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CONTENTS

FD SeriesLab Scale Freeze Dryer (Lyophilizer) ............................................................................................................ 3


LAB-Series Lab Freeze Dryer (Lyophilizer)................................................................................................................... 9
FD Series Pilot scale automatic freeze dryer .............................................................................................................. 13
FD-P Series Process Freeze Dryer ............................................................................................................................ 21
FD-FP series Vacuum Freeze Dryer (Lyophilizer) ....................................................................................................... 24
FD SERIES Lab Freeze Dryer/Lyophilizer

FD SeriesLab ScaleFreeze Dryer(Lyophilizer)


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DESCRIPTION
Vacuum freezing dryer is widely used in the medical,
pharmaceutical, biological, chemical and food and
other fields, FD series is suitable for laboratory use or
low-volume production to meet the requirements of
most laboratories conventional lyophilization.

FEATURES
 Microprocessor control & LCD touch display which

can display drying curve, vacuum, condenser temp.,


run time, ambient temperature.
 Pre-freezing function for samples.

 Large refrigerating capacity and slight noise of

DANFOSS(SECOP) compressor with CFC-FREE


refrigerant.
 304 stainless steel of condenser, table-top, racks &

shelves to ensure corrosion-resistant and easy to


clean; shelves height adjustable.
 Transparent drying chamber is safe and easy to

observe;
 Novel design, small size and easy operation;

 For water based samples, the -55°C condenser is the

perfect choice with effective cost. For samples


containing solvents or with low eutectic points, the -
80 C dual cascade refrigeration condenser provides
maximum performance(optional).
 For labs that needs quick turn-around, electric heating defrost is optional.

 Nitrogen inflation valve is available.

 It includes the following types: Normal type, Top-press type, multi-manifold T type and multi-manifold Top-press type to meet the

various requirements. Normal type suitable for bulk raw products like food, fruit, herbal medicine and other bio material, Top-
press(stoppering) type suitable for vials comes with cap, to stoppering caps into the vials.
 CE/ISO 9001 13485 14001 certificated.

FD-10 Bench-top type


Model FD-10-R FD-10-MR FD-10-TP FD-10-MTP FD-10-MT

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FD SERIES Lab Freeze Dryer/Lyophilizer
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Image

Dry chamber size (D*H) Ф260×430mm Ф260×465mm Ф260×490mm Ф260×540mm /


Total shelf area 0.12 m2 0.12 m2 0.08m2 0.08m2 /
Shelf size(mm) Ф200*4pcs Ф200*4pcs Ф180 * 3pcs Ф180 * 3pcs /
Shelf space height (mm) 70 70 70 70 /
Shelf number 4 pcs 4 pcs 3 pcs 3 pcs /
Trays number 4 pcs 4 pcs 3 pcs 3 pcs /
Ф12mm 920 Pcs 920 Pcs 560 Pcs 560 Pcs
Vials load 24 ports
Ф16mm 480 Pcs 480 Pcs 285 Pcs 285 Pcs
capacity 430×480mm (H*L)
Ф22mm 260 Pcs 260 Pcs 165 Pcs 165 Pcs
Sample load capacity 1.2L 1.2L 0.8L 0.8L /
Flask / 8 pcs / 8 pcs /
Dry rack Included Included Included Included /
Cold trap rack Included Included Included Included Included
Condenser Temp. <-55°C (-80°C or even lower is optional)
Cold trap size. Ф215 * 140 mm (Depth * Height)
Ice remove capacity 3~4kg/24hours
Cold type Air-cooled
Defrost type Natural (Electric is optional)
Ultimate Vacuum <5 Pa (empty)
Vacuum pump Included
Pump rate 2L/S
Install Power 970W
Voltage 220v/50Hz or 110v/60Hz
Dimensions 460*625* (370+430)(mm)
Weight 100 kg 110kg 105kg 120kg 65kg

FD-12 FLOOR TYPE


Model FD-12-R FD-12-MR FD-12-TP FD-12-MTP FD-12-MT
Image

Dry chamber size (D*H) Ф260×430mm Ф260×465mm Ф260×490mm Ф260×540mm /


Total shelf area 0.12 m2 0.12 m2 0.08 m2 0.08m2 /
Shelf size (mm) Ф200*4pcs Ф200 * 4pcs Ф180 * 3pcs Ф180 * 3pcs /
Shelf space height (mm) 70 70 70 70 /
Vials load Ф12mm 920 Pcs 920 Pcs 560 Pcs 560 Pcs 24 ports
quantity Ф16mm 480 Pcs 480 Pcs 285 Pcs 285 Pcs 430×480mm (H*L)
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FD SERIES Lab Freeze Dryer/Lyophilizer

Ф22mm 260 Pcs 260 Pcs 165 Pcs 165 Pcs


Sample load capacity 1.2L 1.2L 0.8L 0.8L /
Flask / 8 pcs / 8 pcs /
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Dry rack Included Included Included Included /


Cold trap rack Included Included Included Included Included
Condenser temp. <-55°C (-80°C or even lower is optional)
Cold trap size Ф215 * 140 mm (Depth * Height)
Ice remove capacity 4 Kg/24h
Cold type Air-cooled
Defrost type Natural (Electric is optional)
Ultimate Vacuum <5 Pa
Vacuum pump Included
Pump rate 2L/S
Install Power 970 W
Voltage 220v/50Hz or 110v/60Hz
Dimensions 460×556×(720+465)(mm)
Weight 120 kg 135kg 130kg 140kg 76 kg

