Manual Asc-270ls Zn2lsme-06

Control No.
ZN2LSME-06
Instruction Manual
of
Automatic Sample Changer for
Solid and Liquid Samples
Model ASC-270LS
NITTOSEIKO ANALYTECH
EC DECLARATION OF CONFORMITY
We hereby declare that the following equipment complies with the essential requirements
of:
Electromagnetic Compatibility Directive: 2014/30/EU

Machinery Directive: 2006/42/EC
RoHS Directive: 2011/65/EU (include(EU)2015/863)
Model Name : Automatic Sample Changer Model ASC-270LS
Standard to which Conformity is Declared:
EN61000-6-3:2007 : Generic standards-Emission standard for residential, commercial

and light-industrial environments
EN61000-6-1:2007 : Generic standards-Immunity for residential, commercial and

light-industrial environments
EN61010-1:2010 : Safety requirements for electrical equipment for measurement,

control, and laboratory use
EN IEC 63000:2018 : Technical documentation for the assessment of electrical and

electronic products with respect to the restriction of hazardous
substances
ISO12100:2010 : Safety of machinery – General principles for design –

Risk assessment and risk reduction
Name of Manufacturer : NITTOSEIKO ANALYTECH CO., LTD.
Manufacturer’s Address : 7-10-1 Chuo-rinkan, Yamato, Kanagawa 242-0007, Japan
EU Office Address : MITSUBISHI CHEMICAL EUROPE GmbH

Willstaetterstr. 30, 40549 Duesseldorf, Germany
Type of Equipment : Laboratory Equipment
Month and year of CE Marking : June, 2017
_______________________
Name : Kaoru Hayashi
Position : General Manager
Date :16 . 07 . 2021

DD.MM.YYYY
Introduction 1
Introduction
Thank you for purchasing our Automatic Sample Changer Model ASC-270LS for solid
and liquid samples.
ASC-270LS is the optional unit for our analyzers. By connecting to our analyzers
(including sample prep-station), up to liquid 120 samples and 49 solid samples can be
measured automatically.
To use the unit efficiently and safely, read this manual and fully understand the
functions and the operation methods before use.
Also read the instruction manual of our analyzers. Read corresponding instruction
manuals of the analysis system including a PC, a printer, and a monitor.
For the general operation, refer to the operation manual.
To use the unit correctly and safely, appoint supervisors and operators before use.
Connectable Electric Furnaces
ASC-270LS is the optional unit for our analyzer. HF-210 (horizontal furnace) can be
connected to ASC-270LS.
Before the use
(1) Do not reprint this manual wholly or partially without permission.
(2) The contents may be changed without notice.
(3) Though this manual was prepared carefully, contact local distributor when mistakes,
omissions, or missing pages are found. The system program windows in this manual
may be different depending on the version of the software.
(4) For any circumstances resulting from usage of the unit, we do not take any
responsibility regardless of (3).
(5) Assign specific operators and supervisors when using this unit.
(6) Follow the contents in this manual. When troubles or damages occur by neglecting
the contents in this manual, we do not guarantee units even within the warranty
period.
NITTOSEIKO ANALYTECH has the copyrights of this manual and the unit software.
Windows is the registered trademark of Microsoft.
Other company and product names are their trademarks and registered trademarks.
ASC-270LS
2 Introduction
ASC-270LS
SAFETY PRECAUTIONS 1
SAFETY PRECAUTIONS
Read this instruction manual with care before use.
If the unit is operated without following descriptions in this manual, security can not be
assured.
Keep the manual at hand when operating the unit. If any questions, errors, or omissions
are found, contact local distributor.
WARNING
Information under this sign explains critical operations which contain risk of
death or serious casualties.
CAUTION
Information under this sign explains critical operations which contain risk of
human casualties or damages to surrounding objects.
POINT
Information under this sign explains important and useful information for
utilizing the unit.
ASC-270LS
2 SAFETY PRECAUTIONS
Warnings and Cautions

Labels
The following labels are attached to this unit. Always follow the instructions on the labels.
Warning or Caution labels Attached places
At the front of ASC-270LS arm
mechanical part
At the front of ASC-270LS arm

mechanical part
At the top of ASC-270LS right back
At ASC-270LS rear
At ASC-270LS tray unit
ASC-270LS
Cautions
Read the following cautions carefully to use the unit correctly and
safely.
Installation
When installing the unit, observe the following precautions.
CAUTION
Install the unit in a place where temperature is 15 to 35 degrees
Celsius. Failure to do so can lead to a fire or unstable operation.
CAUTION
Install the unit in a place free from direct sunlight.
Failure to do so can lead to a fire.
CAUTION
Install the unit in a place free from strong vibration or continuous
weak vibration.
Failure to do so can lead to unstable operation.
CAUTION
Install the unit on a flat surface to avoid displacement of units. Failure
to do so can lead the unit fall.
CAUTION
Install the unit in a place free from a strong electromagnetic field.
Failure to do so can lead to unstable operation.
CAUTION
Install the unit in a place where humidity is 80% or less.
Failure to do so can lead to a fire or cause electric shock.
ASC-270LS
CAUTION
Install the unit in a place free from corrosive gas.
Failure to do so can lead to deterioration of the unit.
CAUTION
Install the unit in a place free from much dust.
Failure to do so can lead to a fire or cause electric shock.
CAUTION
Install the unit in a place where fire is not used.
The high-temperature electric furnace is used for this unit.
Failure to do so can lead to a fire.
CAUTION
Ventilate the room by a ventilating fan, etc. Failure to do so may affect
the health by the vapor or gas generated from chemicals.
CAUTION
When moving the unit, two persons should hold the unit bottom.
The unit is heavy and the injury by dropping the unit on the foot may
be caused.
During Usage
WARNING
Use only specified microsyringes for sample injection.
WARNING
Never touch the unit during operation. Colliding with the arm
mechanical part causes injuries. Do not put a finger into the injection
box.
ASC-270LS
WARNING
Appoint specific supervisors and operators for this unit.
WARNING
Always check for gas leaks before using the unit.
When organic matter suddenly mixes with oxygen or air at high
temperature, explosive combustion can occur.
As a result, glass parts such as pyrolysis tubes can break and lead to
human casualties.
To prevent explosive combustion, samples are vaporized slowly in
argon gas and mixed with oxygen and combusted. Before use, always
check gas piping looseness, O-ring deterioration, septum
displacement, etc. which could lead to gas leakage.
WARNING
Combustible gas is used, so install the unit in well-ventilated rooms
with ventilation systems.
The high-temperature electric furnace is used for this unit.
Flammable materials or flammable liquid around the unit lead to a fire
or cause electric shock.
CAUTION
Check gas flow with a flow meter before injecting a sample.
CAUTION
Never touch a power plug with wet hands to prevent an electric shock.
Failure to do so can lead to electric shock.
CAUTION
Do not modify, damage, or put together the power cable. Do not use a
power cable for current or voltage under the rating.
By placing heavy objects on the cable, heating or putting together the
cable or using the current under the rating, the cable is broken by
temperature raise to cause a fire and electric shock.
ASC-270LS
CAUTION
Do not remove the cover of the unit except for our agent’s
servicemen. Electric shock or fire may be caused.
CAUTION
When handling chemicals, always wear safety gloves and glasses to
protect skin and eyes. Do not inhale chemical vapor.
Maintenance and Inspection
CAUTION
Always check the unit every day before the use.
Failure to check the unit can lead not only to reduced performance of
the unit but also to serious accidents.
ASC-270LS
Table of Contents 1
Table of Contents
Section 1: Names and Functions of the Unit ................................... 1-1
1-1. Names and Functions of Model ASC-270LS Front ..............................................1-1
1-2. Names and Functions of Model ASC-270LS Rear ......................................... 1-3
1-3. Names and Functions around ASC-270LS Sample Injection Box.................. 1-4
Section 2: Parts Check ...................................................... 2-1
2-1. ASC-270LS Common Parts ........................................................................... 2-1
2-2. ASC-270LS Optional Parts ............................................................................ 2-2
2-2-1. ASC-270LS Parts for Solid Samples .................................................. 2-2
2-2-2. ASC-270LS Parts for Liquid Samples ................................................ 2-2
2-2-3. ASC-270LS Tray for 4mL Vials for Liquid Samples ............................ 2-3
2-2-4. ASC-270LS Tray for 2mL Vials for Liquid Samples ............................ 2-3
Section 3: Installation ....................................................... 3-1
3-1. Installation Conditions ...............................................................................................3-1
3-2. Installation Space.......................................................................................................3-2
3-3. Power Preparation .....................................................................................................3-2
3-3-1. Power .............................................................................................................3-2
3-3-2. Grounding ......................................................................................................3-2
3-4. Preparation for ASC-270LS .....................................................................................3-3
3-4-1. Removal of the Clamp for Carriage .................................................... 3-3
3-4-2. Ladle Insertion .................................................................................... 3-3
3-4-3. Line Connection ................................................................................. 3-5
3-4-4. Preparation of the Tray Unit for Liquid or Solid Samples and ............ 3-6
the Head
3-4-4-1. Setting of the Syringe Head and the Syringe ............................. 3-6
3-4-4-2. Setting of the Tray Unit for Liquid Samples ................................ 3-8
3-4-4-3. Chuck Head Setting ................................................................. 3-10
3-4-4-4. Setting of the Tray Unit for Solid Samples ............................... 3-11
3-4-4-5. Disposal Box Setting ................................................................ 3-11
3-4-5. Fixing Plate Setting .......................................................................... 3-12
3-4-6. Connection of HF-210 and ASC-270LS Units .................................. 3-13
3-5. Cable Connection ........................................................................................ 3-16
3-5-1. Communication Cable Connection ................................................... 3-16
3-5-2. Power Cable Connection .................................................................. 3-16
Section 4: ASC-270LS Functions ............................................. 4-1
4-1. Operation Modes ........................................................................................... 4-1
4-2. ASC-270LS Start ........................................................................................... 4-1
ASC-270LS
2 Table of Contents
4-3. Other Tools .................................................................................................... 4-3
4-3-1. Manual/Automatic Boat Setting .......................................................... 4-3
4-3-2. Change of the Chuck or the Syringe Head and the Tray .................... 4-6
4-3-3. Syringe Washing ................................................................................ 4-7
Section 5: Measurement .............................................................................................. 5-1
5-1. Start ............................................................................................................... 5-1
5-2. Setting............................................................................................................ 5-2
5-2-1. Schedule Setting and Measurement Flow .......................................... 5-2
5-2-2. New Schedule Preparation ................................................................. 5-3
5-2-3. Open Schedule .......................................................................5-4
5-2-4. Schedule Edit ..................................................................................... 5-5
5-2-5. Parameter Setting .............................................................................. 5-6
5-2-6. Rule Setting ...................................................................................... 5-12
5-2-7. Selecting “Standby” for “Type”.......................................................... 5-13
5-2-8. Selecting “Blank” for “Type” .............................................................. 5-16
5-2-9. Programs .......................................................................................... 5-19
5-2-9-1. Import of Combustion Condition (ABC Program) ........................ 5-19
5-2-9-2. Setting and Edit of ABC Program ............................................... 5-21
5-2-9-3. Replay ........................................................................................ 5-24
5-2-9-4. Buttons of ABC Program Window............................................... 5-25
5-2-9-5. Import of Sampling and Injection Conditions (ASC Program) ..... 5-26
5-2-9-6. Setting and Edit of ASC Program ............................................... 5-28
5-2-9-7. Buttons of ASC-270LS ASC Program Window ........................... 5-29
5-2-10. Selecting “Standard” for “Type” .............................................. 5-30
5-2-11. Selecting “Sample” for “Type”......................................................... 5-33
5-3. Measurement Preparation ........................................................................... 5-37
5-3-1. Gas Leak Check ............................................................................... 5-38
5-3-2. Heater .............................................................................................. 5-38
5-3-3. Prepare Button ................................................................................. 5-38
5-3-4. Detectors .......................................................................................... 5-39
5-3-5. Sample Boat Prebaking.................................................................... 5-39
5-4. Measurement Start ...................................................................................... 5-41
5-4-1. Continuous Measurement in Liquid Mode ........................................ 5-41
5-4-2. Continuous Measurement in Solid Mode .......................................... 5-44
5-4-3. Manual Operation during Measurement by Schedule ...................... 5-48
5-4-3-1. For Liquid Samples..................................................................... 5-48
5-4-3-2. For Solid Samples ...................................................................... 5-51
5-4-4. Boat Disposal after Measurement by Schedule................................ 5-54
ASC-270LS
Table of Contents 3
5-5. Shutdown ..................................................................................................... 5-54
Section 6: Troubleshooting .......................................................................................... 6-1
Section 7: Error Messages and Measures ................................................................... 7-1
Section 8: Maintenance and Inspection ....................................................................................8-1
8-1. Unit Inspection ............................................................................................... 8-1
8-1-1. Daily Inspection .................................................................................. 8-1
8-1-2. Periodical Inspection .......................................................................... 8-6
8-2. Maintenance .................................................................................................. 8-7
8-2-1. Fuse Change ...................................................................................... 8-7
8-2-2. Ladle and Guide Tube Change .......................................................... 8-7
8-2-3. Pyrolysis Tube Removal..................................................................... 8-9
8-2-4. Vial Wash and Storage at Trace Measurement .................................. 8-9
8-3. Storage of the Unit .................................................................... 8-9
Section 9: Specifications .................................................... 9-1
Section 10: Consumables .......................................................................................... 10-1
10-1. ASC-270LS Consumables ......................................... 10-1
10-2. ASC-270LS Parts Pictures .............................................. 10-2
ASC-270LS
4 Table of Contents
ASC-270LS
Section 1: Names and Functions of the Unit 1-1
Section 1: Names and Functions of the Unit

