WORKSHEET

Kurva Larutan Standar pada

pH 4,5
Konsentrasi (ppm) Serapan (A)
1 0,250
2 0,300
4 0,400
6 0,510
8 0,610
10 0,720
Kurva Larutan Standar pada
pH 6,8
Konsentrasi (ppm) Serapan (A)
1 0,230
2 0,280
4 0,400
6 0,500
8 0,600
10 0,710
Kurva Larutan Standar pada
pH 6,8
Konsentrasi (ppm) Serapan (A)
1 0,230
2 0,280
4 0,400
6 0,500
8 0,600
10 0,710
 Farnormin 50 mg (PRATAPA NIRMALA - Indonesia)
Larutan HCl 0,1 N pH 1,2
Waktu (menit) 10 15 30
Vessel Au %D Au %D Au %D
1 0,408 66,63 0,441 78,21 0,480 91,89

2 0,409 66,98 0,438 77,15 0,483 92,94

3 0,406 65,93 0,435 76,11 0,486 94

4 0,409 66,98 0,437 76,80 0,481 92,24

5 0,405 65,58 0,440 77,86 0,484 93,30

6 0,401 64,17 0,436 76,45 0,487 94,35

7 0,405 65,57 0,437 76,80 0,482 92,60

8 0,406 65,93 0,434 75,75 0,486 94

9 0,408 66,63 0,440 77,85 0,482 92,60

10 0,402 64,52 0,439 77,50 0,479 91,54

11 0,404 65,23 0,436 76,45 0,481 92,24

12 0,403 64,88 0,438 77,16 0,481 92,24

X 65,75 77,01 92,83
SD 0.94 0.75 0.90
RSD 1,4 0,98 0.97
 Farnormin 50 mg (PRATAPA
NIRMALA - Indonesia)
Larutan Dapar Fosfat pH 4,5
Waktu (menit) 10 15 30
Vessel Au %D Au %D Au %D
1 0,359 56,45 0,407 73 0,458 90,58

2 0,361 57,14 0,405 72,31 0,457 90,24

3 0,358 56,10 0,408 73,34 0,455 89,55

4 0,356 55,41 0,403 71,62 0,456 89,90

5 0,362 57,48 0,406 72,65 0,454 89,20

6 0,36 56,80 0,405 72,31 0,450 87,83

7 0,357 55,75 0,407 73 0,458 90,59

8 0,359 56,44 0,402 71,27 0,457 90,24

9 0,361 57,13 0,404 71,96 0,456 89,89

10 0,360 56,80 0,406 72,65 0,453 88,86

11 0,359 56,44 0,408 73,34 0,458 90,58

12 0,358 56,10 0,405 72,31 0,459 90,93

X 56,50 72,48 89,87
SD 0,60 0,65 0,88
RSD 1,06 0,89 0,99
 Farnormin 50 mg (PRATAPA NIRMALA -
Indonesia)
Larutan Dapar Fosfat pH 6,8

Waktu (menit) 10 15 30
Vessel Au %D Au %D Au %D
1 0,334 52,64 0,390 71,60 0,427 84,11

2 0,333 52,30 0,393 72,60 0,429 84,79

3 0,330 51,29 0,391 71,93 0,426 83,77

4 0,330 51,29 0,390 71,60 0,428 84,45

5 0,330 51,29 0,392 72,27 0,425 83,43

6 0,331 51,63 0,389 71,25 0,432 85,80

7 0,330 51,29 0,390 71,60 0,430 85,12

8 0,331 51,63 0,391 71,93 0,426 83,77

9 0,334 52,64 0,393 72,60 0,431 85,57

10 0,332 51,96 0,390 71,60 0,427 84,11

11 0,332 51,96 0,392 72,27 0,429 84,79

12 0,331 51,63 0,389 71,25 0,431 85,47

X 51,81 71,88 84,60
SD 0,51 0,47 0,77
RSD 0,98 0,66 0,91
Tenol (PT Bedjo Farma, Indonesia)
Larutan HCl 0,1 N pH 1,2
Waktu
10 15 30
(menit)
Vessel Au %D Au %D Au %D
1 0.435
0.4 63.82 76.10 0.468 87.68
2 0.441
0.402 64.52 78.21 0.47 88.38
3 0.439
0.401 64.17 77.50 0.469 88.03
4 0.438
0.405 65.57 77.15 0.47 88.38
5 0.439
0.401 64.17 77.50 0.464 86.280
6 0.44
0.402 64.52 77.85 0.469 88.03
7 0.438
0.401 64.17 77.15 0.468 87.68
8 0.439
0.403 64.87 77.50 0.47 88.38
9 0.44
0.402 64.52 77.85 0.469 88.03
10 0.437
0.402 64.52 76.80 0.47 88.38
11 0.438
0.403 64.87 77.15 0.468 87.68
12 0.441
0.4 63.82 78.21 0.467 87.33
X 64.46 77.42 87.85
SD 0.49 0.60 0.607
RSD 0.0076 0.007 0.006
Tenol (PT Bedjo Farma, Indonesia)
Larutan Dapar Fosfat pH 4,5
Waktu
10 15 30
(menit)
Vessel Au %D Au %D Au %D
1 0.357 55.79 0.405 72.31 0.455 89.55
2 0.36 56.82 0.4 70.58 0.45 87.82
3 0.358 56.13 0.405 72.31 0.452 88.51
4 0.359 56.48 0.403 71.62 0.455 89.55
5 0.356 55.44 0.403 71.62 0.4 70.58
6 0.358 56.13 0.404 71.96 0.451 88.17
7 0.358 56.13 0.405 72.31 0.432 81.62
8 0.359 56.48 0.403 71.62 0.433 81.96
9 0.36 56.82 0.405 72.31 0.456 89.89
10 0.357 55.79 0.4 70.58 0.455 89.55
11 0.356 55.44 0.401 70.93 0.453 88.86
12 0.357 55.79 0.402 71.27 0.456 89.89
56.10 71.62 86.33
X

0.47 0.65 5.74
SD

0.008 0.009 0.066
RSD

Tenol (PT Bedjo Farma, Indonesia)
Larutan Dapar Fosfat pH 6,8
Waktu
10 15 30
(menit)
Vessel Au %D Au %D Au %D
1 0.333
52.30 0.386 70.24 0.43 85.12
2 0.33
51.29 0.39 71.59 0.427 84.11
3 0.331
51.63 0.388 70.91 0.428 84.45
4 0.332
51.96 0.387 70.57 0.429 84.78
5 0.33
51.29 0.389 71.25 0.427 84.11
6 0.331
51.63 0.388 70.91 0.428 84.45
7 0.334
52.64 0.387 70.57 0.43 85.127
8 0.33
51.29 0.389 71.25 0.429 84.78
9 0.331
51.63 0.386 70.24 0.428 84.45
10 0.332
51.96 0.389 71.25 0.429 84.78
11 0.331
51.63 0.387 70.57 0.427 84.11
12 0.33
51.29 0.386 70.24 0.429 84.78
51.71 70.80 84.59
X

0.43 0.46 0.36
SD

0.008 0.006 0.004
RSD