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The deformation of porous sandstones; are Byerlee friction and the critical state
line equivalent?
E.H. Rutter, C.T. Glover*
Rock Deformation Laboratory, School of Earth, Atmospheric and Environmental Sciences, University of Manchester, Manchester M13 9PL, UK
a r t i c l e i n f o a b s t r a c t
Article history: Certain rock properties that depend on intergranular fracture and frictional sliding appear to be inde-
Received 15 April 2012 pendent of rock type. This relationship is true for the rock-on-rock frictional sliding coefficient. The
Received in revised form generalization has been widely applied to geomechanical modelling of upper crustal strength. Porous
21 August 2012
sandstones can be relatively weak and poorly cohesive, hence susceptible to deformation involving grain
Accepted 24 August 2012
fragmentation and pore collapse. The critical state theory is commonly applied to describe such
Available online 10 September 2012
behaviour. Previous work showed that the yield surface is substantially independent of rock type when
mean stress and differential stress are normalized by the grain crushing pressure, implying that the
Keywords:
Rock friction
critical state line is rock type-independent and equivalent to the frictional sliding criterion. We test these
Critical state mechanics hypotheses using previously published data for a range of porous sandstones augmented by new
Porous sandstones experimental results on Hollington and Berea sandstones deformed to large strains to define the critical
Rock deformation state line over a wide range of pressures for each rock type. Results confirm the rock type-independence
of the critical state line and show that it is nearly equivalent to frictional sliding. These relationships
point to a simple procedure for estimating approximately the mechanical properties of sandstones based
only on petrographic characteristics.
Ó 2012 Elsevier Ltd. Open access under CC BY license.
s1 s3 ¼ a þ bs3
s ¼ so þ mtanj
should be related to the friction coefficient determined from rock- the differential stress. This outcome means that in the axisym-
on-rock sliding experiments because they both describe essentially metric shortening test the loading path on a Q/P plot rises from the
similar processes of grain fracture and frictional sliding. Farmer abscissa with a slope of 3.
(1983) explicitly interpreted the critical state line as equivalent to Setting M ¼ (s1 s3)/[(s3 Pp) þ (s1 s3)/3] as the slope of the
the Coulomb frictional strength of rocks, with the implication that if line representing the friction data in the Q/P coordinate frame and
the frictional sliding behaviour of crustal rocks is largely indepen- b 1 ¼ (s1 s3)/(s3 Pp) (the corresponding slope in the differ-
dent of rock type, then so too should be the critical state line. ential stress vs effective confining pressure coordinate frame) we
In this paper we set out to test the hypotheses that (a) the can obtain M in terms of b as
critical state line is approximately independent of rock type and (b)
that the critical state line is equivalent to the frictional sliding line, M ¼ 3ðb 1Þ=ð2 þ bÞ (2)
by means of some re-analysis of previously published data together This can be recast in terms of friction angle j (¼ tan 1
m) using
with new data on two silicic porous rock types.
b ¼ ð1 þ sinjÞ=ð1 sinjÞ (3)
2. Friction data of Byerlee (1978) in the Q/P coordinate frame Substituting for b in (2) and rearranging
.
Note that it is implicit that any dependence of the sliding
criterion on the intermediate principal stress is ignored. Whilst
previous studies have investigated the influence of the interme-
diate principal stress on failure of intact rock by fracturing (e.g.
Mogi, 1967; Colmenares and Zoback, 2002), no corresponding
studies exist for its influence on slip on a pre-existing fault surface.
For comparison with critical state data, the friction data in terms
of principal stresses must be further recast in terms of differential
stress (Q ¼ (s1 s3)) and effective mean stress P ¼ (s1 þ 2s3 3Pp)/
3, where Pp is the pore fluid pressure. Q as a measure of distortion-
producing stress can be defined as equal to the maximum Fig. 2. Compilation of friction data (after Byerlee, 1978) with a single best-fit line
deviatoric principal stress, given by (s1 (s1 þ s2 þ s3)/3), but shown, compared to frictional sliding data for porous sandstone, all transformed into
because for axisymmetric loading this is equivalent to 2(s1 s3)/3, the Q/P coordinate frame. The fit according to Byerlee (1978) (bold line) is in two
it has become conventional to plot the differential stress rather segments, corresponding to a friction coefficient (m) of 0.85 at low pressures and 0.6 at
higher pressures. The single best-fit line for the whole Byerlee dataset over the pres-
than the deviatoric stress. For axisymmetric compression, sure range shown has a slope of 1.46 0.014, corresponding to an average m ¼ 0.73.