FD-18 FLOOR TYPE


Model FD-18-R FD-18-MR FD-18-TP FD-18-MTP FD-18-MT

Image

Dry chamber size (D*H) Ф300×445mm Ф300×465mm Ф300×540mm Ф300×570mm /


0.18 m2 0.18 m2 0.09 m2 0.09 m2 /
Total shelf area
0.27 m2 0.27 m2
Ф240 * 4pcs Ф240 * 4pcs /
Shelf size (mm) Ф200 * 3pcs Ф200 * 3pcs
Ф240 * 6pcs Ф240 * 6pcs
70 70 /
Shelf space height (mm) 70 70
50 50
1320 Pcs 1320 Pcs
Ф12mm 990 Pcs 990 Pcs 24 ports
1980 pcs 1980 pcs
T-manifold
Vials load 740 Pcs 740 Pcs
Ф16mm 555 Pcs 555 Pcs 430×480mm (H*L)
capacity 1110 pcs 1110 pcs
Flask rack:
360 Pcs 360 Pcs
Ф22mm 270 Pcs 270 Pcs 610×600mm
540 pcs 540 pcs
1.8L 1.8L
Sample load capacity 0.9L 0.9L
2.7L 2.7L
Flask / 8 pcs / 8 pcs /
Dry rack Included Included Included Included /
Cold trap rack Included Included Included Included Included
Condenser Temp. <-60°C (-80°C or even lower is optional)
Cold trap size Ф270 * 400 mm (Depth * Height)
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FD SERIES Lab Freeze Dryer/Lyophilizer

Ice capture capability 6 Kg/24h


Cold type Air-cooled
Defrost type Natural (Electric is optional)
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Ultimate Vacuum <5 Pa


Vacuum pump Included
Pump rate 4L/S
Power 1400W
Voltage 220v/50Hz or 110v/60Hz
Dimensions 540×610×(963+445)(mm)
Weight 170 kg 185kg 185kg 195kg 105 kg

Standard Configuration
 Stainless steel condenser with opening, stainless steel operation tops, seamless welding with round cornerwhich is anti-corrosion

and easy to clean


 Stainless steel shelf & rack, 4 or 6 pcs shelves optional, shelf removable and spacing height adjustable

 Stainless steel pre-cooling rack with metal cover

 Integrally molded glass dried barrel adopted special plastic will not break

 Used SECOP (DANFOSS) quality compressor, high performance condenser fan, LCD touch display, history data can be stored,

searched and exported to computer.


Model R TP MR MTP MT

Image

Description Normal type Stoppering Manifold Stoppering + Manifold Multi-ports manifold


Freeze Dryer ● ● ● ● ●
Transparent dry ● ● ● ●
chamber
Vacuum pump ● ● ● ● ●
Stoppering device ● ●
Manifold Ports 8 ports (28/ 32mm) 8 ports (28/ 32mm) 24 ports
Freezing rack ● ● ● ● ●
Drying rack ● ● ● ●
Tray 4 pcs 3 pcs 4 pcs 3 pcs

FD-10S, FD-12S, FD-18S Series Shelf heating & program controlling (optional)
 Electric heating element for each shelf, Auto + Manual operation;
 36 Segment programs can be set used for kind of different raw material
 Temperature sensor ensure to monitor temperature of each shelf
 Data can be export to computer for analysis
 7’’ LCD touch display, easy to operate on machine
 Real-time alarm display and historical alarm query function to facilitate
fault diagnosis and equipment maintenance.
 Users can set the level and password, decentralized operation and
management.
 Sensor calibration to ensure long-term accuracy of the measured value
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FD SERIES Lab Freeze Dryer/Lyophilizer
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Optional items
Item No. Item Name Item No. Item Name
FD1001 -80°C Condenser FD10091000 1000ml flask
Fd1002 Defrost device FD1010 Eutectic point test device
FD1003 Refrigerant R404a, R502, R23 and etc FD1011 Vacuum regular device
FD1004 Oil mist filter FD1012 Jar bottle
FD1005 Shelves heating & Program segment control FD1013 Change to SS316 condenser &
Can stored 16 programs, each program can be set up shelves
36segments, correct program data in computing, memorize
the drying curve
FD1006 6pcs shelves instead of 4 pcs FD1014 Capacitance type vacuum gauge
FD1007 Leybold vacuum pump FD1015 Backfill filter
FD1008 Anti-back oil device FD1016 Auto backfill / drainage system
FD1009100 100ml flask
FD1009250 250ml flask
FD1009500 500ml flask

Vacuum Pump for FD series freeze dryer

Adapter Quick-release pipe Small-bore pipe Oil mist collector

Specifications of vacuum pump

Model 2XZ-0.5 2XZ-1 2XZ-2C 2XZ-4C 2XZ-6C 2XZ-8C 2XZ-15C

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FD SERIES Lab Freeze Dryer/Lyophilizer

Pumping Speed: L/S 0.5 1 2 4 6 8 15


Ult. Without gas ballast ≤6×10-2
Vacuum
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With gas ballast ≤6.5 ≤1.33


