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Materials Today: Proceedings xxx (xxxx) xxx

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Materials Today: Proceedings


journal homepage: www.elsevier.com/locate/matpr

Review of the effects of low-velocity impact events on advanced


fiber-reinforced polymer composite structures
Megavannan Mani a,⇑, M. Thiyagu a, Pradeep Kumar Krishnan b
a
Institute of Mechanical Engineering, Saveetha School of Engineering, Saveetha Institute of Medical and Technical Sciences, Saveetha University, Chennai, Tamilnadu 602105, India
b
Department of Mechanical and Industrial Engineering, College of Engineering, National University of Science and Technology, P.O Box 2322, CPO Seeb 111, Al Hail, Oman

a r t i c l e i n f o a b s t r a c t

Article history: Most typical polymer composite materials have the weakest impact characteristics observed in Low-
Available online xxxx Velocity Impact (LVI) events. As a result, typical polymer composite materials are reinforced to improve
their proper application attributes. The Fiber-Reinforced Polymer Composite (FRPC) materials must be
Keywords: converted to enhanced polymer composite structures, such as incorporating nanoparticles and selecting
Low-Velocity Impact appropriate lamination techniques to improve the composite structure impact strength of the polymer
Polymer composite materials. The matrix layer was created using a variety of lamination processes. The hybridization tech-
Nanoparticles
niques with the inclusion of filler material into polymer composite structures were used to produce bet-
Mechanical Characteristics
Functionalization
ter results in impact kinetics for the composite structures. The quasi-static mechanical sequence
approach was used to improve the LVI properties of FRPC. The inclusion of nano-filler particles in polymer
composites to reduce obvious low-velocity impact damage during low-velocity accidents or events is the
subject of this review. This investigation aims to explore if conventional fiber materials with obvious low-
velocity impact damage might be enhanced to overcome the effects of advanced FRPCs.
Copyright Ó 2023 Elsevier Ltd. All rights reserved.
Selection and peer-review under responsibility of the scientific committee of the International Confer-
ence on Advancements in Materials and Manufacturing.

1. Introduction tures [2]. Several publications state that [3,4], carbon/kevlar/basa


lt/glass/epoxy hybrid polymer composites have the highest load-
Fiber Reinforced Polymer Composite (FRPC) materials are gen- bearing capability, and kevlar/epoxy composites have the highest
erally available in numerous industries because of their greater glass transition and viscoelastic properties when compared to
strength, flexibility, greater corrosion resistance, and low density. other hybrid polymer composites. The polymer composite lamina-
The laminations of composite layers are made up of a stacking tion layer resin-rich area of the composite structure was enhanced
sequence approach and a quasi-static approach. Both techniques by the addition of a nano filler with suitable epoxy, and enhanced
are important for laminating the reinforced composites to optimize polymer composite materials prevent the propagation of voids due
the properties of advanced polymer composites (polymer-based to their high lamination bonding properties [5,6].
fiber/epoxy) to protect against low-velocity impact accidents dur- The effects of lamination bonding properties depend upon the
ing low-velocity impact events. In advanced polymer composite different epoxy with the additional amount of nanoparticles, and
laminates (fiber/epoxy-based) different lamination layers were if the burden is suddenly used to enhance the lamination structure,
formed based on their required applications in a laminate of the the structure exposes the high strain rate between the lamination
polymer. The lamination structure, the intermediate layer, of layers of polymer composite structures [7], with the highest
improves the impact absorption strength, shear strength, flexural stiffness property and strain energy rate in the laminate layers
strength and punch shear strength [1]. occurring when the ply angles change between the lamination lay-
In general, conventional polymer composite lamination tech- ers. In fiber-metal polymer composites, the fiber is placed between
niques are not sufficient to maintain the viscoelastic properties the intermediate layer and the target layer to get higher energy
at low-velocity events. In such a case, hybrid lamination methods absorption owing to the LVI crisis [8,9], as well as the plateau
are employed to enhance the qualities of polymer composite struc- direction of the lamination layers of polymer composites, which
exhibits the stiffness rate concerning direction pitch angle. It
causes problems near the edge, and the edge lamination layer is
⇑ Corresponding author. not easily affected compared to conventional composite materials
E-mail address: megavannanm4011.sse@saveetha.com (M. Mani). [10,11]. Based on the various process methodologies involved in

