You are on page 1of 65

ERODE SENGUNTHAR ENGINEERING

COLLEGE
(Autonomous)
(Approved by AICTE, New Delhi, Permanently Affiliated to Anna University - Chennai
& Accredited by NAAC & National Board of Accreditation (NBA), New Delhi.)
PERUNDURAI, ERODE 638 057

DEPARTMENT OF
CHEMICAL ENGINEERING

Curriculum and Syllabus

M.TECH. CHEMICAL ENGINEERING

REGULATIONS - 2019

Choice Based Credit System (CBCS)


(Academic year 2019 – 20)
ERODE SENGUNTHAR ENGINEERING COLLEGE
(Autonomous)
(Approved by AICTE, New Delhi, Permanently Affiliated to Anna University - Chennai
& Accredited by NAAC & National Board of Accreditation (NBA), New Delhi.)
PERUNDURAI, ERODE 638 057

INSTITUTION VISION & MISSION

VISION
Erode Sengunthar Engineering College strives with determination and commitment to provide and
promote world-class Technical Education, in particular to the students of backward rural areas,
transforming them into holistic personalities embedded with discipline, skill and responsibility that make
them patriotic, successful, and self-developed professionals ready to accomplish any job in their career
and life.

MISION
 Provide an idyllic study atmosphere, fine infrastructure, qualified and dedicated faculty and
standardized systems for a strong career foundation.
 Aid and motivate the students and faculty alike for maximum utilization of facilities, making them
innovative and creative in thinking and research, in order to provide technical service to industry and
society.
 Develop multi-skilled personalities to make ESEC, a world leader in Technical Education.

DEPARTMENT OF CHEMICAL ENGINEERING

VISION
 To inculcate continuously and relentlessly to produce top notch Chemical Engineers for the
industrial requirement.
MISSION
 To impart knowledge the students at all levels through vibrant, dynamic and state –of – the –art
intellectual exercise.
 To synergize the efforts of the students and faculty to evolve the innovative practices and
teaching methodologies.
 To generate in atmosphere of continuous learning and research promoting environment-
conscious Chemical Engineers.

Program Educational Objectives (PEOs)

I. Preparing the students with strong fundamental knowledge in Mathematics, Science, English and
Engineering Sciences so as to enable them to analyze the Chemical Engineering related problems.
(Preparation)
II. To prepare the students to design Chemical Engineering equipments, process design by
executing and evaluating the performance including socio-economic impacts to the region. (Core
Competence and Professionalism)
III. To provide problem solving computational skills for process simulation, design and analysis by
using appropriate software and also to give the students an exposure in word processing, spread
sheet, ppt., and to make them use information on the world wide web. (Breadth)
IV. To train the students in communication techniques and to make them aware of job related skills,
emerging technologies in global issues. Giving information on safety aspects, professional ethics
and to maintain harmony with society. (Learning Environment)

PROGRAM OUTCOMES (POs)


PO1:Engineering knowledge: Apply the knowledge of mathematics, science, engineering fundamentals,
and an engineering specialization to the solution of complex engineering problems.

PO2:Problem analysis: Identify, formulate, review research literature, and analyze complex engineering
problems reaching substantiated conclusions using first principles of mathematics, natural sciences, and
engineering sciences.

PO3:Design/development of solutions: Design solutions for complex engineering problems and design
system components or processes that meet the specified needs with appropriate consideration for the
public health and safety, and the cultural, societal, and environmental considerations.

PO4:Conduct investigations of complex problems: Use research-based knowledge and research


methods including design of experiments, analysis and interpretation of data, and synthesis of the
information to provide valid conclusions.

PO5:Modern tool usage: Create, select, and apply appropriate techniques, resources, and modern
engineering and IT tools including prediction and modeling to complex engineering activities with an
understanding of the limitations.

PO6:The engineer and society: Apply reasoning informed by the contextual knowledge to assess societal,
health, safety, legal and cultural issues and the consequent responsibilities relevant to the professional
engineering practice.

PO7:Environment and sustainability: Understand the impact of the professional engineering solutions in
societal and environmental contexts, and demonstrate the knowledge of, and need for sustainable
development.

PO8:Ethics: Apply ethical principles and commit to professional ethics and responsibilities and norms of
the engineering practice.

PO9:Individual and team work: Function effectively as an individual, and as a member or leader in
diverse teams, and in multidisciplinary settings.

PO10:Communication: Communicate effectively on complex engineering activities with the engineering


community and with society at large, such as, being able to comprehend and write effective reports and
design documentation, make effective presentations, and give and receive clear instructions.
PO11:Project management and finance: Demonstrate knowledge and understanding of the engineering
and management principles and apply these to one’s own work, as a member and leader in a team, to
manage projects and in multidisciplinary environments.

PO12:Life-long learning: Recognize the need for, and have the preparation and ability to engage in
independent and life-long learning in the broadest context of technological change.

PROGRAM SPECIFIC OUTCOMES (PSOs)


PSO1: Process Modeling & Simulation – Developing applied knowledge through Process Modeling &
Simulation in Chemical Process Industries.
PSO2: Contemporary Skills – An ability to update knowledge on recent developments in Chemical
Industries.
CURRICULUM
ERODE SENGUNTHAR ENGINEERING COLLEGE, ERODE
DEPARTMENT OF CHEMICAL ENGINEERING

REGULATIONS – 2019
CHOICE BASED CREDIT SYSTEM
I TO IV SEMESTERS CURRICULUM
M.TECH. CHEMICAL ENGINEERING
Minimum credits to be earned : 70
FIRST SEMESTER
Maximum Marks
Code No. Course L T P C Category
CA ES Total
Probability and Statistical
19MCH11 3 1 0 4 40 60 100 BS
Methods
Advanced Transport
19MCH12 3 0 0 3 40 60 100 PC
Phenomena
Advanced Separation
19MCH13 3 0 0 3 40 60 100 PC
Technology
19MCH14 Fluid Phase Equilibria 3 0 0 3 40 60 100 PC

Advanced Chemical 3 0 0 3 40 60 100 PC


19MCH15
Reaction Engineering
Professional Elective - I 3 0 0 3 40 60 100 PE

PRACTICALS

19MCH16 Instrumental Methods of 0 0 4 2 60 40 100 PC


Analysis Laboratory
19MCD01 Business English - I 0 0 4 2 60 40 100 EEC

Total 18 3 4 23 360 380 800 -

SECOND SEMESTER
Maximum Marks
Code No. Course L T P C Category
CA ES Total
19MCH21 Chemical Process Design 3 0 0 3 40 60 100 PC
19MCH22 Computer Control of
3 0 0 3 40 60 100 PC
Processes
19MCH23 Advanced Biochemical
3 0 0 3 40 60 100 PC
Engineering
19MCH24 Industrial Waste 3 0 0 3 40 60 100 PC
Management
Professional Elective - II 3 0 0 3 40 60 100 PE

Professional Elective-III 3 0 0 3 40 60 100 PE


PRACTICALS
19MCH25 Seminar 0 0 4 0 100 0 100 PC

Business 0 0 4 2 60 40 100 EEC


19MCD02
English - II
Total 18 0 4 20 400 340 800 -

THIRD SEMESTER
Maximum Marks
Code No Course L T P C Category
CA ES Total
Process Modelling and
19MCH31 3 0 0 3 40 60 100 PC
Simulation
Professional Elective-IV 3 0 0 3 40 60 100 PE
Professional Elective-V 3 0 0 3 40 60 100 PE
PRACTICALS
19MCH32 Project Work Phase I 0 0 12 6 60 40 100 EEC

Total 9 0 12 15 180 220 400 -

FOURTH SEMESTER
Maximum Marks
Code No Course L T P C Category
CA ES Total

19MCH41 0 0 24 12 60 40 100 EEC


Project Work Phase II
0 0 24 12 60 40 100 -

PROFESSIONAL ELECTIVES

Code No Course L T P C

PROFESSIONAL ELECTIVES I

19MCX01 Environmental Risk Assessment 3 0 0 3


19MCX02 Multiphase Flow 3 0 0 3
19MCX03 Polymer Science and Engineering 3 0 0 3
19MCX04 Petroleum Refinery Engineering 3 0 0 3
PROFESSIONAL ELECTIVES II
19MCX05 Multicomponent Distillation
3 0 0 3
19MCX06 Fluidization Engineering
3 0 0 3
19MCX07 Food Process Engineering
3 0 0 3
19MCX08 Environmental Engineering
3 0 0 3

PROFESSIONAL ELECTIVES III


19MCX09 Safety and Hazard Control
3 0 0 3
19MCX10 Membrane Technologies for Water and Wastewater
3 0 0 3
Treatment
19MCX11 Electrochemical Engineering 3 0 0 3
19MCX12 Computational Fluid Dynamics for Chemical Engineers 3 0 0 3
PROFESSIONAL ELECTIVES IV
19MCX13 Fuel Cell Technology
3 0 0 3
19MCX14 Bioenergy conversion Techniques
3 0 0 3
19MCX15 Solvent Extraction Techniques
3 0 0 3
19MCX16 Waste Water Engineering
3 0 0 3

PROFESSIONAL ELECTIVES V
19MCX17 Pollution Abatement
3 0 0 3
19MCX18 Project Engineering of Process Plants
3 0 0 3
19MCX19 Risk Analysis and Management
3 0 0 3
19MCX20 Total Quality Management
3 0 0 3

Total Credits in Range of Total Credits


S.No. Category I II III IV
Credit % Min Max
1 BS 4 - - - 4 5.71 5% 10%
2 HS - - - - - - - -
3 PC 14 12 3 - 29 41.42 35% 55%
4 PE 3 6 6 - 15 21.42 15% 25%
5 EEC 2 2 6 12 22 31.42 20% 40%
Total 23 20 15 12 70 100

BS- Basic Science ES-Engineering Science HS-Humanities and Social Science

PE- Professional Elective OE- Open Elective PC- Professional Core

MC – Mandatory course CA – Continuous Assessment ES- End semester Examination


EEC-Employability Enhancement
Course
SYLLABUS

SEMESTER-I
R
Department CHEMICAL ENGINEERING Semester I BS
2019
Hours / Week Credit Total Maximum
Course Code Course Name
L T P C Hours Marks
PROBABILITY AND
19MCH11 3 1 0 4 60 100
STATISTICAL METHODS
Course Objective(s): The purpose of learning this course is:
 To review the basic concept of probability and to give the applications of probability distributions.
 To understand the concept of correlation, regression and Estimation Theory.
 To provide information about testing of hypothesis.
 To acquire knowledge of various statistical techniques useful in making rational decision in real life
Problems using non-parametric methods.
 To forecast the future trends using various forecasting methods.
Course Outcomes: At the end of this course, learners will be able to:
 Apply the concept of sampling distributions in their field.
 Acquire the concept of non parametric test in attributes and obtained experimental data.
 Do curve fitting, correlation, regression which will be useful in solving engineering problems.
 Design and analyze the statistical experiments in terms of time series.
 Analyse a queue system.

Unit I PARAMETRIC METHODS 12


Sampling distributions – Types of Sampling- Type I and Type II errors, Large sample test for proportion and
mean – Test of significance for small samples – t and F distributions.