This section describes the names and functions of Automatic Sample Changer Model
ASC-270LS for liquid and solid samples.
1-1. Names and Functions of Model ASC-270LS Front
Fig. 1-1 shows ASC-270LS front and Table 1-1 shows the names and functions.
8
Tray for liquid samples
7 9
11
5
4
Tray for
solid samples
10 2 1
3
Fig. 1-1. ASC-270LS Front
Table 1-1. Names and Functions of Model ASC-270LS Front

No. Names Indications Functions
1 Power switch Power ASC-270LS power switch.
2 Cooler operation COOLER The lamp lights at cooler operation.
indication
3 Automatic operation AUTO The lamp lights at automatic operation.
indication
4 Tray unit Put boats or vials.
5 Position for sample boats 1 to 49 Place boats with samples.
ASC-270LS
1-2 Section 1: Names and Functions of the Unit

6 ABC maintenance cover Cover for the automatic boat controller
The feature is included to carry a
sample boat to the electric furnace.
7 Sample vial positions 1 to 84 Place 6mL vials containing standard
1 to 120 solution and samples.
Trays for liquid samples are two types
(for 84 and 120 vials).
8 Position for a vial for wash Put vials with liquid for wash.
9 Position for vials for waste Put empty vials for removal after
solution syringe rinse.
10 Sample boat box Sample boats are sent into the
pyrolysis tube from here.
Equipped with a liquid sample injection
inlet.
11 Arm mechanical part For moving liquid or solid samples
Open the front door to set a syringe or
a chuck.
ASC-270LS
Section 1: Names and Functions of the Unit 1-3
1-2. Names and Functions of Model ASC-270LS Rear
Fig. 1-2 shows ASC-270LS rear and Table 1-2 shows the names and functions.
1
2
3
4
5
Fig. 1-2. ASC-270LS Rear
Table 1-2. Names and Functions of Model ASC-270LS Rear

1 Ar/O2 gas inlet GAS IN Connect Ar/O2 lines from the electric furnace
(GAS-OUT INNER TUBE).
2 Fuse holder FUSE 4A Use our specified fuse.
TYPE-T
3 Power connector a.c. POWER Use our specified power cables.
4 Signal cable MAIN UNIT For connecting ASC-270LS to an electric
connection part furnace (RS-232C 9-pin cross-type).
5 H/W test switch FUNCTION For function test (For our servicemen).
ASC-270LS
1-4 Section 1: Names and Functions of the Unit
1-3. Names and Functions around ASC-270LS Sample

Injection Box
Fig. 1-3 shows the circumference of ASC-270LS sample injection box and Table 1-3
shows the names and functions.
1
7
8
2
3 4 5
Fig. 1-3. ASC-270LS Injection Box Circumference
Table 1-3. Names and Functions around ASC-270LS Sample Injection Box
No. Names Functions
1 Septum holder Black cap for fixing the septum of the liquid sample
injection inlet
2 O-ring holder For fixing the pyrolysis tube. An O-ring is placed
inside.
3 Cooling unit For cooling the sample boat box and lowering the
temperature of a heated sample boat.
After system connection, it operates automatically
by setting the furnace heater ON in the PC software.
4 Disposal box Put a disposal box here.
5 Sensor for boat check Boat existence judge
6 Head cover Put the cover during operation.
7 Sensor for head Judging whether the head set is for liquid or solid
check samples
8 Head set holder Set a syringe head or a chuck head.
ASC-270LS
Section 2: Parts Check 2-1
Section 2: Parts Check

The procedure for checking ASC-270LS parts is described in this section.
When initially opening the package, check that all listed parts are included.
＊ To purchase the consumables, refer to “Consumables”.
2-1. ASC-270LS Common Parts
Table 2-1. ASC-270LS Common Parts

No. Parts names Quantity Check Remarks
Column
1 ASC-270LS unit 1 pc
2 Ladle 1 pc
3 Thermal insulator for ASC-240S 1 pc
4 Fixing board (3 parts) for ASC-240S 1 set
5 Already set to
Septum holder 1 pc the sample
injection port.
6 Septum (flat) 100 Spare
pcs/set
7 O-ring P-16 (Silicon) 5 pcs Spare
8 Spare,
O-ring G-50 (Silicon) 1 pc For sample
inlet
9 φ 4 Nut (with a ferrule and an insert) 1 set
10 RS-232C cable 9-pin cross-type 1 pc
11 Fuse 4A 2 pcs/bag Spare
Power cable 1 pc Packed in
12 another box
(AC 100/230V or 230/240V, 2m)
13 ASC-270LS instruction manual 1 pc
ASC-270LS
2-2 Section 2: Parts Check
2-2.ASC-270LS Optional Parts
2-2-1. ASC-270LS Parts for Solid Samples
The following parts are optional.
Table 2-2. ASC-270LS Parts for Solid Samples

Column
1 Tray for solid samples 1 pc
2 Chuck head for solid samples 1 pc
3 Disposal box 1 pc
4 Ceramic sample boat 20 pcs Ceramic
5 Glass petri dish 1 set
6 Sample carry tray 1 pc
2-2-2. ASC-270LS Parts for Liquid Samples
Table 2-3. ASC-270LS Parts for Solid Samples

Column
1 Waste tray 1 pc
2 Syringe holder for liquid samples 1 pc
3 Wash solution vial φ 50 × 25L 1 pc
4 Waste solution vial φ 25 × 95L 10 pcs
5 Cap with septum (Connection cap) 1 set
100pcs
6 Quartz wool 5g/bag 1bag
7 Quartz sample boat for ABC 5 pcs
ASC-270LS
Section 2: Parts Check 2-3
2-2-3. ASC-270LS Tray for 4mL Vials for Liquid Samples
Table 2-4. ASC-270LS Tray for 4mL Vials for Liquid Samples

Column
1 Tray for 4mL vials for liquid samples 1 pc
2-2-4. ASC-270LS Tray for 2mL Vials for Liquid Samples
Table 2-5. ASC-270LS Tray for 2mL Vials for Liquid Samples

Column
1 Tray for 2mL vials for liquid samples 1 pc
ASC-270LS
2-4 Section 2: Parts Check
ASC-270LS
Section 3: Installation 3-1
Section 3: Installation
Necessary space, power, and gas lines for ASC-270LS installation are described in this
section.
3-1. Installation Conditions
Install the unit as the following conditions for the long-term stable use.
Refer to “SAFETY PRECAUTIONS” in this manual for details.
• Room temperature is 15 to 35 degrees Celsius.
• Free from direct sunlight.
• No strong vibration and continuous weak vibration.
• The surface for installation is flat and stable.
• No strong electromagnetic field.
• Humidity is under 80%.
• No corrosive gas.
• Free from much dust.
• Fire must not be used.
• No flammable materials.
• The room is ventilated.
• Operate the unit in the person’s presence.
If troubles or damages are caused by negligence of the above conditions, we can not
guarantee the unit even within the warranty period.
ASC-270LS
3-2 Section 3: Installation
3-2. Installation Space
Space needed to install ASC-270LS is as follows. Prepare the space of the horizontal
furnace instruction manual plus the following width. Depending on the system
configuration, prepare enough space for the complete system.
• ASC-270LS size: Width 500mm × Depth 460mm ×Height 600mm Weight: About
27kg (without attachments)
• Secure more than 150mm space between the unit and the back wall.
The following figure shows the combination with HF-210 (horizontal furnace) and GA-
210.
Fig. 3-1. System Installation Example
3-3. Power Preparation
3-3-1. Power
ASC-270LS consumption power is 192VA.

Voltage fluctuation range should be within ±10%.
When voltage fluctuation is over 10%, use a voltage stabilizer.
3-3-2. Grounding
ASC-270LS power cable is 3-line type including a grounding line. A grounded outlet is
required at the table.
Insert power cables into 3-line type power outlets and ground them stably. If the power
outlets are 2-line type, always ground them from the earth terminals of power cables.
Power cable lengths are as follows.

• Power cable for ASC-270LS: 2m
ASC-270LS
3-4. Preparation for ASC-270LS
3-4-1. Removal of the Clamp for Carriage
Remove 3 clamps fixing the arm mechanical part.

Remove the screws indicated by arrows in Fig. 3-2 with a screwdriver. Set the attached
screws. But, screws can not be set to the framed part.
Fig. 3-2. Clamp Removal
3-4-2. Ladle Insertion
Set the ladle to ASC-270LS as follows.
(1) Insert the ladle into the O-ring holder from the iron core side (covered with glass).
Fig. 3-3. Ladle Insertion
ASC-270LS
(2) While checking the injection box from the top, insert the ladle with tweezers to be in
the position in the figure.
(Arrow: Set the ladle tip position around the cutout line right.)
Adjust the tip with tweezers vertically (upward).
* When the unit is not installed, the cover of the injection box can not be opened.
Insert (1) ladle.
* After setting ASC-270LS and HF-210 and starting NSX-2100 application, open
the injection box cover and finally adjust the ladle position. To open and close the
injection box, refer to “4-3-1. Manual/Automatic Boat Setting”. The proper
position of ladle setting is as follows.
Fig. 3-4. Ladle Adjustment
ASC-270LS
3-4-3. Line Connection
Connect a gas line to the guide tube in ASC-270LS as follows.

* The line is connected on delivery.
(1) Remove ABC maintenance cover.

Refer to “8-2-2. Ladle and Guide Tube Change”.
(2) Check that the gas line tip cut is flat and pass a nut. Insert the gas line end deeply to
touch the L-type connector. Connect the nut to the connector and tighten it with
fingers. Stop tightening it when it is fastened suddenly.
(3) Pass the nut through the guide tube. Insert the L-type connector to contact the guide
tube end. Connect the nut to the connector and tighten it with fingers.
Stop tightening it when it is fastened suddenly.
(4) For the two positions in procedure (2) and (3), fix the connector and tighten the nut
with a spanner as follows. After tightening, check that it is not removed.
Gas line : Tightening of about one and quarter turn
Guide tube : Tightening of about one turn
（3）
（2）
Fig. 3-5. Line Connection
Connect ASC-270LS gas lines to the horizontal furnace. Connect the φ4/2 PTFE tube
(white) attached to “GAS-OUT INNER TUBE” of the horizontal furnace rear to “GAS IN”
of ASC-270LS rear with the attached nut and ferrule.
* During the procedure of “3-4-6. Connection of HF-210 and ASC-270LS Units”, connect
the φ4/2 PTFE tube (white) of “GAS-OUT OUTER TUBE” to the branch tube of a
pyrolysis tube.
ASC-270LS
3-4-4. Preparation of the Tray Unit for Liquid or Solid Samples and the
Head
Prepare the tray unit for liquid or solid samples and the head depending on use.
3-4-4-1. Setting of the Syringe Head and the Syringe
CAUTION
Remove and wash the syringe every day.
CAUTION
When inserting the flange part between the holding plates, always check
that it is inserted deeply to prevent syringe breakage.
Set the syringe head to ASC-270LS unit as follows.
(1) Select (i) or (ii) method.

(i) During ASC-270LS installation
The absorption axis can not be raised by start and the syringe head can not
be set. When the unit can be started, set it.
(ii) When ASC-270LS and other unit installation is completed
Start ASC-270LS unit, HF-210 unit, and NSX-2100 application to move the
arm mechanical part to the head change position. Proceed to the procedure
after (2).
* For the movement to the head change position, refer to “4-2. ASC-270LS Start”
or “4-3-2. Change of the Chuck or the Syringe Head and the Tray” after
installation.
(2) Open the cover of the head setting part.

Fit the syringe head to the holder and fix them with 2 screws.
(3) Turn the plunger holder slightly and lower it so that the stopper may fall into a ditch.
ASC-270LS
（3）
（2）
Fig. 3-6. Syringe Head Setting
(4) Open the syringe head door. Raise and open it to the left.
(5) Insert the syringe needle tip into the guide hole of the syringe head end.
Set the flange part between the holding plates.
Hitch the plunger top into the metal cutout part just below the plunger holder.
(6) Close the syringe holder door.

Close and lower the door to fix it. The procedure is opposite to (4).
The right figure shows the setting completion.
（4）（5）（6）
Fig. 3-7. Syringe Setting
(7) Close the cover.
ASC-270LS
3-4-4-2. Setting of the Tray Unit for Liquid Samples
Prepare ASC-270LS tray unit for liquid samples as follows and set it to ASC-270LS unit.
The tray units are for two types (84 or 120 samples) for sample vial setting and a wash
vial/waste vial.
CAUTION
Change a septum for vials every day.
Dispose of waste solution every day.
Change solvents (such as organic solvents and distilled water) for wash
every day.
POINT
Wash solutions or standard samples are different depending on sample
quality. Prepare them by referring to the following examples.
Aqueous samples
Wash solution: Distilled water
Standard sample: Water solution (Solutes are different depending on
measurement items.)
Nonaqueous samples
Wash solution: Organic solvents
Standard samples: Solutions diluted with organic solvents (Solutes are
different depending on measurement items.)
Pour sample up to 80% of a vial and set it to the tray unit for 84 or 120 samples.
CAUTION
Pour standard sample or sample up to 80% of a vial. When liquid is
small, it does not reach a microsyringe tip and sample is not absorbed to
lack sample. Standard samples or samples may contaminate septa.
ASC-270LS
(1) Pour wash solution into a vial for wash and set it to the tray unit A for wash and
waste solution vials. The larger one is for wash.
(2) Set empty vials for waste solution to the tray unit W for wash and waste solution
vials. This slender vial is for waste solution.
(3) After setting all necessary vials for the tray units, set each unit to ASC-270LS unit.
Set the tray unit for liquid samples so that △ symbol in No.1 may be in the left back
to the unit. Set it so that 4 legs may fit in the unit circular holes.
Set the tray unit for wash and waste solution vials so that the vial (A) for wash may
be in the back. Set it so that 4 legs may fit in the unit slit holes.
A
Ｗ
Fig. 3-8. Setting of the Tray Unit for Liquid Samples
A (Vial for wash)
Ｗ (Vial for waste solution)
Fig. 3-9. Setting of Vials for Wash and Waste Solution
ASC-270LS
3-4-4-3. Chuck Head Setting
Set the chuck head to ASC-270LS unit as follows.
(1) Select (i) or (ii) method.