https://doi.org/10.1016/j.matpr.2023.04.255
2214-7853/Copyright Ó 2023 Elsevier Ltd. All rights reserved.
Selection and peer-review under responsibility of the scientific committee of the International Conference on Advancements in Materials and Manufacturing.

Please cite this article as: M. Mani, M. Thiyagu and P. Kumar Krishnan, Review of the effects of low-velocity impact events on advanced fiber-reinforced
polymer composite structures, Materials Today: Proceedings, https://doi.org/10.1016/j.matpr.2023.04.255
M. Mani, M. Thiyagu and P. Kumar Krishnan Materials Today: Proceedings xxx (xxxx) xxx

Table 1
Table 1 Lists the materials employed, the amount of energy used, and the impact [23].

S. References Composite Materials Energy Level Indender


No
1. (Wang et al., 2018) Carbon Polyphenylene 5, 15, 25, & 35 J Hemispherical
12.7 mm dia
2. (Ravandi et al., 2017) Flax/epoxy stitched composites 19.6 J – non perforation 44.6 J – full Hemispherical
perforation 12.7 mm dia
3. (Dogan and Glass/epoxy Glass/polypropylenePVCfoamsandwich 25, 50, 75, 100, & 125 J Hemispherical
Arikan, 2017) composites 12.7 mm dia
4. (Hung et al., 2018 Glass/carbon hybrid epoxy composite with different stacking 6, 8, & 10 J Hemispherical
sequence 16 mm dia
5. (Dhakal et al., 2018) lax unsaturated polyester composites 25, 27, & 29 J Hemispherical
19.8 mm dia
6. (Bandaru et al., 2017) Kevlar/basalt hybrid polypropylene composites 25, 50, & 75 J Hemispherical
12.7 mm dia
7. (Razali et al., 2014) Types of glass fiber epoxy composites 14, 28, 42, & 56 J Hemispherical
10 mm dia
8. (Dehkordi et al., Basalt/Nylon Woven Fabric Composites 15, 30, & 45 J Hemispherical
2010) 12.7 mm dia
9. (Sfarra et al., 2013) Basalt fiber composites Glass fiber composites 7.5, 15, & 22.5 J Hemispherical
12.7 mm dia
10. (Soliman et al., 2012) Carbon epoxy MWCNT composites 15, 24, 30, 60, & 120 J Hemispherical
12.7 mm dia

advanced composites and on their desired applications, to with- ticles and resin-based composite structures’ integral compounds
stand the physical properties of polymer composites to decrease [15].
penetration dominant damage and buckling damage [12], which Consider that the effect of the energy absorption capacity of
are reduced during LVI impact events, by selecting the correct advanced composite materials is high at room temperature com-
polymer material with epoxy, the contribution of toughness char- pared to 600 °C, where the maximum temperature transition is
acteristics is enhanced in low-velocity damaged particles to influenced by the impact strength. The impact characteristic
improve the impact resistance factors of their internal properties reaches a temperature scale of (-200 °C to 600 °C), and hybrid lam-
of toughness in polymer composite materials [13]. ination structures offer a higher rigidity attribute when compared
The various types of stacking methods are used to develop the to other lamination structures [16,17]. The different stacking
polymer composite structure. The following Fig. 1 (a, b, c, & d) sequence methods are also employed to improve the fiber lamina-
shows the stacking technique and direction of fiber orientation. tion structure; carbon fiber lamination material is more efficient
When a sudden impact occurs on a polymer composite structure, than flax fiber lamination material by enriching the low velocity
matrix failure and fiber lamination breakdown occur [14]. Ther- affected zone; thermoset, and thermoplastic-based laminated
moplastic lamination resin particles can be used in advanced PVC core substances are used in sandwich laminates in the hybrid
polymer composites to improve properties such as high molecular composite technique. The thermoplastic lamination structure has a
mass, outstanding impact strength, and excellent energy dissipa- lower bending thickness than the thermoset lamination structure
tion between the lamination layers with the insertion of nanopar- in the sandwich laminate composite [18].

