ND 210

Control No.
ZN2N1ME-06
Instruction Manual
of
Nitrogen Detector ND-210
MITSUBISHI CHEMICAL ANALYTECH

Introduction
Thank you for buying our nitrogen detector Model ND-210.

This unit is for measurement of nitrogen in liquid, solid, and gas samples.
To use the unit efficiently and safely, read this manual and fully understand the functions and the
operation methods before use.
To use Model ND-210 correctly and safely, appoint supervisors and operators before use.
Refer to the Operation Manual for measurement operation using a complete system.
In the NSX-2100 system, the following accessories can be used for different types of samples.
Read the instruction manuals of each additional unit.
(There are some unsupported combinations. When adding new accessories, update the unit software
and the PC program.)
• Electric furnace (HF-210 and VF-210) : For combustion, decomposition, and gas control
• Automatic Boat Controller (ABC-210) : For carrying samples into HF-210
• Automatic Sample Changer for solid samples (ASC-240S)
An automatic boat controller is built in.
• Automatic Sample Changer for liquid samples (ASC-250L)
When using HF-210, use with ABC-210.
• Gas Injector (GI-210 or GI-220) : For gas sample measurement
Before the Use
(1) Do not reprint this manual wholly or partially without permission.
(2) The contents may be changed without notice.
(3) Though this manual was prepared carefully, contact local distributor when mistakes, omissions, or
missing pages are found. The system program windows in this manual may be different depending
on the version of the software.
(4) For any circumstances resulting from usage of results of ND-210, we do not take any
responsibility regardless of (3).
(5) Assign specific operators and supervisors when using this unit.
(6) Follow the contents in this manual. When troubles or damages occur by neglecting the contents in
this manual, we do not guarantee units even within the guarantee term.
MITSUBISHI CHEMICAL ANALYTECH has the copyrights of this manual and the unit software.
Other company and product names are their trademarks and registered trademarks.
SAFETY PRECAUTIONS
SAFETY PRECAUTIONS
Read this instruction manual with care before use.
Keep the manual at hand when operating the unit.
Security can not be assured if the unit is operated without following the instructions in this manual.
Contact a local distributor if any questions, errors, or omissions are found.
WARNING
Information under this sign explains critical operations which contain risk of death or
serious casualties.
CAUTION
Information under this sign explains critical operations which contain risk of human
casualties or damages to surrounding objects.
POINT
Information under this sign explains important and useful information for utilizing the
unit.
Labels
The following labels are attached to this unit. Always follow the instructions in the labels.
Caution labels Attached places

At gas connection part of
ND-210 rear.
1
SAFETY PRECAUTIONS
Read the following cautions carefully to use the unit correctly and safely.
Installation
When installing the unit, observe the following precautions.
CAUTION
Install the unit in a place where temperature is 15 to 35 degrees Celsius.
Failure to do so can lead to a fire or unstable operation.
CAUTION
Install the unit in a place free from direct sunlight.
Failure to do so can lead to a fire.
CAUTION
Install the unit in a place free from strong vibration or continuous weak vibration.
Failure to do so can lead to unstable operation.
CAUTION
Install the unit in a place free from strong electromagnetic field.
Failure to do so can lead to unstable operation.
CAUTION
Install the unit in a place where humidity is 80% or less.
Failure to do so can lead to a fire or cause electric shock.
CAUTION
Install the unit in a place free from corrosive gas.
Failure to do so can lead to deterioration of the unit.
CAUTION
Install the unit in a place free from much dust.
Failure to do so can lead to a fire or cause electric shock.
CAUTION
Install the unit in a place where fire is not used.
Failure to do so can lead to a fire.
2
SAFETY PRECAUTIONS
CAUTION
Install the unit on a flat surface to avoid displacement of units.
CAUTION
Ventilate the room by a ventilating fan, etc. Failure to do so may affect the health by the
vapor or gas generated from chemicals.
CAUTION
When moving the unit, two persons should hold the unit bottom. The unit is heavy and
the injury by dropping the unit on the foot may be caused.
During Usage
CAUTION
Use micro syringes specified by the unit manufacturer.
CAUTION
Appoint specific supervisors and operators for this unit.
CAUTION
Do not touch the power plug with wet hands to prevent electric shock.
CAUTION
Do not modify, damage, or put together the power cable.
Do not use the current under the rating or the power cable of the voltage value.
By placing heavy objects on the cable, heating or putting together the cable or using the
current under the rating, the cable is broken by temperature raise to cause a fire and
electric shock.
CAUTION
Do not remove the covers of the unit except for our servicemen.
Electric shock or fire can be caused.
CAUTION
Check that the earth terminal is properly connected to prevent electric shock.
3
SAFETY PRECAUTIONS
CAUTION
When handling chemicals, put on safety glasses and gloves to protect skin and eyes.
Do not inhale chemical vapor.
Maintenance and Inspection
CAUTION
Check the unit every day before use. Failure to check can lead to reduced performance
of the unit, and even to serious accidents.
In Case of Accidents
WARNING
When accidents occur to this unit, immediately inform supervisors and take an
emergency procedure. While causes are unclear or troubles are not solved,
never restart the unit.
4
Table of Contents
Table of Contents
Section 1: Names and Functions of ND-210 Unit
1-1. ND-210 Unit Names and Functions 1-1
1-2. ND-210 Inside Names and Functions 1-2
1-3. ND-210 Rear Names and Functions 1-3
Section 2: Parts Check
2-1. Parts for ND-210 2-1
2-2. Parts for Vertical Furnace 2-2
2-2-1. Parts for ND-210/SD-210 Gas Dryer Set for Vertical Furnace 2-2
2-2-2. Pyrolysis Tube Set for ND-210 with Vertical Furnace 2-2
(NSX-2100V/oil sample)
2-2-3. Pyrolysis Tube Set for ND-210 with Vertical Furnace 2-3
(NSX-2100V/aqueous sample)
2-2-4. Injection Port Set for ND-210 Manual 2-3
2-3. Parts for Horizontal Furnace 2-3
2-3-1. Parts for ND-210/SD-210 Gas Dryer Set for Horizontal Furnace 2-3
2-3-2. Pyrolysis Tube Set for ND-210 with Horizontal Furnace (NSX-2100H) 2-4
Section 3: Installation
3-1. Installation Conditions 3-1
3-2. Installation Space 3-1
3-3. Power Preparation 3-2
3-3-1. Power 3-2
3-3-2. Grounding 3-2
3-4. Supply Gas Line 3-2
3-4-1. Line Preparation 3-2
3-4-2. Line Connection 3-2
3-5. Preparation of ND-210 for Vertical Furnace 3-3
3-5-1. Lines of Pyrolysis Tube Outlet and the Tube Dryer Vertical Furnace) 3-3
3-5-2. Buffer Tank Setting (Vertical Furnace) 3-5
3-6. Preparation of ND-210 for Horizontal Furnace 3-6
3-6-1. Lines of Pyrolysis Tube Outlet and the Tube Dryer (Horizontal Furnace) 3-6
3-6-2. Lines of the Tube Dryer at the Unit Rear (Horizontal Furnace) 3-7
3-6-3. Buffer Tank Setting (Horizontal Furnace) 3-8
3-7. Ozone Scrubber Setting 3-9
3-8. Vacuum Pump Connection 3-10
3-9. Cable Connection 3-11
3-9-1. Communication Cable Connection 3-11
3-9-2. Power Cable Connection 3-11
3-9-3. Gas Sensor Power Cable Connection 3-11
3-9-4. Vacuum Pump Power Cable Connection 3-11
1
Table of Contents
Section 4: Preparation
4-1. Measurement Principles 4-1
4-1-1. Samples Inappropriate for Measurement 4-2
4-1-2. Interference in Chemiluminescence Method 4-2
4-2. Ozonizer 4-3
4-3. Parameter Settings 4-4
4-4. Measurement Monitor Display 4-9
4-4-1. Real-time Monitor 4-9
4-4-2. Recent 4-9
4-4-3. Monitor Setting 4-10
Section 5: Troubleshooting
5-1. No Power to the Unit 5-1
5-2. No Gas Flow 5-1
5-3. Operation Button “Start” Does Not Flash 5-2
5-4. No Peak 5-2
5-5. Unstable Peak 5-3
5-6. Measurement Time is Too Long 5-3
5-7. Unstable Measurement Values 5-4
5-8. Measurement Does Not End 5-4
5-9. Troubles Occur after Changing Gas Cylinder or Gas Line 5-4
Section 6: Error Messages and Measures 6-1
Section 7: Maintenance and Inspection
7-1. Inspection 7-1
7-1-1. Daily Inspection 7-1
7-1-2. Periodical Inspection 7-3
7-1-3. Performance Inspection 7-5
7-2. Maintenance 7-6
7-2-1. Septum Change 7-6
7-2-2. Washing of Trap Tube and Female Ball Joint 7-6
7-2-3. Reactivation of Catalyst in Pyrolysis Tube 7-6
7-2-4. Change of Catalyst in Pyrolysis Tube 7-6
7-2-5. Tube Dryer Change 7-7
7-2-6. Fuse Change 7-7
7-2-7. Silica Filter Change 7-8
7-3. Storage of the Unit 7-9
Section 8: Specifications 8-1
2
Table of Contents
Section 9: Consumables
9-1. ND-210 9-1
9-2. Consumables for Vertical Furnace 9-1
9-2-1. ND-210 / SD-210 Gas Dryer for Vertical Furnace 9-1
9-2-2. Pyrolysis Tube Set for ND-210 with Vertical Furnace (oil sample) 9-2
9-2-3. Pyrolysis Tube Set for ND-210 with Vertical Furnace (aqueous sample) 9-2
9-2-4. Injection Port Set for ND-210 Manual 9-2
9-3. Consumables for Horizontal Furnace 9-3
9-3-1. ND-210 / SD-210 Gas Dryer for Horizontal Furnace 9-3
9-3-2. Pyrolysis Tube Set for ND-210 with Horizontal Furnace (NSX-2100H) 9-3
9-4. Maintenance Parts 9-3
9-5. Parts Pictures 9-4
3
Table of Contents
4
Section 1: Names and Functions of ND-210 Units
1-1. ND-210 Unit Names and Functions
2 4
1 3
Fig. 1-1. ND-210 Front
Table 1-1. ND-210 Unit Front Names and Functions
No. Names Indications Functions

