- Expt. No.----------0------ > ; Tetra tron! Kody Vs FDS | Aim’ 76 drdomimne the Concindraion of Mmndy 6eludion ly titra ting |___agpinsd ina andar Solution of -forreus. Brmoacnwie Sulphate. lay fore s 2KMnDy + £450, +(DFeSa, —> ky $0, 15 Fe, Ga) xt 2MrsQt BHU Map, + SH" 45 —? Mn*+ yn |_Qxidakion half vraction \- [ett s oh Loni « : Mno, + @ht4 Sse» an" 4 Se" Pte. [Bs boing the Volume _of KMoDy Solution Tequived tp onidised -firrous | Sulpbal cpm the bation ty molarity of kKidndy Solution is Caleuladtd Scanned with CamScannerFeu " ay q% = Meike , = begbop Gres A taskeday GS Bavoye thy Pt Mi Te ¢ “kon Oy = i mM Me = Volume of KMndy @9 NO pbs os oe PNB ef gan a} clerhons = Se— ae Molarity ef Fos = olny Ne ot ~ Veta of EPS = JO mbt , es do = No ef Loss et wlnhont 21 ue syne! aoe © MeV ae Mya Scanned with CamScannerExpt. No. --------2. 2.22... Page No... Preedure + (oem? pipple '$ wade with yabrand ther ringed ucith given ferrous arameniuen Sulphade . A burctte (3 washed pit walter | _||-and then vinged with Kandy Solubom. I is filled vith knit eluiny andfixed te a bande stand - + Anitial Surctie yading ix npled_-b tht upper minusees Leobred Slvto) * Joem> of frre DUS Qyam mium Sulphate p: ¢ pypdled put infp a Clan | Comical flask. pare test Jub Hell A dil t Sulphurtt Atid 1s added. |: The Solution rs tifated a jl) the ution taken tn the Comical flask tums pormanit pale pink Golan . Final Surette Madjng js noled »tttation rs reptatcl for Loncordant| |_ Values 4p This tibation _&, L icaaton. | Obsiryatipn + Burette Selulbn —» kena, + Conical flask ae ammenium Si {phate Solution t | dest ‘ull of clilute hs + Ardiater —> kMndy c el a= £od_ print —> pomanerit Pink. Fipal Molaily of nevis 9.0m Stung t's Molarity a Moltlay mass if =O Dak (5& = 3b g/t Scanned with CamScannerPage No.....2..... Tetpn tN’ KmMndy Vs SHaOy Alice’ To dedemine the Lontentration 0” molarity of potassim |_pemangende Eolidion by titrating [against 0/04 sterdard | Solution of Onalie ged- Prine vp +P brown value of Shandard enalhe acid folios 8 thatrd jure Dey man ron_tir Ati m and in “bot Condition. + 4p this rachon pralit aid 9t{s oxidised to Co, and th kno} GUS tedued 40 folawhss rnanganoys Sulphate Melewuler oven equation —_* 2hMn Oy + 242,50, +5 CH, 0H —> ky SOy t 2MySoyt 1DCO, | Reduction tral martion Cena, tent se— MoM + yihoT nr Or \debi om fal 7atbion [.G0,? —» 2to> Overall ionic Zquahion'- QMpOj_* let! + Sep 0h ——> 2Mn™ + FthOtlocor + By Rerown ing cf rsolume of KMnDy Solution the molarity of khinOy Slut n_b . Scanned with CamScannerGaleton. ‘ » aCe “UG te thoy)»: . 7 Formulae vay * MM &: Myr bet vale voy: RAMs SS ywhye A bye My = Velvime of pri NGS gl a = phot gam ef ebchois = SE) Messe feptan'y ef sonads- aortic: Bl sige: = Volume tf oval? atid = wine a: bee Coss ¢ chi hoes + leas " h Mo row a Scanned with CamScannerExpt. No... Date .. Page No... | Provedure + A 10tm™ Pipelte is anshed with paler ang hen vinsed |_wilh AMwOy Selution It is filled with kbd» Oy bolutim and fized | 140 a S1ang-— *1pem3 of oxalit gerd golubon is pipitted cut into a than ital flask. pe fect tubh pull of dilute Culphurte acid le added | The. Shion i uated muaily te bailing The acl Solin 1s taba | fain st dou Td Wns per ma, pink Colour Final Lurette nedirg 18 noted. Titrabim ls Veputed | -for_Contpvdart values |Observations \ * Bure th. > kMnO, Splution - ‘ Conical Haske = 1D tm? of ORalie gud tltest tube full od ¢ thspy -# A * Adiiater —> kort ( 6ebf -indirator) + End print—> Colpultss fo permanent fol Pink Glur | Repore * Molarity ef KMnby 6-08 u Shungt + Moalority * mohewlar mass Os 002 % 15@ = 21bg fut Scanned with CamScannerNecl t Agh03o> Agcly + Naklos i" white pp Agel + aNKyoH——=—=", Lag 6) yO AHL. ovo > lomph d.