P ¼ (s3 Pp) þ (s1 s3)/3, thus each increment of differential stress The standard error bar shown is for estimation of Q (40.5 MPa). For the porous
during loading increases the mean effective pressure by one third of sandstone data the best-fit slope is 1.43, corresponding to a friction coefficient of 0.71.
132 E.H. Rutter, C.T. Glover / Journal of Structural Geology 44 (2012) 129e140
2.1. Porous sandstone friction a thin coating of hematite around grains. A veneer of quartz cement
around grains provides cohesion. Cores were cut normal to
Frictional sliding data for porous sandstones and fault gouge bedding, which is revealed by grain size and mineralogical banding
were compiled from the following sources (porosities in (about 2 cm wide) with colour (hematite) contrasts. Total initial
parentheses): porosity is 25.6% 0.6% (by helium porosimetry), and grain size
Scott and Nielsen (1991a and 1991b), for Tennessee sandstone distribution mean is 230 63 mm.
(6%); Colorado red sandstone (6.3%); Gold sandstone (13.9%); Berea The Carboniferous Berea sandstone was cored in a single
sandstone (19.9%); DV (Dobbs Valley)-1 sandstone (20.9%); DV-2 direction (normal to weakly-defined bedding laminae) from
sandstone (22.2%); DV-3 sandstone (27.6%). a block supplied by Dr D. Lockner (US Geological Survey). Total
Numelin et al. (2007), natural fault gouge. porosity is 17.7% 0.7% (by density measurement), grain size
Cuss et al. (2003), Tennessee sandstone (7%), Darley Dale distribution mean is 170 50 mm. This rock type was previously
sandstone (13%), Penrith sandstone (28%). described and used extensively in programs of mechanical testing
Mair and Marone (1999), synthetic fault gouge. (e.g. Zhang et al., 1990; Wong et al., 1997; Baud et al., 2000b;
This study, Hollington sandstone (25%) and Berea sandstone Menéndez et al., 1996). The material used here is slightly less
(17.7%). porous than blocks previously (21% porosity) used by Wong, Baud,
These frictional sliding data are plotted separately from the Menéndez and co-workers (op. cit.), and hence is somewhat
compilation of Byerlee (1978) on Fig. 2. All data are reasonably stronger. The solid components consist of 80% equant quartz
consistent with the Byerlee generalization, but within the sand- grains, feldspar (7%), clay minerals (7%), with the remainder
stone group a tendency exists for friction in the more porous rocks carbonate and opaque grains.
to be slightly less than for less porous rocks. Axisymmetric shortening experiments were carried out on
cylindrical specimens 15, 20 or 25 mm in diameter with a length:-
3. New experiments on Hollington sandstone and Berea diameter ratio of 2.5:1, at total confining pressures ranging up to
sandstone 400 MPa, using ReolubeDOS synthetic oil as a confining medium.
The smaller diameter samples were used at the higher pressures to
3.1. Experimental details keep axial loads within the limits of the testing machine. Samples
were jacketed either in polyolefin or heat-shrink tubes, which
In most previous literature (but see Cuss et al., 2003), post-yield support negligibly small loads. Pore volumometry was used to
deformation at large confining pressures was not usually taken to measure porosity changes during deformation, with pore fluid
sufficiently high strains to reach the critical state condition, that is pressure being maintained constant at 2, 10 or 16 MPa. To measure
recognized when strain hardening and volumetric compaction porosity changes during deformation requires that the pore pres-
ceases, and when deformation continues at constant differential sure is kept constant, so that the pore volumometer measures the
stress, potentially with no further microstructural changes. Thus amount of fluid expelled from the rock during compaction, or the
the critical state line could only be defined as the locus of points amount of fluid drawn in during dilatation. Such experiments are
passing though peaks in the yield surface for rocks of different therefore performed under ‘drained’ conditions.