Pa
Speed: r/min(50HZ) 1400
Power Required: Kw 0.18 0.25 0.37 0.55 0.75 1.1 1.5
Diameter of inlet port: mm 16 16 25 25 40 40 40
Temp. rise of pump oil: °C ≯40 ≯45 ≯45 ≯65 ≯70
Oil capacity: L 0.60 0.70 0.10 1.2 2.0 3.0 4.0
447 469 514 514 565 650 770
Overall Dimensions: mm 168 168 168 168 200 240 240
260 260 282 282 342 430 430
Weight: kg 16 17 20 22 40 60 75

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LABSERIES Standard Freeze Dryer/Lyophilizer

LAB-Series LabFreeze Dryer (Lyophilizer)


Features
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 Touch LCD display with microprocessor controller, easy to use.


 Dry chamber using aircraft grade acrylic materials, non-adhesive, high strength, and no leaks.
 Condenser pre-cooling function.
 Used DANFOSS compressor.
 Vacuum pump in Japan or Korea brand, with oil-mist filter can trapping oil mist in the exhaust
gas, reduce environmental and health hazards.
 Can charge nitrogen or inert gas to save after drying.
 Programmable, freezing, drying and defrosting will be program controlled.
 Automatic control system: Temperature heating control for each shelves, heating circulation
monitoring protect, fuzzy PID control algorithm.
 Defrost system: Auto Non-electric heating defrost, more safety and fast.
 Vacuum regular system: vacuum degree regular in sublimation and drying process to avoid
special material foaming or blowing, accelerate lyophilized efficiency (Optional)
 Pulse backfill system: slow, medium, fast three kinds of backfilling mode selection, avoiding the
granular material and flocculent material being blown out effective loss problem inflatable
Freeze dryer with manifold & stoppering
pro duce. (Optional)
system
 Automatic drainage system: interlock with vacuum system after draining to prevent any
failure in vacuum system. (Optional)
 Can be work in automatic or manual operation, manual mode is used to explore the process
parameters, automatic mode for process maturity.
 Data recording system: 1) data can be stored in machine in 3 months; 2) External U-disk storage
(Optional); 3) PC-database storage (Optional)
 Monitoring system: real time system temperature and vacuum degree monitored, acquisition
frequency 50ms / time.
 Lyophilization process recipe storage function: can store 500 set of fixed or user-defined
lyophilized formulation process.
 PC remote monitor system: remote monitor working status of machine, max 1.5km distance
(Optional)
 Eutectic point test function (Optional)
 Calibration function: temperature and vacuum calibration ensures long-term accuracy of the
measured values.
 Freeze-drying curve searchable.

Safety Protection Freeze dryer with -80°C condenser


 Over-current protection
 Over-load protection
 Over-heating of temperature
 Vacuum defense in processing
 36V safety voltage for heating system
 Vacuum pump protection

Configuration Instruction

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LABSERIES Standard Freeze Dryer/Lyophilizer

Normal type(R): suitable for bulk material Stoppering type(S): suitable for sealing
vials material
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Flask-mount type(F): suitable for Stoppering with flask-mount type(FS):


external flask material suitable for bulk, external flask and vials
material

T-manifold type(T): Suitable for -80°C condenser type


external vials or flasks material

Specifications
Model LAB-1R-50 LAB-1S-50 LAB-1F-50 LAB-1FS-50 LAB-1T-50
LAB-1R-80 LAB-1S-80 LAB-1F-80 LAB-1FS-80 LAB-1T-80
Type Normal Stoppering Flask-manifold Stoppering & Flask- T-manifold
manifold
Control Programmed Programmed Programmed Programmed Programmed

Display LCD touch LCD touch LCD touch LCD touch LCD touch

Condenser -55°C -55°C -55°C -55°C -55°C


temperature -85°C -85°C -85°C -85°C -85°C
Water/ice 3L 3L 3L 3L 3L
capture 4L 4L 4L 4L 4L
Compressor 7/8HP 7/8HP 7/8HP 7/8HP 7/8HP
power 2/3HP * 2 2/3HP * 2 2/3HP * 2 2/3HP * 2 2/3HP * 2
Defrost Yes Yes Yes Yes Yes

Dry area (m2) 0.12 0.08 0.12 0.08 -

Shelf 4 pcs 3 pcs 4 pcs 3 pcs -

Vacuum < 8 Pa < 8 Pa < 8 Pa < 8 Pa < 8 Pa

Power 900W 900W 900W 900W 900W


1400W 1400W 1400W 1400W 1400W
Voltage 220/50 220/50 220/50 220/50 220/50
110/60 110/60 110/60 110/60 110/60

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LABSERIES Standard Freeze Dryer/Lyophilizer

Dimensions 470*600*400 470*600*400 470*600*400 470*600*400 470*600*400


(W*D*H)mm 640*640*1000 640*640*1000 640*640*1000 640*640*1000 640*640*1000
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Optional
Item ref. Item name Item ref. Item name

LAB10001 Vacuum regular system, Vacuum trimming needle LAB10024 Paperless recorder, with USB interface
* 1 + vacuum solenoid valve +1

LAB10002 Eutectic point tester (economic type), measuring LAB10025 Remote controlling & monitoring system, RS485
temperature & resistance value