¢ ‘ Scanned with CamScannerDate. Expt. No. Page No. Systennbe pital of Gol = Am meniurs chlectde (tO Fyslimirary best! | stake’ Crystalline plour’ _pohite Solu biljky’. le a ter | Orig inal Lplub’or. Slt tumber- Extpevinoen t : ¢ a nd 7 Salt tlone He SO Tin 2 ayoup acid a dry test pple | y d Nedita! oy ts il ent - Scanned with CamScannerroy es Sais st Us cation Nityt NWT Rao —S> Nard 4 Nit, tHE ‘ Scanned with CamScannerDate .... Page No. Detutiin ef Seve gen p bused Fapeiment atm | Ledutinad Heat Smelling gab aahith val! “ : L ob: oStyy eyenet ~ Salt 4 Alaott Gis a pungent Bere gioup baste | Yadreal pity? fon gives dense whilefama pray be Presens. rr Gncenhated pels when 2 9ps5 rod lipped te via | ‘onfirmatory test for Cutey)! LL ex pint | Cheevyadr i! igiha: rd | selahien t Alese/evle viagech } t | Lepert * » The given inorganic alt [entate Aud va diel — Basie =e | Hone the ghip “cult js Altec. Scanned with CamScannerBr VERE oats kBr f AaNOs ae KN t A Leh Ci, ye Low pt Pale yellow ft Of sifpe® bromide are Spaminglys Solu! an @imm Onin Y hyd voile Scanned with CamScannerDate : Page No. rr Beliminary fest! State Crystalline Colony: _Wipyite Solubility’ Soluble in riginal : ‘old _uzatev | Salt # loncertrabed te S0yln_dyy tat Tadital Br ‘enfin Is Scanned with CamScannerxb aye seancts weige Ba SS AY nw Lr it HDR <> : Aye was Scanned with CamScanner| ft — Py ecjprtate Bere graye basi L8H formed Scanned with CamScannerScanned with CamScannerLEME Ne |} 29 4emb: ~quabrtabur Analysi Man ge dhorga Sulphate ( Mp S0,) | | 4olub libs! Soticb lp }n_Cold water Original Solution: ealf water. Bye flervercente | L Group aud Hisdy ina _dry est tab 2 Kieryetin |e aaa Coppev timings and 1 No ¢ bar attevishe Observal on uabile precipitate ig themed whith \¢ inerfube Scanned with CamScannerMet eee 4th$. ahbot Mosh Biff Colne ; E ‘ ce Mps ted ae Bnet 28 Mnel 4 Nap? rnloie panel wht Pp, Nnlod> + fol Mro ford. v Pa Brow = Scanned with CamScannerDate... Page No. ....2 alt auakion Bath Stlidiva| hile precypllade ie | dil Hel Comes | Pomc echich_i3__ ion je radical: Cj) CxO iment : obsewatie Andon i No Pungent Smellin. vo ! t teat fasts abseved Yads ec City?) 1s. 4 we 0 I bn Expevinoen t _ LOviginal Solution + Alo yhite precipitate dilute Hel & formed f8" is absent LDetubeo GD pour. _ Scanned with CamScannerUxpt. No. 1 Ldetios of iv Group b rachel (|) —éxratren t a clio ortginral sedielibont 2 Ta poset ae —| | akcove t pohieh_ ter " Report The __given_in ergmie Aealt Coylains. L > Acid tedital —> so?” |_| % 05 emt Hone the gluta all Sy 50 x Scanned with CamScannerNOs Copper bd KNos + HrS0y Scanned with CamScannerExpt. No.2 fd Utemadie gualitative : analieie_ afin y - |} Barium Wikele Ceacnoj Ficliminary het! | sfades Crysd alle |__| léedour: _pohide |_||selubittj. Sable in Cold poaler Original Selbion' salt 1 sreber ilies of aud red tals! OL id alt tint. Heo | le Copper tumings {cua done . sf tat tuk : Scanned with CamScannerpng Teer (BRON FING TESTS kaos 4 1b50y Kee + HN, § Febery + 316504 1 RENO >, BF tv (201) 5* HO Fan psoy Xo Siteb (FeCnd CoD] 5, Scanned with CamScannerDate Page No,..1% ef Beste wavals! a Pal hat OF sinel solution "tad Xb a Smedlng + Nacy Chisal Seen 7 [dite wt +S | Pecprtate is dimes | co? pe | fy Qoep bau? -radival Ay ots Ht l +6 | “ned | On, at?) a7¢ abort Scanned with CamScannerSO Balost Mieco! a Ba at is), 605 TTR” Baldo HAY ee a2. (4Gl0) 2 BAP CU 4p . ky O09 at . (c7:000>, Ba t Mt vba Scanned with CamScannera2t observation | Yellmo preapttode_| 4 di lcescort lotro, | is foued No precipltade is Ha), $04 Srlichin _| 7 Original aplich'on t | forme A v Group bathe todice | Ba 6 Corhinned: No pred'pitale_f¢ 4 2 |_ Flame dest = . — _Expuime t [bh sevvetion lL Infenne. 