Fig. 1. Different types of Polymer fabrics with integral compounds. (a) Represents the plain woven fabrics only, (b) Represents the plain woven fabrics with hybrid core
materials, (c) Represents the plain woven fabrics with different hybrid materials, (d) Represents the pure woven fabrics (Non hybrid) [14].

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M. Mani, M. Thiyagu and P. Kumar Krishnan Materials Today: Proceedings xxx (xxxx) xxx

The sandwich thermoset composite structure has a higher den- rigidity [24]. Carbon fiber composites made from recycled materi-
sity and greater rigidity and stability in low-velocity impact als were also compared to processed-recycled reused carbon fiber
response than the thermoplastic sandwich structure, but its defor- composites and pure carbon fiber composites. During impact, vir-
mation properties are inferior [19]. These responses are compli- gin carbon fiber composites demonstrated improved damage pre-
cated in dynamic conditions. The cross-ply orientation vention, better residual strength, and a lower failure angle of
lamination phenomenon technique aids in the improvement of shear. An ultrasonic C scan, photography, and SEM were once uti-
mechanical, delamination, and matrix expansion properties under lized to analyze the damaged material. The orientation of the fibers
repeated low-velocity impact events [20]. Because of these bene- is chosen to optimize the composite characteristics [25].(See
fits, sandwich FRPCs are also used in combination with polymer Figs. 3-9).
composite structures, and Kevlar fiber reinforced polymer struc- The fiber orientation influences the parameters of polymer
tures are more efficient when combined with other polymer struc- composites, as well as basalt-fiber polyester composites with three
tures. Thermoplastic polymer reinforced structures with inter and distinct fiber orientations were created, and among them, three 0°
intralaminar properties outperform thermoset polymers [21,22]. laminated composites outperformed the laminates, both plain-
woven and laminates with cross-ply in terms of LVI. Investigators
have concentrated on fiber metal laminates as a substitute for
2. Low-velocity impacts
improving their properties [26], and the effects of fiber metal lam-
inate composites using glass fiber made by the manual laminate
During low-velocity impact testing, three sorts of reactions are
method with different layer thicknesses and various orientations
common: penetration, intrusion, and rebounding phenomena [23].
were examined in the polymer composites. Based on the results
The impact’s energy is insufficient to damage the sample, causing
of fiber orientation, 90 orientation layers are very efficient. The
the impact to bounce and hit or, on the other hand, cause some
results of interlaced glass fiber composites plus reinforcements
impact energy to be transferred to the specimen, causing it to be
made with different fraction volumes using VBT revealed It was
damaged. The strike in this situation distributes all of its energy
found that a fraction volume of 43–44 percent provided higher
to the sample. The energy of the impact is sufficient to penetrate
impact resistance than that investigated by Sharma et al. [27].
entirely through the specimen in the perforation phenomena,
The combination of polymer structures with varied mass pro-
and some energy is squandered owing to friction between the
portions on the LVI characteristics of the resulting polymer struc-
specimen and the impact, which symbolizes the many types of fail-
ture was investigated. The combination of polymer composites
ure that occurred during the LVI.
with 25% kenaf fiber and 25% glass fiber has the maximum tensile
strength, and these polymer materials are assessed in LVI impact
3. Low-velocity impacts on FRPCs structures reactions. The glass-kenaf fiber combination was evaluated at var-
ious energy levels, including 10 J, 20 J, 30 J, and 40 J. Based on the
In light of the fact that reinforcement only offers load-carrying combination of various polymer architectures, the impact energy
processes, the use of composites has a significant advantage for of 40 J was shown to have the maximum energy absorption capa-
identifying failures in composites. Carbon fiber is one of the bility [28].
high-strength fibers used in ballistic applications. The low-
velocity impacts of basalt and glass fiber polymer composites
are contrasted, as well as composites made by a layering pro- 4. Effects of nano particles in FRPCs on LVI
cess as shown in Fig. 2. Basalt and carbon fiber reinforced polymer
composites outperform LVI performance due to their increased Due to their lightweight, rigidity, and toughness, nanoparticles
play a significant role in advanced FRPC, as high fracture toughness
enhances the composite by adding the appropriate percentage of
nanoparticles to reinforce the application structures during LVI,
and the use of nanofillers is based on morphological, micro struc-
tural, and mechanical properties.
These nanoparticles are available in organic and inorganic nat-
ure, such as nanoparticles, nano clay, and nano emulsions. The use
of different micro particles as reinforcing materials in polymers
increases their properties. The nanoparticles were added to the
composite material in various percentages, and the polymer matrix
hybrid composites, jute, carbon, kevlar, and others were mixed in
the sheet shape into several layers, as necessary to manufacture
hybrid polymer matrix composites. Reinforced hybrid polymer
matrix composites can be made via hand lay-up, compression
molding, spray lay-up, and other procedures [29]. The schematic
representation of making a nano-reinforced composite process is
shown in Fig. 3.
Abu-Okail et al. [30] investigated the effects of alumina nano
particle dispersion techniques used to improve material strength
and also discussed the high-frequency sonication technique used
to improve the qualities of the carbon with glass fiber and a com-
bination of FRPC lamination layers with the filler materials being
Aluminium Oxide (Al2O3) and Graphene Nano Platelet (GNP)
respectively, by adding 1.5% and 3% weight fractions. With except
for-glass fiber, carbon fiber, and hybrid, FRPs achieved exceptional
hardness and flexural strength to overcome low-velocity impact
Fig. 2. Experimental set-up for LVI impact test setup [27]. damage, and M. Hassani Niaki et al. [31] investigated the experi-
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M. Mani, M. Thiyagu and P. Kumar Krishnan Materials Today: Proceedings xxx (xxxx) xxx