LAB10003 Eutectic point tester (standard), measuring LAB10026 Anti-back oil solenoid valve, SEGV brand
temperature & resistance value online & offline,
with software

LAB10004 T type 16 port manifold LAB10027 6 shelves with tray dry chamber

LAB10005 T type 24 port manifold LAB10028 8 shelves with tray dry chamber

LAB10006 T type 52 port manifold LAB10029 4 shelves with trays, 12 port manifold-flasks

LAB10007 T type 104 port manifold LAB10030 6 shelves with trays, 12 port manifold-flasks

LAB10008 Ampoules sealer, sealing torch with tank LAB10031 8 shelves with trays, 12 port manifold-flasks

LAB10009 Vial capper, suitable for 12~30mm LAB10032 3 shelves with trays, 12 port manifold-flasks with
stoppering device

LAB10010 Jars adapter (Wide neck) LAB10033 Auto water drain device, include solenoid valve, drain
pipe & interface

LAB10011 Pulse backfill system, Backfill solenoid valve *1+ LAB10034 Mini dot matrix printer
pipe and adapter

LAB10012 Backfill filter, 0.2u filter LAB10035 Oil mist filter, SEGV

LAB10013 Backfill interface, USA APG, 8mm LAB10036 Oil mist filter, BWVAC

LAB10014 PC-database storing system LAB10037 Oil mist filter, ULVAC

LAB10015 U-disk data recording system, for online/offline LAB10038 Oil mist filter, Leybold
analysis

LAB10016 BWVAC Vacuum pump 1.5L/S LAB10039 ULVAC Vacuum pump 1L/S

LAB10017 BWVAC Vacuum pump 3L/S LAB10040 ULVAC Vacuum pump 2L/S

LAB10018 BWVAC Vacuum pump 6L/S LAB10041 ULVAC Vacuum pump 4L/S

LAB10019 BWVAC Vacuum pump 8L/S LAB10042 Sample temperature monitor, display range -50~100°C

LAB10020 Leybold Vacuum pump 2L/S

LAB10021 Leybold Vacuum pump 4L/S

LAB10022 Leybold Vacuum pump 6L/S

LAB10023 Leybold Vacuum pump 8L/S

Built-in freezing container Ampoules sealer Oil-mist filter 6~8 shelves with dry chamber

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LABSERIES Standard Freeze Dryer/Lyophilizer
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Leybold 6~8 shelves with dry chamber


Eutectic point tester Vial capper vacuum pump and flaks mount

T-
16/24/52/104 manifold Jars adapter Oil anti-back system Backfill filter

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FDSERIES Pilot Freeze Dryer/Lyophilizer

FD Series Pilot scale automaticfreeze dryer


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Features:
Chamber
 Rectangular type dry chamber, Pre-freezing, drying in same chamber without any manual operation.
 Drying chamber & shelves made by polished SS 304 or material contact parts SS316 is optional, adopted high strength, high
transmittance plexiglass door, easy to observe, inside round corner, easy to clean.
 Oil circulation heating type with high temperature precision control, usually suitable for medical, bio field, electric heating type
suitable for food field.
 GUNDFOS shielded circulating pump and PID control electric heating component; circulation liquid used Low-temperature low-
viscosity silicone oil.
 Shelves heating system uses safe voltage, while heating rate controllable. (Electric heating type)

Shelf made of mirror polish stainless steel, each shelf should be tested their roughless and flatness by professional tester in order to
provide uniformity temperature for sample.

Condenser (cold trap)


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FDSERIES Pilot Freeze Dryer/Lyophilizer

 Made by SS304 drum-type cold trap,SS316 is optional for the material which has high corrosivity. with high transmittance
plexiglass door, Integrity or separately condenser and chamber can be chosen.
 Can be made of polish stainless steel.
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 Patented gas diversion technology, cold trapping ice even, ice-catching ability.
 Electric heating around the condenser chamber to remove ice effective. (base on model)

Refrigeration
 Dual-stage cooling, famous hermetic compressor which is low noise, capillary throttling technology, air-cooled or water-cooled
is available.
 Brazed plate heat exchanger.
 Environmental-friendly refrigerant.

Control
 Flexible manual + automatic control, manual groping process, automatic
batch production.
 PLC control with 7’ LCD touch graphic display, can be operated in auto,
semi-auto and manual mode.
 Shelf temperature adjustable, controllable, explore suitable for pilot and
production processes.
 32 programs, each program can be set as 36 segments, curve can be stored, processing parameters can be modified in real
time.
 Built with recorder, with USB interface data can be exported to computer
for analysis, FD-LYO software & computer is optional for controlling by
remote way.
 sensor calibration function, to ensure long-term use of the accuracy of the
measured value.
 Real-time alarm display and historical alarm inquiry function, convenient
fault diagnosis and equipment maintenance.
 Users can set the level and password, decentralized operation and
management.

Vacuum
 Two-stage rotary vane vacuum pump, vacuum is automatic adjust and can be set (optional).
 Ultimate vacuum can reach 5 Pa, in order to reach highest vacuum, Leybold brand vacuum pump is optional.

Others
 Normal type suitable for bulk raw products like food, fruit, herbal medicine and bio material. Stoppering type suitable for vials
comes with cap, to stoppering caps into the vials.
 Inflatable (water) valve with a safety diaphragm valve can be connected to the inert gas source, dry and filled with inert gas, to
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FDSERIES Pilot Freeze Dryer/Lyophilizer

extend the shelf life of the material.