Unit II NON-PARAMETRIC METHODS 12


Chi-square tests - independence of attributes and goodness of fit - Sign test for paired data - Rank sum test –
Kolmogorov Smirnov test for goodness of fit - Mann–Whitney U test - Kruskal Wallis test - One sample run test
- Rank correlation.

Unit III CURVE FITTING 10


Correlation –Multiple Correlation-Regression –Multiple Regression –Linear fit-Quadratic fit-Cubic Splines

Unit IV TIME SERIES AND RELIABILITY 14


Time series-characteristics and Representation- Moving averages –Exponential Smoothing-Auto Regressive
processes. Time series analysis: Variations in time series, Trend analysis, Cyclical variations, Seasonal
variations and Irregular variations. Concepts of reliability-hazard rate-Endropy-Reliability of series and parallel
systems- Mean time to Failure-Mean time Between Failure.

Unit V QUEUING MODELS 12


Markovian queues – Single and Multi-server Models – Little’s formula – Machine Interference Model - Non-
Markovian Queues – Pollaczek Khintchine Formula.

REFERENCE(S):
th
1. Fruend John, E. and Miller, Irwin, "Probability and Statistics for Engineers “, PHI, 8 edition, 2011.
th
2. Jay, L. Devore, "Probability and Statistics for Engineering and Sciences", Cengage Learning, Inc., 8 edition, 2010.

3. Montgomery D.C and Johnson, L.A., "Forecasting and Time Series", McGraw-Hill, New York, 1990.

4. Anderson, O.D., "Time Series Analysis: Theory and practice ", I. North - Holland, Amsterdam, 1982.
Department CHEMICAL ENGINEERING R 2019 Semester I PC
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
ADVANCED TRANSPORT 3 0 0 3 45 100
19MCH12
PHENOMENA
Course Objective (s): The purpose of learning this course is
 The course will accustom the students with import topics in Advanced Transport Phenomena (momentum, heat and
mass transport).
 To develop physical understanding of principles discussed and with emphasis on chemical engineering applications.

Course Outcomes: At the end of this course, learners will be able to


 Ability to set up and solve differential momentum, heat, and mass balances for 1-D steady state problems and
quasi-steady-state problems occurring in laminar and turbulent flows in terms of vector and tensor fluxes.

 Formulate conservation statements in heat, mass, and momentum at multi-scales from microscopic to
macroscopic in both steady and unsteady modes.

 Analyze advanced transport problems in heat; mass and momentum, both macroscopic and microscopic
formulate simultaneous energy and mass balances in chemical processes.

Unit I MOMENTUM TRANSPORT 9


Introduction to concepts and definitions, Newtonian and non-Newtonian Fluid Models, Review of Shell balance
method and Equations of changes for fluid flow problems (Flow over flat plate, though pipes, packed bed and fluidized
beds)Turbulent Flow - Equation of changes, phenomenological theories, Turbulent flow in closed conduits and
analysis of different velocity distributions, Boundary layer theory: Equation of changes, Blasius Exact solution
method, Von Karman Integral momentum method, Boundary layer separation.
Unit II ENERGY TRANSPORT 9
Application of Shell balance and Equations of changes for temperature distributions in heat flow problems Steady state
conduction, Combination of heat transfer resistance, Different method of analysis for Multidimensional Steady and
Unsteady state heat conduction, Convection heat transfer co-efficient, Heat transfer during Laminar and Turbulent
flow in closed conduits
Unit III MASS TRANSPORT 9
Application of Shell balance method and Equations of changes for mass transfer problems, Concentration
distributions for isothermal and non- isothermal mixtures, Multi component systems, with more than one independent
variable and in turbulent flow
Unit IV CONVECTIVE MASS TRANSFER 9
Convective mass transfer and correlation, interphase mass transfer, Macroscopic balance for multi component system,
Mass transfer with chemical reactions
Unit V CONVECTIVE HEAT TRANSFER 9
Dimensional analysis in fluid dynamics, Convection heat transfer, Boiling and Condensation heat transfer, Heat
transfer in Liquid metals, Empirical correlation for high Prandtl Number of fluids, Analogy between momentum and
heat transfer
TEXT BOOK(S):

1. R. Byron Bird, Warren E. Stewart and Edwin N. Lightfoot, “Transport Phenomena”, Revised Second Edition,
John Wiley & Sons, 2007.

REFERENCE(S):
1. James Welty, Charles E. Wicks and Wilson, Gregory L Rorrer, “Fundamentals of Momentum, Heat and Mass
transfer”, 5th Edition, 2008.
2. C. O.Bennet and J. O. Meyers, “Momentum, Heat and Mass Transfer” McGraw Hill, 1995

3. J.P. Holman, “Heat Transfer”, 8th Edition, McGraw Hill, New York, 1997

4. H. Schlichting, Boundary-Layer Theory, 7th edition, McGraw-Hill, Inc.


Department CHEMICAL ENGINEERING R 2019 Semester I PC
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
ADVANCED SEPARATION 3 0 0 3 45 100
19MCH13
TECHNOLOGY
Course Objective (s): The purpose of learning this course is to
 Accustom the students to learn the principle and technical concept of advanced separation processes.

Course Outcomes: At the end of this course, learners will be able to


 Create awareness among students with new and unconventional separation processes

 Acquire sufficient knowledge in energy intensive processes for separation of components

 Students will be equipped with the applications in Down-streaming processes

Unit I GENERAL 9
Review of conventional processes, recent advances in separation techniques based on size, surface properties, ionic
properties and other special characteristics of substances. process concept, theory and equipment used in cross flow
filtration, cross flow electrofiltration, dual functional filter, Surface based solid-liquid separations involving a second
liquid, Sirofloc filter
Unit II MEMBRANE SEPARATIONS 9
Types and choice of membranes, Plate and frame, Tubular, Spiral wound and hollow fibre membrane reactors and their
relative merits, Commercial, Pilot plant and laboratory membrane pemeators involving dialysis, Reverse osmosis,
Nanofiltration, Ultra filtration, Microfiltration and Donnan dialysis, Economics of membrane operations, Ceramic
membranes
Unit III SEPARATION BY ADSORPTION TECHNIQUES 9
Mechanism, Types and choice of adsorbents, Normal adsorption techniques, Affinity chromatography and immuno
chromatography, Types of equipment and commercial processes, Recent advances and process economics

Unit IV IONIC SEPARATIONS 9


Controlling factors, Applications, Types of equipment employed for electrophoresis, Dielectrophoresis, Ion Exchange
chromatography and electrodialysis, Commercial processes.
Unit V OTHER TECHNIQUES 9
Separations involving lyophilization, Perevaporation and permeation techniques for solids, liquids and gases, Industrial
viability and examples, Zone melting, Adductive crystallization, other separation processes, supercritical fluid
extraction, oil spill management, Industrial effluent treatment by modern techniques.
TEXT BOOK(S):

1. King, C. J., “Separation Processes”, Tata McGraw Hill Co., Ltd., 1982.

REFERENCE(S):
1. Nakagawal, O. V., “Membrane Science and Technology”, Marcel Dekker, 1992.
2. Rousseau, R. W. “Handbook of Separation Process Technology”, John Wiley, New York, 1987.
3. Humphrey, J and G. Keller, Separation Process Technology, McGraw-Hill, 1997.
Department CHEMICAL ENGINEERING R 2019 Semester I PC
Course Hours /Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCH14 FLUID PHASE EQUILIBRIA 3 0 0 3 45 100
Course Objective (s): The purpose of learning this course is
 The course will engage the students with important topics in Fluid Phase Equilibria.
 The Focus will be to develop Physical understanding of Principles involved in Fluid Phase Equilibria.

Course Outcomes: At the end of this course, learners will be able to


 Have a deep understanding of thermodynamics of fluid phase equilibria.

 Gain knowledge in Multicomponent mixtures, Phase and Chemical equilibria concepts.

Unit I BASIC CONCEPTS 9


Energy and first Law; Reversibility and second Law; Review of Basic Postulates, Equilibrium
criteria, Legendre Transformation and Maxwell’s relations
Unit II STABILITY AND PHASE TRANSITION 9
Stability of thermodynamic systems, First order phase transitions and critical phenomenon,
Phase rule, Single component phase diagrams, Thermodynamic properties from Volumetric and
Thermal data
Unit III MULTI-COMPONENT MIXTURES 9
Partial molar properties, Fugacities in gas and liquid mixtures, Activity coefficients, Ideal and
Non-ideal solutions, Gibbs-Duhem equation, Wilson, NRTL, and UNIQUAC equations, UNIFAC method
Unit IV PHASE EQUILIBRIUM 9
VLE - Equations of state, Corresponding states, Henry’s Law, Lattice theory, Criticality, High pressure VLE. Other
phase equilibriums- SLE/LLE/VLLE.
Unit V CHEMICAL EQUILIBRIUM 9
Homogeneous gas and liquid phase reactions, Heterogeneous reactions – Phase and Chemical equilibrium

TEXT BOOK(S):
1. Rao., Y.V.C., Chemical Engineering Thermodynamics, University Press, Hyderabad,2005

REFERENCE BOOK(S):
1. Tester, J. W. and M. Modell, Thermodynamics and Its Applications. 3rd Edn. Prentice Hall, New Jersey, 1997.

2. Prausnitz, J.M., Lichtenthaler R.M. and Azevedo, E.G., Molecular Thermodynamics of Fluid Phase Equilibria,
3rd Edition, Prentice Hall India, 1999.
Department CHEMICAL ENGINEERING R 2019 Semester I PC
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCH15 ADVANCED CHEMICAL 3 0 0 3 45 100
REACTION ENGINEERING
Course Objective (s): The purpose of learning this course is
 To study the behavior of catalytic heterogeneous reactors, Gas-Solid catalytic and Non-catalytic reactors and Gas-
Liquid reactors.

Course Outcomes: At the end of this course, learners will be able to


 Understand the kinetics involved in heterogeneous reactions

 Have a great knowledge in Catalysis and Catalytic reactors

 Analyze and design heterogeneous reactors based on the industrial needs.

Unit I KINETICS OF HETEROGENEOUS REACTIONS 9


Catalytic reactions, Rate controlling steps, Langmuir-Hinshelwood model, Eley-Rideal mechanism,
Steady state approximation, Non-catalytic fluid-solid reactions, Shrinking and unreacted core model.
Unit II EXTERNAL DIFFUSION EFFECTS IN HETEROGENEOUS REACTIONS 9
Mass and heat transfer coefficients in packed beds, Quantitative treatment of external transport effects, Modeling
diffusion with and without reaction.
Unit III CATALYSIS AND CATALYTIC REACTORS 9
Catalyst properties – Adsorption Isotherms – Surface reactors – Desorption – Rate limiting steps – Is adsorption of
Cumene rate limiting – Cumene decomposition – Chemical vapour deposition catalyst deactivation – Reaction
Engineering in Microelectronic device fabrication.
Unit IV INTERNAL TRANSPORT PROCESSES IN POROUS CATALYSTS 9
Interpellet Mass and Heat transfer, Evaluation of Effectiveness factor, Mass and heat transfer with reaction.

Unit V ANALYSIS AND DESIGN OF HETEROGENEOUS REACTORS 9


Isothermal and adiabatic fixed bed reactors, Non-isothermal and Non-adiabatic fixed bed Reactors, Two-phase
fluidized bed model, Slurry Reactor Model, Trickle bed reactor model - Experimental determination and Evaluation
of Reaction Kinetics for heterogeneous systems.