Fig. 3. Steps involved in making a nano-reinforced composite [34].

Fig. 4. The schematic Environmental chamber setup for Low-velocity impact test
[38].
Fig. 5. Schematic diagram represents the C-scan results at various temperature
regions [38].

mental behavior made with basalt fibers with nano clay reinforced
structures, Basalt Fiber-Reinforced Polymer (BFRP), with epoxy
resin is used to reinforce clay particles, and poly amine is used to carbon fiber with GO laminates, better values of 10.10 and
harden them. 30.028 N of thrust force were discovered. Smaranika Nayaka
The result of this fiber composite is a structure that improves et al. [33] examined the comparison of carbon fibers and found that
the characteristics of reinforced polymer materials during low- the stiffness of glass fiber reinforced polymer composites is not
velocity impact events, with astonishing findings of 10% improved particularly high, and to improve the stiffness properties of glass
compressive strength, 4.8 percent increased flexural strength, and fibers, nano clay is included in the epoxy matrix. To better under-
41.5 times greater tremendous impact strength and increased ther- stand the behavior of the hybrid composites, the weight percent-
mal stability. The process methodologies of the nano-particles pro- ages of nano clay were 1%, 3%, 5%, and 7%. It was discovered that
cedures were plotted. a 5% loading of nano clay is the best quantity for increasing all
Jogendra Kumara et al. [32] examined the delamination nano- attributes such as hardness, impact strength, flexural strength,
composite of carbon fiber composites to improve the machinability and specific wear rate. However, when the concentration of nan-
index and thrust force of advanced polymer composites by incor- oclays increased, all of the above-mentioned attributes worsened.
porating GO (Graphene Oxide) nanoparticles into the matrix form Hardness rose by 33.8% at 5% nano clay concentration, impact
of carbon fiber polymer composites to enrich the carbon fiber lam- strength by 74.8%, flexural strength by 37.6%, and modulus by
inates by increasing the percentage of GO (% wt). By annealing the 37.5% and 37.67%, respectively.