 CE/ISO 9001 13485 14001 certificated.
 Can be conforms to GMP standard.
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Main characteristics:
FD-10F Series
FD-10F Series FD-10F-R (Silicon oil heating) FD-10F-TP (Silicon oil heating)
Model
FD-10-RE (Electric heating) FD-10F-TPE (Electric heating)
Specification Normal With stoppering

Picture

Shelf area 0.2 m2 0.1 m2


Shelf quantity 2 pcs 1pc
-70°C ~ +65°C
Shelf temp. range
-50°C ~ 70°C
Shelf space height 70mm
Shelf dimension 400×270mm
Drying Ф22mmvials(piece) 440 220
chamber Ф16mm vials (piece) 868 434
Ф12mmvials (piece) 1554 777
Tray dimensions 395×265mm 395×265mm
Tray quantity 2 1
Sample loaded capacity 2L 1L
Stoppering device No Yes
Material SS304 (chamber, shelves, trays)
≤-80°C
Max temp.
≤-60°C (-80°C is optional)
Condenser Ice capture capacity 6Kg/24hs
Defrost Natural (Electric heating is optional)
Material SS304
Vacuum pump Included
Vacuum Vacuum rate 4L/S
Vacuum degree ≤5 Pa

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FDSERIES Pilot Freeze Dryer/Lyophilizer

Style of cooling Air-cooled


Dimension(L*W*H) 655×640×1200mm 655×640×1200mm
Basic Weight 210kg 210kg
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parameters Control method PLC auto + manual


Installation power 2Kw
Voltage 220V/50Hz (can be change to 110V/60Hz)

FD-20F Series
Model FD-20F-R FD-20F-TP
FD-20F Series
Specification Regular Top-press

Pictures

Freeze-drying area 0.3 m2 0.2 m2


Heating method Circulation oil heating Circulation oil heating
Shelves quantity 3 pcs 2+1 pcs
Shelves temp. range -50°C ~70°C -50°C ~70°C
Temp. difference 1°C 1°C
Shelves space 70mm 70mm
Dimensions of shelves 400*270 mm 400*270 mm
Drying chamber
Size of tray 395×265mm * 3 pcs 395×265mm * 2 pcs
Ф22 Bottle (piece) 440 440
Ф16Bottle (piece) 868 868
Ф12 Bottle (piece) 1554 1554
Sample loaded capacity 3L 3L
Stoppering device No Yes
Material SS304 (chamber, shelves, trays) SS304 (chamber, shelves, trays)
Cold trap temperature ≤-75°C ≤-75°C
Cold trap Water-capture capability 6 Kg/24h 6 Kg/24h
Material SS304 SS304
Ultimate Vacuum ≤5 Pa ≤5 Pa
Vacuum pump 2XZ-4 2XZ-4
Pump rate 4L/s 4L/s
Air Cooling room
Style of cooling Air Cooling room temperature≤25°C
temperature≤25°C
Basic parameters
Power supply 220V/50Hz or 110V/60Hz 220V/50Hz or 110V/60Hz
Power 3000W 3000W
Weight 300kg 310kg
Dimension 770x750x1520 mm 770x750x1650 mm
Control method PLC auto + manual PLC auto + manual

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FDSERIES Pilot Freeze Dryer/Lyophilizer

FD-30F Series
FD-30F Model FD-30F-RE FD-30F-R FD-30F-TP
Series Silicon oil circulation Silicon oil circulation
Heating type Electric heating
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heating heating

Picture
Freeze-drying area 0.4 m2 0.4 m2 0.306 m2
Shelf quantity 4+1 pcs 4+1 pcs 3+1 pcs
Shelf temp. range -50 ~ 70°C -50 ~ 70°C -50~70°C
Temp. Difference +/-1°C (balance) +/-1°C (balance) +/-1°C (balance)
Shelf size 300×340mm 300×340mm 300×340mm
Drying Sample loaded capacity 4L 4L 3L
chamber Shelf spacing 50mm 50mm 70mm
Tray size 295×335mm 295×335mm 295×335mm
Tray quantity 4 pcs 4 pcs 3 pcs
Material of chamber Polish SS304 Polish SS304 Polish SS304
Material of Shelves Polish SS304 Polish SS304 Polish SS304
Material of trays SS304 SS304 SS304
Vial load Ф22 vials 728 728 546
capacity Ф16 vials 1440 1440 1080
(pcs) Ф12vials 2600 2600 1950
Cold trap temperature ≤-60°C ≤-75°C ≤-75°C
Ice capture capability 8 Kg/24h 8 Kg/24h 8 Kg/24h
Cold trap Defrost Nature Nature Electric or hot gas
Cold type Air-cooled Air-cooled Air-cooled
Material SS304 SS304 SS304
Style of top-press - - Hydraulic pressure
Ultimate vacuum ≤ 5 Pa ≤ 5 Pa ≤ 5 Pa
Vacuum rate 6L/S 6L/S 6L/S
Basic Dimension (mm) 890×660×1210 920×780×1350 1280*900*1630
parameters Weight 280 kg 400 kg 450 kg
220V/50Hz 220V/50Hz 220V/50Hz
Voltage Freeze dryer
110V/60HZ 110V/60HZ 110V/60HZ
Power 2700W 4500W 5500W
Control PLC auto + manual
method

