of the electrode is dried, / pH glass membrane immerse it in internal solution for Temperature (or sensing metal) several hours and use it when the pompenesiey Pera characteristic is restored. ‘An Example of Electrode Tip (3) How to mount the sensor ‘This is how to mount the removed senor to the mounting fixtures in the way it was mounted before. Z\WARNING Fall Injury @ When you work near the measurement reservoir, take fall prevention measures such as wearing safety belt. {n addition, to prevent injury, wear a helmet, shoes, etc. life jacket, safety Set the internal solution to atmospheric pressure. ~~~ In the case of head pressure type sensor, open the internal solution filling hole to about Imm by rotating the holder cap. The pressure in the sensor becomes atmospheric pressure. «In the case of pressurized type sensor, this operation is not needed. —35-Model HC-168 ee Monning Removing the Sensor em a Open the Internal Solution Filling Hole to about 1mm EIMPORTANT] + Hold the sensor in upright position. If it is laid down oF put it upside down, the internal solution comes out from the internal solution filling hole. @Lower tho sensor to the support bar. ~--- Lower the holder guide of the sensor to the holder Buide support by sliding it atong the support bar. Ft ‘Support bar Holder guide —_} ‘ioe! 267) Holder guide support Mounting the Sensor QF itwith holder clamp. ---- Open the clamp while pushing the section A ofthe holder clamp and push the upper part ofthe sensor to the center of the holder clamp and then close the clamp * Ifother type of holder mounting fixtures is used, fix the sensor by its proper method [= 7.2 “Mounting the Sensor” ~36—Movie HC-765 et. 11 Replnishing ner Solution -- Electrode lead wires Support bar (Model ZN-7) — a so eer) {Press here to unfasten the hook) Hoon Opening / Closing the Holder Clamp @Select the measurement mode. To set the transmitter to measurement condition, set the transmitter to the measurement mode. 4.4 Replenishing Internal Solution (1) Key points of replenishing internal solution (@)IF the internal solution of the sensor is getting low, replenish the solution in the procedure below. [NOTE] «To fill internal solution at the time of preparation before operation, refer to its item. c= 2.3 “Filling Internal Solution” (b)Replenish the internal solution before the level of the internal solution reaches 200mm (20em) above the surface of the sample solution. Sensor Minimum required level of internal solut Minimum Required Level of internal Solution -37-Most HO-163 ete (2) (3) 4 Replenishing intemal Solution ()IF you want to use a powder type “KCI powder for internal solution of non-leak silver chloride lectrode (hereafter called power reagent for internal solution,)” you have to prepare the solution beforehand 2.3(d) *Preparation of internal solution” Replenishing internal solution for head pressure type sensor In the case of head pressure type sensor, replenish the internal solution in the procedure below. Remove the sensor, [>> 4.3(2) “How to remove the sensor” @Replenish the internal solution, «r=» 2.3(2) “Filling internal solution for head pressure type sensor” @®Mount the sensor, ---- => 4.3(2) “How to remove the sensor" Replenishing internal solution for pressurized type sensor In the case of pressurized type sensor, replenish the internal solution in the procedure of each item below. @Remove the sensor, --.. ¢== 4.3(2) “How to remove the sensor” @Stop the pressurization, --~ 1 instrument air is used for pressurization, stop the instrument air at the supply source. ‘+ This operation is not needed if'a manual pressurization pump is used for pressurization @Replenish the internal solution. «--. -== 2.3(3) “Filling internal solution for pressurized type @Pressurize the internal solution, »-.