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M. Mani, M. Thiyagu and P. Kumar Krishnan Materials Today: Proceedings xxx (xxxx) xxx

Mourad et al. [34] studied the damage assessment of polymer


lamination layers with nanoparticles. Different types of nanoparti-
cles were investigated in this study, and nanofillers were dissemi-
nated in epoxy and a high-frequency ultrasonic process to
strengthen it with the help of the kevlar fabric. The 0.5 wt% carbon
nanotube laminated composite structure had the greatest energy
absorbing capacity, and the use of three distinct nanofillers
improved the damage resistance and energy absorption capabili-
ties of the kevlar/Epoxy structure, and the addition of a small num-
ber of nanoparticles to the Kevlar/epoxy composites successfully
increased the strain rates. Based on the results of the damage
assessment of these polymer composite structures to increase
the nano filler content, the composite output capability was
increased. As a result of these studies, we learn that adding
nanoparticles to polymer composite structures improves their
strength.

Fig. 6. Experimental test setup for sandwich composite materials. (a)- Represent 5. Effects of temperature in FRPCs structures on LVI
flat-wise tensile test & (b)- Represent shear tension test [40].
Aviation components are generally made of FRPCs and are sub-
jected to cyclic loads and exposed to variable temperatures over
their useful life. For that purpose, Kakur Naresh et al. [35] studied
the mechanical dynamic characteristics of plain epoxy resin with
the following lamination structures: (0°), (45°), and (90°) carbon/
epoxy composite panels were formed. Carbon fiber sheets with
an asymmetrical orientation of the polymer structure were inves-
tigated. In comparison to the composite laminates, the plain
epoxy samples have lower activation energies, glass transition
temperatures, and higher loss tangents. In comparison to other
laminate designs, CFRP laminates have high storage modulus val-
ues, while other laminates have lower activation energy values.
Khashaba et al. [36] investigated the woven CFRP epoxy com-
posite’s resistance to deterioration over various temperatures,
including ambient temperature ranges. As a result of the weaken-
ing of the polymer matrix structure at higher temperatures (75 °C),
the compressive impact is taken into account with residual
strength, and there is no open iteration. The outcome enhanced
the tension of the composite constructions and demonstrated the
debonding behaviour of the fibre and lamination interfaces. The
findings of the filament-wound carbon/epoxy nanoparticles with
multi-walled carbon nano tubes were compared by utilizing these
structures with a low-velocity impact energy of 15 J and tempera-
Fig. 7. Schematic diagram (a & b) results represent the Thermo graphic images at
the delamination region in different samples [42]. ture changes by Kara et al. [37].
According to the results of two distinct carbon-epoxy polymer
composite structures, the multi-walled CNT had the highest con-
tact force values at ambient temperatures, and the efficient inves-
tigation on 15 J and 25 J, the LVI behaviour of woven-carbon
laminates at ambient temperature levels was investigated. The
findings of the temperature indentation increase at the 15 J energy
version only apply to other energy levels. The impact of the tem-
perature of FRPC on various temperature scale responses in LVI
events, as well as these, was investigated by Wang et al. [38].
The schematic representation of the environmental chamber and
C-scan techniques is shown in Figs. 4 & 5.