(i) During ASC-270LS installation
The chuck opening and closing axis can not be raised by start and the chuck
head can not be set. When the unit can be started, set it.
(ii) When ASC-270LS and other unit installation is completed
Start ASC-270LS unit, HF-210 unit, and NSX-2100 application to move the
arm mechanical part to the head change position. Proceed to the procedure
after (2).
* For the movement to the head change position, refer to “4-2. ASC-270LS Start”
or “4-3-2. Change of the Chuck or the Syringe Head and the Tray” after
installation.
(2) Open the cover of the head setting part.

Fit the chuck head to the holder and fix them with 2 screws.
(3) Turn the plunger holder slightly and lower it so that the stopper may fall into a ditch.
Close the cover.
（3）
（2）
Fig. 3-10. Chuck Head Setting
ASC-270LS
3-4-4-4. Setting of the Tray Unit for Solid Samples
Set the tray unit to ASC-270LS unit as follows.

The tray unit for solid samples can hold 49 boats.
(1) Set the tray unit for solid samples so that △ symbol in No.1 may be in the left back
to the unit. Set it so that 4 legs may fit in the unit circular holes.
Fig. 3-11. Setting of the Tray Unit for Solid Samples
3-4-4-5. Disposal Box Setting
Set the disposal box to ASC-270LS left front as follows.

The folded part should be in the back.
The unit and the box are fixed with a magnet.
Fig. 3-12. Disposal Box Setting
ASC-270LS
3-4-5. Fixing Plate Setting
The following clamps connect ASC-270LS and HF-210 units.

1. Wide fixing plate, 2, Narrow fixing plate, 3. Clamp for fixing the plates, 4. Thermal
Insulating clamp
* For AQF-2100H system, connect ASC-270LS and HF-210 units with the fixing plates.
(1) Set screws to the holes of the attached wide fixing plate and ASC-270LS lower left
to fix the plate.
Fig. 3-13. Wide Fixing Plate Setting (ASC-270LS Side)
(2) Set screws to the holes of the attached narrow fixing plate and HF-210 lower left to
fix the plate.
Fig. 3-14. Narrow Fixing Plate Setting (HF-210 Side)
* The next page describes the procedure for fixing the attached fixing plates.
ASC-270LS
3-4-6. Connection of HF-210 and ASC-270LS Units
Set ASC-270LS to the horizontal furnace (HF-210) as follows.
(1) Open the electric furnace door at the front side of the horizontal furnace.
Pass the O-ring holder through the pyrolysis tube right from the knurled part side.
Pass the O-ring P-16 to the position of 1cm from the right end.
O-ring holder
O-ring P-16
Branch tube
Fig. 3-15. Connection of the Horizontal Furnace to ASC-270L Unit (O-ring Setting)
(2) Lap the wide fixing plate on the narrow fixing plate set in “3-4-5. Fixing Plate Setting”.
The wide fixing plate of ASC-270LS should lap on the narrow plate of HF-210 to
contact the curved part.
Fig. 3-16. Connection of the Horizontal Furnace to ASC-270L Unit

(Fixing Plate Overlap)
ASC-270LS
(3) While turning the pyrolysis tube, insert the tube into the left hole of the sample
injection box without twisting the O-ring.
Direct the branch tube to the bottom and tighten the O-ring holder to fix the pyrolysis
tube.
CAUTION
After inserting the pyrolysis tube deeply, tighten the O-ring holder.
By tightening the holder too tightly, the pyrolysis tube may break.
Tighten it carefully.
(4) Fix the clamp to the fixing plate cutout part with screws.

(Fixing Plate Setting)
(5) Set the φ6/4 elbow joint (30-6RU4-SP) to the branch tube of the pyrolysis tube and
connect φ4/2 PTFE tube (white) connected to the “GAS-OUT OUTER TUBE”.
* The branch tube quantity and the forms may be different depending on
selected units.
(6) Place the thermal insulating clamp for ASC-270LS on the fixing plate to surround the
pyrolysis tube.
ASC-270LS

(Thermal Insulating Plate Setting)
ASC-270LS
3-5. Cable Connection
3-5-1. Communication Cable Connection
Connect the MAIN UNIT connector of ASC-270LS rear to one of ACCEESSORIES

connectors (1 to 8) of the horizontal furnace rear with the attached RS-232C cable.
To connect other communication cables, refer to each instruction manual.
3-5-2. Power Cable Connection
Connect the power cable (2m) to the power connector (a.c. POWER) of ASC-270LS
rear. To connect other communication cables, refer to each instruction manual.
CAUTION
When connecting a power cable to ASC-240S unit, the pyrolysis tube may
break by the unit operation. Connect it while holding ASC-240S unit.
ACCESSORIES(1 to 8)
MAIN UNIT
a.c. POWER
Fig. 3-19. Cable Connection
ASC-270LS
Section 4: ASC-270LS Functions 4-1
Section 4: ASC-270LS Functions

This section describes ASC-270LS functions.
CAUTION
Operate the unit in the person’s presence.
4-1. Operation Modes
ASC-270LS has the following modes.
CAUTION
Before starting measurement in each mode, check measurement and
combustion conditions and ABC program. Improper conditions result in
malfunctions or explosive combustion.
(1) Liquid sample mode

Suck the sample in a vial of the tray with a syringe and inject it into a boat in the
injection box. To use ASC-270LS, put about 20mg quartz wool into a sample boat.
(2) Solid sample mode

A sample boat is chucked in the tray for solid samples and carried into the
injection box.
In either mode, the unit is operated by NSX-2100 application software settings to
measure samples. Measurement procedures are different depending on modes.
Refer to “5. Measurement” for details.
4-2. ASC-270LS Start
For the functions described in 4-3 or later, units and applications except ASC-270LS are
required. Start the unit and the application as follows.
(1) Turn on ASC-270LS power switch.

→ ASC-270LS unit checks the HOME position.
(2) Turn on HF-210 power switch.

Refer to HF-210 instruction manual to start HF-210.
(3) Turn on the power switch of a PC.

(4) Start NSX-2100 application software.
Double-click “NSX-2100” icon of the desk top or start the application from
Windows menu.
“Logon” window is opened.
ASC-270LS
4-2 Section 4: ASC-270LS Functions
(5) User ID: Input NSX-2100. Password: No input

Click [OK] button to display the window.
* By unchecking “Connected to NSX-2100”, only the application starts without
communication with the units.
POINT
Connect the unit for measurement. After starting the application, click “File”
and “Connect” of the menu. After selecting a port, click [Open Port] button.
By communicating with ASC-270LS, the front LED lights and the mode is AUTO.
ASC-270LS
4-3. Other Tools
Table 4-1. Other Tools Functions

No. Items Functions
1 Manual/Automatic Set a boat to the injection box with “Manual/Automatic”.
boat setting * Only “Manual” for the liquid sample mode
2 Change of the When changing the solid or liquid sample mode, the
chuck or the change procedure is displayed.
syringe head and
the tray
4-3-1. Manual/Automatic Boat Setting
CAUTION
Before operation, check that a sample boat is not in the sample injection
box. The sample boat and the arm mechanical part may break.
WARNING
Never touch the unit during operation. Colliding with the arm mechanical
part causes injuries.
Set a sample boat to the sample injection box as follows.

Click “Control”, “Accessories”, “ASC-270LS” and “Boat Setting” of NSX-2100 application
menu or click .
→ The boat setting window is displayed.
Click "Manual setting of the boat" or “Automatic setting of the boat” tab.
ASC-270LS
Window for Setting a Boat Manually
Follow the instructions in the manual boat setting.
(1) Click [Cover Open] button.

→ The sample injection box cover opens. The arm moves to the safe position.
(2) Set a sample boat with quartz wool to the ladle tip in the box.
Fig. 4-1. Manual Setting of the Boat to the Injection Box
(3) Click [Cover Close] button.

→ The arm returns from the wait position. The sample injection box cover closes.
(4) Click [Finish] button.

→The arm moves to the home position.
ASC-270LS
Window for Setting a Boat Automatically
Follow the instructions in the automatic boat setting.
(1) Set a sample boat with quartz wool to the tray No.1 for solid samples.
(2) Click [Start] button.

→ After checking the chuck and the boat in the sample injection box,
the boat on the tray No.1 is picked and set to the sample injection box.
(3) Click [HOME] button.
ASC-270LS
4-3-2. Change of the Chuck or the Syringe Head and the Tray
WARNING
mechanical part causes injuries. Do not put a finger into the
injection box.
POINT
Change each combination (the chuck head and the solid sample, the
syringe head and the liquid sample tray).
→ When the combination is different, the unit does not operate.
The change procedure is as follows.

Click “Control”, “Accessories”, “ASC-270LS”, and “Chuck/Syringe Head Change” of
NSX-2100 application menu or click .
→ “Chuck/Syringe head replace” window opens.
Replacement of Chuck with Syringe

→ The arm moves to the change position.
(2) Remove the chuck head.
(3) Click [Chuck head removal finish] button.

→ S-axis lowers.
ASC-270LS
(4) Set the syringe head and change the tray.

→ Refer to “3-4-4-1 to 3-4-4-5” for the details.
(5) Click [Syringe head setting finish] button.

→ The arm moves to the home position.
Replacement of Syringe with Chuck

(2) Remove the syringe head.
(3) Click [Syringe head removal finish] button.
→ S-axis rises.
(4) Set the chuck head and change the tray.
→ Refer to “3-4-4-1 to 3-4-4-5” for the details.
(5) Click [Chuck head setting finish] button.

4-3-3. Syringe Washing
Remove a syringe to wash it every day. Check plunge deterioration.

When it is deteriorated, change it with new one.
CAUTION
Remove a syringe to wash it every day.
ASC-270LS
WARNING
mechanical part causes injuries. Do not put a finger into the
injection box.
The operation is partially same as “4-3-2. Change of the Chuck or the Syringe Head and
the Tray”.
Click “Control”, “Accessories”, “ASC-270LS”, and “Chuck/Syringe Head Change” of
NSX-2100 application menu or click .

→ “Chuck/Syringe head replace” window opens.
Replacement of Syringe with Chuck

(2) Remove the syringe head to wash a syringe. You can remove a syringe without
removing the head.
(3) Set the removed syringe head. When only the head has been removed, return it.
→ Refer to “3-4-4-1 to 3-4-4-2” for the details of head or tray setting.
(4) Click [Cancel] button.

ASC-270LS
Section 5: Measurement 5-1
Section 5: Measurement
This section describes the measurement method with Model ASC-270LS.
CAUTION
Operate the unit in the person’s presence.
5-1. Start
CAUTION
After adjusting the syringe suction and injection positions or the chuck
release and hold positions, start ASC-270LS automatic operation.
Misalignment causes the unit, syringe, and chuck breakage.
(1) Turn on ASC-270LS front power switch.

→ ASC-270LS unit checks the HOME position.
(2) Turn on HF-210 and detector power switches.
Refer to their instruction manuals to start them.
(3) Turn on the power switches of PC, monitor, and printer.
(4) Start NSX-2100 application software. Double-click “NSX-2100” icon of the desk top
or start the application from Windows menu.
→ “Logon” window is opened.
(5) User ID: NSX-2100. Password: No input. Click [OK] button to display the main
window.
* By unchecking “Connected to NSX-2100”, only the application starts without
communication with the unit.
POINT
Connect the software to units to measure.
After starting the application, click “File” and “Connect” of the menu.
After selecting a port, click [Open Port] button.
By communicating with ASC-270LS, the front LED lights and the mode is AUTO.
ASC-270LS
5-2 Section 5: Measurement
5-2. Setting
ASC-270LS runs different “Type” of measurements continuously.
5-2-1. Schedule Setting and Measurement Flow
The basic measurement flow is as follows.
New schedules Existing schedules

(Edit is required.) (Edit is not required.)
5-2-2. New Schedule 5-2-3. Open Schedule 5-2-3. Open Schedule

Preparation
Set up new schedule items Select schedule file
5-2-4. Schedule Edit
5-3. Measurement Preparation
5-4. Measurement Start
Edit schedule during measurement. (if necessary)
Change measurement conditions during measurement. (if necessary)
Measurement Finish
Edit measurement results. (if necessary)
5-5. Shutdown
ASC-270LS
5-2-2. New Schedule Preparation
The NSX-2100 program is designed for users to create new schedules by using
templates prepared by the manufacturer, distributor or, unit administrator.
Therefore “New Schedule” is normally not required in daily routines.
(1) Click “Schedule Explorer”. (If “Schedule Explorer” is not displayed, click “Schedule
Explorer” on the lower left or, select “View” – “Explorer” – “Schedule” from the
menu.)
(2) Double-click “Group” on the schedule explorer left to display the folder.
(3) Right-click “Folder” and select “New” and “Schedule”.
→ “New Schedule” window is displayed.
3
4 5
6
7 8
1. Schedule Name: Input a schedule name.

2. System: “AQF” for the sample prep-station
“NSX” for the elemental analyzers
To connect ID-210 unit, refer to the instruction manual.
3. Electric Furnace: HF-210 is already selected.
4. Use Detector: When the system is AQF, detectors can not be selected.
When the system is NSX, check “MCD-210”, “ND-210”, or
“SD-210”. (Check units connected.)
5. Measurement Mode: Select a measurement mode when “System” is “NSX”.
6. Accessory: Check ASC-270LS. When “System” is “AQF”, select GA-210.
(Check units connected.)
7. Syringe Type: Select 25, 50, or 100μL.
Standard setting: Chuck or syringe selection Selected setting is default.
B Disposal: Check the box to be default.
8. Units: Select CM-210 or an absorption tube type.
ASC-270LS
(4) Click [OK] button.

→ The schedule is displayed.
5-2-3. Open Schedule
POINT
By using an existing schedule, measurement can be started without
editing schedules.
Opening a Schedule from the Navigation Bar
(1) Click “View” – “Explorer” – “Navigation” of the menu.