Power is supplied to ND-210 by
1 Power switch POWER
turning on this power switch.
2 Power LED LED is on when power switch is on.
Supplies power to ozonizer.
Ozone is generated when following
conditions are met.
3 Ozonizer switch OZONIZER
• ND-210 power switch is on.
• Ozonizer power switch of PC
software is on.
LED is on when ozonizer is on.
4 Ozonizer LED When ozonizer switch of PC is turned
off, LED remains on until vacuum
pump shuts down.
1-1
1-2. ND-210 Inside Names and Functions
1
4
2
Fig. 1-2. ND-210 Inside
Table 1-2. ND-210 Unit Inside Names and Functions

Oxygen gas flow Control flow of oxygen used for ozone
1
controller generation and tube dryer.
Removal of soot generated by
2 Disk filter
incomplete combustion of sample gas.
For cooling the ozonizer.
3 Cooling fan
Never block the air flow.
Cartridge for decomposing ozone.
Set tubes to the exhaust inlet (small) at
4 Ozone scrubber the ozone scrubber top and the bottom
exhaust (big). Connect them to the
tubes of ND-210 rear pump suction
port.
1-2
1-3. ND-210 Rear Names and Functions
2 8
3 9
4 10
11
12
5
Fig. 1-3. ND-210 Rear
Table 1-3. ND-210 Rear Names and Functions

1 Gas sensor GAS SENSOR For ND-210 option.
connector
2 Signal connector MAIN UNIT Connection of ND-210 to the electric furnace.
RS-232C crossing cable is used.
3 Function switch FUNCTION DIP switches for each setting are built in.
Only for maintenance. Do not touch them.
4 Exhaust fan For cooling the NO sensor.
Do not place any objects within 150mm from the
panel.
5 Pump outlet PUMP Power cable connection for vacuum pump.
During ozonizer operation, power is supplied to
this outlet.
1-3
6 Fuse holder FUSE 2A Use proper fuses.
TYPE T
7 Power connector a.c.POWER Use power cable based on our specification.
8 Oxygen exhaust EXHAUST A PTFE tube (φ4/2) comes out here.
O2
9 Sample gas EXHAUST A PTFE tube (φ4/2) for sample gas comes out here.
exhaust SAMPLE To measure nitrogen and sulfur simultaneously,
connect this line to the sulfur detector.
10 Oxygen inlet GAS IN O2 gas inlet.
O2
11 Sample gas inlet GAS IN A PTFE tube (φ4/2) for sample gas comes out here.
SAMPLE Pass the tube through the buffer tank connector and
insert it completely. The line tip should have a
diagonal cut.
12 Pump suction port VACUUM Connect the vacuum pump tube to this tube.
PUMP
1-4

Table 2-1 shows ND-210 parts list.
When initially opening the package, check that all listed parts are included.
For consumables, refer to “Section 9: Consumables”.
2-1. Parts for ND-210
Table 2-1. ND-210 Parts List
Parts names Quantity Check Remarks

No.
column
1 ND-210 1 pc
Ozone scrubber with hose bands 1 pc
2
(large and small)
One is already set to the
3 Hose band (large) 2 pcs tube of the rear pump
suction port.
Three-way connector (4TTT-S) with a
4 1 pc
stainless tube
One for three-way joint
5 Insert (J-4×2INS-S) 2 pcs/set
One for spare
φ4 Nut
6 (with front and back ferrules and 1 set
inserts)
7 PTFE tube φ4/2 1.6m 1 pc
8 RS-232C cable, 9-pin, cross 1 pc
9 Fuse 3.15A 2 pcs/set
Power cable 1 pc Packed in separate box.
10
(AC 100/115V or 230/240V 2m)
ND-210 instruction manual 1 pc
11
(This manual)
ND-210 operation manual for 1 pc
12
vertical furnace
ND-210 operation manual for 1 pc
13
horizontal furnace
Instruction manual for standard 1 pc
14
samples
2-1
2-2. Parts for Vertical Furnace
2-2-1. Parts for ND-210/SD-210 Gas Dryer Set for Vertical Furnace
Table 2-2. Parts List of ND-210/SD-210 Gas Dryer Set for Vertical Furnace

No.
column
1 Tube dryer 1 pc
2 Clamp for tube dryer 1 pc
For sample gas inlet and
3 PTFE tube φ6/4 3cm 2 pcs
outlet of the tube dryer
φ6/4 reducer elbow connector 1 pc For sample gas outlet of
4 the tube dryer
(30-6RUE4-C)
φ6/4 One-touch connector For dry gas inlet and
5 2 pcs outlet of the tube dryer
socket elbow 6-4
6 PTFE tube φ4/2 90cm 1 pc For dry gas exhaust
7 PTFE tube φ4/2 45cm 1 pc For buffer tank
8 Buffer tank 1 pc
9 Buffer tank clamp with two screws 1 set
2-2-2. Pyrolysis Tube Set for ND-210 with Vertical Furnace (NSX-2100V/oil sample)
The following parts are optional and may not be included in the package depending on the purchased
configuration.
Table 2-3. Parts List of Pyrolysis Tube Set for TS Vertical Furnace
No. Parts names Quantity Check column Remarks
1 Outer pyrolysis tube φ30 L375 1 pc
2 Inner pyrolysis tube φ22 L227 1 pc
3 Spring for pyrolysis tube 2 pcs
4 Female ball joint 1 pc Packed in separate
box.
5 Oxidation catalyst 30g (platinum) 1 pc
6 φ6 Connector (30-6U-S), straight 1 pc
2-2
2-2-3. Pyrolysis Tube Set for ND-210 with Vertical Furnace (NSX-2100V/aqueous
sample)
configuration.
Table 2-4. Parts List of Pyrolysis Tube Set (aqueous sample)

No. Parts names Quantity Check column
1 Outer pyrolysis tube φ30 L375 1 pc Packed in separate
box.
2 Pyrolysis tube adapter φ29 L35 1 pc
4 Trap tube for pyrolysis tube bottom 1 pc
5 Oxidation catalyst 30g (platinum) 1 pc
6 φ6 Connector (30-6UE-S), elbow 1 pc
2-2-4. Injection Port Set for ND-210 Manual
configuration.
Table 2-5. ND-210 Parts List of Injection Port Set for ND-210 Manual
No. Parts names Quantity Check column

1 Injection port 1 pc
2 Septum (flat-type) 100 pcs/set
* Syringes for manual injection are required separately.
2-3. Parts for Horizontal Furnace
2-3-1. Parts for ND-210/SD-210 Gas Dryer Set for Horizontal Furnace
Table 2-6. Parts List of ND-210/SD-210 Gas Dryer Set for Horizontal Furnace
No.
column
1 Female ball joint 1 pc
2 Lure lock 1 pc They are already
assembled.
3 Filter holder (PFA-25) 1 pc
4 Silica filter (QR100) 1 pc
5 Lure hub (Female) 1 pc
6 Tube dryer 1 pc
2-3
No.
column
2 pcs For the electric furnace
7 Clamp for tube dryer
rear
For the sample gas inlet
8 PTFE tube φ6/4 3cm 2 pcs and the outlet of the
tube dryer
1 pc For the sample gas
9 φ6/4 elbow connector (30-6RUE4-C) outlet of the tube dryer
φ6/4 One-touch connector For the dry gas inlet and
10 2 pcs the outlet of the tube
socket elbow 6-4 dryer
1 pc For a buffer tank to a
11 PTFE tube φ4/2 45cm tube dryer
12 Buffer tank 1 pc
13 Buffer tank clamp with two screws 1 set
Thermal insulator (with a magnet 1 pc For the electric furnace
14 door
sheet)
Protection plate for a pyrolysis tube 1 pc Spacer for the pyrolysis
15 tube tip
(with a magnet sheet)
2-3-2. Pyrolysis Tube Set for ND-210 with Horizontal Furnace (NSX-2100H)
configuration.
Table 2-7. Parts List of Pyrolysis Tube Set for ND-210 with Horizontal Furnace (NSX-2100H)
No. Parts names Quantity Check column Remarks
1 Outer pyrolysis tube φ30 L410 1 pc
2 Inner pyrolysis tube φ22 L227 1 pc
4 Oxidation catalyst 30g (platinum) 1 pc Packed in separate
box.
φ6/4 reducer elbow connector
5
(30-6RUE4-C) 1 pc
Electric furnace inlet stainless ring for
6
NS (with a ring stopper) 1 set
7 Ring of the electric furnace outlet 1 pc
Heat shield panel of the electric
8 2 pcs/set
furnace outlet
2-4
Necessary space, power, and gas lines for ND-210 installation are described in this section.
3-1. Installation Conditions

Install the unit as the following conditions for the long-term stable use.
Install ND-210 based on the following conditions for long-term stable use.
Refer to “SAFETY PRECAUTIONS” in this manual for details.
• Room temperature is 15 to 35 degrees Celsius. Temperature change is small.