1 sad Elon He | Apple quest n (bur i DL Sroup> boric todicet |) lmake porte boride | is boizind |B x Confimd- || Lan _platium pire fete | | ho Luminous Se au lng A ! I I Fepmt i Inorgan't Grtans + Ald tadital — NO, « Base radical— Bar? tiene “the Given Salt 19 Ba(nios), g Scanned with CamScannera Date .......-..- PeeNo! Page No...).2 Lo | || S4atemedie qualitative analysi6_o) Inaganl¢ call 5. lueininm —sulplate Cale Gas ||| Arhminary dest! tat! Crystalline LColws _ohite ||| sotdilitys Soluble in cold unéey ———— $$ |_Driginal Solution’ salt 2 Lold wmnfev Expuimen t Fall tilde wo? | AD Este offence | 2 Grup 2c'd radial obawed | cps ts aboent Defubson ~) salt tone 16S0y In a try tut tube | «ddd topper fuyningstp | No gas 16 evolved 2 2 | cbave Splich'on and | | Nos” ten 15 absent! put Ct | Ddubor of it aid radical: C502) Exporiroent phswyelor _ Prferen, | coiginal Selah m A whit precipitates iit Group aud Bact, Sebuth faired wohith ities vedi Sa, Jon feass dilute Hol Lsrlabos 1S prewoe- Scanned with CamScannersoy? Bowls WET Napa, 1 Bal, > Basdy b+ abe Leap Atetnte Tes! Noosdy + Pb LU 3 PbS04) 2b HylooNa, awe Scanned with CamScannerExpt. No. ee eee Das Page No... while precipitate y's fy Fipu re _ m4 -/D1me d chit 1s Lnseluble Tedicel g42° ig | th_txcess Lalicte tb bied __Lorfpynnd | | cil —ladical Wty i abead 7 - r ; }—| Relea ofl group basid radial ae |__| -—Cepatinent- Sheevver 2 Lrbrnte. uci pitate ie of D) Group basic vadital ? x at) £ pial ot | observation —__ Dn bevence- bre lion | aptatinous urbe Gi aeup oxic vadice Ala | ppwcipitete is toad AL?" pay be prove NiHy 0. 1 Scanned with CamScannerDate. | Page No.) vi n il | Original Sefetion+- A_guatinpus vobi te | || boi Sobcdion | precipitate i+ formed _ Whywh js soluble in eset Naot $a b_form a clea ft gro. basrc rai A 45 Covfivmed_| ont Qtlatinows urhi te ; MSolid)t Heat pruipitele veaprars| ___t Ke port The giver Inorganic éall_fedain. Acid yadital “—> " ae posit Yadica— AL Hine He’ gren salt pe Ale Gio) 3. | ? Scanned with CamScannerae *ubnale) "ea t apd lath 160, 1160 bein) en ae = talo tine voole Scanned with CamScannerExpt. No. | —||_-Sy stenncetr ¢ qualitative analyst's of Inoyganie Galt 6 Caleium Cay berate Cratos) |__| Pre Uminary test! $$ _____] fale amatpbews elour* Lobe. (Selubility’ Gobuble tn child. tied || \Priginal Aiticiom: sald + dilule etal: Ridubm ef aud raditals!~ L tid Yad) C0" vi Yon Ln . tdi ive Merve sent L Group arid rash A Colewrl es: got wohich Coes Pret . a tons Lime water milky Lorfir mator. Co! | —Expuiment _ pbsnrvati'on Trfevence . fall tool bot Lint usaber doeshot | Troup arid vadirel| | tren ly, ors thegas purn véiley £0," _is Confitrosd | toroeg lime Scanned with CamScannerExpt. No... . Date. . Page No.4... | || Deletion af 2 Grpyp Laid tadical. “@e") | |] Spey ne nd observation Dnteren riginall Gludion t lo white Pectipitate | _£ group baste Yodi | dilud¢ tel 2¢ formed Feet je absent Lnfeven . original Qrlichon + 5) group baste vadit Nitty tl t tecots freupilele re femmed Als pe absenk - Alyn fore radteak |_| Pana vente. Ma ushité. pievipitate fy Group basic radial is formed Mir? ont aoe alcool Be white precpilake | ct formed. Scanned with CamScanner7 atts Ny é io (Ni), 08 \ daele ; isfoo! 