6. Effect of sandwich composites on LVI

The most common material is foam, and it’s used as a core


material in fibre-reinforced polymer structures because it has
excellent mechanical qualities, both dynamic and static, and sev-
eral polymers are used to make foam. Kaoa et al. [39] built bi-
material structures consisting of a lattice framework and polyur-
ethane (PU) foam. This paper explores the foam volume, density,
Fig. 8. Schematic diagram represents the Finite Element model of the impact point and plate thickness employed to determine the LVI of foam com-
[1]. posites. The core density and thickness are more important criteria
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M. Mani, M. Thiyagu and P. Kumar Krishnan Materials Today: Proceedings xxx (xxxx) xxx

Fig. 9. E-glass/epoxy comparison with various hybrid composites: a) tensile stress–strain curves, b) flexural stress–strain curves, and c) puncher load–displacement curves
are shown [3].

for making composite sandwich structures. Based on these criteria, is a non-destructive assessment technique to detect composite
the system exhibited strength, deflection, and energy-absorbing deteriorationand the thermo-graphical techniques is shown in
capacity in LVI events. Vacuum Assisted Resin Transfer Molding Fig. 7 [42]. Bandaru et al. [1] developed three-dimensional
formed three different sandwich composites with a VC foam- Kevlar/basalt-reinforced polypropylene hybrids with angle inter-
based hybrid polymer composite structure with the most excellent locking with the help of vacuum-assisted compression moulding
mechanical properties discussed [40]. technology.
The flexural strength findings were displayed, and the basalt/ The three types of composites with kevlar, Basalt, and hybrid
epoxy hybrid sandwich lamination layer had the maximum three-dimensional structures were examined with the energy level
strength compared to other sandwich laminations. The sandwich set at 120 J for all composites. The basalt/kevlar hybrid composite
composite with the best mechanical qualities underwent rapid with thread weft exhibited the highest strength of the pure basalt/
artificial ageing following ASTM C-481 specifications. The study’s para-aramid structure and the finite element model is shown in
findings will aid in developing the most incredible sandwich com- Fig. 7.
posite material used in aviation applications.The sandwich com- Hybridization methods are an effective lamination technique
posite test arrangement is shown in Fig. 6. for enhancing polymer composite structures in many aviation
Hybrid polymer composites are made up of at least two ele- applications. Diverse stacking sequence techniques with nanopar-
ments to get the benefits of each ingredient in the final material. ticles in advanced materials were used because different polymer
Making hybrid composites reduces material costs while increasing materials were used simultaneously. The hybridization of quasi-
strength and creating environmentally acceptable products. Fibre stacking sequence analysis of three distinct stacking composites
hybridization is a method of toughening polymer composite mate- was researched and compared with E-glass/Epoxy lamination by
rials, which enhances impact resistance. Low-velocity impact poses A. Vasudevan et al. [3]. Kevlar and carbon laminates outperform
a danger to composites since it generates a variety of internal dam- E-glass and epoxy laminates among these three hybridizations.
ages and complicated failure processes, resulting in a significant The E-glass/epoxy comparison with various hybrid composites
loss in the composite structural qualities. It is vital in the aerospace are illustrated in FIg. 9 (a-c)
sector to learn more about low-velocity impacts to forecast the The results of the different stacking sequence concept layers are
onset and progression of such damage [41]. plotted in a graphical curve representation. These values are com-
A glass/carbon fiber-enhanced composite was developed to pared to E Glass/epoxy values in terms of the tensile strength
improve the properties of fibers. Polymer composite E-glass and (Mpa) vs. tensile strain rate (Mpa), flexural strain (percent) vs flex-
plain carbon fiber layers are layered in various sequences. The ural strength (Mpa), and deformation (mm) versus force (N). Hung,
hybrid composites were looked into for multiple degrees of energy, P. et al. [41] studied the LVI effect response of carbon/glass fiber
and the usage of upper and lower layers of the composites was reinforced polymer composite structures. Here, the hybrid com-
made of carbon fiber, contributing to minimizing the dimensions posite with carbon/glass fiber damage and impact responses was
of the impact and the material deflection. Thermo graphic imaging assessed for impact load owing to LVI events. The findings of the

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M. Mani, M. Thiyagu and P. Kumar Krishnan Materials Today: Proceedings xxx (xxxx) xxx

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