• No direct exposure of the unit to wind from air conditioners.
• Free from direct sunlight.
• No strong vibration and continuous weak vibration.
• No strong electromagnetic field.
• Humidity is under 80%. (No condensation).
• No corrosive gas.
• Free from much dust.
• Fire must not be used.
• No flammable materials.
• The surface for installation is flat and stable.
• The room is ventilated.
If troubles or damages are caused by negligence of the above conditions, we can not guarantee units
even within the guarantee term.
3-2. Installation Space

Space needed to install ND-210 is as follows.
• Desk size: Width 220mm × Depth 400mm
• Desk withstand load: About 22kg
• Do not place objects in front of the rear fan.
• Secure at least 150mm of space between the unit and the back wall.
• Install ND-210 to the left of the electric furnace (HF-210 or VF-210).
3-1
3-3. Power Preparation
3-3-1. Power
ND-210 consumption power is 300VA.

Voltage fluctuation range should be within ±10%.
When voltage fluctuation is over 10%, use a voltage stabilizer.
3-3-2. Grounding
ND-210 power cable is 3-line type including a grounding line.

Insert power cables into 3-line type power outlets and ground them stably.
If the power outlets are 2-line type, always ground them from the earth terminals of power cables.
3-4. Supply Gas Line
3-4-1. Line Preparation
The gas line for the electric furnace will branched off, so there is no need to prepare an exclusive line
for ND-210.
3-4-2. Line Connection
(1) Connect a three-way connector (4TTT-S) to the oxygen line inlet of the electric furnace
(VF-210 or HF-210) rear.
(2) Connect a line for oxygen gas to “GAS IN O2” of ND-210 rear.
Fig. 3-1. ND-210 System Line Connection
3-2
3-5. Preparation of ND-210 for Vertical Furnace
3-5-1. Lines of Pyrolysis Tube Outlet and the Tube Dryer (Vertical Furnace)
To remove moisture in sample gas, set a tube-type dehumidifier (tube dryer).
(1) Open the front door of the electric furnace, pass the tube dryer though the rear from the unit duct.
About two-thirds of the tube dryer should be outside of the unit.
(2) Set a φ6 one-touch connector (PLGJ6-4) to the connector of the dryer side.
(3) Connect a PTFE tube φ4/2 90cm and put it out to the unit rear.
(4) Connect a PTFE tube φ6/4 3cm to the dryer tip.
(5) Set one of the following connectors to (4).

• φ6 connector (30-6U-S, straight) set to a female ball joint
• φ6 connector (30-6UE-S, elbow) set to a trap tube
(6) Set the female ball joint or the trap tube for pyrolysis tube bottom to the pyrolysis tube with a clip
(long) φ18 for ball joint.
(1) Put out about (4) Connect a PTFE tube φ6/4

two-thirds of the 3cm.
tube dryer to the
unit rear from
the unit duct.
(6) Set female ball joint or
trap tube for pyrolysis
tube bottom with clip
for ball joint.
(3) Connect
PTFE tube (2) Connect one-touch
φ4/2 90cm
and put it connector (5) Set φ6
out to the (PLGJ6-4) to the connector
unit rear. connector of tube (30-6U-S).
dryer.
Fig. 3-2 Lines (1) of the Tube Dryer
3-3
(7) Fix the tube dryer to the unit rear with a wire.
(9) Connect the PTFE tube of ND-210 “EXHAUST O2” to the connector of the tube dryer side.
(10) Connect the PTFE tube of ND-210 “EXHAUST SAMPLE” to a duct leading to a ventilation
system. When using ND-210 together with the SD-210, connect this line to SD-210 “SAMPLE
IN”.
(10) Connect the tube

from “EXHAUST
SAMPLE” to the
exhaust or SD-210
“SAMPLE IN”.
(8) Set a one-touch

connector to the
connector of the
tube dryer. (7) Fix the tube dryer to
the unit rear.
(9) Connect
“EXHAUST
O2” tube to the
tube dryer.
Fig. 3-3 Lines (2) of The Tube Dryer
3-4
3-5-2. Buffer Tank Setting (Vertical Furnace)
Combustion gas from the electric furnace is passed through a tube dryer, once stored in a buffer tank,
and then transmitted into the detector. The procedure for setting a buffer tank is as follows.
When setting lines to the buffer tank, use the sleeve inside the nut to fix firmly.
(1) Set a buffer tank to ND-210 rear with screws.
(2) Take the PTFE tube from “GAS IN SAMPLE” of ND-210 rear and insert it though the inlet
connector of the tank. Insert it completely. The line tip should have a diagonal cut.
(To connect SD-210 to ND-210, cut the line tip to be flat. To switch back to one detector after
cutting the line tip flat, the tube tip should be 5mm from the top surface of the buffer tank.)
(3) Set a φ6/4 PTFE tube 3cm to the dryer top. Connect a φ6/4 reducer elbow connector
(30-6RUE4-C) to the end.
(4) Connect a φ4/2 PTFE tube 45cm to (3) and connect the free end to the other connector (not pass
through) of the buffer tank.
(3) Set φ6/4 PTFE tube 3cm to tube

dryer. Set φ6/4 elbow connector
(30-6RUE4-C) to PTFE tube.
(1) Fix buffer tank

with screws.
(4) Connect φ4/2 PTFE tube 45cm

to the tube dryer tip and (2) Insert the tube of “GAS
connect it to the buffer tank. IN SAMPLE” into
buffer tank.
Fig. 3-4. Connection of Buffer Tank Lines of ND-210 Rear
3-5
3-6. Preparation of ND-210 for Horizontal Furnace
3-6-1. Lines of Pyrolysis Tube Outlet and the Tube Dryer (Horizontal Furnace)
To remove moisture in sample gas, set a tube-type dehumidifier (tube dryer).
(1) Set a φ6/4 PTFE tube 3cm to both ends of the tube dryer.
(2) Set the filter to the female ball joint.
(3) Connect the tube dryer to the opposite side of the filter.
(5) Set the female ball joint to the pyrolysis tube with a clip φ18 (long) for ball joint.
(1) Connect the two points of a φ6/4PTFE tube

3cm.
(4) Set φ6 one-touch
connector (PLGJ6-4).
(3) Set filter to tube dryer.
(2) Set filter to female ball joint.

Refer to “7-2-7. Silica Filter
Change” to assemble a filter.
(5) Set the female ball

joint to the pyrolysis
tube with a clip φ18
(long) for ball joint.
Fig. 3-5 Connection of the Tube Dryer
3-6
3-6-2. Lines of the Tube Dryer at the Unit Rear (Horizontal Furnace)
(1) Fix the tube dryer to the electric furnace rear with a wire lock.
(3) Connect the PTFE tube of “EXHAUST O2” of ND-210 rear to (2) φ6 one-touch connector
(PLGJ6-4) from the furnace rear.
(4) Connect the φ4/2 PTFE tube of “EXHAUST SAMPLE” of ND-210 rear to the duct to the exhaust
utilities. (When checking the gas leakage of the whole system, connect the attached ball joint
here.)
(2) Connect a one-touch

connector (PLGJ6-4)
to the connector of
tube dryer.
(1) Fix tube dryer
to the electric
furnace rear. (3) Connect the PTFE tube of
“EXHAUST O2” to the
tube dryer side.
(4) Connect the PTFE tube of

“EXHAUST SAMPLE” to
the exhaust. (The connection
point of the ball joint for gas
leak check)
Fig. 3-6 Line Connection of the Tube Dryer
3-7
3-6-3. Buffer Tank Setting (Horizontal Furnace)
Combustion gas from the electric furnace is passed through the tube dryer, stored in the buffer tank,
and then transmitted into the detector. The procedures for setting the buffer tank and connecting the
lines are described. When connecting lines to the buffer tank bottom, use the sleeve inside the nut to
fix them firmly.
(1) Set a buffer tank to ND-210 rear with screws.
(2) Take the PTFE tube from “GAS IN SAMPLE” of ND-210 rear and insert it deeply through the
inlet connector (with sleeves) of the tank. The line tip should have a diagonal cut.
(3) Set the φ 6/4 elbow connector (30-6RUE4-C) to the dryer tip.
(4) Connect the tube dryer tip and the buffer tank connector (which does not pass through) by using
the φ4/2 PTFE tube 45cm.
(1) Fix the buffer

tank with
screws.
(3) Set φ 6/4

elbow
connector to
the dryer tip.
(2) Insert the tube of “GAS IN

SAMPLE ” deeply into the
(4) Connect tube dryer tip and buffer tank buffer tank. (When the tip
connector (which does not pass is not cut diagonally, allow
5mm space at top.)
through) by using φ4/2 PTFE tube
45cm.
Fig. 3-7 Line Connection of Buffer Tank and Tube Dryer at ND-210 Rear
3-8
3-7. Ozone Scrubber Setting
To treat gas after combustion, set an ozone scrubber (a cartridge for ozone treatment) to the clamp of
the unit front.
CAUTION
Do not clog the exhaust outlet to avoid the following conditions.
• Pyrolysis tube falls off from the flange.
• Gas accumulates inside the pyrolysis tube and the glass breaks from high pressure.
(1) Open the door of ND-210 front and set the ozone scrubber to the clamp. The exhaust inlet (small)
should come to the top side.
(2) Connect the smaller flexible tube to the exhaust inlet (small) and fix it with a clamp.
(3) Connect the larger flexible tube to the exhaust outlet (big) and set a hose band.
Exhaust Inlet
Small (outer diameter 4mm)
For exhaust gas containing
ozone
Exhaust Outlet
Large (outer diameter 8mm)
For sending scrubber-treated
exhaust gas into vacuum
pump
Fig. 3-8. Ozone Scrubber Setting
3-9
3-8. Vacuum Pump Connection
Connect ND-210 to a vacuum pump.
(1) Connect suction tube for vacuum pump to the connector of suction tube
coming from “VACUUM PUMP” of ND-210. Fix with hose band.
(2) Cut the suction tube for vacuum pump to a suitable length and connect the
free end to the vacuum pump. Fix with hose band.
(3) Turn on the power switch of vacuum pump.
(Power is supplied from ND-210, so power switch of pump should always
be on.)
Tube coming from “VACUUM PUMP” of ND-210
Hose band
Connector
Hose band
Suction tube
connection port
Hose band
Vacuum pump
Suction tube for
vacuum pump
Fig. 3-9. Vacuum Pump Connection
3-10
3-9. Cable Connection
3-9-1. Communication Cable Connection
Connect one of 1 to 8 “ACCESSORIES” connector of the electric furnace (HF-210 or VF-210) rear to
“MAIN UNIT” connector of ND-210 rear with attached RS-232C cable.
3-9-2. Power Cable Connection
Connect a power cable to “a.c. POWER” connector of ND-210 rear.
3-9-3. Gas Sensor Power Cable Connection
Connect a power cable for an optional gas sensor to “GAS SENSOR” connector of ND-210 rear.
3-9-4. Vacuum Pump Power Cable Connection
Connect the vacuum pump power cable to “PUMP” of ND-210 rear outlet.
Gas sensor (option)