TEXT BOOK(S):
1. Carberry, J. J., “Chemical and Catalytic Reaction Engineering”, Dover Publications, 2001.

REFERENCE BOOK(S):

1. Froment, G. F. and Bischoff, K. B., “Chemical Reactor Design and Analysis”, 2 nd Edition, John Wiley & Sons,
New York, 1997.
Department CHEMICAL ENGINEERING R 2019 Semester I PC
Course Code Course Name Hours/Week Credit Total Maximum Marks
L T P C Hours
19MCH16 INSTRUMENTAL 0 0 4 2 30 100
METHODS OF
ANALYSIS
LABORATORY
Course Objectives: The purpose of learning this course is
 To enable the students to develop a sound working knowledge on modern instruments which is used for
analyzing chemical samples.
Course Outcome: At the end of this course, learners will be able to
 Gain knowledge about working principles of Sophisticated instruments like UV visible
Spectrophotometer, conductivity meter etc.,
LIST OF EXPERIMENTS
1. Validate Lambert-Beer's law in UV-VIS Spectrophotometer using given sample.
2. Determine the strength and amount of given solution using conductivity meter
3. Determine the amount of ion present in the given solution using Potentiometer.
4. Determine the amount of acid present in the whole of the given sample by using pH meter.
5. Determine the amount of dissolved oxygen in the given sample.
6. Using Flame Photometer, prepare a standard graph of Concentration and Photo-detector value for a
given compound.
7. Identify the reactor which works on cavitation principles and carry out the experimental
studies.
8. Determine the flash point & fire point of the given sample.
9. Determine the smoke point of the given sample.
10. Determine the viscosity of the lubricating oils by viscometer method.
LIST OF EQUIPMENT FOR BATCH OF 30 STUDENTS
1. UV-Visible spectrophotometer 1 No.
2. Conductivity meter 1 No.
3. Potentiometer 1 No.
4. pH meter 1 No.
5. Dissolved Oxygen meter 1 No.
6. Flame photometer 1 No.
7. Sonochemical Reactor 1 No.
8. Flash and Fire point apparatus 1 No.
9. Smoke Point apparatus 1 No.
10. Viscometer 1 No.
Department ENGLISH R 2019 Semester I EEC
Hours/Week Credit
Course Code Course Name Total Hours Maximum Marks
L T P C
19MCD01 BUSINESS ENGLISH - I 0 0 4 2 30 100
Course Objective (s): The purpose of learning this course is to
 Develop inter personal skills and be an effective goal oriented team player.
 Develop professionals with idealistic, practical and moral values.
 Develop communication in writing techniques.
 Develop creative thinking.
Course Outcomes: At the end of this course, learners will be able to
 Analyze their strength and weakness.
 Understand the importance of non verbal communication.
 Communicate and present their ideas creatively.
 Prepare Resume and write report effectively on their own.
UNIT I SELF INTRODUCTION 6
Self-Analysis – Self Introduction – Ice breaking - Identify Strength and Weakness – Self-esteem and Confidence
UNIT II PRESENTATION SKILLS 6
Non-Verbal – Body Language of self and others Presentation Skills – Stages involved in an effective presentation
– Selection of topic, Content, Aids – Engaging the audience - Time management.
UNIT III GRAMMAR 6
Parts of Speech, Synonyms, Antonyms, Word Groups, and Verbal Analogy
UNIT IV THINKING ABILITY 6
Out of box thinking - General behaviors for creative thinking.
UNIT V RESUME PREPARATION 6
Preparing Resume, CV and Report.
REFERENCES:

1. 1. Andrews, Sudhir “How to Succeed at Interviews”, 21st Reprint. Tata McGraw-Hill, New Delhi, 1988.
SEMESTER-II

Department CHEMICAL ENGINEERING R 2019 Semester II PC


Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCH21 CHEMICAL PROCESS DESIGN 3 0 0 3 45 100
Course Objective (s): The purpose of learning this course is to
 Accustom the students to understand advances in the design of chemical process equipment.
 Exposure to classic and current procedures in the chemical process design field.

Course Outcomes: At the end of this course,


 Students will have awareness on advances in process engineering design of many process equipments.
 Exposed to process integration approach before proceeding for design any process Equipments.
 Awareness on use of Aspen plus for simulation different process.

Unit I INTRODUCTION 9
The Hierarchy of Chemical process Design- Overall process Design, Approaches to design.
Unit II CHOICE OF REACTORS AND SEPARATORS 9
Reaction path, Reactor performance, Practical reactors, Separation of Heterogeneous mixtures, Homogeneous fluid
mixtures.
Unit III SYNTHESIS OF REACTION – SEPARATION SYSTEMS 9
Process recycle, Batch processes, Process yield
Unit IV DISTILLATION SEQUENCING 9
Using simple columns, Using columns with more than two products, Distillation Sequencing-Using thermal
coupling.
Unit V HEAT EXCHANGER NETWORK & UTILITIES – ENERGY TARGETS 9
Heat recovery pinch, The Problem table Algorithm, Utilities Selection, Energy targets capital &
Total Cost targets -Number of Heat Exchanger Units, Area Targets, Number of Shells Targets, Capital Cost Targets,
Total Cost Targets.

TEXT BOOK(S):
1. Smith, R., “Chemical Process Design”, McGraw Hill, New York, 1995.

REFERENCE BOOK(S):
1. Douglas, J.M., “Conceptual Design of Chemical Process”, McGraw Hill, New York,1988.
Department CHEMICAL ENGINEERING R 2019 Semester II PC
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCH22 COMPUTER CONTROL OF 3 0 0 3 45 100
PROCESSES
Course Objective (s): The purpose of learning this course is
 Understand the important topics in Computer Control of processes.
 Develop understanding of principles discussed and with emphasis on Computer Control of processes.
 Exposed to classic and current technology related to Computer Control in Chemical Engineering.

Course Outcomes: At the end of this course, learners will be able to


 Have a good knowledge in controller tuning
 Know the type of controller that can be used for specific problems in chemical industry
 Design of controllers for interacting multivariable systems
 Design of digital control systems
Unit I REVIEW OF SYSTEMS 9
Review of first and higher order systems, Closed and Open loop response. Response to step, Impulse and Sinusoidal
disturbances. Transient response - Block diagrams.
Unit II STABILITY ANALYSIS 9
Frequency response, design of control system, controller tuning and process identification. Zigler-Nichols and Cohen-
Coon tuning methods, Bode and Nyquist stability criterion. Process identification.
Unit III SPECIAL CONTROL TECHNIQUES 9
Advanced control techniques, Cascade, Ratio, Feed forward, Adaptive control, Smith predictor, Internal model
control
Unit IV MULTIVARIABLE CONTROL ANALYSIS 9
Introduction to state-space methods, Control degrees of freedom analysis and analysis, Interaction, Bristol arrays,
Nieder linski index - Design of controllers, Tuning of multivariable controllers.
Unit V SAMPLE DATA CONTROLLERS 9
Basic review of Z transforms, Response of discrete systems to various inputs. Open and closed loop response to step,
Impulse and sinusoidal inputs, Closed loop response of discrete systems - Design of digital controllers - Introduction to
PLC and DCS.

TEXT BOOK(S):
1. D.R. Coughanour, ‘Process Systems analysis and Control’, McGraw-Hill, 2nd Edition, 1991.
2. D.E. Seborg, T.F. Edger, and D.A. Millichamp, ‘Process Dynamics and Control’, John Wiley and Sons, 2nd
Edition, 2004.
REFERENCE BOOK(S):

1. B.A.Ogunnaike and W.H.Ray, “Process Dynamics, Modelling and Control”, Oxford


Press, 1994.
2. W.L.Luyben, ‘Process Modelling Simulation and Control for Chemical Engineers’,
McGraw Hill, 2nd Edition, 1990.
3. B.W. Bequette, ‘Process Control: Modeling, Design and Simulation’, PHI, 2006.

4. S. Bhanot, ‘Process Control: Principles and Applications’, Oxford University Press,


2008.
Department CHEMICAL ENGINEERING R 2019 Semester II PC
Course Hours/ Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCH23 ADVANCED BIOCHEMICAL 3 0 0 3 45 100
ENGINEERING
Course Objective (s): The purpose of learning this course is
 To allow the students to know the crucial chemical engineering aspects of the development of biological
processes associated with everything from raw materials to product recovery, relevant to industries.

Course Outcomes: At the end of this course, learners will be able to


 Know the different types of reactors used in biochemical engineering and their uses.

 Understand the kinetics of batch and continuous reactions.

 Exposed to design principles associated with biochemical engineering

Unit I IDEAL REACTORS 9


Concept of ideal reactors based on flow characteristics, Design of ideal reactors using material and energy balance
equations. Single reactors, with ideal flow condition, Comparison of volumes of plug flow reactor and chemostats.
Multiple reactors-Methods to show how total volume is affected in multiple reactors. Searching for mechanism –
Arrhenius equation – Batch reactor analysis for kinetics (Synchronous growth and its application in product
production).
Unit II KINETICS OF BATCH AND CONTINUOUS REACTIONS 9
Growth Kinetics: Batch growth quantifying cell concentration, Growth profiles and kinetics in batch culture, fed
batch growth, continuous growth and their growth kinetic quantification, Chemostat growth, Semi-continuous/
Exponential feeding strategy. Maximizing the yield of intermediate product in series reactions.
Unit III DESIGN PRINCIPLES 9
Design principles – Non isothermal reactions and Pressure effects;
Unit IV RTD STUDIES 9
Non-ideal flow in bioreactors-reasons for non-ideality, Concept of RTD studies, Characterization of non-ideality
using RTD studies, Various distribution functions, Conversions using tracer studies. Diagnosing the ills of non-ideal
bioreactors, Various models of non-ideal flow.
Unit V DESIGN OF REACTORS 9
Design and analysis of bioreactors - Stability and analysis of bioreactors, Biomass production and effect of dilution
rate - Design and operation of various bioreactors, viz. CSTR, Fed batch systems, Air-lift bioreactors, Fluidized bed
bioreactors - Scale up of bioreactors - Criteria for selection of bioreactors.

TEXT BOOK(S):
1. James E Bailey, David F Ollis Biochemical Engineering Fundamentals, Tata McGraw-Hill, 2 nd Edition, 2001.

2. Rajiv Dutta, Fundamentals of Biochemical Engineering, Springer Publishing House, 2008.


REFERENCE BOOK(S):

1. D. Ramakrishna et al., Advances in Biochemical Engineering, Springer-Verlag Berlin and Heidelberg GmbH &
Co. KG, 2008.
Department CHEMICAL ENGINEERING R 2019 Semester II PC
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCH24 INDUSTRIAL WASTE 3 0 0 3 45 100
MANAGEMENT
Course Objective (s): The purpose of this course is to
 Train the students in different waste management techniques.
 Know the Techniques for transformation of waste materials into products that can be beneficially utilized.
 Gain knowledge about Proper Waste Management with the goal of utilizing the waste material in best possible
way.