- <== 2.4 “Pressurizing the Internal Solution” ®Mount the sensor, ----- [=~ 4.3(3) “How to mount the sensor” —38-Mosel C263 ote 15. leasing the electrode 4.5 Cleaning the electrode (1) Procedures for cleaning the electrode and inspection of liquid junction {@)If the pH glass membrane or sensing metal (for ORP electrode) at the tip of the electrode is contaminated, this may cause chat in electromotive force of electrode or may cause deterioration of response. Clean it in a cycle in accordance with the progression of contamination, (B)IF the liquid junction at the tip of the electrode is clogged by ditt or ifa sample solution flows backward to the inside of the electrode through the liquid junction, the problem of electrode @Remove the sensor, C= 4.3(2) “How to remove the sensor” @Stop the supply of instrument air. ~~ If instrument air is used for pressurization, stop the instrument air at the supply source. + In the case of head pressure type sensor, or if a manual pressurization pump is used for pressurization, this operation Is not needed. @Set the inside of the sensor to atmospheric pressure. ~~ in the case of pressurized type sensor, loosen the cap for internal solution filling hole and then close it. © In the case of head pressure type sensor, this operation is not needed. @Remove the protection piping. «~~ Remove the protection piping and washer at the tip ofthe [IMPORTANT] * When you remove the protection piping, be careful not to loosen the electrode packing. {fit is loosened, internal solution flows out. Electrode packing _- (internal golution flow out, loosened} tecirode —| Weshe— em | ee Leni notch / () Temperature | Usvid junction Protection — Temperate peg Compensation ts gas membrane U (ersersing meta} Protection Piping and Tip End of Electrode Clean the tip of the electrode. ...- Immerse the tip of the electrode in clean water (such as city water) and remove the dirt gently from the pH glass membrane (or sensing metal), liquid junction ‘and temperature compensation element using absorbent cotton, etc « Ifdirt does not come off by washing with clean water, refer to the items below. Inthe case of pH meter ~~ [=> 4.5(2) “Cleaning the pH electrode with tough dirt” In the case of ORP meter ~~» => 4,5(3) “Cleaning the ORP electrode with tough dirt” —39-Mek: HC-763 ee the less @ Put on the protection piping. ~~ Put on the protection piping in the way it was before (IMPORTANT) ein the case of pressurized type sensor, be sure to put on the protection piping before starting pressurization. If pressurized while the protection piping is removed, the electrode and internal solution may come out. ®Pressurize the internal solution. -- Pressure the internal solutiuon for pressured type sensor. (> 2.4 "Pressurizing the Internal Solution” @Check the tiquid junction. tmmerse the tip of the electrode in a glass beaker containing clean water and check that a small amount of internal solution flows out from the liquid junction and the following symptoms do not occur. If these symptoms oceur, itis necessary to replace the electrode. ‘The liquid junction is clogged. ~~ Internal solution does not flow out from the liquid junction. Reverse flow through the liquid junction, -»-~ The liquid junction area in the electrode is changed in color caused by reverse flow of sample solution, ete + IF it is difficult co see the liquid junction, loosen the protection piping slightly so that it can be seen clearly and when the inspection is finished, put it back to the way it was before. @Mount the sensor. »... [> 4.3(3) “How to mount the sensor” @Pertorm calibration, .. Perform calibration (in the case of ORP meter, check its performance using ORP standard solution.), C= Instruction manual of the transmitter UIMPORTANT] + Be sure to perform calibration after electrode is cleaned If the indication cannot be adjusted in calibration, regardless of thorough cleaning, the electrode is considered to be deteriorated and thus replace the electrode with anew one, C= 4.6 “Replacing the Electrode” (2) Cleaning the pH electrode with tough dirt (a)For pH electrode that dirt does not come off by washing it with clean water, use cleaning agent as described below to wash it, referring to 4.5(1) “Procedures of cleaning the electrode and inspection of liquid junetion.” (b)Setect an appropriate cleaning agent from soap water, neutral detergent, 5% hydrochloric ecid, ‘and other, and use absorbent cotton, etc. dipped with selected cleaning agent to rub off dirt. A\WarRninc Toxic Material @ Hydrochloric acid is toxic material. Handle it safely such as by wearing protective ‘equipment, referring to its material safety data sheet (MSDS). (c)For organic dirt such as fats and oils, neutral detergent is