Communication cable
Power cable for vacuum pump
Power cable
Fig. 3-10. Power Cable Connection
3-11
3-12
4-1. Measurement Principles
Sample is injected into a high-temperature (600 to 1100℃) pyrolysis tube by argon carrier gas.
After nitrogen compounds in the sample are pyrolyzed, it is combusted, oxidized, and converted to
nitric oxide (NO). After removing moisture from the combustion gas by a dehumidifier (tube dryer),
the following oxidation reaction occurs by reaction of NO with ozone.
NO + O3 → NO2 + O2 + hν
By this reaction, 590 to 2,500nm wavelength light is generated.
The optical intensity of this light is proportional to the NO concentration at a wide frequency range.
After emitted light is detected by a photomultiplier tube and signal processing is run, an area value is
obtained. Using the relation between area and concentration (calibration curve) obtained from
standard solutions, the total nitrogen concentration in the sample is calculated.
Though some samples generate interfering substances such as SOx and CO in the process of
decomposition to NO, there is little influence on measurement by chemiluminescence method by
pressure reduction method.
NSX-2100V(ND) Constant MFC: Mass flow controller
injection Outer pyrolysis tube
Ar ・ Sample for oil samples： Inner pyrolysis tube
MFC ・ Aqueous sample： Adapter
PC
Buffer PR
MFC
tank
O2 Photo-multiplier tube
Tube dryer (PMT)
Furnace
Ozonizer Ozone scrubber

Chemiluminescence
Oxidation cell
Trap tube Exhaust
catalyst
for aqueous MFC
samples
Vacuum pump
NSX-2100H(ND) MFC: Mass flow controller
O2
MFC
Buffer tank
PC MFC
PR
MFC
Ozonizer Tube dryer
Photo-multiplier tube Ar
(PMT)
Furnace
Injector
Ozone scrubber Chemiluminescence
cell
Exhaust Inner pyrolysis tube
Oxidation catalyst Outer pyrolysis tube
Vacuum pump Filter
Fig. 4-1. Measurement Principle
4-1
4-1-1. Samples Inappropriate for Measurement
For nitrogen in samples such as azo compounds and hydrazine compounds, N2 is generated as the
main compound when pyrolyzed in a pyrolysis tube.
Therefore, recovery is extremely low in chemiluminescence method and measurement can not be run
accurately.
4-1-2. Interference in Chemiluminescence Method
• Interference Element Concept
There are two types of interference elements in chemiluminescence method.

Substances which react with ozone and generate chemiluminescence light will cause positive
interference.
Substances which takes away excitation energy from the excited NO2 will cause negative
interference.
• Positive Interference
The following substances may show positive interference.
(a) Carbonyl compounds of iron and nickel

(b) Olefins such as ethylene and trimethyl ethylene
(c) Sulfides such as dimethyl sulfide and hydrogen sulfide
The frequency of chemiluminescence light from (a) substances overlap with ozone’s
chemiluminescence. But these substances are unlikely to exist in the sample gas, and
practically, there is no problem.
The chemiluminescence from (b) and (c) can be omitted in most cases by optical filters, but
in some special cases, these substances can interfere with the measurement.
Samples including chlorine (e.g. sea water) generate Cl2 and sometimes interfere with
measurement. Use acid gas removal kit (optional) to avoid this.
• Negative Interference
Negative interference occurs when interference element removes excitation energy from
excited molecules. Therefore, interference occurs when measurement element coexists with
interfering substances.
Water and carbon dioxide show negative interference. Water is removed by the dehumidifier.
When carbon dioxide concentration is stable, NO concentration is influenced at a fixed rate.
By the reduced pressure method, the pressure within the chemiluminescence cell is reduced
and intervention among molecules is decreased. Therefore, the influence of carbon dioxide
can be decreased to an irrelevant level.
4-2
4-2. Ozonizer
ND-210 is equipped with an ozonizer. To start the ozonizer, power and oxygen gas must be supplied
to the unit and NSX-2100 application program must be started.
POINT
When a schedule is not selected, the ozonizer can not be turned on.
Open a schedule and click [Prepare] button before running the following steps.
(1) Click or select “Control”, “Detectors”, “ND-210”, “Ozonizer”, and “On” from the menu
bar.
The check window is displayed.
(2) Click [OK] button. The ozonizer starts.
4-3
4-3. Parameter Settings
POINT
• Parameters do not need to be newly set each time. Set parameters when necessary.
• Use “Auto” mode for usual measurements.
• Set ‘Timer’ mode when “PMT sensitivity” is set to “Low Concentration” and
integration start and end can not be detected properly.
(1) Open a schedule.

(2) Click [Parameter] button.
(3) Click [ND-210] in the left section.
→ The below window is displayed.
(4) Click the right section and change parameters. (Gray items can not be changed.)
Refer to “Table 4-1. Parameters List” in the next page.
(5) Click [Step List] button to return to the step list. Changed parameters are saved at this time.
4-4
(6) Select “PMT sensitivity” and “Mode” in ND item of “Step List”.
Refer to “Table 4-1. Parameters List”in the next page for details.
Table 4-1. Parameters List

Names Contents/Input ranges Default Values Units
PMT Select sensitivity of Electric
photomultiplier tube. furnace
sensitivity
High: For Low Concentration: For Low For High
0.1 to 100μg/ml (indication) Concentration Concentration
Low: For High Concentration:

10 to 5000μg/ml (indication)
Mode Auto: Automatic detection of
signal start and end
Auto Timer Auto Timer
Timer: Signal processing by setting
start and end time
O2 flow Control of O2 flow rate for ozone Vertical 600 600
generation and tube dryer ml/min
(0 to 2000) Horizontal 300 300
Detection start Start time for peak detection can

0 0 sec
waiting time be changed. (0 to 999)
This value defines the time a peak Vertical
60 60
Start detection start will be searched after start of
continuance measurement. sec
Horizontal
time No detection during ‘Detection 120 120
start waiting time’ (0 to 9999)
If no peak end is detected after
Compelled end 300 300
this parameter time has passed
time after start sec
from peak start, measurement is
detection 540 540
aborted. (0 to 9999)
Start position Measurement start position can
OFF OFF
fixing be fixed. (ON/OFF)
Waiting time Set waiting time until integration
of integration start after measurement start in 5 5 sec
start “Timer Mode”. (0 to 999)
Set time from measurement start Vertical 240 240
Measurement to end in ‘Timer Mode’. sec
time Horizontal
(0 to 9999) 540 540
4-5
Parameter Details
(1) PMT sensitivity

Select either sensitivity depending on sample concentration.
• Low Concentration: Sensitivity for the measurement of only trace range

• High Concentration: Sensitivity for general measurement to high-concentration range
Table 4-2. PMT Sensitivity Settings

Aqueous samples Nonaqueous samples (oil)
Electric PMT Nitrogen Injection Nitrogen Injection
furnace sensitivity concentration volume concentration volume
(μg/ml) (μl)
Low 0 to 50 90 0 to 50μg/ml 90μl

concentration 0 to 200μg/ml 20μl
Vertical
furnace High 0 to 200 25 5 to 2000μg/ml 20μl
concentration 10 to 5000μg/ml 10μl
Low 0 to 25μg/g 40mg
concentration 0 to 50μg/g 20mg
Horizontal
furnace High 0 to 2500μg/g 20mg
concentration
0 to 5000μg/g 10mg
(2) Measurement mode (Standard: Auto)
To detect start and end points of signal processing, select “Auto” or “Timer” and input required
parameters.
Auto: Peak is automatically detected by judging the start and end points based on the slope of
the baseline.
Timer: When measuring samples with very low concentration, peak start and end sometimes
can not be detected automatically. In this case, select “Timer” to set start and end times and run
signal processing based on the set times.
(3) O2 flow (Standard value: 600ml/min for vertical furnace, 300ml/min for horizontal furnace)
O2 for ozone generation and tube dryer
Table 4-3. Injection Volume and Recommended O2 Flow
Injection volume (μl) O2 flow (ml/min)
20 to 40 200
40 to 60 400
60 to 90 600
4-6
(4) Parameters for Auto mode

1. Detection start waiting time
(Standard value: 0sec for vertical furnace and horizontal furnaces)
Waiting time between measurement start and peak detection. Peak start will not be detected
during this time.
2. Start detection continuance time