Course Outcomes: At the end of this course, learners will be able to


 Know the overall Waste Management System and the definitions involved in it
 Exposed to the topics of Material recycling, Metals, Treatment of liquid waste streams,
 Have a deep understanding of Solid Waste Management, Radioactive wastes and Emerging technologies
associated with it.
Unit I SOLID WASTE – CHARACTERISTICS AND PERSPECTIVES 9
Definition - Types – Sources – Generation and Estimation. Properties: Physical, Chemical and
Biological – Regulation
Unit II COLLECTION, TRANSPORTATION AND PROCESSING TECHNIQUES 9
Onsite handling, Storage and Processing – Types of Waste Collection Mechanisms - Transfer
Stations : Types and location – Manual component separation - Volume reduction : Mechanical,
Thermal – Separation : Mechanical, Magnetic Electro Mechanical
Unit III ENERGY GENERATION TECHNIQUES 9
Basics, Types, Working and Typical conversion Efficiencies of Composting – Anaerobic Digestion
– RDF – Combustion – Incineration – Gasification – Pyrolysis
Unit IV HAZARDOUS WASTE MANAGEMENT 9
Hazardous waste – Definition - Potential sources - Waste sources by industry – Impacts –
Waste control methods – Transportation regulations - Risk assessment – Remediation
Technologies – Private public partnership – Government initiatives.
Unit V ULTIMATE DISPOSAL 9
Landfill – Classification – Site selection parameters – Design aspects – Leachate control –
Environmental monitoring system for LandFill Gases.

TEXT BOOK(S):
nd
1. Tchobanoglous, Theisen and Vigil, Integrated Solid Waste Management, 2 Edition, McGraw Hill, New York,
1993.
2. Howard S. Peavyetal, Environmental Engineering, McGraw Hill International Edition, 1985.
REFERENCE BOOK(S):
1. LaGrega, M., et al., Hazardous Waste Management, McGraw Hill, 2nd edition, 2001.

2. Stanley E. Manahan. Hazardous Waste Chemistry, Toxicology and Treatment, Lewis Publishers, Chelsea,
Michigan, 1990
3. Parker, Colin and Roberts, Energy from Waste – An Evaluation of Conversion Technologies, Elsevier Applied
Science, London, 1985.
Department CHEMICAL ENGINEERING R 2019 Semester II PC
Course Code Course Name Hours / Week Credit Total Maximum Marks
L T P C Hours
19MCH25 SEMINAR 0 0 4 2 30 100

Course Objective (s): The purpose of this seminar is to


 Make the student to update himself to the current advancements in Chemical Engineering field.

Course Outcomes: At the end of this course, students will be able to


 Update themselves to the current technology in the Chemical Engineering and its allied field.

Method of Evaluation:
 Students are expected to present two seminars along with report on any recent topic in Chemical
Engineering. They will be evaluated depending upon their presentation which includes the content of the
seminar, way of presentation, relevant to the current technology etc.,
Department ENGLISH R 2019 Semester II EEC
Hours / Week
Course Credit Total Maximum
Course Name
Code L T P C Hours Marks
19MCD02 BUSINESS ENGLISH-II 0 0 4 2 30 100
Course Objective (s): The purpose of learning this course is to
 Acquire skills for using English in workplace effectively
 Communicate for essential business needs
 Prepare students for taking BEC Vantage level examination which is an International Benchmark for English
language proficiency of Cambridge English Language Assessment (CELA)
 Enhance the communicative ability from Intermediate to Upper Intermediate level
Course Outcomes: At the end of this course, learners will be able to
 Facilitate students to get International recognition for work and study.
 Exploit English confidently in the International business environments.
 Learned to be part in business discussion, read company literature, write formal and informal business
correspondences and listen and understand business conversations.
Unit I GRAMMAR AND VOCABULARY 6

Simple, compound and complex sentences - Direct and indirect speech - Conditionals - Business vocabulary –
Collocations – Discourse markers
Unit II LISTENING 6

Listening to identify topic, content, function - Sentence stress - Rhythm – Intonation

Unit III READING 6

Reading graphs and charts - Skimming and scanning texts - Job advertisements - Read business articles for
Specific Information – Understanding the structure of a text – Error identification
Unit IV WRITING 6

Formal and Informal English - Longer Documents: writing individual paragraphs to longer text, Business
Correspondence , Reports and proposals – Transcoding
Unit V SPEAKING 6
Collaborative task - Turn taking (initiating and responding appropriately) - Negotiating - Exchanging –
Language Functions: suggesting - comparing and contrasting –expressing -Finding out facts, attitudes and
opinions - Commonly mispronounced words
SEMESTER-III

Department CHEMICAL ENGINEERING R 2019 Semester III PC


Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCH31 PROCESS MODELING AND 3 0 0 3 45 100
SIMULATION
Course Objective (s): The purpose of learning this course is
 To give an overview of various methods of process modeling, different computational techniques for
simulation.
 To learn the techniques, rather than specific applications in order to take up modeling and simulation
challenges in his profession.
Course Outcomes: At the end of this course, learners will be able to
 Develop process models based on conservation principles and process data

 Solve the process models by using various computational techniques

Unit I INTRODUCTION 9
Introduction to modeling and simulation, Classification of Mathematical models, Conservation equations and
auxiliary relations.
Unit II STEADY STATE LUMPED SYSTEMS 9
Degree of freedom analysis, Single and network of process units, Systems yielding linear and non linear algebraic
equations, Flow sheeting – Sequential modular and equation oriented approach, tearing, partitioning and precedence
ordering, Solution of linear and non-linear algebraic equations.
Unit III UNSTEADY STATE LUMPED SYSTEMS 9
Analysis of liquid level tank, Gravity flow tank, Jacketed stirred tank heater, Reactors, Flash and distillation
column, Solution of ODE initial value problems, Matrix differential Equations, Simulation of closed loop systems.
Unit IV STEADY STATE DISTRIBUTED SYSTEM 9
Analysis of compressible flow, Heat exchanger, Packed columns, Plug flow reactor, Solution of
ODE boundary value problems.
Unit V UNSTEADY STATE DISTRIBUTED SYSTEM 9
Analysis laminar flow in pipe, Sedimentation, Boundary layer flow, Conduction, Heat exchanger, heat transfer in
packed bed, Diffusion, Packed bed adsorption, Plug flow reactor, Hierarchy in model development, Classification
and solution of partial differential equations – Empirical Modeling, parameter estimation, Population balance and
stochastic modeling.

TEXT BOOK(S):

1. Ramirez, W., "Computational Methods in Process Simulation", 2nd Edition, Butterworths,New York, 2000.

2. Luyben, W.L., "Process Modelling Simulation and Control", McGraw-Hill Book Co., 1973.

3. Felder, R. M. and Rousseau, R. W., “Elementary Principles of Chemical Processes’’, JohnWiley, 2000.

4. Franks, R. G. E., “Mathematical Modelling in Chemical Engineering’’, John Wiley, 1967.


Department CHEMICAL ENGINEERING R2019 Semester III EEC
Course Code Course Name Hours / Week Credit Total Maximum Marks
L T P C Hours
19MCH32 PROJECT WORK 0 0 12 6 90 100
PHASE I
Course Objective (s): The purpose of this course to
 Allow the student to do a project work in his interested core chemical engineering field and it also allow them
to update to the current advancements in Chemical Engineering field.

Course Outcomes: At the end of this course, students will be able to


 Update themselves to the current technology in the Chemical Engineering and its allied field.

Method of Evaluation: Students have to do a research-based project in the department or in an industry and
submit a detailed report at the end of Phase I

SEMESTER-IV
Department CHEMICAL ENGINEERING R 2019 Semester IV EEC
Course Code Course Name Hours / Week Credit Total Maximum Marks
L T P C Hours
19MCH41 PROJECT WORK 0 0 24 12 180 100
PHASE II
Course Objective (s): The purpose of this course to
 Allow the student to do a project work in his interested core Chemical Engineering field and it also allow
them to update to the current advancements in Chemical Engineering field.

Course Outcomes: At the end of this course, students will be able to


 Update themselves to the current technology in the Chemical Engineering and its allied field.

Method of Evaluation: Phase II of Project Work is a continuation of Phase I of Project. Students submit a report
at the end of Phase II.
Department CHEMICAL ENGINEERING R 2019 Semester I PE
Course Hours / Week Credit Total Maximum Marks
Code Course Name L T P C Hours
19MCX01 ENVIRONMENTAL RISK 3 0 0 3 45 100
ASSESSMENT
Course Objective (s): The purpose of learning this course is
 To illuminate the general principles of environmental risk assessment
Course Outcomes: At the end of this course, learners will be able to
 Understand about the risk analysis, available methodologies, risk contours for failure scenarios, safety
measures design and past accident analysis.

Unit I INTRODUCTION TO RISK ANALYSIS 9


Risk analysis introduction, Quantitative risk assessment, Rapid risk analysis – Comprehensive risk analysis –
Identification, Evaluation and Control of risk
Unit II RISK ASSESSMENT 9
Risk assessment – Introduction and available methodologies, Risk assessment steps, Hazard identification,
Hazard assessment (Consequence analysis), Probabilistic hazard assessment (Fault tree analysis)
Unit III FAILURE ANALYSIS 9
Overall risk contours for different failure scenarios – Disaster management plan – Emergency planning – onsite and
offsite emergency planning, Risk management ISO 14000, EMS models – case studies – Marketing terminal,
Gas processing complex.
Unit IV ACCIDENTS 9
Safety measures design in process operations. Accidents Modeling – Release modeling, Toxic release and dispersion
modeling, Fire and Explosion modeling.
Unit V MITIGATING INDUSTRIAL ACCIDENTS 9
Past accident analysis: Flux borough – Mexico – Bhopal analysis. Government policies to manage environmental risk

TEXT BOOK(S):

1. Crowl D.A and Louvar J.F. Chemical Process Safety; Fundamentals with applications, Prentice hall
Publication, 2002.
2. Khan F.I and Abbasi, S.A., Risk assessment of Chemical Process Industries; Emerging
Technologies, Discovery Publishing House, New Delhi, 1999.

REFERENCE BOOK(S):

1. Houstan H.B., Process Safety Analysis, Gulf Publishing Company, 1997.


Department CHEMICAL ENGINEERING R 2019 Semester I PE
Course Hours / Week Credit Total Maximum Marks
Code Course Name L T P C Hours
19MCX02 MULTIPHASE FLOW 3 0 0 3 45 100
Course Objective (s): The purpose of learning this course is
 To analyze, characterize the multiphase systems and appreciate the role of structure in
multiphase flows.
 To understand the limitations of modeling in multiphase flows and
 To comprehend engineering problems involving multiphase flows.
Course Outcomes: At the end of this course, learners will be able to
 Develop a sound knowledge on underlying concepts of multiphase flows and different
approaches to model such flows under different conditions.

Unit I CHARACTERISTICS OF MULTIPHASE FLOWS 9


Significance of multiphase flows, Important non-dimensional numbers, Parameters of characterization, Particle size
measurement, Size distribution and moments, Size distribution models
Unit II PARTICLE FLUID INTERACTION 9
Equation of motion for a single particle, Calculation of drag, Motion of a particle in two dimensions, Effects
of unsteady and non-uniform flow fields, Effect of acceleration, Effect of coupling; Interaction between particles,
Mechanism of interaction, Interparticle forces, Hard sphere model, Soft sphere model, Discrete element modeling,
Semi-empirical methods, Kinetic theory, Force chains.
Unit III MODELING OF MULTIPHASE FLOWS 9
Flow patterns - Identification and Classification - Flow pattern maps and transition – Momentum and energy
balance - Homogeneous and separated flow models - Correlations for use with homogeneous and separated flow
models - Void fraction and slip ratio correlations – Influence of pressure gradient- Empirical treatment of two phase
flow - Drift flux model - Correlations for bubble, Slug and Annular flows

Unit IV CONSERVATION EQUATIONS 9


Averaging Procedures - Time, Volume and ensemble averaging, Quasi-one-dimensional flow, Two-fluid Volume -
Averaged equations of motion, Turbulence and two-way coupling.
Unit V SAMPLE DATA CONTROLLERS 9
Flow regime and hydrodynamic characteristics of packed bed, Fluidized bed, Pneumatic Conveying, bubble column,
Trickle beds; Conventional and novel measurement techniques for multiphase systems including CARPT,
Laser Doppler anemometry, Particle Image Velocimetry.

