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  • Ic8b00753 Si 001

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    The document describes a two-step synthesis method for producing VO2(M) materials with tuned crystallinity. It includes a table showing the carbon content of samples before and after annealing, and a figure showing the microstructure of V2O3 particles obtained after annealing a VOx-2min sample, including SEM, TEM, and HRTEM images. The annealing reduces the carbon content and produces single crystalline V2O3 particles with a d-spacing of 0.37 nm corresponding to the [012] plane.

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    ic8b00753_si_001

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    The document describes a two-step synthesis method for producing VO2(M) materials with tuned crystallinity. It includes a table showing the carbon content of samples before and after annealing, and a figure showing the microstructure of V2O3 particles obtained after annealing a VOx-2min sample, including SEM, TEM, and HRTEM images. The annealing reduces the carbon content and produces single crystalline V2O3 particles with a d-spacing of 0.37 nm corresponding to the [012] plane.

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    © All Rights Reserved
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    3 views3 pages

    Ic8b00753 Si 001

    Uploaded by

    binir88610
    The document describes a two-step synthesis method for producing VO2(M) materials with tuned crystallinity. It includes a table showing the carbon content of samples before and after annealing, and a figure showing the microstructure of V2O3 particles obtained after annealing a VOx-2min sample, including SEM, TEM, and HRTEM images. The annealing reduces the carbon content and produces single crystalline V2O3 particles with a d-spacing of 0.37 nm corresponding to the [012] plane.

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    © All Rights Reserved
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    Supporting Information

    Two-step synthesis of VO2 (M) with tuned crystallinity


    Shian Guan, Aline Rougier, Oudomsack Viraphong, Dominique Denux, Nicolas Penin, Manuel Gaudon*
    CNRS, Univ. Bordeaux, ICMCB UMR 5026, Pessac, F-33600, France

    S1
    Sample: Before annealing Sample: After annealing
    VEG 12.42% S-0min 3.11%
    VOx-2min 7.89% S-2min 1.86%
    VOx-3min 0.98% S-3min 0.24%
    VOx-5min 1.14% S-5min 0.10%

    Table S1. Carbon content of samples before and after annealing at 500°C in the vacuum, measured from CHNS elementary
    analyzer.

    S2
    Figure. S1. Microstructure of V2O3 particles (S-2min) obtained by post annealing VOx-2min sample at 500 ; (a) SEM
    image; (b) TEM image; (c) HRTEM collected at the edge of a single particle and (d) its corresponding d-spacing of 0.37 nm,
    as indexed to [012] plane.

    S3

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