→ The navigation opens.
(2) (i) To open existing schedules
Select a schedule for measurement at “Schedule for a template” in “Template
Setting” window. Check that a schedule name (such as a template) is displayed and
click [Open] button.
(ii) Copy and open an existing schedule.

Select a schedule of the copy source. The selection method is same as (i).
Click [Open New Schedule] button on “Open Schedule” window.
The original schedule (template) is copied and the schedule is opened.
(The opened schedule is saved to the folder selected in “Work folder”.)
The year and date, a three-digit serial number and the template name are
assigned to the copied schedule.
ASC-270LS
Opening a Schedule from Schedule Explorer
(1) Click “View” – “Explorer” – “Schedule” from the menu.

→ “Schedule Explorer” opens.
(2) Click “Folder” in the left tree. (Only when there are several folders)
→ The schedule is displayed in the right.
(3) Double-click a schedule file under “Name”.
5-2-4. Schedule Edit
Edit schedules for measurement.

(1) Click “View” – “Explorer” – “Schedule” of the menu and double-click a schedule.
→ The schedule is displayed.
(2) Click items which need to be edited.

* ASC-270LS parameter settings are described in “5-2-5. Parameter Setting” in
the next page.
* Prepare step list in the schedule window to set information required for
measurement. The details are described in the following sections.
5-2-7. Selecting “Standby” for “Type” (Boat prebaking and others)
5-2-8. Selecting “Blank” for “Type” (Blank measurement)
5-2-10. Selecting “Standard” for “Type” (Calibration curve preparation)
5-2-11. Selecting “Sample” for “Type” (Sample measurement)
* For “ASC-270LS” and “GA-210”, “Blank” and “Standard” are not used in “Type”.
ASC-270LS
5-2-5. Parameter Setting
Parameters for Liquid Samples
(1) Click [Parameter] button of a schedule.

(2) Select “ASC-270LS LS” from the left unit list.
→ The following window is opened.
(3) Set each parameter.

* Refer to “Table 5-1” for setting contents.
ASC-270LS
Table 5-1. Parameter Settings for ASC-270LS (Liquid Samples)

Items Contents Input ranges Units
Common Parameters
Syringe Type＊1 Syringe capacity Set the syringe size selected when μL
indication preparing a schedule.
25, 50, 100
Injection Position Injection positions Horizontal
Liquid Type Select liquid Water

types.
Sampling Parameters
Sampling height Sample suction Needle tip height from the bottle mm
height bottom
0 to 40 3
Solvent Flush Solvent flush Not used for ASC-270LS μL
volume suction volume
Solvent Flush/ Solvent flush / Not used for ASC-270LS μL/sec

Spike Std absorption spike standard
rate suction speed
Solvent Air volume Solvent air Not used for ASC-270LS μL

volume
For sucking air
before solvent
flush
Pre Air volume Pre Air volume 25μL: 0 to 3 3 μL

For sucking air 50μL: 0 to 6 6
before sucking 100μL: 0 to 12 8
samples
Post Air volume Post Air volume 25μL: 0 to 3 0 μL

For sucking air 50μL: 0 to 6 0
after sucking 100μL: 0 to 12 0
samples
Air removal times*2 Air removal times 0 to 10 0 Reps
Air absorption rate Suction rate 25μL: 0.4 to 12.5 10 μL/sec

(mL/min) 50μL: 0.4 to 25.0 20
100μL: 0.4 to 50.0 20
ASC-270LS

Air discharge rate Discharge rate 25μL: 0.4 to 12.5 12.5 μL/sec
50μL: 0.4 to 25.0 25.0
100μL: 0.4 to 50.0 50
Air removal volume Air removal 10 to 50 %
volume (Ratio to the syringe volume) 30
Injection
Injection port height Injection positions 0 to 40 0 mm
Washing Parameters
Washing solution Suction rate 25μL: 0.4 to 12.5 10 μL/sec
absorption rate (mL/min) 50μL: 0.4 to 25.0 20
100μL: 0.4 to 50.0 20
Washing solution Discharge rate 25μL: 0.4 to 12.5 12.5 μL/sec
discharge rate 50μL: 0.4 to 25.0 25.0
100μL: 0.4 to 50.0 50
Wash height Washing solution Needle tip height from the wash mm
suction height bottle bottom
0 to 50 3
Washing solution Suction volume 10 to 50 (ration to the syringe %
absorption volume capacity) 30
Wait Time after Fill Wait time 0 to 10 1 sec
Air Fill Rate Air suction rate 25μL: 0.4 to 12.5 10 μL/sec
50μL: 0.4 to 25.0 20
100μL: 0.4 to 50.0 20
Rinse Parameters＊3
Rinse absorption Suction Rate 25μL: 0.4 to 12.5 10 μL/sec

rate (mL/min) 50μL: 0.4 to 25.0 20
100μL: 0.4 to 50.0 20
Rinse discharge Discharge rate 25μL: 0.4 to 12.5 12.5 μL/sec
rate 50μL: 0.4 to 25.0 25.0
100μL: 0.4 to 50.0 50
Rinse solution Suction volume 10 to 50 (ration to the syringe %
absorption volume capacity) 30
Wait Time after Fill Wait time 0 to 10 1 sec
ASC-270LS

Air Fill Rate Air suction rate 25μL: 0.4 to 12.5 10 μL/sec
50μL: 0.4 to 25.0 20
100μL: 0.4 to 50.0 20
Needle tip wash times
times before rinse Times of needle tip 0 to 10 1
wash
Needle tip wash Wash volume 10 to 50 (ration to the syringe %

volume before rinse capacity) 30
Other
Precedent rinse Rinse with the Enable or Disable
next sample * It is valid only when “Automatic
during step operation” is checked in “Rule”
measurement window.
* When “Enable” is set, the next
step during measurement can not
be changed.
Multi Injection times Repetitive Not used for ASC-270LS Reps
discharge times 1 to 9 (Only for the vertical
furnace)
* The function of several injections
for one measurement It is
particularly useful when TRU is
connected.
The underlined values are defaults for new schedule preparation.
Set values by liquid sample properties.
For viscous samples, air bubbles may enter into the syringe or the motor may be locked
at discharge. Change the discharging or sucking speed to proper values.
*1. Syringe sizes are different depending on units and measurements.
*2. Air removal
When taking liquid into a syringe, small air bubbles enter by lifting the plunger.
This function is for removing them from the syringe.
Suction volume is same as sample injection volume.
*3. Rinse
Usually, rinse with sample solution. When “Spike std.” or “Rinse” is set to “Bottle B
setting”, rinse solution (rinse vial position B) is used.
ASC-270LS
Parameters for Solid Samples
(1) Click [Parameter] button of a schedule.

(2) Select “ASC-270LS SS” from the left unit list.
→ The following window is opened.
(3) Set each parameter.

* Refer to “Table 5-2” for setting contents.
Table 5-2. Parameter Settings for ASC-270LS (Solid Samples)

Waiting time after Wait time 0 to 999 1 sec
closing a sample
injection box (sec)
*1
The underlined values are defaults for new schedule preparation.

Setting of wait time after closing the sample injection box:
When the sample injection box opens and closes, the detector baseline sometimes
fluctuates. Set the wait time to stabilize. (Preset values are saved each schedule.)
* Time from closing the sample injection box to ABC operation.
ASC-270LS
Air Segment Use Examples
Air Segment: Air for separating samples

This function prevents liquid from contacting the syringe plunger end and samples
from mixing with solvents or distilled water used for solvent flush.
What is Air Segment?

The function is for discharging samples completely with air.
Use it with “Solvent Flush”.
Combination examples:
1) Standard setting for the horizontal furnace
Pre Air + Sample
2) Setting for pushing out “OIL” with solvents
Solvent Air (unused) + Solvent Flush (unused) + Pre Air + Sample
3) When setting all functions
Solvent Air (unused) + Solvent Flush (unused) + Pre Air (5μL) + Sample (10μL) +
Post Air (3μL)
(Fig. 5-1 shows the window displayed when pressing the button, “ASC –Fill” in the
schedule.)
POINT
“Solvent Air” and “Solvent Flush” are not used for ASC-270LS.
Set sample volume at “Volume” in a schedule. In ASC-270LS parameter,
set it so that it should be under the selected syringe capacity.
Sample volume maximum = Syringe Capacity – (Total volume of Air
Segment + Solvent Flush)
Click of ASC- Fill.
→ The details of injection volume

is displayed.
Fig. 5-1. Air Segment Example
ASC-270LS
5-2-6. Rule Setting
(1) Click [Rule] button of a schedule.
→ “Rule” window is displayed. Display contents are different depending on

detectors.
* Continuous measurement can be run by ASC-270LS.

While “Automatic step operation” is checked, continuous measurement is run
automatically step by step on the “Schedule”.
By unchecking “Automatic step operation”, operation is stopped each step.
Click [Start] button to resume measurement.
* By setting “Precedent rinse” to “Enable” while “Automatic step operation” is
checked, the next step can not be edited.
ASC-270LS
5-2-7. Selecting “Standby” for “Type”
Prepare step lists for boat prebaking and detector and electric furnace control.
One operation is run every step.
(1) Click or press <Alt>, <E>, and <E> keys sequentially.

→ “Step Editor” window is displayed.
(2) Set “Standby” to “Type” and select “Syringe” or “Chuck” for “SC”.
(3) Set items by referring to the following table. (Display contents are different
depending on measurement types.)
ASC-270LS
Table 5-3. Standby Input Items

Types Contents
Boat Prebake (When Set the following items and prebake a boat.
“Syringe” is selected.) 1. Times: Set 1 to 99.
2. ABC: Select ABC program number.
3. B No.: Unused
Boat Prebake (When Set the following items and prebake a boat.
“Chuck” is selected.) 1. Times: 1 Fixed
2. ABC: Select ABC program number.
3. B No.: Specify a boat position (sample tray No.).
4. B Disposal: Check it to dispose of a boat automatically.
5. Not Used: Check it when setting a sample boat
manually to the sample injection box.
Heater Standby For switching the electric furnace heater control.
Heater On The cooling unit is turn On and Off by Heater button on
PC.
Heater Off
Wait By setting waiting time (0 to 999 min. 0 to 59 sec.), the
next step is run after this time.
Set it after heater temperature rise or waiting for detector
stabilization to start the automatic measurement.
Step Break For suspending measurement
Click [Start] button to run the next step.
Gas Valve Off For closing the gas controller valve
Gas Standby For opening the gas controller valve
GA-210 End For finishing GA-210 operation
Processing
Clear of Effluent For clearing the effluent volume counter

Counter
(4) Select and click the appropriate button from the table below.
ASC-270LS
Table 5-4. Buttons in Step Editor

Buttons Contents
Add Add a step to the bottom of the step list.
Insert Insert a line above a step with a cursor.
Insert Below Insert a line below a step with a cursor.
Constant Auxiliary function for inputting the same contents repetitively
The following window is displayed.
1. Set a boat number of the start (left) and the end (right) to “ASC-
270LS B No.”
2. Set “Repeat”.
3. Click [Add] or [Insert] button.
4. By checking “Increment by pressing [Add] button”, only [Add]
button is active, the cursor moves to the bottom step of the
added schedule, and 1 is added to “B No.” in “Step Editor”
window.
Setting example 1
To repeat each measurement of the bottle 1 to 3 two times, set
the items by the above window and click [Add] button.
Setting example 2
After checking “Increment by pressing [Add] button” and clicking
[Add] button, click [Constant] button. Continuous input is easier
by the count-up of the start bottle number.
Overwrite The step with a cursor is overwritten.
(5) For another control, repeat (3) to (4).

(6) Change “Type” for measurement.
Proceed to “5-2-8. Selecting “Blank” for “Type” ” (When using MCD, ND, SD, or ID),
“5-2-10. Selecting “Standard” for “Type” ” (When using MCD, ND, SD, or ID), or “5-2-
11. Selecting “Sample” for “Type”.
(7) Click [Close] button to close “Step Editor” window.
ASC-270LS
5-2-8. Selecting “Blank” for “Type”
Prepare a step list for blank measurement. One measurement is run every step.
* “Blank” in “Type” is not used for ASC-270LS and GA-210.

(2) Set “Blank” to “Type”.
depending on measurement types.
Table 5-5. Input Items for Blank Measurement

Items Contents Input Units
ranges
ABC Click of ABC program No. *1 1 to 999
ASC: Set the position of a sample boat on the tray. 1 to 40

B No.
Not Used Check this item to operate the unit only by ABC program. (No sample
boat transfer in between the tray and the sample injection box)
Type System blank: Blank coming from the unit, gas, and a boat Click [Rule]
button in the schedule and select a calculation method from “Blank use
method”.
Solvent Blank 1, 2: (It is displayed depending on measurement items.)
For subtracting the dilution solvent blank. Use solvent blank 1 and 2
differently. (Example: Solvent Blank 1 to subtract standard sample from
diluted solvent. Solvent Blank 2 to subtract sample from diluted solvent)
ASC-270LS
Click [Rule] button in the schedule and select each blank calculation
method from “Blank use method”.
Activated carbon blank: (AOX-1 or AOX-2 are displayed) For
subtracting activated carbon blank
Blank of activated carbon washed with KNO3 is measured and
subtracted from sample measurement values.
Solvent Conditioning, Conditioning: For combusting solvent to remove
impurities in a pyrolysis tube. Measurement result is excluded.
Measurem TCL (total chlorine) or TS (total sulfur),
ent mode others
Volume Sample volume *2 0 to 9999.999 μL, mL
mg
Click of “ABC” right in “Step Editor” window to select a program number. Refer to
“5-2-9. Programs” for details.
*2. Input “Volume”.
CAUTION
Sample volume should not be over 30mg or 50μL. When injecting more
than 50μL sample, spread about 20mg quartz wool on a sample boat and
check ASC-270LS combustion conditions. When sample volume is too
large or ASC-270LS program is improper, incomplete combustion may
occur. Change ASC-270LS program depending on sample properties.
(4) Select a button from the following table and click it.
Table 5-6. Buttons in “Step Editor” Window

Buttons Contents
The right window is displayed.
1. Set the boat number of
the start (left) and the
end (right) to “ASC-
270LS B No.”
(5) Repeat (3) and (4) by measurement times.