5 Cty, a + COM y oes Catcoontty 1 Cty dyy, Cergeor) sf mae 7! Scanned with CamScanner_observatyon. Lnfurrmte - |} Original er ydlow pretipitate| YD _ Gow b bose _|bdil Gk coor th GO, fs formed rradie ol pall is Origine’ Solution’ No phile_priuipitate gioup bas it Yad ¢ Is a 24 Original sofudjion t [A chi te preupitale is VL Mox P beste yodital med [lovin He Con firmed. Experiment Salt 4 lontentrated Brick ved Cofpur's tut, maakt a poste Obtained a janitt en _platinun the_nem=_lem'nou Eat hh rganic Sal Contains + bud valiad —> ts «Basie ‘radial —> Hue the. 4ive® Salk je Lalor. % Scanned with CamScanner- — Date... Expt. No. (et 7 Page No.1. DSS || Sy sb imeh'e Malitetive analysrs ef inorganic Salt -2 | Sbertium Chievide Cit? —| Preliminary tes bi a _ stale’ _G ystalline a || eleur: write Solubility Soluble yn Cold water i LOvignal ola libdy'- fold + (old water _Petedien of aud radials! _ Cbeewation tnt alt tdilute Wet No_Phisk C Group awd Obseyved Yadied Co, Ga (Pedution ob Gvup aud radial: (70, Ex prviment Dbsevatren LSalt tne Hel in a Gives celpurl fuming dry Lest fube fest gives dense ite fumes when a Glass tad _dipped jn Thfennce. fife are | radical tl jen amyn eniure _pydvoxide (5 Scanned with CamScannerExpt. No... | Dedeatien of Bane fade || Detectimn of see grouy> Basie yadial | cnt) |e experimen bsorelion [ Gagerance |__| Hoginial seluctaen t Ne pungird smelling |__ Bere group baste vadital Talatte colicin tttat | Gat ge evolved Ait is absend || expatiment- (fltasci |loniginel solubiorst- [eat tel is *faod || Detertim ef 1 So0uy> basic Scanned with CamScannerSr uw . Sitle + (Ry) 9005 ——* Seog) Latin) Sh 1B UG (CIWS t Cott Ros, , 2 Aimemium Su lplall Clay Cod) 5 + (NW) Sdy ———?. Cte tooty. + Sess ey la sag Scanned with CamScannerua Ta rfeven e+ whe preipttate | VY ty barit radi |i formed Tabs cathe el __ Lieut. I Origin al Cobb + fe f Flame drt! Lapesioent 1 Salt stone. Ul make Lt imson ved lotr a paste. Lanite_ an Ie pptainta Yedizal gy2t vs Plotinurs wire b the Lonfirmed. | ner Luminnu’ e R port The given Ynmegerie Salt Antain $+ ~_peid edital —> tL Basie radical —>_ srt the the que Soh 18 Grech Scanned with CamScannerS07" Baul tet o> aig Nor 80, + Both ———s yd tanate \, ¢ bind s2_ ¢--- \nyott yah Scanned with CamScannerD: [ox No... cas: ~ Page No....-¥ os Pre | Systenat’e gualelabie —anelysis of xgonic Salt | —Magnesivm sulphaleC Mg 504) a | Prelinainary dest! jState! Crystalling Coleut’ white }—||Soelubility: Soluble _in told _weater Original Solution! Salt FE fold watey LDetechen ef aud x9 dicale! b+ dibete ent | isk hel 2 group atid vadical = |__évolbyed | Loz is gbsent» ||, Detubron ef f Group acid mdral Ltd. By = Fypiriment Observation lererve. LSalt tlm tosov | py 9as te suobwd: D Group avid vadital| in_a dy fest -fube | LL BY app abst} ite ae wluhion | No-gas iS _svolved Sipupacid yedizak la Copper humingg : _ fs absent Scanned with CamScanner“yt, - : nena yeh + Hy ot £ tH) 2AtPCy > NHL GD Scanned with CamScanner£kpaiment | Ovizinal gobudrnt Mo Peregent Spalling| | Alan t tea t- Gas i$ obsevy,d Blain of) GrouP basie aadital oped z | -Retutim ef f Group basic radical : Coe) Coxpeciment | Otlervation [ Th fernce . Oxiginal oft ¢- | No utile preu slat £ Group botie radi Ldilite Hel + 4, § | {med Gat ne absent No gelatinuoes white Precipitate 4s fenme a zt) Pets | tea WV Group baie radital L——Nn“and 2rare aled) Scanned with CamScannerDate ___ Obgevotion No white precipitate An fonnce 4 froup bette Yodo 2" cy (at art abod vi Gapup baste vadivad A vohife. pecppitate formed Marty's pretend and lonfirmd The_gitn inorganit salt Contains. + Acrd Yadiral —> soy>> + Botte vadival 21g Hones the Giten Jt 1 NgSo, C L} 8 Scanned with CamScannerae ib Natl t Aq N®s ——» + Nanos Wt ppl Agel tontyot Eng Enrgty}cl 4 ateD Sruibl Comp of Scanned with CamScannerDate Expt. No... Page No... W. 2ydenndic_guelitatur analyst's of inorgante éall 9 — Barlure “chleride (Fach) Preliminary test !