(Standard value: 60sec for vertical furnace, 120sec for horizontal furnace)
Peak start detection point will be searched for this time after measurement start.
3. Compelled end time after start detection
(Standard value: 300sec for vertical furnace, 540sec for horizontal furnace)
Measurement will be terminated if peak end can not be detected within this time.
4. Start position fixing (Standard setting: OFF for vertical and horizontal furnaces)
By setting this function to ON, integration starts without peak start detection after “1.
Detection start waiting time”. Starting position of each measurement can be fixed with this
function.
Automatic mode signal detection (Single peak)
Signal strength
4. Start position fixing

Integration start
Peak start
detection
Integration
start Integration end
Measurement start Peak end detection Measurement
end
1
Detection start 5 sec.
waiting time
2. Start detection continuance time

3. Compelled end time after start detection
Measurement time
* After detecting peak start, the software will look back into the accumulated data and start
integration from 5 seconds before the peak start detection.
4-7
(5) Parameters for Timer mode

1. Waiting time of integration start (Standard value: 5sec for vertical and horizontal furnaces)
Setting of time from measurement start to integration start
2. Measurement time (Standard value: 240sec for vertical furnace, 540sec for horizontal
furnace)
Setting of time from measurement start to measurement end
Timer mode signal detection (Single peak)
Signal strength
Measurement Integration
Measurement end
start start
(Integration end)
1
Waiting time of
integration start
2. Measurement time
4-8
4-4. Measurement Monitor Display
The display contents of a detector monitor are described.
POINT
By connecting SD-210, ND monitor is displayed automatically.
Click of the toolbar or click “View”, “Detector”, “ND-210”, and “ND Monitor” of the
menu to re-display the window.
4-4-1. Real-time Monitor
“N Signal strength” is drawn continuously in “Real-time” monitor.

z N Sensor: Current signal strength transmitted from ND-210 is displayed.
z Gain: Gain magnification is displayed.
4-4-2. Recent
N Signal charts of 5 most recent measurements are drawn in “Recent” window.
By selecting “Schedule Name”, it is changed to the color of the selected drawing.
4-9
4-4-3. Monitor Setting
By clicking “Option”, the monitor settings can be changed.
• Chart Scale: The setting of the vertical axis of the displayed chart can be changed.
• Passage Time: The setting of the horizontal axis of the displayed chart can be changed.
• [Clear Chart] button: The displayed chart can be cleared.
• Background chart: It is displayed only when recent data are displayed.
The measurement selected at the schedule step can be displayed in the
background. By measuring a sample while the maximum chart of
calibration curve measurement is displayed, sample concentration within
the calibration curve can be checked.
4-10
CAUTION
Do not remove ND-210 cover except for our servicemen.
Electric shock or fire may be caused.
5-1. No Power to the Unit
Causes Countermeasures
ND-210 main power switch is not Turn on the front power switch.
ON.
The power cable is disconnected Connect the power cable firmly to the power
from the power connector. connector.
The power plug is not inserted Connect the power plug firmly to the outlet.
properly into the outlet.
Power is not supplied to the Check by connecting some other electronic
outlet. instrument to the same outlet.
Power fuse is broken. (1) Take off the fuse holder of the unit with a flathead
screwdriver.
(2) Check the conduction between both ends with a
tester.
(3) If there is no conduction, change the fuse with
new one.
5-2. No Gas Flow
The gas cylinder valve is closed. Open the gas cylinder valve.
Remaining gas is insufficient. When remaining gas is low, change the cylinder.
The valve for room gas supply is Open the valve.
closed.
Line is disconnected. Check the connection of the complete gas line.
Connect firmly if any disconnections are found.
Lines are clogged. Check for any clogging in the gas lines. Replace any
clogged parts.
5-1
5-3. Operation Button “Start” Does Not Flash

Unless all conditions for the operation button are met, the button does not flash.
When all connected units meet all conditions and ‘Ready’ marks (green arrows) are displayed at all
icons of the system tree, units are ready.
Check items Countermeasures

No schedule is set to Click [Prepare] button in a schedule to set the
“Measurement schedule”. schedule to “Measurement schedule”.
Parameters are transmitted into the unit and the unit
is ‘Ready’ after stabilization.
All steps in the schedule are Add a new step into the schedule.
already measured.
Parameter PC setting time is long. When “Waiting time for step sequences (sec)” is
long, shorten it.
ND-210 is not ready. For the ND-210 to be 'Ready', all 5 below conditions
must be fulfilled.
1. O2 gas is supplied to the unit.
2. The ozonizer switch is ON.
Click the ozonizer icon and click [Yes] button in the
displayed window. The ozonizer icon can not be ON
without clicking [Prepare] button in the schedule.
3. The cell heater temperature is stable (38 to 42
degrees Celsius).
4. Cooler temperature is stable (2 to 6 degrees
Celsius).
5. Baseline is stable. (Refer to the next item.)
The detector baseline is unstable. When the baseline is stable over “Baseline threshold
(absolute value)”, the system blank is high. Try the
following steps.
1. Wash all glass parts such as pyrolysis tubes.
2. Change the gas purification filter
3. Overhaul the detector.
4. Set “Baseline threshold (absolute value)” to a
higher value and check stability.
5-4. No Peak
ND-210 is not selected as a Select ND-210 when preparing a new schedule.
detector in the schedule.
ND-210 power is OFF. Turn on the power switch.
Electric furnace temperature has Check the temperature in the PC window. If the
not reached the set value. temperature has not reached the set value, turn on the
heater via the heater switch icon.
5-2
Clip for ball joint is not attached. Attach the ball joint firmly with the clip.
The ball joint at the bottom of the
pyrolysis tube is not attached.
Samples are not injected Check the syringe. When using ASC-250L unit,
correctly. check that the syringe needle is not curved, restart the
ASC-250L, and adjust the injection position.
Refer to “4-3-1. Setting the Injection Position” of
ASC-250L instruction manual for details.
Carrier gas is leaking. Check for gas leakage. Refer to “Gas Leak Check” of
the Operation Manual for details.
Sample concentration is too low. Check peak with a standard sample.
The signal cable between the Connect the signal cable.
electric furnace and ND-210 is
not connected.
5-5. Unstable Peak
O2 gas flow rate is improper. The carrier gas and the combustion gas flow of the
electric furnace are as follows. Select a furnace in the
parameter window to set them.
Check the indication of the oxygen flow adjuster of
ND-210 front door.
Refer to “(3) O2 flow” of “Parameter Details” in “4-
4. Parameter Setting”.
Pyrolysis tube is contaminated. Clean the contaminated pyrolysis tube:
• Brush the pyrolysis tube with detergent.
• Soak the tube in a washing solution.
In either case, wash the pyrolysis tube with
pure water and dry before use.
Disk filter is contaminated. When the disk filter is contaminated, change it with
new one. When the PTFE tube around the filter is
contaminated, wash it or change it.
Silica filter is contaminated. For the horizontal furnace (HF-210), the silica filter
may be contaminated.
When the silica filter is contaminated, change it with
new one. Wash the filter holder.
The detector is contaminated. The detector is contaminated by incomplete

combustion. Flow O2 gas at 200ml/min to wash the
inside while the ozonizer is running. When it is not
resolved, contact our local distributors.
5-3
5-6. Measurement Time is Too Long
Clip for ball joint is not attached. Connect the clip firmly.
5-7. Unstable Measurement Values
Oxygen pressure is improper. Set gas pressure as follows.
Adjust the secondary pressure of cylinder or the stop
valve to 200 to 400 kPa with the reducing valve.
Temperature setting of the electric Set proper temperatures.
furnace is improper?
Gas is leaking from pyrolysis tube Check gas leakage. Refer to ‘Gas Leak Check’ of
connection part. the operation manual for details.
Pyrolysis tube is contaminated. Clean the contaminated pyrolysis tube:
• Brush the pyrolysis tube with detergent.
• Soak-wash in a washing solution.
In either case, wash the pyrolysis tube with
pure water and dry before use.
Quartz wool in the pyrolysis tube Change the quartz wool in the pyrolysis tube.
is deteriorated. Refer to ‘Filling of Quartz Wool’ of the operation
manual for details.
Clip for ball joint is removed. Connect the clip firmly.
5-8. Measurement Does Not End
Measurement time is long with When it is difficult to detect the end point with
“Auto” mode. “Auto” mode, select “Timer” mode.
Sample concentration is high. Change “PMT sensitivity” from “For Low
Concentration” to “For High Concentration”. When
“For High Concentration” is already selected, sample
concentration may be too high and the range may be
over. Reduce sample size or dilute before
remeasurement.
5-9. Troubles Occur after Changing of Gas Cylinder or Gas Line

Cylinder gas contamination or line contamination are suspected as trouble causes.
• Raise gas pressure slightly and purge lines.
• When troubles are not solved even by purging, change gas cylinder with a new one.
5-4
Section 6: Error Messages and Measures

This section describes error messages and measures displayed when troubles occur.
CAUTION
When “DANGER” or “WARNING” are displayed in the PC monitor, this
indicates risk of serious accidents. When these messages are displayed, deal with
the troubles immediately.
When errors occur, messages are displayed in the PC monitor.