ASC-270LS
(6) To measure by other types, change “Type”.

Proceed to “5-2-10. Selecting “Standard” for “Type” ” or “5-2-11. Selecting “Sample”
for “Type” ”.
ASC-270LS
5-2-9. Programs
5-2-9-1. Import of Combustion Condition (ABC Program)
When installing NSX-2100 application software newly, select and import ABC program.
The following describes the procedure to import combustion conditions (ABC Program).
(1) Click of [ABC No.] right in a schedule.
→ “ASC-270LS ABC Program” window is displayed.

(2) Click [Option] button. When other buttons are inactive, click [Import] button.
ASC-270LS
(3) “Open” window is displayed. Click a detector or mode folder and [Open] button.
(4) Select a program and click [Open] button. Two or more files can be selected with
[Shift] or [Ctrl] button and a mouse. (Display contents are different depending on
detectors or measurement modes.)
(5) “ASC-270LS ABC Program” window is displayed and the selected program is
imported. (When the same program number is listed, another number is allotted.)
(6) To close “ASC-270LS ABC Program” window, click [Cancel] button or [×] button of
the upper right.
* In case the window is opened from a schedule, a selected program number is input
into a current step in the schedule by clicking [Select] button.
ASC-270LS
5-2-9-2. Setting and Edit of ABC Program
Set the boat position and time to combust sample by ABC Program of ASC-270LS unit.
(1) Click of [ABC No.] right in a schedule.
→ “ASC-270LS ABC Program” window is displayed.
* For program setting, proceed to (2).
For the addition or edit, proceed to (3).
(2) Click a program and [Select] button. (It also can be selected by double-click.)
→ The window is closed and the selected number is displayed in the step list.
(3) Click [Option] button of the lower left. (When other buttons are inactive)
Click a program to edit, [Edit] button or, [Add] button.
→ “Edit ABC Program” window is displayed.
1
2
3
4
10
11
12
13
5
6
7 8
ASC-270LS
(4) Set or edit the following items.

1. No.: Change the program number.
2. Program Name: Change the program name.
3. Injection Limit: For prevention of the mistakes of program number selection or
sampling volume.
By checking this box and setting maximum sample size, the check window is
displayed at measurement start when sample size inputted in a schedule is
larger than this preset value.
4. ABC Parameter: Preset values can be changed.
Select a boat position and click [Edit] button.
→ “ABC Parameter” window is displayed.
Set “Pos.”, “Wait Time”, and “Speed”. Click [OK] button after the setting.
→ “ABC Parameter” window is closed.
POINT
For wait time at a newly-prepared boat position, 10 seconds are set as the
default. Always set the wait time.
5. Combustion time: The combustion time from the home position to the end
position
6. “The order should be 1st, 2nd, 3rd, …. End, Cool, and Home.”: By checking this
box, the check window is displayed when the position is incorrect.
Click [OK] button and [Sort] button to rearrange the steps in the correct
sequence.
7. Gas Parameters: The following preset values can be changed.
Table 5-7. Titration Parameters

Items Contents (Default values)
Delay Time For setting the delay time from measurement start to detection
start or a larger value than the sum of all boat positions and the
end position waiting time. (120 sec.)
This item is displayed when using a detector, MCD-210.
Ar Time For setting time (30 sec.) from sample boat arrival at the end
position to argon gas flow into an inner pyrolysis tube
O2 Time For setting the time (600 sec.) for flowing oxygen gas through
the inner pyrolysis tube after Ar Time
When measurement ends during O2 Time, argon gas flows
again.
8. Detector Memo: The detector type is displayed.
ASC-270LS
9. Attribute Information: For preventing the program deletion by mistake.

The check box can be checked only when “User ID” is administrator-level.
10. [Add] button: A line is added below the selected line. Set ABC parameters as
the step 4. (When no line is selected, a line is added to the bottom of the
parameter list.)
11. [Delete] button: A selected line is deleted.
12. [Up] and [Down] buttons: For moving selected line.
13. [Sort] button: For sorting “Position” in order of 1st, 2nd, 3rd (in ascending order
of position distance)…END, COOL, HOME.
→ Changed contents are saved and “ASC-270LS ABC program” window is
displayed.
* Click [Cancel] button to return to “ASC-270LS ABC program” window without
saving them.
ASC-270LS
5-2-9-3. Replay
To check combustion parameters, operate selected ABC program.
POINT
Before replay, check the following points.
* Gas flowing
* Removal of a ball joint of a dehydrating tube or an outer pyrolysis tube
(1) Click a program in “ASC-270LS ABC Program” window.
(2) Click [Option] button. (When other buttons are inactive)

(3) Put a sample on a sample boat and set it to the sample inlet box.
(4) Click [Replay] button.
→ The check window is opened.
(5) Click [Yes] button.
→ ASC-270LS operates by the selected program.
* When HF-210 and ASC-270LS are not Ready, the next operation can not be run.
* Click to display ASC-270LS condition.

(6) To close “ASC-270LS ABC Program” window, click [×] button of the upper right.
ASC-270LS
5-2-9-4. Buttons of ABC Program Window
The button functions except “Import”, “Edit”, and “Replay” are as follows.
1. [Add]: For preparing a new ABC program. Set each item like [Edit]. (Refer to “5-2-9-2.
Setting and Edit of ABC Program”.)
2. [Delete]: For deleting ABC program of selected numbers. Click a program and
[Delete] button.
It can not be deleted while “Read-only” is checked. Click [Edit] button and uncheck
“Read-only”.
3. Set as Default: A selected ABC program is set as default. When preparing or

inserting a new step in a schedule, this number is displayed as default.
* When “Type” of a step is “Sample”
4. Set as Default Prebake: A selected ABC program is set as default prebake. When
preparing or inserting a new step in a schedule, this number is displayed as default.
* When “Type” of a step is “Standby” (Boat Prebake)
5. [Export]: For outputting ABC program of a selected number in xml format.
The output is the specified folder at save. Without change at save, it is “ABC Program”
folder in the folder with an installed NSX-2100 application program.
6 [Cancel]: For closing “ASC-270LS ABC Program” window.
ASC-270LS
5-2-9-5. Import of Sampling and Injection Conditions (ASC Program)
Import sampling and injection conditions as follows.
(1) Click of [ASC No.] right in a schedule.

* It is valid only when “SC” is “Syringe”.
→ “ASC-270LS ASC Program” window is displayed.
(2) Click [Option] button. When other buttons are inactive, click [Import] button.
(3) “Open” window is displayed. Click a detector or mode folder and [Open] button.
ASC-270LS
(4) Click a program and [Open] button. (Display contents are different depending on
detectors or measurement modes.)
(5) “ASC-270LS ASC Program” window is displayed and the selected program is
imported.
(When the same program number is listed, another number is allotted.)
(6) To close “ASC-270LS ASC Program” window, click [Cancel] button or [×] button of
the upper right.
* In case the window is opened from a schedule, a selected program number is input
into a current step in the schedule by clicking [Select] button.
ASC-270LS
5-2-9-6. Setting and Edit of ASC Program
Set the speed of sampling or injection, wait time, wash times, and rinse times by ASC
program function.
(1) Click of [ASC No.] right in a schedule.

→ “ASC-270LS ASC Program” window is displayed.
* For program setting, proceed to (2).

For the addition or edit, proceed to (3).
(2) Click a program and [Select] button. (It also can be selected by double-click.)
→ The window is closed and the selected number is displayed in the step list.
(3) Click [Option] button of the lower left. (When other buttons are inactive)
Click a program to edit, [Edit] button or, [Add] button.
→ “Edit ASC-270LS Program” window is displayed.
1
2
3
(4) Set or edit the following items.

1. Program No. : Change the program number.
2. Program Name: Change the program name.
ASC-270LS
3. Sampling
Fill Rate: Select the syringe suction speed from the drop-down list.
Post Fill Delay: Set the wait time until the next operation after the suction.
4. Injection
Inj. Rate: Select the syringe injection speed from the drop-down list.
Post Inj. Delay: Set the wait time until the next operation after the injection.
5. Wash times: Set syringe wash times.
6. Rinse times: Set syringe rinse times.
7. Attribute Information: Click the check box to prevent program deletion.
→ Changed contents are saved and “ASC-270LS ASC program” window is
displayed.
＊ Click [Cancel] button to return to “ASC-270LS ASC program” window without
saving them.
5-2-9-7. Buttons of ASC-270LS ASC Program Window
The button functions except “Import” and “Edit” are as follows.

1. [Add]: For preparing a new ASC program. Set each item like [Edit]. (Refer to “5-
2-9-6. Setting and Edit of ASC Program”.)
2. [Delete]: For deleting ASC program of selected numbers. Click a program and
[Delete] button.
It can not be deleted while “Read-only” is checked. Click [Edit] button and uncheck
“Read-only”.
3. Set as Default: A selected ASC program is set as default. When preparing or
inserting a new step in a schedule, this number is displayed as default.
* When “Type” of a step is “Sample”
4. [Export]: For outputting ASC program of a selected number in xml format.
The output is the specified folder at save. Without change at save, it is the folder
with an installed NSX-2100 application program.
5. [Cancel]: For closing “ASC-270LS ASC Program” window.
ASC-270LS
5-2-10. Selecting “Standard” for “Type”
Prepare a step list for calibration curve preparation. One measurement is run every step.
* “Standard” in “Type” is not used for ASC-270LS and GA-210.

(2) Set “Standard” to “Type”.
depending on measurement types.)
Table 5-8. Standard Input Items
Items Contents Input Units
ranges
ABC Click of ABC program No. *1 1 to 999
ASC: B No. Set the position of a sample boat on 1 to 40

the tray.
Not Used Check this item to operate the unit only by ABC program.
Check it when measuring volatile liquid standard samples.
No sample boat transfer between the tray and the sample injection
box
Type Calibration curve: Measure standard samples to prepare
calibration curves.
System Check, Cell Check: Refer to MCD-210 Operation Manual for
the horizontal furnace.
Calib. ID Generally leave blank.
ASC-270LS
Input it when preparing several calibration curves from the result

of standard sample measurement run with one schedule. To use
the inputted ID, select the ID in the schedule window.
(Usually leave it blank. “Unnamed”is displayed in “Calib. ID” of
the standard sample measurement result window.)
By selecting a calibration ID which is not in a schedule,
concentration is not calculated.
Measurement TCL (total chlorine) or TS (total sulfur), others
mode
Volume Standard sample volume *2 0 to μL, mL,mg
9999.999
Concentration Concentration of standard sample 0 to mg/L, g/mL,
9999.999 ppm,ppb, ppm
(w/w), ppb (w/w)
Density It can be input by selecting a w/w 0.0001 to
unit. 9.9999
Mass For standard samples g, ng*3
It is calculated automatically by
input “Volume” and “Concentration”.
*1. Click of “ABC” right in “Step Editor” window to select a program number.
Refer to “5-2-9-2. Setting and Edit of ABC Program” for details.
CAUTION
When sample volume is too large or ASC-270LS program is improper,
incomplete combustion may occur. Change ASC-270LS program
depending on sample properties.
*3. Click [Rule] button to change “Unit” in “Standard”.
ASC-270LS
Buttons Contents
The right window is displayed.
1. Set the boat number
of the start (left) and
the end (right) to
“ASC-270LS B No.
(5) Repeat (3) and (4) by measurement times.

(6) To measure by other types, change “Type”.
Proceed to “5-2-11. Selecting “Sample” for “Type” ”.
ASC-270LS
5-2-11. Selecting “Sample” for “Type”
Prepare a step list for sample measurement. One measurement is run every step.

(2) Set “Sample” to “Type” and select “Syringe” or “Chuck” for “SC”. Display contents
are different depending on detectors.
depending on measurement types. )
ASC-270LS
Table 5-10. Input Items for Samples

Items Modes Contents Input ranges Units
Type Common AQF: “Abs. Injection”, “Abs. Inj.&Col”, “Abs. Collection”,
“External Inj. 1 to 6 ”.
NSX: Sample, Standard check
Measurem Common AQF Fixed
ent mode NSX: Depending on detectors
Sample ID Common Input a sample ID.
Repetition Common Set repetitive times. 1 to 5 Times
times
Volume Liquid Input liquid sample volume*1. 0 to 100% of μL
samples Select the unit. a syringe size
Solid Input solid sample volume*1. 0 to 9999.999 μL
samples Select the unit. mg
ABC Common Click of ABC program No. *2 1 to 999
B No. Liquid Set the position of a vial on the tray. 4mL: 1 to 84

samples 2mL: 1 to 120
Solid Set the position of a sample boat on 1 to 49
samples the tray.
ASC Liquid ・Click to select ASC program number. *3
samples Set the parameters of sampling, injection, wash, and rinse.
・ Manual operation procedure*4
Solid ・Manual operation procedure*4

samples
・Boat disposal selection*5
ASC-270LS
CAUTION
When sample volume is too large or ASC-270LS program is improper,
incomplete combustion may occur. Change ASC-270LS program
depending on sample properties. Sample volume should be up to 30mg
or 50μL. When the total of liquid sample injection volume is over 110% of
syringe capacity, “Fill” numbers in a step list turn red. (Continuous
measurement can not start. By step edit during continuous measurement,
the measurement stops at this step.)
When injecting more than 50μL liquid sample, spread about 20mg quartz
wool on a sample boat and check ASC-270LS program (combustion
conditions).
*2. Click of “ABC” right in “Step Editor” window to select a program number.
*3. Click of “ASC” right in “Step Editor” window to select a program number.
*4. Click “Manual” in “Step Editor” window to use manual function. Refer to “5-4-3.
Manual Operation during Measurement by Schedule” for details.
*5. Click “B Disposal” in “Step Editor” window to use boat disposal function. Refer to “5-
4-4. Boat Disposal after Measurement by Schedule” for details.
Buttons Contents
Insert Below Insert a line below a step with a cursor.
ASC-270LS