- ss] Slate Crystallp a ric thie 1 | Solubilrey * Original Salubion! - falt tlold untey. Pe be of arid radials’ eee ae “AA joresent » ion wt fumes walk a glass Yod die! i) Niet & 5 a tty chk cag 2 fomap 2nd P silver nibett Slction | te dmmd vohich Is Sabb poe In ot! Scanned with CamScannerDate... Me. Page No... Experimn t Dr éginal lustient | Cedi in. Experiment Neo precipitale orig jnal eplution + 1 Gbeeved - | niet ce) +t Nee, DY Excess HS. Scanned with CamScanner= Scanned with CamScannerpola rar uit te thy | [hor - fumipaws Report: Tht__given inergarle sal} (pntains Acid vadic— cl A + Basie yadizal ~S Ba* i Hert ate give? Sal je Rach. Scanned with CamScannerScanned with CamScannerSyehmabie gualifabve pisel beorgeie £ald-io | Strontium nitrate (4 r£n02J oI | Prelim ia y fel | Mdade! Crystalline \Golowr white \bolubilrty' FHteoy 4 & FeSoy t 3H SO, 1 RHINO, Fesoy t NOt SHO Lh l80y) 1. ben py Tie: weiedey ro No SON WIS th sy Scanned with CamScanner| vlzos_o phaly prpared | | fermnus cotudinn , add Gre Héoy_ jurcbi en of the Date. A_byewn bing is] ol formed at the N00 5 Lonfirmed| + eae - Scanned with CamScannerott we XE Dak oo ngredacte WHY) 9008 + Sve, TF CH Cool AB SyO3Y + gH (Hs Coody Sv + Cort Hoo Scanned with CamScannerDate gt is ‘tena |P lod i ure wojreto tie ner _lumino __| | | Ror t* = dad vadicol —> NOs — ic_vadital—> Sx>t - Hn te Ginn GH te Sx (nos) Scanned with CamScannernyt S04” Rael: Test ote Na&07 karte omeal Scanned with CamScannerDate Page No... Sistah qual nels ¢ hovganic as Tne Sufhal Cznsow) | |__| |elade’ Crystal poe Colour. wehide 1 eee ca Oniginal. Loidivn! Salt +t lolt_water Scanned with CamScannerNo Pensed Smulling Gos I Objpyd nic Vadial i Senrvals 7 ; Mo _wapite ppl L_Group basic adie) is frmd | PB ie ghar _| s o . 2 |_ Zxprimnt OBeeate pn : original eel b il é Sriginal scbach im Pi ap lal j Eepuipunt Serato Tofu ple AHty LA) tayo | 70 Guletinew® robibe Is Scanned with CamScannerznt® . znloud a — ee + ar Ler cwrik) Syne at - Pes ZA stat —s Enel, Hh sf W Neow Tet Zrele + Noe en bth Pact : A> sy White ppl eo. ; zm Za (oll, + Scanned with CamScannerThe Fin Liga Salt Col ains. || itd dita °-— 602 Scanned with CamScanner :Expt. No... Page No.2. (| Spelemehie qua lide analysis Of Irotgan'¢ Salt “2. 7 Zine _monotarberale [Znlbs) |_| Preliminary tat! |_| state’. Ampy phous |_!|Colouy! white |_| |Solubility! Seluble 1m Cold clude tuck iginal Seber | ji L Sup a14 radical Dy i Greed » Scanned with CamScanneroa ° Zn? " Pas oye . ey ZOMYNHE —s p04: ently ab te Zt 4444 —s 425% Noo Tee ¢ Arntb + Ange > enor» t+ pod be ; coe Waite pt Sot Zr lon), 1 Hol —— Na, 20 + 2H? Ghuble Scanned with CamScannerScanned with CamScannerr Expt. No. - . == p—~|* tid yarival > C02” Lt) * Buic rdiyal 5 oft The_given_inergmit_ salt Cordains — }|__Heree tS, alt le znlD» - 2 OS Scanned with CamScannerCE REC AMMONIUM NI Ratt Teer : : Reo + (My) 9 Ce (DSI, ——9 (ROW. Cty NH \ aleee? Cert arma onier nibiote Fink o tad ‘Nd Tabs -tecd rae 3 fie | ECHO" 7°—Tha Cotamse] 3H qt Chlovae . : - Violet Comphr Scanned with CamScanner| Bret NO. ---2-------22--- Pore, Functional Groves I Of GANEL GmponDs. _| ‘Tests FOR | tll Functional Group ests -for—alechels- | C8) Carte ammoiem nitrate fest At ts used d | [ Cxpnimmurt [chewsataon Tnfarere |_| | organ Compound + -fuo chops of | Pik cx ved Fndiescles the prune |__|] Cee ammonite nitral ¢:Soléioo- Colour appar of altobolt e- oven bakenwrll __ cs Wd Las reagent tsk ‘ i Scanned with CamScannerBY Dini TR opHenlyL HYDREZINE C2, 4: can r) N-NH 4 NO; Oo eNe Tt e-é Ht HN-AH celle aie ce — andiet Mes Naik Dany, [4¢ fore Eo. tony PETE TEM vite ot was SE Hadioadk ideitag (: 6 ee -.Cobibutts bh srtayt ESV ie. att (pat yt » AMINGS v “Gobgivis ttt HR Gigued i“ Aniline aie 3 CORBYLOMINE The ee Rare t CHts +reot OMe tdeel t3eg etoab chant Ys Abeaea Nb tydatele Sanat alls ; Scanned with CamScannerDate....-----.