FD-50F Series
FD-50F Series Model FD-50F-RE FD-50F-R FD-50F-TP
Heating type Electric heating Silicone oil circulation Silicone oil circulation

www.labfreez.com ~ 17 ~
FDSERIES Pilot Freeze Dryer/Lyophilizer
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Picture

Drying chamber Freeze-drying area 0.6 m2 0.7 m2 0.5 m2


Shelf quantity 6 pcs 4+1 pcs 3+1 pcs
Shelf temp. range -50°C ~70°C -50°C ~70°C -50~70°C
Temp. Difference +/-1°C (balance) +/-1°C (balance) +/-1°C (balance)
Shelf size 300×340mm 480×360mm 410×410mm
Shelf spacing 50mm 50mm 70mm
Sample load capacity 6L 7L 5L
Tray quantity 6 pcs 4 pcs 3 pcs
Tray size 295×335mm 475×355mm 405×405mm
Material of chamber Polish SS304 Polish SS304 Polish SS304
Material of Shelves Polish SS304 Polish SS304 Polish SS304
Material of trays SS304 SS304 SS304
Vial load capacity Ф22 vials (piece) 1408 1408 1050
Ф16 vials (piece) 2728 2728 2058
Ф12vials (piece) 4920 4920 3705
Cold trap Cold trap temperature ≤-60°C ≤-75°C ≤-75°C
Ice capture capability 10 Kg/24h 10 Kg/24h 10 Kg/24h
Electric defrost Nature Nature Electric or hot gas
Cool type Air cooled Air cooled Air cooled
Material SS304 SS304 SS304
Basic parameters Style of top-press - - Hydraulic pressure
Ultimate vacuum ≤5Pa ≤5Pa ≤5Pa
Vacuum pump Included Included Included
Pump rate 8L/S 8L/S 8L/S
Dimension (mm) 890×670×1410 1000×785×1420 1490×850×1620+240
Weight 450kg 600kg 800 kg
Voltage Freeze dryer 380V±10%50Hz/60Hz 380V±10%50Hz/60Hz 380V±10%50Hz/60Hz
Power 4500W 5500W 6500W

FD-100F Series
FD-100F Series Model FD-100F-R FD-100F-TP
Heating type Silicone oil circulation Silicone oil circulation

Picture

www.labfreez.com ~ 18 ~
FDSERIES Pilot Freeze Dryer/Lyophilizer

Drying area 1.0 m2 1.15 m2


Shelf quantity 6+1 layer 4+1 layer
Shelf Temp range -50°C ~70°C -50~70°C
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Shelf temp. difference ±1°C (balance) ±1°C (balance)


Shelves size 480*360mm 480×600mm
Tray size 475×355mm 475×595mm
Drying chamber
Tray quantity 6 pcs 4 pcs
Raw material loaded capacity 10L 11L
Height space 70mm 70mm
Material of chamber Polish SS304 Polish SS304
Material of Shelves Polish SS304 Polish SS304
Material of trays SS304 SS304
Ф22 vials (PCS) 2112 2460
Vials load capacity Ф16 vials(PCS) 4092 4788
Ф12vials (PCS) 7920 8624
Condenser temp. ≤-75°C ≤-70°C
Condenser capability 15 Kg/24h 15 Kg/24h
Cold trap
Defrost Electric heating Electric heating
Material SS304 SS304
Vacuum pump Included Included
Ultimate Vacuum ≤5 Pa ≤5 Pa
Pump rate 15L/S 15L/S
Style of top-press - Hydraulic pressure
Basic parameters Cooling type Air cooled Air cooled
Dimension (mm) 1170×830×1665 1640×1100×1630+350
Voltage 3p-380~400V/50Hz 3p-380~400V/50Hz
Install Power 6500W 7500W
Weight 700kg 1000kg
Control method PLC auto + manual

FD-200F Series
FD-200F Model FD-200F-R FD-200F-TP
Series Heating type Silicone oil circulation Silicone oil circulation

Picture

Freeze-drying area 2.25 m2 1.98 m2


Shelves quantity 5+1pcs 4+1pcs
Drying Shelf Temperature -50°C ~70°C -50°C ~70°C
chamber Shelf Temp. Accuracy ± 1°C ± 1°C
Shelf spacing 80~100mm 80~100mm
Size of shelves 500*900*20 mm 610*810*20 mm
www.labfreez.com ~ 19 ~
FDSERIES Pilot Freeze Dryer/Lyophilizer

Raw material load capacity (be better) 22L 20L


Material of chamber Polish SS304 Polish SS304
Material of Shelves Polish SS304 Polish SS304
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Material of trays SS304 SS304