porosities. All experiments were carried out at room temperature at strain
New experimental data were therefore obtained from the rates near 104 s1 for Hollington sandstone and 2 105 s1 for
porous Hollington and Berea sandstones, with the particular aim of the less permeable Berea sandstone. The effectiveness of drainage
testing to sufficiently high strains that the critical state line at large in fluid saturated tests was checked by observing the rapidity of
differential stresses is intersected by the stress path for axisym- response to small pore pressure steps. Hollington sandstone was
metric compression. These data therefore complement the low tested both oven-dried (at 75 C) and saturated with the same fluid
strain data previously reported in the literature. as the confining medium. Berea sandstone specimens were tested
The Hollington red sandstone comes from a quarry on the water-saturated with a pore pressure of 2 or 10 MPa. Baud et al.
outcrop of the Triassic Sherwood sandstone group in Staffordshire, (2000b) reported comparative data on the effect of water on the
England. The solid components (Fig. 3a) are dominated by 70% strength of Berea sandstone (amongst other porous sandstone
equant quartz sand grains with the remainder consisting of feldspar types). Although a weakening effect on Berea sandstone occurs, it is
(17%), clays (8%), detrital mica (3%) and opaques (2%), including small and little greater than the range of experimental error.
Fig. 3. (a) Thin section photomicrograph of undeformed Hollington sandstone (plane-polarized light), showing near-equant grains. Pore space is filled with coloured epoxy resin.
(b) Thin section micrograph showing impingement fracture of quartz grains in Hollington sandstone subjected to effective hydrostatic pressure equal to P* (190 MPa). Plane-
polarized light, pore space is filled with coloured epoxy resin.
E.H. Rutter, C.T. Glover / Journal of Structural Geology 44 (2012) 129e140 133
increase in cross-sectional area with each increment of axial Specimen Total conf. press. Pore press. Differential stress Fault angle
shortening strain was first calculated assuming constant volume (deg s1)
ˇ
number (MPa) (MPa) (MPa) at
deformation, then compensation was applied for the volume Yield Const. Vol. Friction
change obtained from the pore volumometer, which reduces the stress
assumed amount of cross-sectional area increase when volume (a) Hollington Sandstone (dry [pore pressure ¼ 0] or oil wet, 25% porosity)
compaction occurs. Homogeneous deformation must be assumed 107 0 0 20 e e 0
105 36 17 82 e 66 27
for these calculations.
9 40 16 65 e 45 e
Measurements of differential stress at small (elastic) strains 16 43 16 100 e 78 27
were made to an accuracy of 1 MPa and hydraulic pressure 8 46 16 74 e 65 30
measurements to 0.5 MPa. The resolution of pore volumometer 104 56 17 78 e 82
measurements was 0.5 mm3. Axial displacements were measured 7 78 16 80 e 80 e
21 80 16 107 e 90 e
from outside the pressure vessel to a resolution of 0.01 mm, but
103 96 18 120 e 113 e
after correcting for confining pressure and axial load-dependent 40 103 16 84 105 e e
axial apparatus distortion, the accuracy of strain measurements is 19 106 16 110 e 83 e
estimated to be about 0.2%. The effects of heterogeneous defor- 25 123 17 100 150 e e
mation of the sample and the correction required for cross- 23 110 17 85 145 e e
37 124 16 90 e 80 e
sectional area changes mean that differential stresses reported at 24 130 17 95 202 e e
high strains are probably accurate to only 5%, but the largest 80 135 16 89 172 e e
contributor to scatter in experimental results is likely to be vari- 33 137 0 100 304 e e
ability between different rock samples arising from bedding 6 152 16 58 203 e e
41 169 16 82 e e e
laminae heterogeneities.