- Expt. No, Page No...MJ..... t fy, Corbonylie acids. bservation | Trfevene—_. Organ’ Compound +f daop of thy laleel |_m_fruiy Sli The Lay! (‘au 23 dyops of fone: tisoy heat aud pon»! Dn 42 1S Lerehirand| Tnenon | amine I |_|) foo dye tet o Dia js duster atomedi _ Sr we \ Expert : | Dbanair Tr frene- ‘Organic Composndtt God un, “gage Tod dye k Primacy arematee | rife tdi) He slool sald dbtamd: | antne_is Cooymed | Font inl . ae Scanned with CamScannerExpt. Nowe Date Phere Page No....WY PREPARATION OF LYOPYTITC AND LYOPHOBLC Sols. | PruipleThe_Ly ephilic éols ave tiutty fomed ty mixing Grd shakira | | tha Substente witha Suitehe Lid: lyeph obic Scls Larne be | | Pupared ty drut mtring and Shaking - Spurial nitods arc emplopd —t2_prepare ty pophobie gels. | Chemicals vequived:- ‘| de Fag. el bum ie ure ic lution (59 In tool pe Chipride i 24 In 100ml bey Me Aluminium fhlbvide Seidron C2¢ in 100m4 water fstab /@um- spp mg b- inu4 Oxide 2g Ind | wat) Prove dun.‘ [4-—Beparation of Lyophili c pl: LD fog Albumin So. D_Prepaw 100ml of 5+ Cw/v y cb v In 250 @ porcelain dich i the jn and pour itin ” ” ‘on Stir’ ensure Thad the Sl is. Yn @ 250ml broker and boil it A 1 ith Gnstant stiri PasteintpemLof boiling voater wits Constant _stiming - kup wale oiling apd titring. pr. Lp minut®, Cools ensure thot Sol is wrllprerand. A Aigastioe of bpptebi | L- fame hydroxide L Aluwibi ue hyd teride - 1) Teke toom of distilld voaky In @ 260m! booby and bail it- Scanned with CamScanner[fied tl 29 of foes chloride Lalominnn chard peuter tbs) |_water and L-4 Stir it wo |_|} Peer Lomt ef ferent Chloride [aluminium Chloride éolution pryaad.| ||| tn tep Git) and tunsfer /¢ tele boiling under wel th Constant. | iing- ifft ill n [white bol obfaintd - | LP Arse rm Take loom! of dishilad sale in @ 250 ml beaker Scanned with CamScannerScanned with CamScannerDate. Expt. NO Page No... . [Eipeinant Me 2 Purfiatin of Sol by daygs. Ain To purity prymared bol by atalysi®- A | Chimitals Wpuived * \ uw - Collojd af dispusion of 099 altumin ui 2 _Parchynent | tallorbant japa : i f Urany) abe sulphate: ~_Sher_nitiat Scanned with CamScannerisetal Of Castor Sudoils |S vs Machin oil ; ey vt bs Scanned with CamScannerpt. NO.----2---c-r-r0° Page No..MS._ O] (Bprment nel! Rol_of umulesfying aguat in abl te cuss of. I | od Hm oils: ‘ Lim! To shialy the rele. of emulsifying aged in stabilizing te | Lenin of append offs _| || An 4nulsion Contains Liquid disperse! phase and Aiguid cbisprrsion) soud)ipre' by 2b je d dissolving 1 Yin lont_| a L5ral of dbl d bo - The eelichins in te ba tha are er and Let festee| Croubion Fett ngeimg a | Sin ade és rel bing Stop Bek Scanned with CamScannerEquabin Letras th 2Ucheagy > e00h TR Nock om. + th.0es) Soucy °Tolel lune afte Sehadion Scanned with CamScannerLiat ot Ea of ocnthn_or_ tee of readin [Ain< Ze Stidly the etl ef Cental oro the-ede of atin |_—Beteeven Sadler teicsulthalr and Ay deodhloric Azrt | |Brnuiph~ Sodium fh oculphatie eeludion vals with dilule by droc hore rid and fomms a SulPhuv pretipibal ¢ of Sulphur The fire taken for_ 7 fuinanoun fale ton Can be used to jeditabe Carat of qucton- | Apparobes and Chemicals regiaared !- Ipomt Conical lak - Sonrl mausrivg | lind theymonkry and @ &topyostes o.1M Seliu mbit te Sobubn [M_fydvochlbrie acid- av | Froce dun be | || Fie tem clean conical flask ay fakon apd Lebeled 21 1,2; % ards _| 2.tme of D05M Sodium phivsulbhole Solubien jstoben Inthe Cental flask | Jabuled 1 13+ Jomt Of dilube hydrochlon'e arid 5 aalded and immediately Step Lock 's| Started: eae . weith_g Cross Te flask (¢ suaed fp mixhe Solubson ore! Plu. 1 paper tnorfed | Marka Goss is obs d cfipm the. top tohan the Gross 18 just revisit A 8 Kbbhd & Cxpoinmnt ip raped by adding) tO. of im piel to the Cmicalflse 1214) 9 Containing Lom ¥ diffrent Cntertrchons of Sadiv™ Thinsulate Siuttion cs, babulote beside - Scanned with CamScannerScanned with CamScannerDate Page No....M% Scanned with CamScannersushin 2 sagan satan) RHA ——ASAV IPDS He OCS 50.65 tae why Scanned with CamScannerExpt. No... [eine ~ The |_| | Gentrally tote Gomi a shal Lea at eltimprabae_ on. [Hand bydicacy elas rate. 