Ф22 vials (PCS) 4100 3600
Vials load
Ф16 vials (PCS) 7800 6800
capacity
Ф12 vials (PCS) 14400 12600
Max temperature ≤-75°C ≤-75°C
Water-capture capability 40 Kg/24h 40 Kg/24h
Condenser
Defrost water soaking water soaking
Material SS304 or SS316 SS304 or SS316
Vacuum degree ≤5 Pa ≤5 Pa (Range:1~300Pa)
Dimension 1200*2100*1700 (mm) 1300*3300*2500 (mm)
Basic Max Power 13.5kw 15kw
parameters Weight 2300 kg 2600 kg
Data Process RS232 Interface or USB
Control method PLC auto + manual
Compressor Bitzer or TECUMSEH, 2 set
Power 7 Kw
Refrigeration Refrigerant R507 & R23
unit Cooling type Air cooled
Pressure controller DANFOSS
Expansion valve DANFOSS

Optional items for FD Pilot type


Item No. Item Name

FDF1001 Stainless steel shell (SS304 or SS316)

FDF1002 Rotary Device

FDF1003 Control software

FDF1004 PC

FDF1005 Eutectic point tester

FDF1006 Leybold vacuum pump

FDF1007 Defrost device (for special model)

FDF1008 Air compressor (for Pneumatic door opening)

FDF1009 Vacuum pump solenoid valve

FDF1010 External material change to SS304

FDF1011 Condenser, trays, shelves change to SS316

FDF1012 6 port manifold system (extra port customizable)

FDF1013 Data logger

FDF1014 Backfill filter

FDF1015 Capacitance type vacuum gauge

FDF1016 Vacuum regulation system

www.labfreez.com ~ 20 ~
FD-P SERIESProcess Freeze Dryer/Lyophilizer

FD-P Series Process Freeze Dryer


For medicine use
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Main Functions
 Shelf pre-freezing function.
 Can be filled with nitrogen or inert protect
machine after working.
 lyophilized automatic control system:
procedural programming, both freeze- dried
and defrost control procedures.
 Shelf: adopting international advanced
welding technology without leak (three- year
warranty).
 Lyophilized end point test system:
automatic lyophilized end testing parsed end
of the drying stage, to ensure that the
moisture content of the material to reach the
standards.
 Vacuum regulator systems: sublimation and
vacuum drying process analytical
adjustment, avoid special material to 1~5 m2
foaming & blowing, accelerate lyophilization efficiency.
 Pulse backfill system: slow, medium, fast three backfill mode selection, avoiding the issue for the end of
the freeze-dried granular material and flocculent inflatable produce effective substances are blown away
loss.
 Large industrial touch screen, human-computer interaction is good, easy to understand, no instructions
are also available for easy operation.
 Monitoring system: real-time monitoring system temperature, vacuum, acquisition frequency 50ms / times.
 Lyophilization process recipe storage function: can store 2000 group fixed or user-defined lyophilized
formulation process.
 PC remote monitoring system: remote monitoring equipment operating conditions, as far as monitoring
distance 1.5KM.
 Eutectic point test function (optional).
 Process data recording system (optional).
 Calibration function: temperature and vacuum calibration ensures long-term accuracy of the measured
values.
 Lyophilized curve inquiry function (available temperature and vacuum degree curve, convenient process
optimization and lyophilized effect verification).

Features
◎ Cabinet:
Cabinet design according to GB150-2011 / PED ASME standards, in line with FDA and GMP standards. Internal
cabinet with large rounded design, with mirror polished surface, bottom of the box with tilt design, also i n
line with CIP and SIP drainage requirements. It can withstand: 0.15Mpa to 0.5Pa full range of positive and
negative pressure.

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FD-P SERIESProcess Freeze Dryer/Lyophilizer

◎ Shelf: adopts international advanced welding process. Internal


welding, TIG welding and orbital welding technology
◎ Condenser: with polishing technology, surface bright and
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smooth. Water vapor channel optimized design to ensure small


molecule surge resistance, more efficient water capture.
◎ Refrigeration system uses world famous refrigeration
compressors, refrigeration system security and stability.
◎ Vacuum system: vacuum pipe with automatic orbital welding,
ensure welding firm appearance. Using helium vacuum leak
detector testing to ensure vacuum system to achieve high vacuum
requirements.
◎ CIP system CIP system valves and pneumatic actua tors are
imported original, to ensure stable operation, safe and reliable. CIP
system piping with automatic orbital welding, ensure welding firm
appearance. CIP vacuum system piping using helium leak detector
testing to ensure vacuum system to achieve high vacuum requirements. water pump imported from Germany
to remove residual moisture after cleaning, cleared completely.
◎ SIP system uses a pulsating pre-vacuum steam sterilization, with Fo value display and recording, with
complete safety interlock and interlock functions, box comes with a cooling function. Triple overpressure
protection, to ensure absolute safety. Case high pressure vessel design, manufacturing process, all components
of industrial X-ray machine detected by testing, ensure that the overall firm, resistant to high pressure. Valves
are used in place disinfection system temperature up to above 350 °C of the original imports. Pneumatic
actuators are imported original, ensure stable operation, safe and reliable. Reign disinfection system with
automatic orbital pipe welding, welding to ensure strong and beautiful. SIP system piping using helium vacuum
leak detector testing to ensure vacuum system to achieve high vacuum requirements. Remove residual moisture
after sterilization imported from Germany, water ring pumps, pumping speed, completely clear. Maximum
sterilization temperature up to 150 °C.
◎ Process Control System, meet FDA 21 CFR PART 11 electronic records, electronic signatures cannot be
modified requirements. Precisely controlled, repeatable, can be restored.
◎ Plate heat exchanger, using the world-class plate heat exchanger, heat transfer efficiency.
SIP type suitable for the use of the pharmaceutical sector. CIP type suitable for use in the field of biological
engineering. Common type suitable for industrial, food and other fields use