Table 6-1. shows the error messages. In case countermeasures do not solve the problems, contact
local distributor.
Table 6-1. Error Messages
No. Error messages Countermeasures

23 Command reception error during the An improper command was received
system down during system down.
Restart the whole system. If the same
error occurs even after the restart,
contact local distributor.
25 Ozonizer hardware switch off error The ozonizer was turned ON from the
software while the ozonizer’s hardware
switch was OFF.
42 Parameter range error Received parameter values are abnormal.
43 Gain setting error Received parameter values are abnormal.
50 EEPROM input and output error The memory control error occurred
during memory input and output.
(WIP timeout)
Check the software versions of ND-210
and PC and contact local distributor.
51 EEPROM input and output error The data writing error occurred during
memory input and output.
(WEL timeout)
52 EEPROM input error The identification characters input from
the memory are not matching.
(Different identification characters)
6-1

53 EEPROM input error The check sum input from the memory
(Different check sum) is not matching.
54 EEPROM input error The parameter input from the memory is
(Parameter error) abnormal.
121 No telegraph An unclear command was received.
ND-210 software version may be old.
Check the versions of ND-210 software
and system program and contact local
distributor.
124 Control command reception error Parameter change or start command was
during sequence control received during sequence control.
distributor.
126 SRQ reception error during SRQ SRQ command was received before
response SRQ reply completion.
distributor.
143 No N signal strength data of elapsed The N signal strength data of the elapse
time requested by SRQ time requested by SRQ do not exist in
the ring buffer.
distributor.
144 The number of N signal strength data of The N signal strength data of the elapse
elapsed time requested by SRQ is time requested by SRQ are different
different from the number in the ring buffer.
distributor.
150 Mass flow controller connection error At initialization, the communication
with mass flow controller failed.
6-2

151 Mass flow controller parameter setting The parameter setting to mass flow
error controller failed.
152 Mass flow controller flow acquisition Failed to acquire flow data from mass
error flow controller.
Restart the whole system.
If the same error occurs even after the
restart, contact local distributor.
153 Mass flow controller flow control error During gas flow control, flow was more
than ±10% or ±30ml of the preset value
(whichever is larger) for 5 seconds.
Restart the whole system.
If the same error occurs even after the
restart, contact local distributor.
154 Cell heating temperature control error Cell heating temperature is over the
control range (0 to 50 degrees Celsius).
155 PMT cooling temperature control error PMT cooling temperature is over the
control range (0 to 50 degrees Celsius).
156 Ozonizer switch off error during Measurement was stopped by turning off
measurement the ozonizer switch during measurement.
Restart ND-210 or turn on the switch
again to restart measurement. If the
switch is turned off even after the
reconnection, contact local distributor.
158 PMT cooling peltier disconnection After 45 minutes from PMT cooling
error start, it is more than 15 degrees Celsius.
If the same error occurs even after
restarting ND-210, contact local
distributor.
159 PMT cooling temperature sensor After 45 minutes from PMT cooling
disconnection error start, it is less than 1 degrees Celsius.
If the same error occurs even after
restarting ND-210, contact local
distributor.
6-3
6-4

The maintenance and inspection to use ND-210 safely in the proper conditions are described in this
section.
Maintain and inspect the unit effectively using the maintenance information of NSX-2100 application
software.
7-1. Inspection
7-1-1. Daily Inspection
CAUTION
Always conduct daily inspection before measurement. Failure to check the unit can lead
to reduced performance of the units, and even to serious accidents.
Table 7-1. Daily Inspection Items
No. Items Contents

1 Gas leak check Check O2 gas leakage with the flow meter for gas
leak check.
2 Septum change Change the septum every day before measurement
start.
3 Contamination check of female Check that it is not contaminated with soot.
ball joint
4 Contamination check of the inner Check that it is not discolored.
tube of a tube dryer
5 Filter contamination check When using the unit with the horizontal furnace,
check that the filter is not contaminated.
The details of each inspection procedure are as follows.
Gas Leak Check
Check that supply gas (O2) does not leak as follows.
(1) Connect the ball joint of the ‘flow meter for gas leak check’ to the outlet of the pyrolysis tube.
(2) Check that the preset gas flow agrees with the indicated value of the flow meter.
Septum Change
When a septum is set to the injection port, change to a new one before measurement every day.
Refer to “7-2-1. Septum Change” for details.
7-1
Contamination Check of Female Ball Joint
Check female ball joint contamination as follows and wash the joint.
(1) Check for soot contamination caused by incomplete combustion.
(2) If it is contaminated, wash it. Refer to “7-2-2. Washing of Trap Tube and Female Ball Joint” for
details.
Contamination Check of the Inner Tube of the Gas Dehumidifier
Check the inner tube contamination as follows and wash the joint as follows.
(1) Check whether the inner tube is discolored. The color gradually changes from to translucence to
brown.
(2) If it is discolored, change with a new one. Refer to “7-2-5. Tube Dryer Change” for details.
* If the inner tube is discolored by incomplete combustion of a sample, it can not be used
anymore. Change with a new one.
Filter Contamination Check
When using the horizontal furnace, check filter contamination and change it if necessary. Refer to
“7-2-7. Silica Filter Change” for details.
(1) Disassemble the line with filter.
(2) Check that the filter is not contaminated.
(3) When it is contaminated, change it with a new one with tweezers.
7-2
7-1-2. Periodical Inspection
Table 7-2. shows the periodical inspection items.
CAUTION
Always conduct periodical inspection in the specified cycle. Failure to check the unit can
lead not only to reduced performance of the unit but also to serious accidents.
Table 7-2. Periodical Inspection Items
No. Items Contents Frequency

1 Check of pyrolysis tube Check for discoloration (whitening). Every 3 to 4
devitrification If the tube is devitrified, change the weeks
tube with a new one.
2 Quartz wool change Replace the quartz wool inside the Every 3 to 4
pyrolysis tube with fresh wool. weeks
3 Reactivation and change of When the recovery rate by standard Every 3 to 4
catalyst in pyrolysis tube sample is low, reactivate or change weeks
catalyst.
4 Washing of the female ball joint, Wash the female ball joint, the filter Every month
the filter holder, and the filter holder, and the filter connection tube
connection tube with washing solution.
5 Tube dryer check When the inner tube of the tube dryer Every month
is brown, change it with new one.
6 Washing of the trap tube at the Refer to “7-2-2. Washing of Trap Every month
bottom of the pyrolysis tube Tube and Female Ball Joint”.
7 Silica filter change When using the unit with the After
horizontal furnace, change the silica incomplete
filter with new one. combustion
or every
month
8 Ozone scrubber change Change ozone scrubber with a new Every 800
one. hours or 6
months
9 Check of gas flow indication Check that the O2 flow indication of Every year
PC agrees with the flow meter.
If they do not agree, contact local
distributor.
Table 7-3. Check Items at Periodical Inspection
Items Maintenance items
Visual check of unit Check the following points.
· Contamination and dust
· Proper fixation of parts
· Proper connection of tubes and connectors
7-3
Insulation test Measure the insulation between the power terminal
and the ground terminal of the chassis.
It should be 2MΩ or more.
Operation Run regular measurement.
inspection
Inspect the above items to measure in normal conditions.
When troubles are found, repair them and inspect them again.
When troubles are unclear or found in the unit inside, contact local distributor.
The details of inspection procedure are as follows.
Check of Pyrolysis Tube Devitrification
CAUTION
Pyrolysis tube devitrification reduces mechanical strength of the tube and has a high risk
of breakage. White discoloration of a pyrolysis tube is devitrification.
When fine cracks are seen in the devitrified area, mechanical strength is low.
Change the tube immediately.
Inspect pyrolysis tube devitrification by the following procedure.
Inspection frequency: Every 3 to 4 weeks or after measurement of samples containing much salt such
as sea water
· Pyrolysis tube inspection and change
(1) Judge mechanical strength of a pyrolysis tube by visually checking the devitrified part.
* When fine cracks are seen in the white devitrified part, mechanical strength is low.
(2) When the pyrolysis tube is devitrified and mechanical strength is low, change the pyrolysis tube
immediately.
Change of Quartz Wool in Pyrolysis Tube
Inoxidizable salts and metals in samples are accumulated on the quartz wool in the pyrolysis tube.
Inspection frequency: Every 3 to 4 weeks or after measurement of samples containing much

salts and/or metals
When the quartz wool is harder or powdery, change it immediately.
Refer to the operation manual for details.
Reactivation and Change of Catalyst in Pyrolysis Tube
When the recovery rate by standard sample is low, reactivate catalyst or change with fresh catalyst.
For the reactivation, refer to “7-2-3. Reactivation of Catalyst in Pyrolysis Tube”.
For the change, refer to “7-2-4. Change of Catalyst in Pyrolysis Tube”.
Inspection frequency: Every 3 to 4 week, or when baseline is unstable
7-4
Washing of Female Ball Joint
Wash female ball joint every month or when it is contaminated.

Refer to “7-2-2. Washing of Trap Tube and Female Ball Joint” for details.
Washing of Trap Tube of The Pyrolysis Tube
When dehumidified water has accumulated in the trap tube, dispose and wash the inside.
Refer to “7-2-2. Washing of Trap Tube and Female Ball Joint” for details.
Silica Filter Change
Exchange the filter at the pyrolysis tube outlet every month or when contamination is seen. Refer to
“7-2-7. Silica Filter Change” for details.
Change of Ozone Scrubber
After about 800 hours or 6 months from the start of usage, change the ozone scrubber (a cartridge for
ozone treatment). Refer to “3-7. Ozone Scrubber Setting”.
By the maintenance information of NSX-2100 application software, elapsed time is counted and notice
is indicated. When the notice of ozone scrubber change is indicated, change it and click “Help”,
“Maintenance Note”, and “Settings” of the menu. Click [Clear] button of “Elapsed time of ozone
scrubber” of “ND-210” tab.
7-1-3. Performance Inspection
Inspect the performance by referring to “Results” of the operation manual.
Table 7-4. Performance Inspection Item

No. Items Frequency
1 System check Every week
7-5
7-2. Maintenance
7-2-1. Septum Change
It is recommended to change the septum to a new one before measurement every day.
7-2-2. Washing of Trap Tube and Female Ball Joint
Remove the trap tube of the pyrolysis tube bottom or the female ball joint every 1 to 2 weeks to check
for water accumulation. When it is contaminated by incomplete combustion of samples, wash it.
(1) Wipe the contamination of female ball joint with absorbent cotton soaked in toluene.
(2) Mix acetone with distilled water in the proportion of one to ten to prepare washing solution.
(3) Immerse the joint in the washing solution.
(4) Rinse with distilled water and dry.
7-2-3. Reactivation of Catalyst in Pyrolysis Tube
When the baseline is unstable in the graph of ND-210 monitor window of NSX-2100 application
program, first change the quartz wool. When it is unstable even after the change, reactivate catalyst as
follows.
(1) Transfer catalyst from pyrolysis tube into another container.