TEXT BOOK(S):

1. Clift, R., Weber, M.E. and Grace, J.R., Bubbles, Drops, and Particles, Academic Press, New York, 2005.

2. Crowe, C. T., Somerfield, M. and Tsuji, Y., Multiphase Flows with Droplets and Particles,
CRC Press, 2011.
REFERENCE BOOK(S):
1. Fan, L. S. and Zhu, C., Principles of Gas-solid Flows, Cambridge University Press, 2005.
2. Govier, G. W. and Aziz. K., “The Flow of Complex Mixture in Pipes”, Van Nostr and Reinhold, New York,
1972.
3. Kleinstreuer, C., Two-phase Flow: Theory and Applications, Taylor & Francis, 2003
Department CHEMICAL ENGINEERING R 2019 Semester I PE
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCX03 POLYMER SCIENCE AND 3 0 0 3 45 100
ENGINEERING
Course Objective (s): The purpose of learning this course is
 Students will be able to know the general aspects of polymers and their types.
 To know the physical and chemical properties of polymers.
Course Outcomes: At the end of this course, students will be able to
 Gain a wider knowledge in Polymer Science and Engineering and their importance in Chemical Engineering
field.
Unit I GENERAL ASPECTS OF POLYMERS 9
Classification, Mechanisms and methods of Polymerization, Properties - Molecular weight, Glass transition
temperature, Crystallinity, Thermal, Electrical and Mechanical properties.
Unit II APPLICATION ORIENTED POLYMERS 9
Resins-PVC-Silicon oil and resin, Fibrous polymers-nylon 66, Polyacrylonitrile, Adhesives Epoxides,
phenol formaldehyde, urea formaldehyde.
Unit III ELASTOMERS 9
Natural rubber, styrene-butadiene, poly isopropane-neoprene, silicon rubber, thermoplastic elastomer.
Unit IV PROCESSING OF POLYMERS 9
Processing additives, plasticizer, anti-aging additives, surface and optical properties, modifiers, fire retardants,
additives for rubber and elastomer, various molding techniques.
Unit V GRID GENERATION 9
Mechanical properties, tensile strength and hardness, electrical properties, volume resistivity, dielectric strength,
optical properties glass, light transmission and refractive index, Chemical analysis - Elemental and Functional
analysis.

TEXT BOOK(S):

1. Miles, D.C & Briston, J.H. “Polymer Technology”, Chemical publishing Co: Inc: NY:1979

2. Maturine Morton, “Rubber Technology”, 3rd Edition, Van Nostrand Re Inhold, NY:1987.

REFERENCE BOOK(S):

1. Masic L. “Thermoplastics Materials Engineering”, Applied Science Publishers Ltd, NY:1986


Department CHEMICAL ENGINEERING R 2019 Semester I PE
Course Hours / Week Credit Total Maximum Marks
Code Course Name L T P C Hours
19MCX04 Petroleum Refinery Engineering 3 0 0 3 45 100
Course Objective (s): The purpose of learning this course is
 To know the refinery distillation process and their importance in Petroleum refinery.
 To gain knowledge on lube refining processes, wax refining processes.
 To study the hydroprocessing treatment techniques and their applications in Petroleum refineries.
Course Outcomes: At the end of this course, students will be able to
 Students develop a wider knowledge on basics of refinery distillation process.
 Have a deep understanding on lube refining processing technologies as well as wax refining methods.
Unit I REFINERY DISTILLATION PROCESS 9
Desalting and Stabilization of crude, Process description of typical simple distillation, Fractional distillation, crude oil
distillation, Vacuum Distillation etc. Degree of separation (5-95 gap) and degree of difficulty of separation (Δ t 50),
Packie charts, ASTM, TBP and EFV Distillation.
Unit II FUEL REFINING 9
Cracking, Coking, Reforming, Alkylation, Isomerisation, Polymerization, Sweetening, Visbreaking. Thermal and
Catalytic Solvent extraction and Adsorption with respect to refining industry.
Unit III LUBE REFINING 9
Solvent extraction, Dewaxing , Propane deasphalting
Unit IV WAX REFINING 9
Deoiling of crude wax, Crystallization, Catalytic, Sweetening Process, Microcrystalline and Petroleum wax
applications.
Unit V HYDRO PROCESSING TREATMENT TECHNIQUES 9
Hydro cracking, Hydro treating, Hydro finishing, Process description of typical light ends unit, Acid gas removal
using gas treating processes, Hydrogen Production and Hydrogen Management in refineries.

TEXT BOOK(S):
1. Nelson W L, “Petroleum Refinery Engineering”, McGraw Hill Book Co., 1985.
2.
Watkins R N, “Petroleum Refinery Distillation”, Gulf Publishing Co.

REFERENCE BOOK(S):

1. Gary J H and Handework G E, “Petroleum Refining Technology and Economics”, Marcel Dekker, Inc., 2001.

2.
Waquier J P, “Petroleum Refining” Vol. I & II Editions, Technip, 1995.
Department CHEMICAL ENGINEERING R 2019 Semester II PE
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCX05 MULTI-COMPONENT 3 0 0 3 45 100
DISTILLATION
Course Objective (s): The purpose of learning this course is
 To study the various distillation methods and their applications.
 To understand the limitations involved in Multi-component distillation
Course Outcomes: At the end of this course, learners will be able to
 Students develop a sound knowledge on underlying concepts of Multi-component distillation and
different approaches to model such flows under different conditions.
Unit I THERMODYNAMIC PRINCIPLES 9
Fundamental Thermodynamic principles involved in the calculation of vapor – liquid equilibria and enthalpies of
multi component mixtures – Use of multiple equation of state for the calculation of K values – Estimation of the
fugacity coefficients for the vapor phase of polar gas mixtures – calculation of liquid – phase activity coefficients.
Unit II THERMODYNAMIC PROPERTY EVALUATION 9
Fundamental principles involved in the separation of multi component mixtures – Determination of bubble-point
and Dew Point Temperatures for multi component mixtures – equilibrium flash distillation calculations for
Multi-component mixtures –separation of multi component mixtures at total reflux.
Unit III UNSTEADY STATE LUMPED SYSTEMS 9
General considerations in the design of columns – Column sequencing – Heuristics for column sequencing –
Key components – Distributed components – Non-Distributed components – Adjacent keys. Definition of
minimum reflux ratio – Calculation of R m for multi component distillation – Underwood method – Colburn
method.
Unit IV VARIOUS METHODS OF MCD COLUMN DESIGNS 9
Theta method of convergence – Kb method and the constant composition method –Application of the
Theta method to complex columns and to system of columns – Lewis Matheson method – Stage and
reflux requirements – Short cut methods and Simplified graphical procedures.
Unit V VARIOUS TYPES OF MCD COLUMNS 9
Design of sieve, Bubble cap, Valve trays and structured packing columns for multi component distillation –
Computation of plate efficiencies.

TEXT BOOK(S):

1. Holland, C.D., “Fundamentals of Multicomponent Distillation”, McGraw Hill BookCompany, 1981.

2. Van Winkle, “Distillation Operations”, McGraw Hill Publications, 1987.


REFERENCE BOOK(S):
1. “Distillation Dynamics and Control” by P.B. Deshpande, Arnold USA 1985.
2. Coulson and Richardson's Chemical Engineering Volume 6 (Design), 2 nd Edition, by R.K.Sinnott, Pergamon
Press, Oxford, UK (1993).

Department CHEMICAL ENGINEERING R 2019 Semester II PE

Course Hours / Week Credit Total Maximum


Code Course Name L T P C Hours Marks
19MCX06 FLUIDIZATION 3 0 0 3 45 100
ENGINEERING
Course Objective (s): The purpose of learning this course is
 Students will be able to find extensive application of Fluidization in Process Industry and also in combustion.
 To make the student aware of fundamentals of Fluidization and understand the design aspects of fluidized bed
systems.
Course Outcomes: At the end of this course,
 Students will be in a position to design a fluidized bed system for different applications.

Unit I APPLICATIONS OF FLUIDIZED BEDS 9


Introduction, Industrial application of fluidized beds, Physical operations and reactions.
Unit II FLUIDIZATION AND ANALYSIS OF DIFFERENT PHASES 9
Gross behavior of fluidized beds - Bubbles in dense beds - Emulsion phase in dense bubbling beds Flow pattern
of gas through fluidized beds.
Unit III HEAT AND MASS TRANSFER IN FLUIDIZED BED SYSTEMS 9
Phase juxtapositions operation shifts, Reversal points, Degree of segregation, Mixing Segregation equilibrium
Generalised fluidization of poly disperse systems, liquid phase Mixing and gas phase mixing.
Unit IV ELUTRIATION AND ENTRAINMENT 9
Mass transfer – Gas Liquid mass transfer, Liquid Solid mass transfer and wall to bed mass transfer, Heat transfer –
Column wall – to – bed heat transfer, Immersed vertical cylinder to bed heat transfer, Immersed horizontal cylinder
to bed heat transfer.
Unit V DESIGN OF FLUIDIZED BED SYSTEMS 9
Design of fluidization columns for physical operations, Catalytic and Non - Catalytic reactions, Three Phase
Fluidization

TEXT BOOK(S):

1. Kunii, D. and Levenspiel, O., “Fluidization Engineering”, Second Edition, Butterworth-Heinemann, London,
1991.
2. Kwauk, M., “Fluidization - Idealized and Bubbleless with applications”, Science Press,
1992.
REFERENCE BOOK(S):

1. J. F. Davidson and Harrison, "Fluidization Engineering", 10th Ed, Academic Press, London, 1994.

Department CHEMICAL ENGINEERING R 2019 Semester II PE


Course Hours / Week Credit Total Maximum Marks
Code Course Name Hours
L T P C
19MCX07 Food Process Engineering 3 0 0 3 45 100
Course Objective (s): The purpose of learning this course is
 To understand the principles involved in food processing and food preservation techniques
 To know about the process time calculations involved in food processing.
Course Outcomes: At the end of this course, students will be able to
 Have a sound knowledge in the field of Food processing and Food preservation methods.
 Obtain a wider interest towards equipments used during food processing.
Unit I PROCESS TIME CALCULATIONS 9
Sterilizers and accessories used in canning industries; Engineering aspects of pasteurizer; homogenizer, evaporators
(basic principle and single-effect evaporator) and concentrators used in food industries; Seaming machine.
Unit II CONSTRUCTION OF COLD STORAGE 9
Different types of freezers including plate contact freezer, Air blast freezer, Cryogenic freezing and refrigerated vans.