The following window is displayed.
1. Set the boat number of the start (left) and the end (right) to “ASC-
270LS B No.”
4. By checking “Sample ID appending Bottle No.”, a bottle number is
added to the sample ID bottom.
5. By checking “Increment by pressing [Add] button”, only [Add]
button is active, the cursor moves to the bottom step of the added
schedule, 1 is added to “B No.” in “Step Editor” window.
Setting example 1
To repeat each measurement of the bottle 1 to 3 two times, set the
items by the above window and click [Add] button.
(5) Repeat (3) and (4) above by measurement times.
ASC-270LS
5-3. Measurement Preparation
Prepare ASC-270LS and other units before measurement.
CAUTION
Properly set the syringe head, the mircrosyringe, vials, and the tray unit.
POINT
When sampling highly volatile liquid, use a gastight microsyringe.
Previously set a sample boat to the sample inlet box. Set high volatile
sample just before measurement. Pour liquid up to 80% not to
contaminate standard sample or sample with a septum.
 Liquid: Quartz boat/ solid: ceramic boat or quartz boat
 Sample boat prebake (for liquid or solid samples)
 Manual setting of a sample boat to the sample inlet box (for liquid or solid
samples)
 Change of the sample injection box septum (for liquid sample measurement)
 Microsyringe wash (for liquid sample measurement)
 Washing solution and sample setting (for liquid sample measurement)

1. Pour washing solution into an exclusive vial and set it to the position.
2. Set an empty vial for effluent to the position.
3. Generally empty the vial for effluent before measurement. When the volume is
over, measurement suspension is indicated.
To use the effluent counter, click “Control”, “Accessories”, “ASC-270LS”, “LS”,
and, “Options”.
ASC-270LS
To clear the effluent counter, click “Control”, “Accessories”, “ASC-270LS”, “LS”,

and “Clear of effluent counter”.
It also can be set in a step.
4. Place vials with sample set in a schedule to the position on the tray.
5-3-1. Gas Leak Check
Refer to “Gas Leak Check” of the operation manual for details.
5-3-2. Heater
Click [Heater ON] button of the navigation bar or of the toolbar.

→ The check window is opened. Click [OK] button.
(To turn off the heater switch, click of the toolbar.)
To automate this operation, prepare a step list with “Heater ON” selected for “Type” by
referring to “5-2-7. Selecting “Standby” for “Type”.
5-3-3. Prepare Button
Click [Prepare] button of a schedule.

→ Schedule parameters are transmitted to the system and measurement
preparation finishes.
ASC-270LS
5-3-4. Detectors
Prepare a detector by referring to instruction manuals of detectors.
5-3-5. Sample Boat Prebaking
Contamination causing measurement value fluctuation may be adherent to a sample

boat. To remove this blank, prepare sample boats and prebake them before sampling.
CAUTION
If sample boats are chipped or cracked or heavily contaminated, do not
use them. They may break during sample boat operation or combustion.
POINT
To prevent contamination, handle sample boats with clean tweezers
(stainless). Do not touch them with hands or place them directly on a
table.
(1) When a schedule is not open, click “Open Schedule” in the navigation and [Open
new Schedule] button.
→ A new schedule is displayed.
(2) Check that “Boat Prebake” is indicated in “Item”.

To add a new boat prebake, click ▼ to select “Standby” and “Boat Prebake”.
To insert a step, click . Refer to “5-2-7. Selecting “Standby” for “Type” ” for
details.
(3) Change ABC Program No.. Click of ABC No. to select “Prebake”.
* For ABC program setting details, refer to “5-2-9. Programs”.
ASC-270LS
For the solid sample mode, select “Chuck” for “SC” and set sample boats to the tray
with tweezers. Proceed to the procedure (5). For the liquid mode, proceed to (4).
CAUTION
part causes injuries. Do not put a finger into the sample injection box.
(4) Set a sample boat to ASC-270LS sample injection box with tweezers.
* To set a sample boat manually, refer to “4-3-1. Manual/Automatic Boat Setting”.
* The boat also can be set by clicking “Manual” of “ASC”. Refer to “5-4-3. Manual
Operation during Measurement by Schedule” for details.
(5) When [Start] button flashes after clicking [Prepare] button, click it.
→ ASC-270LS operates and prebaking set in a schedule is run.
* To check ASC-270LS operation, click or “View” and “Accessories” from the

menu to open “Accessories” window.
(6) Boat prebaking (set in a schedule) is run automatically.
* By checking “Manual” in a step list, the unit is in a standby state after one
prebaking (4 to 5 minutes). Change the boat and click [Start] button again.
* Set the prebaked boat to a glass petri dish with tweezers and place a cover to
prevent contamination.
ASC-270LS
5-4. Measurement Start
For samples which can be measured continuously, refer to “5-4-1. Continuous

Measurement in Liquid Sample Mode” or “5-4-2. Continuous Measurement in Solid
Sample Mode”. For samples which can not be measured continuously or sublimation
samples, refer to “5-4-3. Manual Operation during Measurement by Schedule”.
Select measurement methods by samples.
CAUTION
This sample changer samples liquids and solids. When analyzing liquid
or solid samples, change the head as well as the pyrolysis tube of an
electric furnace by sample composition. (Use a mullite tube for inorganic
solid samples.)
5-4-1. Continuous Measurement in Liquid Mode
WARNIG
POINT
To measure liquid samples continuously, use the following sample boat.
Quartz sample boat for ABC
Parts number: TX2SBT 5pcs/set
This sample boat cannot be put on a solid sample tray and carried with a
chuck head.
(1) Pour sample into a vial.

(2) Set the following items to a schedule (step list).
* Refer to “5-2-11. Selecting “Sample” for “Type” for details.
ASC-270LS
1. Type: Select “Sample”.

2. ID: Input an ID.
3. Mode: AQF; fixed, NSX; Depending on detectors
4. B No.: Specify the vial number.
5. Volume and unit: Input sample volume and select the unit.
6. Repetition: Specify repetition times.
7. SC Hardware: Select the head (syringe) for an operation mode.
8. ABC No.: Select ABC program.
9. ASC No.: Select ASC program.
10. Manual: Check it to suspend automatic measurement for manual injection.
Uncheck it at continuous measurement.
* For manual operation during measurement, refer to “5-4-3. Manual
Operation during Measurement by Schedule”.
(3) Set a schedule (liquid mode parameters).
* Refer to “5-2-5. Parameter Setting”.
(4) Set sample vials to ASC-270LS tray.
Conform B No. to the tray number.
(5) Repeat (1) to (4) to set all sample information to the schedule.
(6) Click [Prepare] button after schedule input.
(7) When the unit is stable and ready for measurement, [Start] button of the toolbar
flashes.
For continuous measurement start or restart, “Setting of a liquid sample boat”
window is displayed. Refer to “4-3-1. Manual/Automatic Boat Setting” for details.
(9) Start measurement.

→ “Measuring” is displayed in “Status” of “Result” in the schedule.
POINT
Click to display ASC-270LS condition. The tray sample boat color
changes as follows by the state.
Aqua: Before measurement
Red : During measurement
Gray : After measurement
(10) After measurement, the buzzer beeps and “Measurement end by AQF” or
“Finished” is indicated in “Status” of “Result” column of the schedule.
→ When the next measurement is ready, [Start] button flashes and measurement
of the next step list starts.
ASC-270LS
* After all operations of step lists in the schedule, ASC-270LS unit stops.
* Click [Cancel] button to suspend the measurement of this step.
(Measurement can be suspended.)
Measurement Suspension
Click [Rule] button of the right top in a schedule and uncheck “Automatic step
operation” checkbox of “Motion” to suspend measurement. Measurement can be
suspended to change parameters or unfinished schedules.
Trouble Occurrence during Measurement
CAUTION
If any problems occur during measurement, click [Stop] button in the
NSX-2100 system program to stop it emergently.
Resolve the cause of the emergency stop and check that the unit is in proper condition.
Measurement can not be continued. Therefore measure with the same schedule from
the beginning.
ASC-270LS
5-4-2. Continuous Measurement in Solid Mode
CAUTION
POINT
For continuous measurement by the sampler, use the following sample
boat.
Ceramic sample boat for ASC and ABC
Parts number: TX3SCY 100pcs/set
Parts number: TX3SCX 10pcs/set
(1) Set a sample to a sample boat.
POINT
To prevent contamination, handle sample boats with clean tweezers
(stainless). Do not touch them with hands or place them directly on a
table. Store it in a glass petri dish when not setting it to ASC-270LS tray
just after weighing.
(2) Set the following items to a schedule (step list).

* Refer to “5-2-11. Selecting “Sample” for “Type” for details.
ASC-270LS
1. Type: Select “Sample”.

2. ID: Input an ID.
3. Mode: AQF fixed, NSX; Depending on detectors
4. B No.: Specify the boat number.
5. Volume and unit: Input sample volume and select the unit.
6. Repetition: Specify repetition times.
7. SC Hardware: Select the head (chuck) for an operation mode.
8. ABC No.: Select ABC program.
9. B Disposal: Check it to dispose of boats after measurement.
* Refer to “5-4-4. Boat Disposal after Measurement by Schedule”.
10. Manual: Check it to suspend automatic measurement for manual injection.
* For manual operation during measurement, refer to “5-4-3. Manual Operation
during Measurement by Schedule”.
* By connecting a balance with communication functions to a PC, weighed sample
size can be imported.
Refer to “3-9. Balance Connection” in HF-210 instruction manual.
(3) Set a schedule (solid mode parameters).

* Refer to “5-2-5. Parameter Setting”.
(4) Set sample boats to ASC-270LS tray with tweezers.
Conform B No. to the tray number.
(5) Repeat (1) to (4) to set all sample information to the schedule.
(6) Click [Prepare] button after schedule input.
(7) When the unit is stable and ready for measurement, [Start] button of the toolbar
flashes.
* At the solid sample mode, “Boat check in the injection box” window is displayed.
It is displayed at the first start of continuous measurement.
(9) Sample injection box boat check
Check that no boat remains in the box.
CAUTION
Before the next operation, check no sample boat remains in the tray
position for return. The boat and the arm mechanical part may break.
ASC-270LS
When a boat remains after check, specify the boat return position.
→ Select “Disposal position” or “Boat tray No. 49”.
Click [Start] button.
* Click [Close] button.
(10) Restart measurement by the schedule.
* Click [Cancel] button to cancel measurement start.
POINT
Click to display ASC-270LS condition. The tray sample boat color
changes as follows by the state.
Aqua : Before measurement
Red : During measurement
Gray : After measurement
(11) After measurement, the buzzer beeps and “Measurement end by AQF” or
“Finished” is indicated in “Status” of “Result” column of the schedule.
→ When the next measurement is ready, [Start] button flashes and measurement
of the next step list starts automatically.
* After all operations of step lists in the schedule, ASC-270LS unit stops.
* Click [Cancel] button to suspend the measurement of this step.
(Measurement can be suspended.)
ASC-270LS
Pausing Measurement Sequence
Click [Rule] button of the right top in the schedule and uncheck “Automatic step
operation” checkbox of “Motion” to pause after the current measurement step is finished.
Measurement can be suspended to change parameters or unfinished schedules.
CAUTION
If any problems occur during measurement, click [Stop] button in
the NSX-2100 system program to stop it emergently.
the beginning.
ASC-270LS
5-4-3. Manual Operation during Measurement by Schedule
5-4-3-1. For Liquid Samples
CAUTION
CAUTION
Before the next operation, check no sample boat remains in the tray
position for return. The boat and the arm mechanical part may break.
When “Manual” is checked in a schedule step list, the procedure for manual operation
during measurement is as follows.
(1) Just after schedule start, the following window is displayed.
Click the following button depending on conditions.
1
2
3
To inject sample manually with a syringe, select 1 or 2 in the above window.

When GA-210 has been selected as an accessory, use 1 to 4 depending on absorption
solution setting timing.
[1] button: Boat setting → Sample injection → Absorption solution setting
→ Sequentially run the procedure (2) to (6).
[2] button: Sample injection → Absorption solution setting
[3] button: Absorption solution setting → Boat setting → Sample injection
[4] button: Absorption solution setting → Sample injection
ASC-270LS
(2) The sample injection box opens, the arm moves to the wait position, and it suspends.
The boat setting window is displayed.
(3) Put quartz wool to a prebaked sample boat and set it to the sample injection box.
Hitch the boat to the ladle tip.
Fig. 5-2. Sample Boat Setting
(4) Click [Start] button of the boat setting window. The box closes, the arm moves to the
wait position, and it suspends. The sample injection window is displayed.
(5) Take sample into a microsyringe. (The sample volume set in a schedule)
Inject it into the boat from the sample injection port septum. (Contact the needle tip
to the quartz wool to remove sample.)
Fig. 5-3. Manual Injection
ASC-270LS
(6) Click [Start] button to start measurement.

→ After measurement, “Measurement end by AQF” is indicated in “Status” of
“Result” . When the next measurement is ready, the buzzer beeps and [Start] button
flashes.
ASC-270LS
5-4-3-2. For Solid Samples
Sublimation Sample Measurement
CAUTION
POINT
Sample size change by sublimation affects the results. Measure the
samples by “ASC Manual” without setting a sample boat to the tray.
Input “Volume” after weighing sample and set a sample boat to the
sample injection box.
Set the contents of “5-4-2. Continuous Measurement in Solid Sample Mode” to a

schedule step list.
･ Check “Manual”.
When “Manual” is checked during measurement by schedules, the procedure is as
follows.
(1) Just after schedule start, the following window is displayed.
Click the following button depending on conditions.
1
2
3
4
For liquid sample injection or solid sample setting, select 1 or 2 in the above window.
When GA-210 has been selected as an accessory, use 1 to 4 depending on absorption
solution setting timing.
[1] button: Boat setting → Absorption solution setting → Liquid sample injection
[2] button: Boat setting (solid sample setting) → Absorption solution setting
[3] button: Absorption solution setting → Boat setting → Liquid sample injection
[4] button: Absorption solution setting → Boat setting (solid sample setting)
ASC-270LS
(2) The sample injection box opens, the arm moves to the wait position, and it suspends.
The boat setting window is displayed.
(3) Put quartz wool to a prebaked sample boat and set it to the sample injection box.
Hitch the boat to the ladle tip.
* For “1” and “3” liquid samples
→ Set quartz wool to a sample boat for liquid.
* For “2” and “4” solid samples
→ Set sample to a sample boat for solid.
Fig. 5-4. Sample Boat Setting
(4) Click [Start] button of the boat setting window.

