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  • T NG H P NH3BH3

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    Ammonia borane is a promising solid hydrogen carrier for portable power devices using proton-exchange membrane fuel cells. The document reports a high-yielding (95%) and high-purity (98%) method for preparing ammonia borane at a preparative scale. It also describes the first systematic study of a transitional metal-catalyzed alcoholysis of ammonia borane, compares the methanolysis and hydrolysis of ammonia borane, and reports on regenerating ammonia borane from ammonium tetramethoxyborate.

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    Tổng hợp NH3BH3

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    Ammonia borane is a promising solid hydrogen carrier for portable power devices using proton-exchange membrane fuel cells. The document reports a high-yielding (95%) and high-purity (98%) method for preparing ammonia borane at a preparative scale. It also describes the first systematic study of a transitional metal-catalyzed alcoholysis of ammonia borane, compares the methanolysis and hydrolysis of ammonia borane, and reports on regenerating ammonia borane from ammonium tetramethoxyborate.

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    © All Rights Reserved
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    3 views1 page

    T NG H P NH3BH3

    Uploaded by

    hunggiang2887
    Ammonia borane is a promising solid hydrogen carrier for portable power devices using proton-exchange membrane fuel cells. The document reports a high-yielding (95%) and high-purity (98%) method for preparing ammonia borane at a preparative scale. It also describes the first systematic study of a transitional metal-catalyzed alcoholysis of ammonia borane, compares the methanolysis and hydrolysis of ammonia borane, and reports on regenerating ammonia borane from ammonium tetramethoxyborate.

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    of 1

    2007

    Boron
    I 0055 Preparation of Ammonia Borane in High Yield and Purity, Methanolysis, and Re-
    generation. — Ammonia borane is a promising solid hydrogen carrier, particularly for
    48- 017 power generation in portable devices that employ proton-exchange membrane fuel
    cells. Its synthesis on a preparative scale with high yields (95%) and very high purity
    (98%) is described. In addition, the first systematic study of a transitional metal-cata-
    lyzed alcoholysis of (III), comparison of the methanolysis and the hydrolysis of (III),
    and the regeneration of (III) from ammonium tetramethoxyborate are also described.
    — (RAMACHANDRAN*, P. V.; GAGARE, P. D.; Inorg. Chem. 46 (2007) 19,
    7810-7817; Dep. Chem., Purdue Univ., West Lafayette, IN 47907, USA; Eng.) —
    Schramke

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