79 175 16 65 258 e e
100 186 17 35 272 e e
3.2. Experimental results 101 190 16 60 248 e e
17 192 16 45 e e e
Results are summarized in Table 1 and graphically in Figs. 4 and 5. 18 195 17 50 e e e
106 196 16 40 390 e e
Under steadily increasing effective hydrostatic pressure, both rocks 30 207 0 40 362 e e
displayed near-linear elastic compression of the pore space. Pore 10 220 16 38 273 e e
collapse of Hollington sandstone occurred at P* ¼ 190 15 MPa (12 35 235 0 65 417 e e
tests). Fig. 3b shows the damage done at the grain scale to Hollington 12 258 16 27 279 e e
31 260 0 80 460 e e
sandstone during permanent isotropic compaction. P* was not
36 291 0 85 684 e e
attained for Berea sandstone within the range of the hydraulic pump 75 309 22 60 e e e
used, but is expected to be at about 450 MPa. 76 316 17 60 e e e
For small effective confining pressures under axisymmetric Hydrostatic 206 16 mean value, 15 MPa of e
loading, both rock types failed by localized faulting with stress 12 tests
(b) Berea sandstone (water wet, 17.7 % porosity)
drop. At higher effective confining pressures, faulting became 10 12 2 110 e 20 24
suppressed, leading to a transition to failure by distributed ductile 1 42 2 202 e 104 28
cataclastic flow. Yield (the onset of permanent, inelastic deforma- 9 82 2 240 e 200 32
tion, given with an estimated accuracy of about 5% of the reported 2 102 2 245 e 230 31
16 102 2 272 e 230 34
differential stress) was often recognized from the differential stress
11 142 2 322 330 e 39
vs strain curve (Fig. 4), but it is most clearly expressed by deviation 12 210 10 278 332 e e
of the volumetric strain or porosity change curve from the hydro- 15 250 10 250 353 e e
stat (Fig. 5). Yield stress values for Hollington sandstone show 13 300 10 170 371 e e
considerable scatter. It is suspected that this scatter is due to 14 345 10 320 659 e e
Fig. 4. Representative stress/strain and porosity change curves for (a) Berea sandstone and (b) Hollington sandstone. Beside each curve is shown test number and effective confining
pressure (MPa). In both cases localized faulting changes to compactive ductile flow with increasing effective confining pressure. At the higher pressures, a long period of post-yield
strain-hardening flow ends when flow stress and porosity become constant.
Fig. 5. Relations between porosity change and effective mean stress for Berea sand-
stone and Hollington sandstone (specimen number and effective confining pressures 4. Discussion of experimental results
shown). In each case elastic porosity decrease occurs with increasing hydrostatic
pressure. P* (effective pressure at onset of permanent compaction) was reached only 4.1. Comparison of the critical state line with frictional sliding data
for Hollington sandstone (at 200 MPa effective pressure). During axial shortening
deformation, deviation (in most cases by compaction) from the elastic hydrostat occurs
at progressively higher effective mean pressures for higher initial confining pressures. Fig. 8 compares differential stress Q with effective mean stress
The point of deviation defines the yield condition. P at critical state, determined at the attainment of steady flow/
E.H. Rutter, C.T. Glover / Journal of Structural Geology 44 (2012) 129e140 135
Fig. 6. Graphical summary of data (Table 1) for yield stress and attainment of constant
volume/constant flow stress deformation (critical state) for Hollington sandstone. Tie
lines of slope 3 (stress path lines) link corresponding points for the same experiment. Fig. 7. Compilation of yield stress and critical state data for Hollington and Berea (from
The ductile strain accumulated between yield and constant volume flow tends to be this study and Wong et al., 1992) sandstones and also comparable data for Penrith and
greater when the tie line for initial confining pressures up to P* is longer. For some Darley Dale sandstones from Cuss et al. (2003) (porosities indicated in parentheses).
tests, applied confining pressure was greater than P*, leading to rising yield stresses, Data show how the yield curves expand for rocks of progressively lower porosity and
and the longest post-yield ductile flow tie-lines, that correspond to greater rates of how the critical state data lie on a single trend for all rock types, that passes through
strain-hardening, rather than to greater post-yield permanent strains. the apices of successive yield surfaces.