(2) Wash the catalyst with distilled water several times. Be careful not to break down the grains.
(3) Drain off and completely dry the washed catalyst.
(4) Fill quartz wool and reactivated catalyst into the pyrolysis tube by referring to “Filling of Quartz
Wool” in the Operation Manual. Set the tube by referring to “Assembly and Setting of Pyrolysis
Tube” in the Operation Manual.
(5) Prebake the tube for 3 to 4 hours at the same furnace temperature and gas flow as at measurement.
7-2-4. Change of Catalyst in Pyrolysis Tube
When the performance does not recover even after reactivating the catalyst according to “7-2-3.
Recovery of Catalyst in Pyrolysis Tube”, change and oxidize catalyst as follows.
(1) Fill quartz wool and new catalyst into pyrolysis tube by referring to “Filling of Quartz Wool” in the
Operation Manual.
(2) Set the pyrolysis tube by referring to “Assembly and Setting of Pyrolysis Tube” in the Operation
Manual.
At this time, do not set a trap tube or a female ball joint at the bottom of the pyrolysis tube.
(3) Set the temperature of both furnaces to 800 degrees Celsius in the electric furnace parameter
window.
7-6
(4) Set O2 gas to “300ml/min” in the electric furnace parameter window.

For the manual gas unit, adjust it manually.
(5) Combust catalyst in (3) and (4) conditions for about 5 hours and oxidize.
CAUTION
Before catalyst oxidation treatment, always remove trap tube or female ball joint.
During catalyst oxidation treatment, acid gas is sometimes generated from catalyst.
7-2-5. Tube Dryer Change
Change the tube dryer as follows.

(1) Remove female ball joint.
(2) Remove the DRY gas line connected to the tube dryer.
(3) Remove the PTFE tubes connected to the dryer inlet and outlet to remove the tube dryer.
(4) Set a new tube dryer.
(5) Reset the gas lines.
7-2-6. Fuse Change
Change a fuse as follows.
(1) Turn the cap of the unit rear fuse holder (FUSE) counter clockwise with a flathead screwdriver.
(2) Remove the fuse from the fuse holder and set new one.
(3) Turn the cap clockwise to fix it.
7-7
7-2-7. Silica Filter Change
When changing the filter, refer to the following figure to disassemble the line with the filter, change the
filter, and assemble it again.
CAUTION
When handling a silica filter or other filters, use tweezers.
(1) Remove the line with filter from HF-210 left side and disassemble it.
(2) Change the silica filter with tweezers.
(3) Refer to “Fig. 7-1. Filter Assembly” to assemble the line with the filter again.
Concave Set the surface with 4

holes to the holder side.
Silica filter
Fit them.
Fit O-ring to the groove.
Convex
Fig. 7-1. Filter Assembly
7-8
7-3. Storage of the Unit

Storing of ND-210 when it will not be used for a long time is as follows.
The cautions for storing ND-210 on a table are as follows.

· Remove power cable and deodorization kit line.
· Disconnect the connection cable between ND-210 and electric furnace (HF-210 or VF-210).
· Remove detector from electric furnace (HF-210 or VF-210).
· Remove lines from the gas purification filter (Moisture Trap C) and plug both ends.
· Cover tube ends with films to prevent contamination.
· Put a cover over the whole unit.
If the ND-210 is to be stored in another place, store in places with the following conditions.
· Room temperature is 45 degrees Celsius or less.
· No direct sunlight
· No strong vibration and continuous weak vibration
· No strong electromagnetic field
· Humidity is under 80%.
· No corrosive gas
· Fire must not be used.
· Free from much dust
· Flat places
7-9
7-10
Section 8: Specifications
8-1. Standard Specifications
Model Model ND-210

Analysis methods Oxidation decomposition
Chemiluminescence method (reduced pressure method *1)
Samples Nonaqueous samples: Nitrogen compounds in petroleum and
petrochemicals *2
Aqueous samples: Nitrogen compounds in liquids except nonaqueous
samples *2 *5
Catalyst Oxidation catalyst (Platinum)
Measurement range Nonaqueous samples: Refer to “Table 8-1. Measurement Range of
Nonaqueous Samples”. *3
Aqueous samples: Refer to “Table 8-2. Measurement Range of
Aqueous Samples”. *3
Two-step change (Low concentration and high concentration ranges)
Sample volume Horizontal furnace: Solid 1 to 30mg, Liquid 1 to 50μl,
Gas 5 to 25ml *4
Vertical furnace: Nonaqueous samples; Liquid 200μl or less,
Gas 5 to 25ml *4
Aqueous samples; Liquid 100μl or less
Measurement time Within 4 minutes/measurement
(When nitrogen absolute volume is 2μg, measurement time depends
on the absolute amount.)
Gas Oxygen gas: Purity 99.8% or more, 300±100kPa
Dimension 220 (W) × 375 (D) × 500 (H) mm
Weight 22kg
Temperature and 15 to 35 degrees Celsius, 80%RH or less (No condensation)
humidity
Power AC 100/115/230/240V, 50/60Hz, 300VA
*1. Our recommended vacuum pumps are required for analysis.
*2. As nitrogen (N2) or diazo compound are not converted into nitrogen oxide at combustion, they
can not be measured.
*3. Usual samples: Samples which are combustible under 1100 degrees Celsius and have no
interference.
*4. For gas sample measurement, use an optional gas injector. For GI-210, sample volume is 1 to
10ml.
*5. Only the vertical furnace is applicable for aqueous sample measurement.
8-1
Table 8-1. Measurement Range of Nonaqueous Samples
VF-210 HF-210
Measurement
Liquid Gas Solid Liquid Gas
sensitivity
Low 4 to 2000ng 4 to 2000ng 20 to 2000ng 20 to 2000ng
concentration 0.05 to 20μg/ml 0.4 to 200mg/m3 0.5to 50μg/g 0.5 to 50μg/ml
range (90μl) (10ml) (40mg) (40μl)
High 10 to 50000ng 10 to 50000ng 10 to 50000ng 10 to 50000ng
concentration 1 to 5000μg/ml 0.1 to 5000mg/m 3
1 to 5000μg/g 1 to 5000μg/ml
range (10μl) (10ml) (10mg) (10μl)
Table 8-2. Measurement Range of Aqueous Samples
VF-210
Measurement Liquid
sensitivity
Low 1 to 2000ng
concentration
range 0.01 to 20μg/ml (90μl)
High 10 to 50000ng
concentration
range 1 to 5000 μg/ml (10μl)
8-2. ND-210 Repeatability

Repeatability is as follows. Measure with a gas cylinder of specified purity. Set gas purification
filters (Parts number: TS6GPR) to new gas lines.
* At nonaqueous samples, always connect the optional unit for injecting sample gradually at a
constant rate.
* For the unit inspection of the system including the detector, mechanical repeatability is checked
by Liquid Sample Injector ASC-250L.
8-2
Repeatability Using VF-210
(1) Table 8-3 shows the repeatability of aqueous samples (standard sample: ammonium sulfate
solution) using ASC-250L.
Table 8-3. Aqueous Sample Repeatability Using ASC-250L
Concentration (μg/ml) Injection Volume (μl) RSD (%) n=5

0.1 90 ≦8%
0.5 90 ≦8%
1 40 ≦3%
50 25 ≦3%
100 25 ≦3%
(2) Table 8-4 shows the repeatability of nonaqueous samples (standard sample: pyridine /toluene
solution) using ASC-250L.
Table 8-4. Nonaqueous Sample Repeatability Using ASC-250L
Concentration (μg/ml) Injection Volume (μl) RSD (%) n=5

0.1 90 ≦8%
0.5 90 ≦8%
1 40 ≦3%
50 20 ≦3%
100 20 ≦3%
(3) Table 8-5 shows the repeatability (standard sample: pyridine /hexane solution) using GI-210 and
GI-220. For GI-210 and GI-220, standard sample injection volume is 10μl or less and the
repeatability is different from other optional units. For sample injection volume, GI-210 is 10ml
and GI-220 is 25ml. They are different from the following repeatability.
Table 8-5. Repeatability Using GI-210 and GI-220
Concentration (ppm) Sample volume (μl) RSD (%) n=5

0.5 ≦8%
1 ≦8%
10
5 ≦3%
50 ≦3%
* When using GI-210 or GI-220, the repeatability at sampling strongly affects measurement
repeatability.
8-3
Repeatability Using HF-210
(1) Table 8-6 shows the repeatability (standard sample: pyridine/toluene solution) using HF-210
and a sample injector.
Table 8-6. Nonaqueous Sample Repeatability Using HF-210 and Sample Injector
Concentration (μg/ml) Sample volume (μl) RSD (%) n=5

0.5 40 ≦10%
1 40 ≦5%
50 20 ≦3%
100 20 ≦3%
* The repeatability at sampling strongly affects measurement repeatability.
8-4
9-1. ND-210
Table 9-1. ND-210 Consumables List
No. Parts names Parts numbers Quantity