appropriate and 5% hydrochloric acid is suitable for inorganic substances such as calcium carbonate. (d)When cleaning agent is used, be sure to wash away the cleaning agent thoroughly with pure water afterward. -40-Mee 11C-263 ae 45° Ctesing the leet (3) Cleaning the ORP electrode with tough dirt (a)For ORP electrode that dirt does not come off by washing it with clean water, use cleaning as described below to wash it, referring to 4.5(1) “Procedures of cleaning the electrode and inspection of liquid junction”. If oxidized film is formed on the surface of the sensing metal, response is slowed down and unstable indication may occur agent (b)Immerse the electrode in 5% nitric acid solution for about 10 minutes and then rinse it off thoroughly with water, If the characteristic does not return to normal in this method, follows the method (c) below. Z\WARNING Toxic Material © Nitric acid is toxic material. Handle it safely such as by weering protective equipment, referring to its material safety data sheet (MSDS) (©) Scrape off a thin layer of metal surface using a razor or a cutter, Ifthe electrode characteristic does not return to normal even in this method, replace the electrode, [NOTED e Avoid the method to grind the electrode with sandpaper. Depending on the type of sandpaper, its element sticks tothe metal surface ofthe electrode and its potential may become unstable -4-Move: 10-763 a6 16 Replacing the Flestede 4.6 Replacing the Electrode (1) Replacing the electrode for head pressure type sensor In the case of head pressure type sensor, replace the electrode inthe procedure below. [NOTE * When you install electyode to a sensor not filled with i of preparation before operation, instead of following the description here, refer to 2 Installing electrode for head pressare typs al solution such as atthe time 2) Pseasnen Electrode load wires —Holder cap Inlerna solution fling hole Electrode packing \ \ Washer | Heider \ Ptecten ping ‘sO area Se Replacing the Electrode for Head Pressure Type Sensor Remove the sensor. »--- (=> 4.3(2) “How to remove the sensor” @Remove the electrode lead wires. «---- Remove the terminals on the end of the electrode lead wires from the terminal block of the transmitter. = Instruction manual of the transmitter @Drain the internal solution, - Remove the holder cap from the holder and transfer the internal solution to an outside container. @Disassomble. ---- Remove the protection piping and extract the electrode from the holder, and remove the washer and electrode packing from the electrode ®Remove the electrode. ----- Remove the used electrode together with the electrode lead wires and holder cap. ©Cleaning, --.. Wash the protecting piping, washer, electrode packing, and holder with clean water. install anew electrode. «c= 2.2(2) “Installing electrode for head pressure type sensor” @Fill internal solution, --- Prepare a new internal solution and fill in the sensor. (= 2.3(2) “Filling internal solution for head pressure type sensor” @Mount the sensor, + C= 4.3(3) “How to mount the sensor” @ Perform calibration. «~~: Perform calibration (in the case of ORP meter, check its performance using ORP standard solution.) [= Instruction manual of the transmitter [IMPORTANT] « Be sure to perform calibration after electrode is replaced, —42-Mast 0-768 ote 56 Replacing the Fete (2) Replacing the electrode for pressurized type sensor Electrode lead wires Crimping termina Core WE (Accessories for electrode) ap ‘Washer \ (Accessory for electiode) Les SL rape paca = 7 {Accessory for electrode} ~)) << Cage Ovfing (P28 or P26) \ {Installation can be made without removing this ng) rode packin \ \ ‘ ‘ Para \ Lock rut Holder Protection piping | \ Electrode Replacing the Electrode for Pressurized Type Sensor In the case of pressurize type sensor, replace the electrode in the procedure below. [NOTE) + When you install electrode to a sensor not filled with internal solution such as atthe time of preparation before operation, instead of following the description here, refer to 2.2(2) “Installing electrode for head pressure type sensor” Remove the sensor.» (=> 4.3(2) “How to remove the sensor” @®Remove the electrode lead wires, ~~~ Remove the terminals on the end of electrode lead wires from the terminal