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KNOs «gy TF — END3z Cay) wr < Cuspyls) tq ——> Cus0yteq) a gate what ad Kalba TT crahangeys 2 sai A stages phservedim and coltulahion '~ uray 8 Initial Hemppabut = 1K 2aik Final» ¢m pocanitte cor Bob yeh a RRRBES shay Change In tempryaberes GE Pig PAB EES Mass f Kis Jakeo = pq > aogier’ Molriwlav mass of KND3'= Jolt q rat Urtume of the Solutim = |potm* Mas of the Srlvbon = foog= O1K7 Spajtc heat of He Ghdim = 4200 T/tyX- Heat abeorkyd dushathe Piptess MhassP- fot charge hanpevabse Ox Ih L252 Frnt 4 heat aberrbe4 voher gne tal af polation nitrate I$ diggolv4 In yoat tt 7O = 197364 Scanned with CamScannerExpt: NO.-----------0- coe oe a No... 6? | a Exim” Wels Delrin ol etalpy of Sali 2... Date... 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No. Page No...4\__ |_ Experiment do 17! Inn! Ta dene Re cap uutralr, ss . stony a ere Per Tee per dp nuitialized by. anequtvalert | mined .prnmurt | eet iets fergie tquivalont Hf an_avidd pubralteed is Lalbtulated - Ab ge 4, tutbale of nosttaleation. | ApRoalie and Chemicals Youired'" Pibene bottle fitted Wits | thetmometer Gnd Stinav, IN KLIN Naot: Booeedure! Lbo er of In Hell taken in a polythene bottle fitted | with thermometer and sire JODem® af In| Naot is token jm a 250m ot _ beaker. Both the Solibom ave prpt in R_water bathefor |S minula| inte - token. 5. attain} Yeady a ps robe D pet it be DE yf thal “we tek: | Bust Enialpy pf-nrchalination of lie! wits acl boil = Gort lest $e Scanned with CamScannerColewlation of thd / . Tidy! dem yaduyt of Chloe: PaO. . 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A_ loppe red itdippd to tk. dale bridge of kel te usta do Connect | D : J, 1s which petitive i d zy , | ; laity are D tb the Veh mehr at Shown. r n ALS Lom, ehitic Curie will byin b fw and vo. ing i d_ which indiaby the_tmf of the Gil. Thy, ts yeading No- | bre pro is d while keeping the & le jon; a4 1M ng the Contertation Zink “ —- ahdion O02 and D-b)u- ‘thes a 22 and 4 oie vended Scanned with CamScannerobrevahion apd Caleutation es Scanned with CamScannerAV Page No... ee Expt. NO. ----------------0 Date __ = Chrom, 22 Sepuahion #03 t in 4 Atay mi Al ito ala F 2a ofr te Y extrart or inks b abd np te ell tome, “hve a ely Ky Val “ 4 [May Ae bis ype ef Chremadognaph sil Su, [is wad Motine adsaied ot hebben tripe ats o Sbetinwry phat and be. SsRent auts as the oncbile pha. Tou ria fre to_bt Sponated. 18 Spalted at tm end of ths paper. Tei Then [diged ina. poarch by patra on 2 ee Cant thet he spot. 28 above he &rbynt e Slant is te G, tom antl Lm, | as thy, rupli Ke Son ala tr Be ard yp | Li falled a Chrenalepan tlertion Ry: = Dist heuld re asennt — n4 it 2 ~ Fu Gf Alrthi 5 | rears a ed Coluckion te spurte d om the referee Cire wa Lali ie soy eta! ine Og Cae [ater Hind Aunt dd Hel isthe nage 2d Chromatt t oily by foper is dippid hh di mi at lc watt ps | plate ond “tht Cl ptm a at i peti a Paral = By valwe (ll Ard Scanned with CamScannerTaw O babaadyy o WTAE can . Bap’ sh Nasty ASE AW O Wee va gees Te sant 2 Nang Fiat Og sit WANE PRAT OM AT iy \ {Death 4 ” eS ay stde way Sr Yah ats Dag Be yquare vb ver Scanned with CamScannerapts NO.------2o-n-nnnn = | Gapliamisln_ A= Separation of ly done tihuents of Ea mavdore af en Ne nd ae eal Mateid! YQuined en abt hp a “Rubber Gal- xed sal Jack Io 6 CNOs >» Ethanol b-OM Hn, | Page No... 