* For “1” and “3” liquid samples
The box closes, the arm moves to the wait position, and it suspends.
The sample injection window is displayed.
* For “2” and “4” solid samples
After the box cover closes, measurement starts.
ASC-270LS
(5) Take sample into a microsyringe. (The sample volume set in a schedule)
Inject it into the boat from the sample injection port septum. (Contact the needle tip
to the quartz wool to remove sample.)
Fig. 5-5. Manual Injection
(6) Click [Start] button to start measurement.

→ After measurement, “Measurement end by AQF” or “Finished” is indicated in
“Status” of “Result”. When the next measurement is ready, the buzzer beeps and
[Start] button flashes.
CAUTION
If any problems occur during measurement, click [Stop] button in the
NSX-2100 system program to stop it emergently.
the beginning.
ASC-270LS
5-4-4. Boat Disposal after Measurement by Schedule
Dispose of sample boats used after measurement.

When “B Disposal” is checked in a schedule step list, dispose of used boats and finish
measurement. The disposal can be set every schedule step.5. Shutdown
(1) Shut down the system by referring to the operation manual.
(2) Turn off ASC-270LS power switch.
(3) Turn off the power switches of other units except the electric furnace. To shut down
the electric furnace and optional units, refer to each instruction manual.
(4) Shutdown of PC and peripherals

1. Select “Shut down” of Windows start menu.
2. Turn off the power switches of a monitor and a printer.
ASC-270LS
Section 6: Troubleshooting 6-1
Section 6: Troubleshooting
The troubleshooting of the hardware or the software when using ASC-270LS unit and
the system program is described in this section.
When troubles are not solved even after checking the following contents, contact local
distributors.
* Only troubleshooting about ASC-270LS unit is described. For troubleshooting about

analyzers, refer to each instruction manual.
CAUTION
Do not check power with wet hands to prevent electric shock.
No Power to ASC-270LS
Causes Countermeasures
□ The power switch of ASC- Turn ON the power switch.
270LS front is not ON.
□ The power connector of Connect the power connector.
ASC-270LS rear is
removed.
□ The power plug is not Connect the power plug firmly.
connected to the outlet.
□ Power is not supplied to Check by connecting another electronic instrument to
the outlet. the same outlet.
□ ASC-270LS power fuse is (1) Remove the fuse holder of the unit back with a
broken. flathead screwdriver.
(2) Check the conduction between both ends with a
tester.
(3) If there is no conduction, change the fuse with new
one.
ASC-270LS
6-2 Section 6: Troubleshooting
No Peak
□ Sample was not injected Check the syringe.
correctly.
□ Carrier gas leak Check gas leak.
Refer to “Gas Leak Check” of the Operation Manual
for details.
□ Sample concentration is Check the peak with a standard sample.
too low for sensitivity.
No Automatic Start Even by Connection to the Analyzer
□ The power switch of ASC- Turn ON the power switch.
270LS front is not ON.
□ The communication cable Firmly insert the signal connector for the main unit
to the horizontal furnace is connection of ASC-270LS rear.
removed. Firmly insert the optional connector of the horizontal
furnace (HF-210).
□ ASC-270LS front LED Click “File” and “Connect” of the menu in NSX-2100
(AUTO) is not ON. application. Click [Open Port] button to connect ASC-
270LS.
By connecting ASC-270LS, the LED (AUTO) of ASC-
270LS front is ON and measurement can be run.
ASC-270LS
Section 7: Error Messages and Measures 7-1
Section 7: Error Messages and Measures

This section describes displayed error messages and measures when troubles occur.
＊ The error messages about ASC-270LS unit are described here. For analyzer error
messages, refer to the instruction manuals.
When errors occur, messages are displayed in PC monitors.
Table 7-1. ASC-270LS Error Messages
ERROR Error messages Countermeasures
No.
21 An invalid command An unknown command was received.
was received. ASC-270LS software version may be old.
After checking the software versions of ASC-
270LS and a PC, contact our local distributor.
22 AUTO/MANUAL A command valid only for AUTO was received
selecting error during manual mode.
ASC-270L software version can be old.
After checking the software versions of ASC-
270LS and a PC, contact our local distributor.
24 Operation start A movement command was received during
command reception movement.
during operation ABC software version may be old.
After checking ABC software and PC software
versions, contact our local distributor.
25 X-axis and Y-axis While Z-axis is lower than the origin, the
move command command was X and Y axes move by 0.5mm or
reception more.
during Z-axis fall While Z-axis is lowered, more than 0.5mm is
unavailable. Move them by 0.5mm or by 0.5mm or
more after raising Z-axis.
27 Tray /headset The combination of the tray or the head set is
attachment error different.
For solid samples, reset the boat tray and the
chuck head. For liquid samples, reset the vial tray
and the syringe head. When the error occurs even
after the reset, contact our local distributor.
28 Start command run After stop command transmission, a start
error command was received without the return to home
position. Run the start command after the return.
ASC-270LS
7-2 Section 7: Error Messages and Measures

No.
29 Teaching data error Teaching data write/read failed. Flushed data
corrupted during write. Write teaching data again.
To prevent the unit break, do not run initial
operation (including power-on/off) before write.
41 No operation No operation parameter command is received,
parameter setting therefore the operation can not be started. Restart
ASC-270LS. If the same error occurs after the
restart, check ASC-270LS and PC software
versions and contact our local distributor.
42 Parameter-related Restart ASC-270LS.
error When the same error occurs even after the restart,
check ASC-270LS and PC software versions and
contact our local distributor.
45 Received command The data line of received commands was over 61
overflow digits. Communication data are wrong. Restart
ASC-270LS. When the same error occurs even
after the restart, check ASC-270LS and PC
software versions and contact our local distributor.
46 Start error with START command was transmitted without
unreceived parameter parameter transmission. Retransmit parameters.
When the same error occurs even after
retransmission, restart ASC-270LS. When the
same error occurs even after the restart, check
ASC-270LS and PC software versions and contact
our local distributor.
47 INIT command Return the axis to the origin before moving the
request axis. When the same error occurs even after that,
check ASC-270LS and PC software versions and
contact our local distributor.
50 Tray number error No specified sample number in the tray
After checking the tray, revise the number.
When the same error reoccurs even after the
revise, restart ASC-270LS. When the same error
occurs even after the restart, check ASC-270LS
and PC software versions and contact our local
distributor.
51 Tray attachment error The tray is different. No tray or an improper tray is
set when moving to specified sample. Set a proper
tray. When the same error occurs even after the
reset, check ASC-270LS and PC software versions
and contact our local distributor.
ASC-270LS

No.
52 X-axis timeout error X axis did not return to the home position within
specified time. Restart ASC-270LS. When the
same error occurs even after the restart, contact
our local distributor after checking ASC-270LS
software and PC software versions.
53 Y-axis timeout error Y axis did not return to the home position within
same error occurs even after the restart, contact
our local distributor after checking ASC-270LS
software and PC software versions.
54 Z-axis timeout error Z-axis did not return to the home position within
same error occurs even after the restart, check
55 S-axis timeout error S-axis did not complete operation within specified
time. Restart ASC-270LS. When the same error
distributor.
56 ABC timeout error ABC did not complete operation within specified
time. Restart ASC-270LS. When the same error
distributor.
57 ABC cover ABC cover did not open or close within specified
open/close timeout time. Restart ASC-270LS. When the same error
error occurs even after the restart, check ASC-270LS
distributor.
58 LIMIT sensor error X-axis or Y-axis sensor was detected.
X-axis or Y-axis Restart ASC-270LS. When the same error
reoccurs even after the restart, check the software
versions of ASC-270LS and PC and contact our
local distributor.
59 LIMIT sensor error The ABC limit sensor was detected. Restart ASC-
ABC 270LS. When the same error occurs even after the
restart, check ASC-270LS and PC software
versions and contact our local distributor.
60 Teaching data error Teaching data write/read failed. Flushed data
corrupted during write. Write teaching data again.
To prevent the unit break, do not run initial
operation (including power-on/off) before write.
ASC-270LS

No.
61 Memory initialization Teaching data range was empty or the contents
were improper at the power-on and the default was
written. The setting value is different, therefore the
adjustment is required. Check ASC-270LS and PC
62 X-axis and Y-axis X and Y axes did not operate at initial
error at initialization operation. (Close ABC cover and run initial
operation.)
(Raise Z-axis above the origin.)
(Close ABC cover and run initial operation.)
63 X-axis and Y-axis ABC cover could not open or close while X and Y
error at ABC cover axes were not in the wait positions. Move them to
open/close the positions to open and close the cover.
64 X-axis and Y-axis While Z-axis is lower than the origin, the
error during Z-axis fall command was X and Y axes move by 0.5mm or
more. More than 0.5mm is unavailable as Z-axis
height. Move them by 0.5mm or by 0.5mm or more
after raising Z-axis.
65 Z-axis fall error No Z-axis fall by trouble occurrence
(While the chuck head is set and ABC cover is
closed, Z-axis did not lower. Open the cover and
lower the axis.)
(No Z-axis fall at the irregular position
It can not fall at ABC top. Move X and Y axes and
lower Z-axis.)
66 Axis operation while No axis operation while origin search is required.
origin search is (X-axis / Y-axis / Z-axis / S-axis)
required Retry axis operation after initial operation.
When the same error occurs even after that, check
67 Axis operation while No axis operation while origin search is required.
origin search is (ABC axis)
required Retry axis operation after initial operation.
When the same error occurs even after that, check
68 Boat detection error 1 A boat could not be checked at the sensor
position. Set a boat to the tray.
ASC-270LS

No.
69 Boat detection error 2 A boat could not be checked at the sensor
position. It may not be in ABC or could not be
chucked. Check that it returned to ABC in a proper
state. When it remains in the box, remove it
manually. When it does not return, remove it while
the electric furnace temperature is lowered.
70 Software LIMIT The axis moves out of the software limit.
The setting value may be wrong.
(X-axis / Y-axis / Z-axis / S-axis moves out of the
software limit.)
Restart ASC-270LS. When the same error occurs
even after the restart, check ASC-270LS and PC
71 Software LIMIT ABC ABC moves out of the software limit.
The setting value may be wrong.
Restart ASC-270LS. When the same error occurs
even after the restart, check ASC-270LS and PC
99 During initialization Please wait for a while.
When troubles are not solved even after checking the following contents, contact our
local distributor.
ASC-270LS
ASC-270LS
Section 8: Maintenance and Inspection 8-1
Section 8: Maintenance and Inspection

The maintenance and inspection to use ASC-270LS safely in the proper conditions are
described in this section. For the maintenance and inspection of the analyzer, refer to
the analyzer’s instruction manual.
8-1. Unit Inspection
8-1-1. Daily Inspection
Table 8-1 shows the daily inspection items.
CAUTION
Always conduct periodical inspection in the specified cycle. Failure to check
the unit can lead not only to reduced performance of the units, but also to
serious accidents.
Table 8-1. Daily Inspection Items

No. Items Contents
1 Unit cleaning Check the unit contamination and clean it if
necessary.
2 Gas leakage check Check the leakage of O 2 and Ar gases with the
flow meter for gas leak check.
3 Sample injection box septum When injecting liquid sample from a septum,
change the septum before measurement once a
day.
4 O-ring of the sample When the O-ring is contaminated or broken,
injection port change it.
5 Tray unit (for liquid or solid Wash the tray unit every 1 to 2 weeks.
samples)
6 Head (syringe/chuck) When contamination is heavy or operation is
slow, clean the head.
7 Syringe Before and after use, wash it with solvent which
solves samples well. Dry the inside with alcohol
after washing.
Always inspect and maintain the needle tip
before measurement.
Check weighing volume every month.
8 Vial (for samples) Always change a septum before measurement.
ASC-270LS
8-2 Section 8: Maintenance and Inspection
No. Items Contents

9 Vial (for wash) Always change a septum before measurement.
Always change wash solution before
measurement.
10 Vial (for waste solution) Always change a septum before measurement.
Always dispose of waste solution before
measurement.
11 Boat (for samples) Check that a sample boat is not contaminated or
devitrified.
Check that quartz wool on a sample boat is soft
and not contaminated.
The details of each inspection procedure are as follows.
Gas Leakage Check
Check that supply gas (O 2 or Ar) does not leak. Refer to “Gas Leak Check” of the
detector operation Manual for details.
(1) Connect the ball joint of the flow meter (optional) for gas leak check to the outlet of
the pyrolysis tube.
(2) Check preset gas flow and the indicated value of the flow meter.
Sample Injection Box Septum Change
Always turn the cap and remove it to change the septum before measurement
Check of the O-ring of the Sample Injection Port
If the O-ring G-50 of the sample injection port is damaged or contaminated, change it
with a new one.
(1) Open the cover of ASC-270LS sample injection box.

* To open and close the sample injection box, refer to “4-3-1. Manual/Automatic
Boat Setting”.
(2) Remove the O-ring with tweezers to change it.
ASC-270LS
O-ring
Fig. 8-1. Change of the O-ring of the Sample Injection Port
(3) Close the cover of ASC-270LS sample injection box.
(4) Check no gas leak from O-ring.