1 Ozone scrubber TN6RPZ 1 pc
(with large and small hose bands)
2 O-ring (P-22) TNP22 5 pcs/set
3 Aqueous ammonium sulfate (N-100ppm) 100ml TN122 1 pc
4 Quartz wool 10g TNQWL 1 bag
5 Disk filter (25JP050AN) DT2NFS 2 pcs/set
6 Gastight microsyringe 25μl (SGE) MSSGG2 1 pc
9 Gastight microsyringe 250μl (SGE) MSSGGQ 1 pc
Fuse 3.15A FU31MS 2 pcs/set
* Possible syringe volume is different depending on sample type.
• NSX-2100V, NSX-2100H (Aqueous samples): 25, 50, 100μl

• NSX-2100V (Nonaqueous samples): 25, 50, 100, 250μl
9-2. Consumables for Vertical Furnace
9-2-1. ND-210 / SD-210 Gas Dryer for Vertical Furnace
Table 9-2. ND-210 / SD-210 Gas Dryer Consumables List

1 Tube dryer TN6RPC 1 pc
2 Clip (long) for ball joint φ18 DT1BJC 1 pc
3 φ 6/4 Elbow connector (30-6RUE4-C) NJ64UEC 1 pc
4 φ 6/4 One-touch connector socket elbow 6-4 NJP64SE 2 pcs/set
5 PTFE tube φ4/2 10m TX3RPP 1 pc
9-1
9-2-2. Pyrolysis Tube Set for ND-210 with Vertical Furnace (oil sample)
Table 9-3. Consumables List of Pyrolysis Tube Set for ND-210 with Vertical Furnace
(oil sample)
No. Parts names Parts Quantity
numbers
1 Outer pyrolysis tube φ30 L375 branch tube ball joint FN2QPG 1 pc
2 Inner pyrolysis tube φ22 L227 TS8QPN 1 pc
3 Inner pyrolysis tube for heavy oil FN2IQH 1 pc
4 Spring for pyrolysis tube SX1QSP 4 pcs
5 Female ball joint TN5LJT 1 pc
6 Oxidation catalyst 30g (platinum) TN5CAT 1 pc
7 φ6 Connector (30-6U-S) TS8J66 1 pc
9-2-3. Pyrolysis Tube Set for ND-210 with Vertical Furnace (aqueous sample)
Table 9-4. Consumables List of Pyrolysis Tube Set for ND-210 with Vertical Furnace
(aqueous sample)
numbers
1 Outer pyrolysis tube φ30 L375 branch tube ball joint FN2QPG 1 pc
2 Pyrolysis tube adapter φ29 L35 FN2QPA 1 pc
4 Trap tube of the pyrolysis tube bottom N2NVTR 1 pc
5 φ6 Connector (30-6UE-S) NJ6UES 1 pc
6 Oxidation catalyst 30g (platinum) TN5CAT 1 bag
9-2-4. Injection Port Set for ND-210 Manual
Table 9-5. Consumables List for Injection Port Set for ND-210 Manual

numbers
1 Septum (flat-type) TN5SIS 100 pcs/set
9-2
9-3. Consumables for Horizontal Furnace
9-3-1. ND-210 / SD-210 Gas Dryer for Horizontal Furnace
Table 9-6. ND-210 / SD-210 Gas Dryer Consumables List

1 Tube dryer TN6RPC 1 pc
2 Clip (long) for ball joint φ18 DT1BJC 1 pc
3 φ6/4 Elbow connector (30-6RUE4-C) NJ64UEC 1 pc
4 φ6/4 One-touch connector socket elbow 6-4 NJP64SE 2 pcs/set
5 PTFE tube φ4/2 10m TX3RPP 1 pc
6 Silica filter (QR-100) TS6SIF 100 sheets/bag
9-3-2. Pyrolysis Tube Set for ND-210 with Horizontal Furnace (NSX-2100H)
Table 9-7. Consumables List of Pyrolysis Tube Set for ND-210 with Horizontal Furnace
(NSX-2100H)
numbers
1 Outer pyrolysis tube φ30 L410 FN1QPG 1 pc
2 Inner pyrolysis tube TX3QPN 1 pc
4 Oxidation catalyst 30g (Platinum) TN5CAT 1 pc
5 Female ball joint TN5LJT 1 pc
6 φ6/4 elbow connector (30-6RUE4-S) GA164E 1 pc
7 Ring of the electric furnace outlet AQ3RIS 1 pc
9-4. Maintenance Parts
Table 9-8. List of Maintenance Parts

1 Flow meter for gas leakage check (500ml/min) TX3RPF 1 pc
2 Flow meter for gas leakage check (1L/min) TX3FFF 1 pc
3 Quartz wool poker TX2RTL 1 pc
9-3
9-5. Parts Pictures
Table 9-9. ND-210 Parts Pictures

No. Parts names Pictures
1 TN6RPZ
Ozone scrubber
(with large and small hose
bands)
2 TNP22
O-ring (P-22)
3 TN122
Aqueous ammonium sulfate
(N-100ppm) 100ml
4 TNQWL
Quartz wool 10g
5 DT2NFS
Disk filter (25JP050AN)
6 MSSGG2
Gastight microsyringe 25μl
(SGE)
7 MSSGG5
(SGE)
8 MSSGG1
(SGE)
9 MSSGGQ
(SGE)
9-4

10 FU31MS
Fuse 3.15A
11 TN6RPC
Tube dryer
12 DT1BJC
Clip (long) φ18 for ball joint
13 NJ64UEC
φ6/4 Elbow connector
(30-6RUE4-C)
14 NJP64SE
φ6/4 One-touch connector
socket elbow 6-4
15 TX3RPP
PTFE tube φ4/2 10m
16 TN5SIS
Septum (flat-type)
9-5

17 FN2QPG
Outer pyrolysis tube φ30 L375
branch tube ball joint
18 TS8QPN
Inner pyrolysis tube φ22 L227
19 FN2IQH
Inner pyrolysis tube
for heavy oil
20
FN2QPA
Pyrolysis tube adapter φ29 L35
21 SX1QSP
Spring for pyrolysis tube
22 TN5LJT
Female ball joint
23 TS8J66
φ6 Connector (30-6U-S)
24 N2NVTR
Trap tube of the pyrolysis tube
bottom
25 NJ6UES
φ6 Connector (30-6UE-S)
26
TN5CAT
Oxidation catalyst 30g
(platinum)
9-6

27
TN5QP
Pyrolysis tube φ29 L415
28
TNP29
O-ring (P-29)
29
FN1QPG
Outer pyrolysis tube φ30 L410
30 TX3QPN
Inner pyrolysis tube
31
AQ3RIS
Ring of the electric furnace
outlet
32
TS6SIF
Silica filter (QR-100)
33 TX3RPF
Flow meter for gas leakage
check (500ml/min)
34 TX3FFF
Flow meter for gas leakage
check (1L/min)
35 TX2RTL
Quartz wool poker
9-7
9-8

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MITSUBISHI CHEMICAL ANALYTECH

Thank you for buying our nitrogen detector Model ND-210.

Before the Use

(1) Do not reprint this manual wholly or partially without permission.

(2) The contents may be changed without notice.

Caution labels Attached places

When installing the unit, observe the following precautions.

Maintenance and Inspection

Section 1: Names and Functions of ND-210 Units

1-1. ND-210 Unit Names and Functions

Fig. 1-1. ND-210 Front

Table 1-1. ND-210 Unit Front Names and Functions

No. Names Indications Functions

1-2. ND-210 Inside Names and Functions

Fig. 1-2. ND-210 Inside

Table 1-2. ND-210 Unit Inside Names and Functions

No. Names Indications Functions

Fig. 1-3. ND-210 Rear

Table 1-3. ND-210 Rear Names and Functions

No. Names Indications Functions

Section 2: Parts Check

2-1. Parts for ND-210

Table 2-1. ND-210 Parts List

Parts names Quantity Check Remarks

2-2. Parts for Vertical Furnace

Parts names Quantity Check Remarks

Table 2-4. Parts List of Pyrolysis Tube Set (aqueous sample)

2-2-4. Injection Port Set for ND-210 Manual

No. Parts names Quantity Check column

* Syringes for manual injection are required separately.

2-3. Parts for Horizontal Furnace

3-1. Installation Conditions

• Room temperature is 15 to 35 degrees Celsius. Temperature change is small.

3-2. Installation Space

3-3. Power Preparation

ND-210 consumption power is 300VA.

ND-210 power cable is 3-line type including a grounding line.

3-4. Supply Gas Line

3-4-1. Line Preparation

3-4-2. Line Connection

Fig. 3-1. ND-210 System Line Connection

3-5. Preparation of ND-210 for Vertical Furnace

To remove moisture in sample gas, set a tube-type dehumidifier (tube dryer).

(4) Connect a PTFE tube φ6/4 3cm to the dryer tip.

(5) Set one of the following connectors to (4).

(1) Put out about (4) Connect a PTFE tube φ6/4

Fig. 3-2 Lines (1) of the Tube Dryer

(10) Connect the tube

(8) Set a one-touch

Fig. 3-3 Lines (2) of The Tube Dryer

3-5-2. Buffer Tank Setting (Vertical Furnace)

(1) Set a buffer tank to ND-210 rear with screws.

(3) Set φ6/4 PTFE tube 3cm to tube

(1) Fix buffer tank

(4) Connect φ4/2 PTFE tube 45cm

Fig. 3-4. Connection of Buffer Tank Lines of ND-210 Rear

To remove moisture in sample gas, set a tube-type dehumidifier (tube dryer).

(2) Set the filter to the female ball joint.

(1) Connect the two points of a φ6/4PTFE tube

(3) Set filter to tube dryer.

(2) Set filter to female ball joint.

(5) Set the female ball