Safety:
 Independent Overcurrent protection for various facilities
 Independent overload protection for various facilities
 Conditions allow individual facilities operating
 Heating overtemperature protection
 Product vacuum freeze-drying process protection
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FD-P SERIESProcess Freeze Dryer/Lyophilizer

 Vacuum pump protection


 System logic interlock
 Meet the GMP standard
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Model Shelf Shelf Shelf size (mm) Temp. accuracy(°C) Condenser Vials load Shelf Condenser Power
area qty water capacity (22mm) temp. (°C) temp. (°C) (KW)
(m2 ) (L)

FD-P1 1.08 4+1 450*600 ±1.0 20 2100 -60-80 <-85 9

FD-P2 2.19 4+1 600*900 40 4200 12

FD-P3 3.24 6+1 600*900 60 6300 21

FD-P5 4.86 6+1 900*900 100 9450 24

FD-P7 7.56 7+1 900*1200 150 15750 44

FD-P10 9.72 9+1 900*1200 200 19950 58

FD-P13 12.96 9+1 1200*1200 260 26250 67

FD-P15 16.1 9+1 1200*1490 320 33600 75

FD-P20 19.67 11+1 1200*1490 400 42900 104

FD-P25 25.0 14+1 1200*1490 500 52500 125

FD-P30 31.5 14+1 1490*1490 600 60900 134

FD-P40 42 14+1 1490*1990 800 84000 174

FD-P50 51.0 17+1 1490*1990 1000 105000 210

15 m2 20m2

25m2 40m2

www.labfreez.com ~ 23 ~
FD-FP SERIES Process Freeze Dryer/Lyophilizer

FD-FP Series Vacuum Freeze Dryer(Lyophilizer)


For food processing
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Main application of food freeze dryer:


Vacuum freezing and drying technology is currently the
most advanced technology for food dehydration
processing in the world. Compared with the commonly
used drying method, the freeze-dried food produced with
this technology features long period of quality assurance,
good re-hydration nature, good-looking color, good flavor,
taste and high content of nutritious components. The
dried food basically remains unchanged in its volume and
shape, looks like sponge and has no shrinking. This
drying technology can be widely used in process of
vegetables, fruits, condiments, aquatic products,
biological products, medicine, beverage, exemplar etc.

Main part of food freeze dryer:


FD-FP series vacuum cryogenic drying equipment mainly includes food pre-freezing system, drying bin system, heating system, vacuum
system, refrigerating system, material conveying system, medium system, pneumatic system, cleaning and sterilizing system.

Main technical parameters of food freeze dryer:


Model FD-FP1 FD-FP5 FD-FP10 FD-FP20 FD-FP30 FD-FP40 FD-FP60 FD-FP75 FD-FP90 FD-FP100

Shelf area (m2) 1 5.5 11.4 22.4 35.6 45.6 59.28 74.88 89.8 100

Chamber size Diameter Φ600 Φ1200 Φ2300 Φ2300 Φ2300 Φ2400 Φ2500 Φ2500 Φ2500

(mm) Depth 700 1480 1300 2250 3300 4300 3170 4200 5200

Shelf quantity (pcs) 4+1 8+1 10+1 10+1 10+1 10+1 13+1 13+1 13+1

W 400 360 600 600 600 600 600 600 600


Shelf size
D 625 1000 950 1900 2850 3800 3800 4800 5800
(mm)
H 20 20 15 15 15 15 15 15 15

Shelf height space (mm) 60 60 80 80 80 80 80 80 80

Carts quantity (pcs) 0 1 1 2 3 4 4 5 6

W 395 330 460 460 460 460 460 460 460


Tray size
D 625 350 640 640 640 640 640 640 640
(mm)
H 30 20 40 40 40 40 40 40 40

Tray quantity 4 48 40 80 120 160 208 260 312

www.labfreez.com ~ 24 ~
FD-FP SERIES Process Freeze Dryer/Lyophilizer

Heating medium Silicone oil

Temp. range (℃) RT -120℃

Ice capture capacity (KG) 20 100 200 400 600 800 1000 1500 2000
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Condenser temp. (℃) -50 or -70

Condenser cooling method Direct evaporation

Defrost type Hot water spray

Defrost water capacity (Kg) 230 1000 200 400 600 800 1000 1500 2000

Ultimate vacuum (Pa) 10Pa 10Pa 10Pa 10Pa 10Pa 10Pa 10Pa 10Pa 10Pa

Install power (KW) 6.5 12 24 46 70 85 110 160 200

Cooling type Air cooled Water cooled

Cooling water (T/H) / 8 20 30 40 50 60 80 100

Cooling water pipe diameter (mm) / DN40 DN50 DN50 DN65 DN65 DN65 DN65 DN80

W 2010 2500 4000 6000 9000 9000 9000 1300 16000

Dimensions (mm) L 1300 1400 2100 2100 2100 2400 2900 2900 2900

H 1720 1600 2300 2300 2300 2600 3200 3200 3600

Weight (T) 1 4.8 8.6 17.5 26 32 40 40 80

www.labfreez.com ~ 25 ~

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