* When gas leaks, check the O-ring is set properly and recheck gas leak.
ASC-270LS
Tray Unit Cleaning
Check tray unit contamination every 1 to 2 weeks and clean it if needed.
CAUTION
When the tray unit is contaminated with sample, immediately clean it.
When it is left contaminated, a vial or a boat is not stored in proper
positions and it may collide with the syringe or the chuck head. The unit
may break at worst.
Syringe Wash
After measurement, always wash a syringe and store it as follows.
CAUTION
After measurement, always wash a syringe. When it is left unwashed, a
plunger adheres to it to put load on the unit at plunger operation.
The unit may break at worst.
(1) Wash the syringe inside with solvent which quite solves the sample adhered to the
syringe. Also wipe plunger contamination with a paper towel.
(2) Dry the inside with alcohol after washing.
(3) To protect the needle tip, store the syringe in an exclusive case.
(4) In the following cases, change the syringe with new one.
• The syringe plunger moves slowly.
• The PTFE part of the plunger tip is thin and the plunger is loose.
＊ To set the syringe, refer to “3-4-4-1. Setting of the Syringe Head and the
Syringe”.
ASC-270LS
Inspection of the Syringe Needle Tip
Always inspect the needle tip before measurement. Repair or change it if needed.
(1) In the following cases, repair the tip with sandpaper or a file.
• The needle tip is curved.
• Foreign particles adhere to the needle.
(2) When the needle is curved, change the syringe with new one.
＊ To set the syringe, refer to “3-4-4-1. Setting of the Syringe Head and the
Syringe”.
Check of Syringe Weighing Volume
Check the syringe weighing volume with water every month. Measure weight with a
balance.
Sample Boat Contamination Check
When sample boat contamination or devitrification are heavy, change a sample boat
with new one.
POINT
If sample boat discoloring (turn white) is devitrification, the mechanical
strength is reduced and it may break. When fine cracks are in the devitrified
part, the mechanical strength is low. Change it immediately.
When using the horizontal furnace, check that quartz wool on a sample boat is soft and
not contaminated before measurement. When it is not soft and clean, change it with
new one.
(1) Pack about 10mg quartz wool to the sample boat of ABC unit with tweezers
(2) Always prebake a boat after changing quartz wool about three times.
Refer to “5-3-5. Sample Boat Prebaking” for details.
ASC-270LS
8-1-2. Periodical Inspection
Table 8-2 shows the periodical inspection items.
CAUTION
Always run periodical inspections every 6 to 12 months.
Failure to check the unit can lead not only to reduced performance of the
unit but also to serious accidents.
Table 8-2. Periodical Inspection Items

No. Items Contents
1 Visual check of the Contamination and dust
unit Stability of connected parts
Proper connection and fitting of connectors
2 Greasing CAUTION
At the unit inside operation, always remove the
power cable to prevent serious accidents by
malfunctions.
ASC-270LS have the mechanical parts.
Grease moderately the rail and the sliding screws.
Also grease them when it makes abnormal noises or
after dust is removed.
Recommended grease: Lithium soap grease containing
extreme-pressure additive in mineral base oil
3 ASC-270LS insulation Measure the insulation between the power terminal and
inspection the earth terminal of the chassis.
It should be 2MΩ or more.
4 Operation inspection Connect ASC-270LS unit to the analyzer and measure
regularly.
If any problems are found by the above inspections, solve the problem and re-check the
unit. When troubles can not be solved or they may be in the unit, contact our local
distributor.
ASC-270LS
8-2. Maintenance
8-2-1. Fuse Change
(1) Turn off the power switch and remove the power cable.
(2) Insert a flathead driver into the fuse holder dent of the unit rear and pull out the fuse
holder.
(3) Change the fuse with a new one and push the holder.
8-2-2. Ladle and Guide Tube Change
(1) Remove the screws in ASC-270LS right and the L-shape ABC maintenance cover.
Fig. 8-2. Removal of ABC Maintenance Cover
(2) Loosen the φ6/4 reducer elbow joint of the guide tube right and the clamp to remove
them from the guide tube.
Fig. 8-3. Removal of the Joint and the Guide Tube Clamp
ASC-270LS
(3) Loosen the O-ring holder of the sample injection box right.
Fig. 8-4. O-ring Removal
(4) While turning the guide tube, move it to the right by about 5cm.
Fig. 8-5. Pullout of the Guide Tube
(5) Slowly pull out the guide tube to the right while holding the ladle.
(6) To set a new ladle and guide tube, insert the ladle into the guide tube and follow the
opposite procedure.
ASC-270LS
8-2-3. Pyrolysis Tube Removal
Remove a pyrolysis tube by the opposite procedure to “3-4-6. Connection of HF-210

and ASC270LS Units.”.
8-2-4. Vial Wash and Storage at Trace Measurement
At trace measurement (1ppm or less), do not use a dryer for regular glass.
By air convection in the dryer, contaminated air attaches contaminant to a vial to affect
measurement values.
To restore vials, pour pure water such as ion exchange water or ultrapure water into a
container with a seal cap to wash it. Immerse vials washed with equivalent pure water
into this container. At this time, completely remove air attached to the vial inside.
Raise this vial, dry it well, and rinse with sample just before sample injection.
8-3. Storage of the Unit
Store ASC-270LS unit as follows when it is not used for long time.
The cautions for storing the unit on a table are as follows.

• Remove a power cable.
• Remove the cable to the horizontal furnace.
• Remove ASC-270LS unit from the horizontal furnace.
The cautions of the storage place are as follows.

• Install the unit in a place where room temperature is 45 degrees Celsius or less.
• Store the unit in a place free from direct sunlight.
• No strong vibration and continuous weak vibration.
• Store the unit in a place free from a strong electromagnetic field.
• Store the unit in a place where humidity is 80% or less.
• Store the unit in a place free from corrosive gas.
• Store the unit in a place where open fire is not used.
• Store the unit in a place free from much dust.
ASC-270LS
ASC-270LS
Section 9: Specifications 9-1
Section 9: Specifications
Standard Specifications
Common items to liquid and solid samples

Names Automatic sample changer for solid and liquid samples
Model ASC-270LS
Samples When using the vial tray: Liquid samples
When using the boat tray: Solid samples and involatile liquid
samples *
Boat cooling Electronic cooling
Ambient temperature 10 to 35 degrees Celsius (No fluctuation during measurement)
Power AC 100/115/230/240V, 50/60Hz, 192VA
Dimensions 500 (W) × 460 (D) × 600 (H) mm
Weight About 27kg
Operation Analyzers (Refer to “Introduction” for connectable analyzers.)
Automatic (Start from the analyzer with a PC)
Manual (By PC setting in the analyzer side)
Solid samples
Volume 30mg or less
Sample boat quantity 49 pcs
Boat operation 99 positions + end position + cooling position
Sample boat material Ceramic (Standard )
Liquid samples
Sample container Vial with a septum, 4mL capacity, 2mL capacity
Sample vial quantity 4mL: 84pcs, 2mL 120pcs
Injection system Microsyringe 25, 50, 100μL
Wash container Vial with a septum, 36mL capacity
Washing solution Such as pure water, ion exchange water, or organic solvents
Discharge container Vial with a septum, 40mL capacity
* Volatile liquid samples can be injected from the sample injection port with a
microsyringe.
ASC-270LS
9-2 Section 9: Specifications
ASC-270LS
Section 10: Consumables 10-1
Section 10: Consumables

This section describes the consumables.
10-1.ASC-270LS Consumables
Table 10-1.ASC-270LS Consumables

No. Parts names Parts Quantity Remarks
numbers
1 Guide tube TX3RTG 1 pc
2 Ladle for ABC-210 BL1RDL 1 pc
3 Ceramic sample boat TX3SCX 10 pcs/bag
4 Ceramic sample boat TX3SCY 100 pcs/bag
5 Quartz sample boat for ABC TX2SBT 5 pcs/set *1
6 Quartz sample boat SC7SCQ 5 pcs/set *2
7 Septum (flat) TN5SIS 100 pcs/set
8 Septum holder TX3SED 1 pc
9 For the right
and the left of
O-ring P-16 (Silicon) TX020 5 pcs/set the sample
injection box
10 O-ring G-50 (Silicon) TNG50 5 pcs/set For the box top
11 Glass plate for the sample injection TX3BSI 1 pc For the box
box cover
12 Sealing packing for the sample TN10SP 2 pcs/set For the box
injection box cover
13 Fuse 4A FU04MS 2 pcs/set
14 Pyrolysis tube O-ring holder 4mm TX0103 1 pc Guide tube
right
15 Pyrolysis tube O-ring holder 8mm TX3SCF 1 pc Pyrolysis tube
left
16 φ6/4 elbow connector (30-6RUE4-S) GA164E 1 pc
17 Wash solution vial φ 50 × 25L SC7LSBA 1 pc
18 Waste solution vial φ 25 × 95L SC7LSV 10 pcs/set With a cap
19 ASC-270LS wash/discharge cap SC7LSVC 100 pcs/set
20 Gastight microsyringe 25μL (SGE) MSSGG2 1 pc
*1. For manually setting a sample boat to the sample injection box or removing it
*2. For automatically setting a sample boat to the sample injection box with the sampler
ASC-270LS
10-2 Section 10: Consumables
10-2. ASC-270LS Parts Pictures
Table 10-2. ASC-270LS Parts Pictures

No. Parts numbers Pictures
TX3RTG
1 Guide tube (for ABC and
ASC)
BL1RDL
2
Ladle (for ABC and ASC)
TX3SCX
3 Sample boat (for ABC and
ASC, ceramics, 10pcs)
TX3SCY
4 Sample boat (for ABC and
ASC, ceramics, 100 pcs)
TX2SBT
5
Quartz sample boat for ABC
SC7SCQ
6
Quartz sample boat
TX3SED
7
Septum holder
TN5SIS
8
Septum (flat)
TX020
9
O-ring P-16 (Silicon)
TNG50
O-ring G-50 (Silicon)
10
ASC-270LS
Section 10: Consumables 10-3
(Continued to the next page)

(Continued from the previous page)

TX3BSI
11 Glass plate for the sample
injection box
TN10SP
Sealing packing for the
12 sample injection box
3mm in thickness 2mm in thickness

FU04MS
13
Fuse 4A
TX0103
Pyrolysis tube O-ring holder
14
(4mm in thickness)
15 TX3SCF
Pyrolysis tube O-ring holder
(8mm in thickness)
16 GA164E
φ6/4 elbow connector
(30-6RUE4-S)
17 SC7LSBA
Wash solution vial φ 50 ×
25L
18 SC7LSV
Waste solution vial φ 25 ×
95L
(Continued to the next page)
ASC-270LS
10-4 Section 10: Consumables
(Continued from the previous page)

19 SC7LSVC
ASC-270LS wash/discharge
cap
20 MSSGG2
Gastight microsyringe 25μL
(SGE)
21 MSSGG5
(SGE)
22 MSSGG1
(SGE)
23 FU04MS
Fuse 4A
24 TN5SIS
Septum (flat)
ASC-270LS

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Control No.

Electromagnetic Compatibility Directive: 2014/30/EU

Model Name : Automatic Sample Changer Model ASC-270LS

Standard to which Conformity is Declared:

EN61000-6-3:2007 : Generic standards-Emission standard for residential, commercial

EN61000-6-1:2007 : Generic standards-Immunity for residential, commercial and

EN61010-1:2010 : Safety requirements for electrical equipment for measurement,

EN IEC 63000:2018 : Technical documentation for the assessment of electrical and

ISO12100:2010 : Safety of machinery – General principles for design –

Name of Manufacturer : NITTOSEIKO ANALYTECH CO., LTD.

Manufacturer’s Address : 7-10-1 Chuo-rinkan, Yamato, Kanagawa 242-0007, Japan

EU Office Address : MITSUBISHI CHEMICAL EUROPE GmbH

Type of Equipment : Laboratory Equipment

Month and year of CE Marking : June, 2017

Date :16 . 07 . 2021

Connectable Electric Furnaces

(1) Do not reprint this manual wholly or partially without permission.

(2) The contents may be changed without notice.

Warnings and Cautions

At the front of ASC-270LS arm

At the top of ASC-270LS right back

At ASC-270LS tray unit

When installing the unit, observe the following precautions.

Maintenance and Inspection

Section 1: Names and Functions of the Unit

Fig. 1-1. ASC-270LS Front

Table 1-1. Names and Functions of Model ASC-270LS Front

No. Names Indications Functions

1-2. Names and Functions of Model ASC-270LS Rear

Table 1-2. Names and Functions of Model ASC-270LS Rear

1-3. Names and Functions around ASC-270LS Sample

Fig. 1-3. ASC-270LS Injection Box Circumference

Section 2: Parts Check

＊ To purchase the consumables, refer to “Consumables”.

2-1. ASC-270LS Common Parts

Table 2-1. ASC-270LS Common Parts

2-2.ASC-270LS Optional Parts

2-2-1. ASC-270LS Parts for Solid Samples

The following parts are optional.

Table 2-2. ASC-270LS Parts for Solid Samples

No. Parts names Quantity Check Remarks

2-2-2. ASC-270LS Parts for Liquid Samples

The following parts are optional.

Table 2-3. ASC-270LS Parts for Solid Samples

No. Parts names Quantity Check Remarks

2-2-3. ASC-270LS Tray for 4mL Vials for Liquid Samples

The following parts are optional.

No. Parts names Quantity Check Remarks

2-2-4. ASC-270LS Tray for 2mL Vials for Liquid Samples

The following parts are optional.

No. Parts names Quantity Check Remarks

3-1. Installation Conditions

3-2. Installation Space

Fig. 3-1. System Installation Example

3-3. Power Preparation

ASC-270LS consumption power is 192VA.

Power cable lengths are as follows.

3-4. Preparation for ASC-270LS

3-4-1. Removal of the Clamp for Carriage

Remove 3 clamps fixing the arm mechanical part.

Fig. 3-2. Clamp Removal

3-4-2. Ladle Insertion

Set the ladle to ASC-270LS as follows.

Fig. 3-3. Ladle Insertion

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