constant volume flow with Q vs P for frictional sliding in porous similarity can form part of a useful basis for first-pass modelling of
sandstones previously presented in Fig. 2. Also included are data on the mechanical behaviour of porous sandstones.
serpentinite (from Rutter et al., 2009) rendered porous (20%) by In making such generalizations, we recognize that force-
dehydration to olivine plus talc at 550 C at low effective pressure, fitting all critical state data into a single linear envelope can
and then mechanically tested at 450 C. The results show that the
critical state concept applies equally to high temperature defor-
mation that involves pore collapse and that the critical state line
slope remains the same.
The frictional sliding slope for sandstones is 1.43, corresponding
(via Eq. (4)) to a friction coefficient of 0.71. The critical state best-fit
line slopes at 1.18 0.05, corresponding to a friction coefficient of
0.58. Thus the data do not support the view that the two slopes are
identical, as suggested by Farmer (1983), Muir Wood (1990), and
Schultz and Siddharthan (2005). They are, however, closely similar,
and the experimental errors implicit in the two datasets overlap
within the data range. The differences in central tendency of the
two groups of data may be attributable to the fact that, whilst both
describe similar physical processes of grain fracture, rotation and
frictional sliding, they do not describe similar degrees of fracture
damage. Intensely localized frictional sliding in a fault zone
involves much greater degrees of damage than distributed cata-
clastic flow, perhaps involving several orders of magnitude differ-
ence in accommodated local strain. The particle-size distributions
and their porosities are likely to be different at the same effective Fig. 8. Q vs P plot for frictional sliding in porous sandstones (data sources as in Fig. 2)
pressure, and it seems likely that these differences will be reflected with critical state data for porous sandstones indicated (with initial porosity shown).
in differences in mechanical behaviour. However, in the same way Included also are data on serpentinite at 450 C rendered porous by dehydration to
olivine þ talc (after Rutter et al., 2009). The friction slope (1.43) is slightly higher,
that sliding friction is to a useful approximation independent of corresponding to a friction coefficient of 0.71, than the critical state slope
rock type, the critical state line is likewise independent, even (1.18. 0.046), that corresponds to a friction coefficient of 0.59. The standard error bar
though the slopes are not identical. As we explore below, this shown is for estimation of Q (40.4 MPa).
136 E.H. Rutter, C.T. Glover / Journal of Structural Geology 44 (2012) 129e140
obscure more subtle differences in real trends for individual rock alternative way to plot critical state data, appears to be indepen-
types with respect to the general pattern of behaviour. Such dent of rock type.
differences can be crucial to distinguishing between different As suggested above, the critical state data may lie slightly below
mathematical models of yield cap evolution, as explored by Baud the frictional sliding data because, at the same effective mean
et al. (2006). pressure, the comminuted rock in a narrow fault zone is likely to be
more compact, finer-grained and hence more microstructurally
4.2. Post-yield porosity evolution ‘evolved’. In the same way that porosity decreases systematically
along the critical state line, a similar evolution might be expected
As cataclastic flow proceeds with strain hardening in the post- for fault gouge derived from framework silicates. Some experi-
yield part of the loading path, it is accompanied by progressive mental studies have shown that gouge porosity evolves with
porosity reduction until the critical state condition is reached. progressive shearing, e.g. Marone et al. (1990). Several studies
Wong et al. (1992) and Wong and Baud (1999) presented data for showed that compaction, as measured by reducing thickness of
Berea sandstone that shows how the attainment of a given porosity a synthetic granular gouge layer or fluid expulsion, accompanies
defines a succession of expanding yield loci, in the same way that progressive shearing (Marone et al., 1990; Mair and Marone, 1999;
rocks of initially lower porosities are characterized by initially Crawford et al., 2008), tending to a constant porosity at steady-state
larger yield curves. Rutter et al. (2009) showed similar behaviour sliding. Presently, insufficient data are available to evaluate
for dehydrated serpentinite and the same can be demonstrated in whether porosity at the attainment of stable sliding varies
the behaviour of Hollington sandstone. Loading paths starting from systematically with effective mean pressure for a range of gouge
progressively higher effective pressures therefore arrive at the types and over a sufficiently wide range of pressures.