Unit III PRINCIPLES USED IN DRYING 9


Various types of driers (basic principle and drying time) – Tray drier, Roller drier, Spray drier, Fluidized bed drier,
Freeze drier and Solar drier.
Unit IV HEAT EXCHANGERS 9
Heat Exchangers (including Paraflow HEs); Extruders – Basic Principles and types, Difference between single
and Twin-Screw extruders - Kneader - Oil expeller
Unit V PROCESSING TECHNIQUES 9
Structure, Composition and Nutritional values of eggs; Egg processing, Byproduct Utilization -Commercial
Processing of lecithin and other Egg solids, Utilization of Egg derived products as food Ingredients - Fertilizer from
shells.

TEXT BOOK(S):
1. Barbosa-Canovas, ‘Novel Food Processing Technologies’, CRC Press Edition, 1999.
2. Dutta AK & Anantheswaran RC, ‘Hand Book of Microwave Technology for Food Applications’, 1999.

REFERENCE BOOK(S):
1. Pearson AM & Gillett TA, “Processed Meats”, CBS Publishers, 1996.
2. Cole DJA & Lawrie RA, Meat, AVI Publications, 1975.
Department CHEMICAL ENGINEERING R 2019 Semester II PE
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCX08 ENVIRONMENTAL 3 0 0 3 45 100
ENGINEERING
Course Objective (s): The purpose of learning this course is
 Students will be able to have knowledge on the basics of Environmental Engineering and their importance of
protecting for a sustainable future.
Course Outcomes: At the end of this course, learners will be able to
 Students will have awareness about the environment and the current strategies to control the existing
pollution problems.
 Able to know the recycling methodology of wastes and the importance of alternative fuels
Unit I ENVIRONMENT AWARENESS 9
Environment – Friendly chemical Process; Hazard and risk analysis; Environmental Audit.
Unit II CHEMICAL ENGINEERING PROCESSES 9
Unit Operations – Application of abatement of water pollution; Current strategies to control air pollution;
Disposal of solid wastes
Unit III RECYCLING METHODOLOGY 9
Economic recovery and recycling of waste; Transport fuel- Biodiesel for a cleaner environment.
Unit IV CLEAN TECHNOLOGY 9
Towards Eco- friendly products of chemical industry; Pesticides –Their transfer and Transformation
in the environment, Biological and Electrochemical technology for effluent treatments.
Unit V POLLUTION PREVENTION 9
Mass exchange network synthesis for pollution control and minimization Implications of environmental
constraints for process design, policies for regulation of environmental impacts, Concept of common
effluent treatment; Environmental legislations, Role of Government and Industries

TEXT BOOK(S):

1. Rao, C.S Environmental Pollution Control Engineering, Wiley- Eastern Ltd. 1991.

2. Peavy H.S. Rowe D.R., and George Technologies, Environmental Engineering, McGraw
Hill Book Company, New York, 1985.
3. Rao M.N and H.V.N. Rao. “Air Pollution”, Tata McGraw Hill Publishing Co. Ltd.1989.
REFERENCE BOOK(S):
1. Theodore L and Buomlore A.J ‘Air Pollution Control Equipments’, Prentice Hall Inc, NY.1982.

2. Gilbert M.Masters, “Introduction to Environmental Engineering and Science”", Prentice – Hall of India, New
Delhi, 1994.
3. Wahi S.K., Agnihotri A.K and Sharma J.S (Editors) “Environmental Management in Petroleum Industry”,
Wiley Eastern Ltd., New Delhi 1996.
4. Smith, R., “Chemical Process Design”, McGraw Hill, New York, 1995.
Department CHEMICAL ENGINEERING R 2019 Semester PE
II
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCX09 SAFETY AND HAZARD CONTROL 3 0 0 3 45 100
Course Objective (s): The purpose of this course is
 To understand about basics of safety and its importance in Chemical industries.
 To Study the Accident analysis, Risk analysis and disaster management procedures thoroughly.

Course Outcomes: At the end of this course, learners will be able to


 Understand the basics of safety and their principles involved in it.

 Analyze the causes for accidents and gain knowledge about the prevention methods

 Have a wide exposure towards disaster management, risk assessment and Safety considerations to be followed
in any industry.

Unit I BASICS OF SAFETY 9


Conventional and modern concepts of safety, Basic Principles and concepts in hazard identification, Chemical hazards,
Process and operation hazard, Hazards from utilities like air, water, steam etc., Occupational health hazards, Hazard and
Operability Studies, Safety Audits.
Unit II ACCIDENTS 9
Past Accident Analysis, Consequence Analysis of Fire, Gas/Vapour, Dispersions and Explosion, Vulnerability models,
Fault and Event Tree Analysis.
Unit III RISK ANALYSIS 9
Safety in Plant Design and layout - Risk Assessment
Unit IV SAFETY CONSIDERATIONS 9
Safety measures in handling and storage of chemicals - Process plant - Personnel Protection -First Aid.
Unit V DISASTER MANAGEMENT 9
Disaster Mitigation, Emergency Preparedness Plans.

TEXT BOOK(S):
1. Well, G.S Safety Process Plants Design, George Godwin Ltd., London, John Wiley and Sons, New York, 1980.

2. Frank P. Less, Loss Prevention in Process Industries, Vol. I and Vol. II Butterworth, London,
1980.

REFERENCE BOOK(S):
1. Safety in Chemical and Petrochemical Industries, Report of the Inter Ministry Group Dept. of Chemicals and
Petrochemicals, Govt. of India, ICMA Publications. 1986.
2. Marshal, V.C Major Chemical Hazards, Ellis Harwood Ltd. Chichester, U.K. 1987.
3. Guidelines for Chemical Process Quantitative Risk Analysis, Published by Centre for Chemical Process Safety
of the AIChE., New York, USA. 1989.

Department CHEMICAL ENGINEERING R 2019 Semester II PE


Course Hours / Week Credit Total Maximum
Code Course Name L T P C Hours Marks
19MCX10 MEMBRANE 3 0 0 3 45 100
TECHNOLOGIES FOR
WATER AND
WASTEWATER
TREATMENT
Course Objective (s): The purpose of learning this course is
 To study the latest membrane technologies involved in water and wastewater treatment.
 To learn about Membrane bioreactors, their principles and application in water and wastewater treatment.

Course Outcomes: At the end of this course, learners will be


 Exposed to the Advanced Membrane Technologies in Water and Wastewater Treatment.
 Have gained knowledge in different types of bioreactors and their applications along with their design
aspects.
Unit I INTRODUCTION 9
Solid Liquid separation systems-Filtration systems- Theory of Membrane separation – Mass Transport
Characteristics Cross Flow filtration-Membrane Filtration- Types and choice of membranes, porous, non porous,
symmetric and asymmetric – Plate and Frame, spiral wound and hollow fibre membranes – Liquid Membranes
Unit II BIO-METHANATION 9
Microfiltration – Ultra filtration- Nano Filtration – Reverse Osmosis – Electro dialysis-Per-evaporation -Membrane
manufactures – Membrane Module/Element designs – Membrane System components – Design of Membrane
systems - Pump types and Pump selection – Plant operations – Economics of Membrane systems
Unit III MEMBRANE BIOREACTORS 9
Introduction and Historical Perspective of MBRs, Bio-treatment Fundamentals, Biomass Separation MBR
Principles, Fouling and Fouling Control, MBR Design Principles, Design Assignment, Alternative MBR
Configurations, Commercial Technologies, Case Studies.
Unit IV PRETREATMENT SYSTEMS 9
Membrane Fouling – Pretreatment methods and strategies – Monitoring of Pretreatment– Langlier Index, Silt Density
Index, Chemical cleaning, Bio-foulant control
Unit V CASE STUDIES 9
Case studies on the design of membrane based water and wastewater treatment systems – Zero Liquid effluent
discharge Plants

TEXT BOOK(S):

1. Water Environment Federation (WEF), Membrane Systems for Wastewater Treatment, McGraw-Hill, USA,
2005.
2. Symon Jud, MBR Book – Principles and Application of MBR in Water and Wastewater Treatment, Elsevier,
2006.

REFERENCE BOOK(S):
1. K. Yamamoto and Urase T, Membrane Technology in Environmental Management, Special issue, Water
Science and Technology, Vol.41, IWA Publishing, 2000.
2. Jorgen Wagner, Membrane Filtration Handbook, Practical Tips and Hints, Second Edition, Osmonics Inc., 2001
3. Mulder, M., Basic Principle of Membrane Technology, Kluwer Academic Publishers, 1996
4. Noble, R.D. and Stern, S.A., Membrane Separations Technology: Principles and
Applications, Elsevier, 1995
Department CHEMICAL ENGINEERING R 2019 Semester II PE
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCX11 ELECTRO-CHEMICAL 3 0 0 3 45 100
ENGINEERING
Course Objective (s): The purpose of learning this course is
 To provide an adequate mastery in the principles involved in the electrochemical process and its
applications.
Course Outcomes: At the end of this course, learners will be able to
 Students would have knowledge on basic Electro-chemical concepts, electrodes and Electro-dialysis and
Electro-polymerization.
Unit I BASICS OF ELECTROCHEMISTRY 9
Review basics of Electrochemistry: Faraday’s law - Nernst Potential –Galvanic cells – Polarography, The electrical
double layer: its role in electrochemical processes –Electro-capillary curve –Helmoltz layer –Guoy –Steven’s layer –
Fields at the interface.
Unit II MASS TRANSFER IN ELECTROCHEMISTRY 9
Mass transfer in Electrochemical systems: Diffusion controlled electrochemical reaction – The importance of
convention and the concept of limiting current. Over potential, Primary and Secondary current distribution – Rotating
disc electrode.
Unit III CORROSION AND ITS TYPES 9
Introduction to corrosion, Series, Corrosion theories derivation of potential- Current relations of activities
controlled and diffusion controlled corrosion process. Potential-pH diagram, Forms of corrosion - Definition,
Factors and control methods of various forms of corrosion, Corrosion control measures - Industrial boiler water
corrosion control – Protective coatings –Vapor phase inhibitors – Cathodic protection, Sacrificial anodes –Paint
removers.
Unit IV ELECTROLYTIC PROCESSES 9
Electro deposition – Electro refining – Electroforming – Electro polishing – Anodizing – Selective solar coatings,
Primary and secondary batteries – Types of batteries, Fuel cells.
Unit V ELECTROCHEMICAL REACTORS AND ITS APPLICATIONS 9
Electrodes used in different electrochemical industries: Metals-Graphite –Lead dioxide –Titanium substrate insoluble
electrodes –Iron oxide –Semiconducting type etc. Metal finishing cell design - Types of electrochemical reactors,
Batch cell, Fluidized bed electrochemical reactor, Filter press cell, Swiss roll cell, Plug flow cell, Design equation,
Figures of merits of different type of electrochemical reactors.

TEXT BOOK(S):
1. Picket, “Electrochemical Engineering”, Prentice Hall, 1977.
2. Newman, J. S., “Electrochemical Systems”, Prentice Hall, 1973.