block of the transmitter. C= Instruction manual of the transmitter @Stop the supply of instrument air. If instrument air is used for pressurization, stop the instrument air at the supply source. @Remove the cage. ---- Loosen the cap and pull out the taper packing slightly, and while holding the senor straight up in vertical position, loosen the lock nut and then rotate the cage to remove it from the main body. ®Drain the internal solution. «-- Transfer the internal solution in the sensor to an outside container. ®Disassemble. ~~. Remove the protection piping and remove the electrode from the holder and then remove the washer and electrode packing from the electrode. @Remove the cap, etc. --- Cut off the electrode lead wires near the cap and remove the cap, washer and taper packing from the electrode lead wires. © To use the electrode again, cut off the crimped terminals from the end of each core wire and remove the cap, etc. from the electrode lead wires. To use it, it is necessary to attach crimping terminals to the lead wires again. @®Remove the electrode, «--- Remove the used electrode together with electrode tead wires. @Cleaning, --- Wash the protection piping, washer, electrode packing and holder with clean water. @install a new olectrodo, ---- = 2.2(3) “Installing electrode for pressurized type sensor” ~ 43 —Mesh C768 te 56 Rey sc the etre Ft internal solution Prepare a new internal solution and put it i the sensor 2.303 illing internal solution for pressurized type sensor" @Pressurize the internal solution. = 2.4 “Pressuri ng the Internal Solution” @Mount the sensor, --.. c= 4.3(3) “How to mount the sensor” @Pertorm calibration, .--- Perform calibration (in the case of ORP meter, check its performance using ORP standard solution), (= Instruction manual of the transmitter IMPORTANT] © Be sure to perform calibration after electrode is replaced. ~44—Masi HC-763 at 5.) Ptenniing the location of Fire 5. Troubleshooting 5.1 Determining the location of failure It is possible to determine which side, sensor or transmitter, the cause of the failure is originated by temporarily connecting a normal electrode. Prepare a normal electrode. --- Prepare a normal electrode provided as a spare part for one year « Prepare an electrode of the same type as the one currently used. @Select maintenance mode. ~~ If the transmitter is in operating condition, set the transmitter to the maintenance mode. C= Instruction manual of the transmitter @Remove the electrode lead wires from the terminal block of the transmitter. -~-- Remove all of the electrode lead wires or the lead wires of sensor cable (when connector box is used) from the terminal block of the transmitter, C= Instruction manual of the transmitter @Connect a normal electrode instead. —---- Connect the lead wires of a normal electrode to the terminal block of the transmitter, making sure the numbers of core wires are connected to their corresponding terminals. C= Instruction manual of the transmitter ®Perform calibration. Perform calibration (in the case of ORP meter, check its performance using ORP standard solution). C= Instruction manual ofthe transmitter ®Determination. «Determine the failure as follows depending on the calibration result, ete ‘* When normal calibration was obtained «-~- Transmitter is normal. Therefore, the failure originates from a problem on the sensor side including the electrode. Take action referring to 5.2 Cause of Failure and Necessary Action”. ‘+ When normal calibration was not obtained » Transmitter is considered faulty, Take action referring to the instruction manual of the transmitter. Even if the transmitter returns to normal but still normal calibration cannot be obtained, itis presumed that the cause of failure originates from both sides of the transmitter and sensor. Take action referring to 5.2 “Cause of Failure and Necessary Action”. DRostore the connection, -- Remove the lead wires of the electrode connected in Step @ and connect the electrode lead wires or the lead wires of the sensor cable removed in Step © above, [> Instruction manual of the transmitter @Select the measurement mode. ~~. To return to normal measurement, set the transmitter to the measurement mode. [=~ Instruction manual of the transmitter -45-