critical state line at higher differential stresses and hence at lower
porosities and greater degrees of microstructural damage. 4.3. Controls on the value of P*
Fig. 9 shows a compilation that demonstrates how porosity at
critical state decreases as effective confining pressure P increases From a theoretical model based on pore collapse by Hertzian
for the several different rock types referred to above, plus Gosford indentation cracking, Zhang et al. (1990) proposed that P*, the
and Boise sandstones (Edmond and Paterson, 1972; Wong et al., effective hydrostatic pressure required for the onset of grain
1997; Baud et al., 2000b). This is a projection of the critical state crushing, is determined by the product of initial porosity f and
line onto the P (MPa) vs porosity (%) plane and a hyperbolic grain radius r, such that a plot of log P* vs log (f r) is linear with
function a slope 3/2. This corresponds to the normal consolidation curve.
Fig. 10 shows such data compiled by Wong et al. (1997),
P ¼ ð1=f% 0:037Þ=0:000149 (5)
augmented by our data for Hollington and Berea sandstones,
together with that for Penrith and Tennessee sandstones (Cuss
is shown fitted to these data. The curve can also be taken as the line
et al., 2003). The new data are consistent with the earlier compi-
separating localized faulting behaviour from distributed ductile
lation. A least-squares best-fit line
flow (the brittleeductile transition). Thus this graph shows how the
effective confining pressure required for ductility varies with initial
log P*ðMPaÞ ¼ 0:603 1:09 logðf rðmmÞÞ (6)
porosity. Rutter and Hadizadeh (1991), Scott and Nielsen (1991b),
Wong et al. (1992), Menéndez et al. (1996), Wong et al. (1997) and is shown, with a standard error of 0.25 on log P*, or about 17% of
Wong and Baud (1999) compiled data on the brittleeductile tran- the value of P*.
sition for various sandstones in this way (Fig. 9). This curve, as an Schultz et al. (2010) employed the relation log P* ¼ 1.5 log (f r)
to estimate P* for Navajo sandstone. The slope in this equation is
constrained by the Hertzian model and the line passes approxi-
mately through the centroid of the data (Fig. 10), but empirical Eq.
(6) is a significantly better descriptor of the presently available data.
Fig. 11. Compilation of yield data for porous sandstones from Wong et al. (1997) augmented by data on Hollington and Berea sandstones (this study), dehydrated serpentinite
(Rutter et al., 2009) and Penrith, Darley Dale and Tennessee sandstones (Cuss et al., 2003). Dashed curves show upper and lower limits to yield behaviour for P/P* <1 according to
Wong et al. (1997) Data for Hollington and Penrith sandstones and dehydrated serpentinite extending to the region P/P* >1 are also shown to follow a similar trend. Porosity (%)
shown in parentheses with each rock type.
138 E.H. Rutter, C.T. Glover / Journal of Structural Geology 44 (2012) 129e140
vesicular basalt) (e.g. Shimada, 1981; Heap et al., 2011; Zhu et al.,
2011). Porous carbonate rocks behave mechanically in a compa-
rable way to sandstones but can be more complex owing to
potentially more complex pore/cement relationships and the
capacity of calcite for a degree of intracrystalline plastic deforma-
tion even at low temperatures. We have therefore not attempted to
analyze their behaviour together with silicic sandstones.
reservoir sandstones from simply-acquired petrographical Hettema, M.H.H., Schutjens, P.M.T.M., Verboom, B.J.M., Gussinklo, H.J., 2000.
Production-induced compaction of a sandstone reservoir: the strong influence
information.
of stress path. SPE Resource Evaluation and Engineering 3 (4), 342e347.
Issen, K.A., Rudnicki, J.W., 2000. Conditions for compaction bands in porous rock.
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