REFERENCE BOOK(S):
1. Barak, M. and Stevenge, U.K., “Electrochemical Power Sources - Primary and Secondary Batteries” 1980.
2. Mantell, C., ‘‘Electrochemical Engineering’’, McGraw Hill, 1972.
3. Best Practices Manual for Biomass Briquetting, I R E D A, 1997
Eriksson S. and M. Prior, The briquetting of Agricultural wastes for fuel, FAO Energy and
4. Environment paper, 1990
Department CHEMICAL ENGINEERING R 2019 Semester II PE
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCX12 COMPUTATIONAL FLUID 3 0 0 3 45 100
DYNAMICS FOR CHEMICAL
ENGINEERS
Course Objective (s): The purpose of learning this course is
 To demonstrate competence in setting up Computational Fluid Dynamics models for some industrially
important applications. This technical competence in building and conducting CFD simulations is a skill
which enhances employability.
Course Outcomes: At the end of this course, learners will be able to
 Gain hands-on experience with a commercial CFD program

 Formulate problems that can be solved with a CFD program

 Critically evaluate simulation results

 Communicate the results in oral and written form


Unit I CONSERVATION LAWS AND TURBULENCE MODELS 9
Governing equations of fluid flow and heat transfer – Mass conservation, Momentum and energy equation,
Differential and integral forms, Conservation and non-conservation form - Characteristics of turbulent flows, Time
averaged Navier Strokes equations, Turbulence models-one and two equation, Reynolds stress, LES and DNS
Unit II FINITE DIFFERENCE APPROXIMATION 9
Fundamental principles involved in the separation of multi component mixtures – Determination of bubble point
and Dew Point Temperatures for multi component mixtures – Equilibrium flash distillation calculations for
multi component mixtures –Separation of multi component mixtures at total reflux
Unit III FINITE VOLUME METHOD 9
Diffusion problems – Explicit and Implicit time integration; Convection-Diffusion problems, Properties of
discretisation schemes, Central, Upwind, Hybrid, Quick schemes - Solution of discretised equations.
Unit IV FLOW FIELD COMPUTATION 9
Pressure velocity coupling, Staggered grid, Simple algorithm, PISO algorithm for steady and unsteady flows
Unit V GRID GENERATION 9
Physical aspects, Simple and multiple connected regions, Grid generation by PDE solution, Grid generation
by algebraic mapping.

TEXT BOOK(S):

1. Anderson, J.D., “Computational Fluid Dynamics: The Basics with Applications”, McGraw-Hill, 1995.

2. Fletcher, C. A. J., “Computational Techniques for Fluid Dynamics”, Springer Verlag, 1997.

REFERENCE BOOK(S):
1. Anderson, J. D., “Computational Fluid Dynamics: The Basics with Applications”, McGraw-Hill, 1995.

2. Fletcher, C. A. J., “Computational Techniques for Fluid Dynamics”, Springer Verlag, 1997.
Department CHEMICAL ENGINEERING R 2019 Semester III PE
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCX13 FUEL CELL TECHNOLOGY 3 0 0 3 45 100
Course Objective (s): The purpose of this course is
 To understand about fuel cells, their Working Principle, Types, Design and Performance analysis.

Course Outcomes: At the end of this course, learners will be able to


1. Basics and working principles of the Fuel cell technology.

2. Selection the suitable materials for electrode, catalyst, membrane for the fuel cells.

3. The mass transfer process such as pressure drop and velocity distribution in single cell as well as stack.

Unit I BASICS OF FUEL CELLS 9


Overview of fuel cells: Low and high temperature fuel cells; Fuel cell thermodynamics - Heat, Work potentials,
Prediction of reversible voltage, Fuel cell efficiency.
Unit II FUEL CELL KINETICS 9
Fuel cell reaction kinetics - Electrode kinetics, Overvoltage, Tafel equation, Charge transfer reaction,
Exchange currents, Electro catalysis - Design, Activation kinetics, Fuel cell charge and Mass transport - Flow field,
Transport in electrode and electrolyte.
Unit III CHARACTERIZATION TECHNIQUES 9
Fuel cell characterization - in-situ and ex-situ characterization techniques, i-V curve, Frequency response analysis;
Fuel cell Modelling and system integration: - 1D model – Analytical solution and CFD models.
Unit IV SAFETY CONSIDERATIONS 9
Balance of plant; Hydrogen production from Renewable sources and storage; Safety issues, Cost expectation and
Life cycle analysis of fuel cells.
Unit V FUEL CELL POWER PLANTS 9
Fuel cell power plants: Fuel processor, Fuel cell power section (fuel cell stack), Power Conditioner - Automotive
applications, Portable applications

TEXT BOOK(S):

1. O'Hayre, R.P.,S. Cha, W. Colella, F.B.Prinz, Fuel Cell Fundamentals, Wiley, NY (2006).
REFERENCE BOOK(S):
1. Bard, A. J., L. R., Faulkner, Electrochemical Methods, Wiley, N.Y 2004

2. Basu, S. Fuel Cell Science and Technology, Springer, N.Y, 2007

3. Fuel Cell Technology Handbook, edited by Gregor Hoogers, CRC Press 2003.
Department CHEMICAL ENGINEERING R 2019 Semester III PE
Course Hours / Week Credit Total Maximum Marks
Code Course Name Hours
L T P C
19MCX14 BIO-ENERGY CONVERSION 3 0 0 3 45 100
TECHNIQUES
Course Objective (s): The purpose of learning this course is
 To know about the different types of biomass and its characteristics.
 To study the various principles involved in bio-energy conservation techniques and their importance.
Course Outcomes: At the end of this course, learners will be able to
 Know the types of biomass and their advantages and importance along with the applications.
 Understand the major principles involved in various Bio-energy conservation techniques.
Unit I INTRODUCTION 9
Biomass: types – Advantages and drawbacks – Indian scenario – Characteristics – Carbon Neutrality –Conversion
mechanisms – Fuel assessment studies
Unit II BIO-METHANATION 9
Microbial systems – Phases in biogas production – Parameters affecting gas production – Effect of additives on
Biogas yield – Possible feed-stocks - Biogas plants – Types – Design – Constructional details and Comparison –
Biogas appliances – Burner, Illumination and Power generation – Effect on engine performance.
Unit III COMBUSTION 9
Perfect, Complete and Incomplete – Equivalence ratio – Fixed Bed, Fluid Bed – Fuel and Ash handling – Steam cost
comparison with conventional fuels. Briquetting: types of Briquetting – Merits and demerits – Feed requirements
and preprocessing – Advantages – Drawbacks
Unit IV GASIFICATION 9
Heat exchangers (including Paraflow HEs); Extruders – Basic principles and types, Difference between single- and
twin - Screw extruders - Kneader; Oil expeller
Unit V PYROLYSIS AND CARBONIZATION 9
Types – Process governing parameters – Thermo gravimetric analysis – Differential Thermal Analysis – Differential
Scanning Calorimetry – Typical yield rates.

TEXT BOOK(S):
1. Khandelwal KC, Mahdi SS, ‘Biogas Technology’, – A Practical Handbook, Tata McGraw Hill,1986.
2. Mahaeswari, R.C. ‘Bio Energy for Rural Energisation’, Concepts Publication, 1997.

REFERENCE BOOK(S):
1. Tom B Reed, ‘Biomass Gasification – Principles and Technology’, Noyce Data Corporation, 1981.
2. ‘Best Practices Manual for Biomass Briquetting’, IREDA, 1997
Eriksson S. and M. Prior, “The briquetting of Agricultural Wastes for Fuel”, FAO Energy and
3. Environment Paper, 1990
Department CHEMICAL ENGINEERING R 2019 Semester III PE
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCX15 SOLVENT EXTRACTION 3 0 0 3 45 100
TECHNIQUES
Course Objective (s): The purpose of this course is
 To develop a sound knowledge on equilibrium in liquid-liquid system, HETS, NETS, HTU, NTU, dispersion and
coalescence in extractors and design of extraction column.

Course Outcomes: At the end of this course, learners will be able to


 Understand the equilibrium in liquid-liquid system and its applications.

 Know the concepts of design of extraction column and its application in chemical engineering field.

Unit I EQUILIBRIUM IN LIQUID-LIQUID SYSTEM 12


Binary and ternary liquid equilibria, Tie-lines, Critical solution temperature, Tie line correlations, Contour/prism
diagrams, Binary / Ternary prediction methods of activity coefficient, Theory and Prediction of diffusivity in liquids,
Theory of inter phase mass transport, Estimation and Prediction of mass transport coefficients.
Unit II DIFFERENTIAL / STAGE-WISE EQUILIBRIUM CONTACT OPERATIONS 9
Equilibrium stage-wise contact, Single and multiple contacts with co-current and countercurrent flow of phases
for immiscible and partially miscible solvent phases, Calculation methods, Fractional extraction with reflux
of raffinate and extract. Differential contact, HETS,NETS, HTU, NTU concepts and Estimation of these parameters,
Mass transfer efficiency, Axial mixing and Residence time distribution in extractors and their estimation.
Unit III DISPERSION AND COALESCENCE IN EXTRACTORS 12
Characteristics of dispersion involving single and multiple nozzle distributors, Drop size and formation and
coalescence, Mean drop size at dispersion and their settling velocities/relative characteristics velocities. Effect of
drop oscillation ,wobbling and Internal circulation, Effect of surface active agents, Prediction of drop size and
characteristics velocity in spray , packed and mechanically agitated contactors as in RDC, pulsed columns, solute
transfer effects on drop dynamics.
Unit IV DESIGN OF LIQUID EXTRACTION COLUMNS 12
Design of extractor height and diameter, Prediction of flow capacities in terms of flooding rates, Regime of
operating envelops, Hydrodynamic design variables such as hold up, characteristic velocities, pressure drop, Effect
of direction of solute transfer on these variables and their prediction methods, Correction of mass transfer data,
Axial mixing correction for column height, Interfacial area estimations, using slow, fast and instantaneous
Reactions and their application with models for mass transfer coefficients.

TEXT BOOK(S):
1. Laddha, G. S. and Degaleesan, T. E., ‘‘Transport Phenomena in Liquid Extraction”, Tata McGraw Hill, New
Delhi, 1976.
2. Hanson, C., Baird, M. H. I. and Lo, T. C., “Hand Book of Solvent Extraction”, Wiley –International, New
York, 1983.
REFERENCE BOOK(S):
1. Hanson, C., “Recent Advances in Liquid Extraction”, Pergamon Press, London,1972.
Department CHEMICAL ENGINEERING R 2019 Semester III PE
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCX16 WASTE WATER 3 0 0 3 45 100
ENGINEERING
Course Objective (s): The purpose of this course is
 To understand about basics waste water engineering and its current scenario in chemical engineering field.
 To Study the industrial waste water treatment techniques and reuse methodologies of wastewater.

Course Outcomes: At the end of this course, learners will be able to


 Understand the basics of waste water engineering and their principles involved in it.

 Have a wide exposure towards the industrial waste water treatment techniques and reuse methodologies of
wastewater.