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No-£2: Drpneatio of tom Hie: Te Ppt Loyal of ys goon wa “Fang Moty's [thy Mobs all 2 nas gram any go> | cea double Salk 4 Gan be pr Mi tela tulhale Cee so, ni hon DSoy bie) | | gubaler Sabine Of Lis pac ng Pee Gal Uelane of | pp etthetnd (ny) on [and Covlieg Crystals ef Mobs's a ae fane net | ‘Appoatus_ond Chemical yegvrred! Ty, [| ti fam sali asd lett fg |_|| Ferrous eee |_| |__¢thanol- ee dilute Silpburie’ guid end _| Procedure’ ; - 7 ¢ and 65 inn Dolum 5: ane hia y 2 mob ‘ |_ Abou! Fmindes b pl vlahed re 2 Abst 2ml of dituh Sulphie acid te added the abovequeler Gnd it }. pound into the first buabev_Contorin | Toe nent Bae with ‘2d tn anoteer bi The fil Low-flomt y LG: The China dish is Covered with a nd kept inan undisturbed plate ofr Covling- Well fee loyal willbe obbind afr bone tine [||| 4+ Theme Ligue iS dumped and the (yystals in he china Dk die hare prashed wih a atmal guanbly of athens): Scanned with CamScannerf —— eee spt NO = Sete ced by pasty bebacun he golds ob tugh eben teetghted: The Colo cond Bapisot Crystals axe | | Pasult ue ae Crystals Ligh Green Viel Cass [the fais ehlsimd) = 124 a Ca [— — WIL Scanned with CamScannerPrortion . ee ) Scanned with CamScanner[has tht immul bs £0, ab (sou), tds 0. AL fy, er Hh Stallephy . no prepared | the. it of aes Loluhons of Alo . es __ whe Pro cedure 5 tz ium ie pin @ beabey- Fis ditafyr) in 4 minimum amount at dithlhd water wit gentle heating. a: 26:59 af abuminium Sulphate it tahun in another bear ibad. hy aaa of Cotanteded sulphate asd ave added Abut ZomL | dhe fer (5 aa ‘eat i igh id bo tortrout distur bant 7 the lag Armd Q4L Separated by Ceca 2g the anche d_puighted: wr §_and ae L —___— Scanned with CamScannerExpt. No. ---------+-+-----. C Result 1 of the byctale = a J | | Shape of the Gy stale = © dbechedval = Yiuld its in Scanned with CamScannerthmicol veathion HS OY t Scanned with CamScannerir t | én periment No_2y! = ins _ Be PP 0 pure Sermele ol bare cn il caraldehyds |_Sediu Ay dronide we gad yre bid Spirit Proveduce “ L 25ml of wubb d Liedabe $0 mol. of ae aldee is — a than Conical fle Tu Contint> en allud to stend for abet Sra [ee Cold wafer. fal_yellrw Crystals of dibenzal atetne prow pitales. H-is_| ed Crystallise d yo ified gpivit - |_ Rew) |_| Yrld = LE GZ a Scanned with CamScannerChanicel seaufien nu woals’ Scanned with CamScannerDate oo Page No. re d Preparation of ti Ate’. Te prepare. a. — ofp 0m ace danilhde. | = iltbantanita from acetanilide. | “Popa and tharcal regi il . ml ef te tound_bo Homd lash lebath | _—beaberspreesiriey Cyber funnel and. li Mer papey « hth lide_Gne. | pific acid One cy Phurle » 9 lauak relied opin te Retake — | Proceduae +109 ol —quulencl_acelonid is pled tna asp ml rund belond dst ard foal ghd tb aula adds | @clded to iL Boer cae cat ih antl ——___] las & ae | |ls- ‘the flask is rum ize both and allowed nd About BE mins af Yorn temperature b The teathion omixtere {8 poured on a Crushed te Cortatoed ina bubkey and alloord 45 stand fox 1S roses MH: The pve ipitates of A nibo acetanilide i Separated by filbestion wahed with Cold patty and with ethyl alinbol CI A Scanned with CamScannerChemical rene firm pazonium Her _.Phapyl-azc- By vo Seeiogt wee Scanned with CamScannerLE Date | fatianthe! ao unthvo! &6 rime ASS Drapanst | Bim! To prepare ptm rin tig — fi Bra (grmahit aod deus S-—————_____| a tne pvp ts er ty etree pate = pydvoxide 9 lasial aude atid and oe Protedure t ine, &ml L 8m] bere & Te Solution is (oaled to gf tia an ice : : 3-b a “S: Silichoo 13 -faker in a beaker aad Leo ur rs hapltrol IS added S d_bensine 42rqium ¢honde im_is adde 4 stm to the P- oaphiol ~ Naot! minfures b The moisture i¢ allmoed to fend efor Ipmid and ar Byangy- ted dye fs foltend ‘ ot The prrcluct reiryslabed pusing Glial acetic get o- fits Yuld = 2-54 e Scanned with CamScanner