Unit I INTRODUCTION 9
Industrial scenario - Uses of Water by industry - Sources and types of industrial wastewater –
Industrial wastewater disposal and environmental impacts - Reasons for treatment of industrial wastewater –
Regulatory requirements - Industrial waste survey - Industrial wastewater generation rates, characterization
and variables – Population equivalent - Toxicity of industrial effluents and Bioassay tests - Preventing
and minimizing wastes at the source - Individual and Common Effluent Treatment Plants - Joint treatment
of Industrial wastewater.
Unit II INDUSTRIAL WASTEWATER TREATMENT 9
Equalisation - Neutralisation - Oil separation - Flotation - Precipitation - Heavy metal Removal– Refractory organics
separation by adsorption - Aerobic and anaerobic biological treatment -Sequencing batch reactors – High Rate
reactors
Unit III ADVANCED WASTEWATER TREATMENT AND REUSE 9
Chemical oxidation - Ozonation - Photocatalysis - Wet Air Oxidation - Evaporation – Ion
Exchange – Membrane Technologies - Nutrient removal - Land Treatment.
Unit IV RESIDUALS MANAGEMENT 9
Residuals of Industrial Wastewater Treatment - Quantification and Characteristics of Sludge- Thickening, Digestion,
Conditioning, Dewatering and Disposal of sludge -Management of RO rejects
Unit V CASE STUDIES 9
Industrial Manufacturing Process description, Wastewater Characteristics and Waste Treatment flow sheet
for Textiles - Tanneries - Pulp and Paper - Metal finishing - Petroleum Refining -Chemical industries - Sugar
and Distilleries - Dairy - Iron and steel - Fertilizers – Industrial Clusters and Industrial Estates.

TEXT BOOK(S):
1. Eckenfelder W.W, “Industrial Water Pollution Control”, McGraw Hill, 1999.

2. Arceivala, S.J., “Wastewater treatment for Pollution control”, Tata McGraw Hill, 1998.
REFERENCE BOOK(S):
1. Pollution prevention and abatement handbook – Towards Cleaner Pordcution”, Worldbank and UNEP,
Washington, 1998.
Department CHEMICAL ENGINEERING R 2019 Semester III PE
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCX17 POLLUTION ABATEMENT 3 0 0 3 45 100
Course Objective (s): The purpose of this course is
 To understand about basics of pollution and its effects in environment.
 To Study the different types of pollution along with the ways in which they can be reduced.

Course Outcomes: At the end of this course, students will be able to


 Understand the basics of pollution and its causes and effects.
 Analyze the causes for pollution and suggest some measures to overcome those problems.
 Have a wide exposure towards different types of pollution and its adverse effects.
Unit I INTRODUCTION 9
Man and Environment, Types of Pollution, Pollution controls aspects, Industrial pollution, Pollution monitoring
and analysis of pollutants, Indian pollution regulations.
Unit II WATER POLLUTION 9
Water pollution- Source of Pater Pollution- Measurement of quality- BOD- COD- Colour and odor-PH-
heavy metals- Treatments etc .,(Qualitatively) - Industrial Waste Water treatment (qualitatively) and recycle.
Unit III WASTE MANAGEMENT AND DISPOSAL TECHNIQUES 9
Solid wastes- Quantities and Characterizations – industrial – Hazardous Waste- Radioactive waste- Simple
treatments and Disposal techniques (Qualitatively treatment).
Unit IV AIR POLLUTION AND ITS EFFECTS 9
Air pollution-Types and Sources of gaseous pollutants-Particulate matter-Hazardous air
Pollutants - Global and Atmospheric Climatic change (Greenhouse effect)- Acid rain – Industrial exhaust –
Characterization and Methods of decreasing the pollutants content in exhaust gases.
Unit V NOISE POLLUTION 9
Noise Pollution –Sound level-Measuring transient noise-Acoustic Environment-Health Effects of Noise –
Noise Control - Introduction to Cosmic pollution.

TEXT BOOK(S):
1. Jeffrey Pierce J, Environmental Pollution and Control, Butterworth-Heinemann; 4 th edition, 1997.

2. Rao. C.S. Environmental Pollution Control Engineering, New age International Publishers, 2006.

REFERENCE BOOK(S):

1. Safety in Chemical and Petrochemical Industries, Report of the Inter Ministry Group Dept. of Chemicals and
Petrochemicals, Govt.of India, ICMA Publications. 1986.
Department CHEMICAL ENGINEERING R 2019 Semester III PE
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCX18 PROJECT ENGINEERING OF 3 0 0 3 45 100
PROCESS PLANTS
Course Objective (s): The purpose of this course is
 To understand about basics of project engineering involved in process plants.
 To Study the methods of planning and the management techniques associated with it.

Course Outcomes: At the end of this course, learners will be able to


 Understand the criteria of selection of a project based on industrial needs.

 Execute the project that has been assigned in a clear way by applying all the principles involved in it.

Unit I INTRODUCTION 9
Project definition, Project Profile and standards, Feedback information (MIS), Evaluation and Modification,
Selection, Criteria.
Unit II PLANNING METHODS 9
Planning the process, Strategic and Managerial Planning, Organizing the Process Planning, Cost and costing, Cost
Control systems, Economic Balancing, Network Planning, Methods(PERT/CPM), Engineering Flow Diagrams, Cost
requirements, Analysis and Estimation of Process Feasibilities (Technical/Economical) Analysis, Cost–Benefit Ratio
Analysis, Project Budgeting, Capital Requirements, Capital Market, Cash Flow Analysis, Breakeven strategies.
Unit III PLANT ENGINEERING MANAGEMENT 9
Plant Engineering Management, Objectives, Programme, Control, Plant Location and Site Selection, Layout
diagrams, Selection and procurement of equipment and machineries, Installation, Recommission, Commissioning
and Performance Appraisal, Strategies choice and Influence, Product planning and development, Provision and
Maintenance of service facilities.
Unit IV SAFETY METHODS 9
Process safety, Materials Safety and Handling regulations, Safety in equipment and machinery operations,
Design considerations of safety organization and control, Pollution, Pollution control and Abatement, Industrial
Safety Standard Analysis
Unit V POLICY STUDIES 9
Government regulations on procurement of raw materials and its allocation. Export – Import regulations,
Pricing policy, Industrial licensing procedure, Excise and other commercial taxes, Policies on depreciation and
corporate tax, Labour laws, Social welfare legal measurements, Factory act, Regulations of Pollution Control Board.

TEXT BOOK(S):
1. Cheremisinoff, N. P., Practical Guide to Industrial Safety: Methods for Process Safety Professionals,
CRC Press, 2001.
2. Peters,
th
M. S., Timmerhaus, C. D. and West, R. E., “Plant Design and Economics for Chemical Engineers”,
5 Edition, McGraw Hill, 2003.
REFERENCE BOOK(S):
1. Couper, J. R., Process Engineering Economics, CRC Press, 2003.
Department CHEMICAL ENGINEERING R 2019 Semester III PE
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCX19 RISK ANALYSIS AND 3 0 0 3 45 100
MANAGEMENT
Course Objective (s): The purpose of this course is
 To understand about basics of risk analysis and management methods.
 To Study the risk assessment procedures and its application in chemical engineering.

Course Outcomes: At the end of this course, learners will be able to


 Understand the basics of risk analysis and management methods.

 Analyze the risk assessment procedures and principles involved in it.

 Have a wide exposure towards handling and storage of chemicals and environmental management
techniques.

Unit I INTRODUCTION 9
General: Risk types, Completion, Permitting, Resource, Operating, Environmental, Manageable, Insurable,
Risk Causes, Risk Analysis types and causes.
Unit II RISK TECHNIQUES 9
Techniques: General, Risk adjusted discounted rate method, Certainty Equivalent Coefficient method, Quantitative
Sensitivity analysis, Probability distribution, Coefficient of Variation method, Simulation method, Crude Procedures,
Payback period, Expected monetary value method, Refined procedures, Shackle approach, Hiller’s Model,
Hertz Model, Goal Programming.
Unit III RISK MANAGEMENT 9
Risk Management: Emergency relief Systems, Diers Program, Bench scale experiments, Design of Emergency
relief systems, Internal Emergency Planning, Risk Management Plan, Mandatory Technology Option Analysis,
Risk Management alternatives, Risk Management Tools, Risk Management Plans, Risk index method, Downfire
and Explosion method, Mond index Method.
Unit IV RISK ASSESSMENT 9
Risk Assurance and Assessment: Property Insurance, Transport insurance, Liability insurance, Pecunious insurance,
Risk Assessment, Scope Canvey study, Rijimond pilot study, Low Probability high consequence events. Fault tree
analysis, Event tree analysis, Zero Infinity dilemma.
Unit V STORAGE AND HANDLING OF CHEMICALS 9
Risk Analysis in Chemical Industries: Handling and Storage of Chemicals, Process plants, Personnel Protection
equipments. Environmental Risk Analysis, International Environmental Management system, Corporate
Management System, Environmental Risk Assessment, Total Quality Management, Paradigms and its Convergence.

TEXT BOOK(S):
1. Srivastav, S., “Industrial Maintenance Management”, Sultan Chand & Co., 1998.
2. Rao, P. C. K., “Project Management and Control”, Sultan Chand & Co., Ltd., 1996.

REFERENCE BOOK (S):

1. Sincero, A. P. and Sincero, G. A., “Environmental Engineering – A Design Approach”, Prentice Hall of India,
1996.

2. Pandya, C. G., “Risks in Chemical Units”, Oxford and IBH Publishers, 1992.
Department CHEMICAL ENGINEERING R 2019 Semester III PE
Course Hours / Week Credit Total Maximum
Code Course Name Hours Marks
L T P C
19MCX20 TOTAL QUALITY 3 0 0 3 45 100
MANAGEMENT
Course Objective (s): The purpose of this course is
 To understand about concepts of TQM and the principles associated with it.

Course Outcomes: At the end of this course, learners will be able to


 Understand the implementation methods of TQM and its way of application in chemical industries.

Unit I CONCEPTS OF TQM 9


Philosophy of TQM, Customer focus, Organization, Top management commitment, Team work quality philosophies
of Deming, Crosby and Muller.
Unit II TQM PROCESS 9
Techniques: General, Risk adjusted discounted rate method, Certainty Equivalent Coefficient method, Quantitative
Sensitivity analysis, Probability distribution, Coefficient of variation method, Simulation method, Crude Procedures,
Payback period, Expected monetary value method, Refined procedures, Shackle approach, Hiller’s model,
Hertz model, Goal programming.
Unit III TQM SYSTEMS 9
Risk Management: Emergency relief Systems, Diers program, Bench scale experiments,
Design of emergency relief systems, Internal emergency planning, Risk management plan, mandatory technology
option analysis, Risk management alternatives, risk management tools, risk management plans, Risk index method,
Downfire and Explosion method, Mond index Method.
Unit IV QUALITY SYSTEM 9
Risk Assurance and Assessment: Property Insurance, Transport insurance, Liability insurance, Pecunious insurance,
Risk Assessment, Scope Canvey study, Rijimond pilot study, Low Probability high consequence events. Fault tree
analysis, Event tree analysis, Zero Infinity dilemma.
Unit V IMPLEMENTATION OF TQM 9
Risk Analysis in Chemical Industries: Handling and Storage of Chemicals, Process plants, Personnel Protection
equipments. Environmental Risk Analysis, International Environmental Management system, Corporate
Management System, Environmental Risk Assessment, Total Quality Management, Paradigms and its Convergence.

TEXT BOOK(S):
1. Rose J. E., “Total quality Management”, Kogan Page Ltd, 1999.
2. Bank, J., “The essence of Total Quality Management”, Prentice Hall of India, 1993.
REFERENCE BOOK (S):
1. Bonds, G., “Beyond Total Quality Management”, McGraw Hill, 1994.

2. Osada, T., “The 5S’s, The Asian Productivity Organization”, 1991.

You might also like