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  • Alur Analisis

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    Ardi Mahardika
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    yooo

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    alur analisis

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    yooo

    Copyright:

    © All Rights Reserved
    Download as PPTX, PDF, TXT or read online from Scribd
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    6 views1 page

    Alur Analisis

    Uploaded by

    Ardi Mahardika
    yooo

    Copyright:

    © All Rights Reserved
    Download as PPTX, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    of 1

    1. Preparasi Sampel 3.

    Penentuan Ferri Oksida dengan metoda Volumetri


    Sampel Semen Sampel
    Timbang 1 Kg Timbang sebanyak 1 gram
    Masukkan ke dalam Larutkan dengan Akuades 100 mL
    Tong Penghomogen Tambah 10 mL HCl
    Homogenkan selama Panaskan selama 30 menit
    1 jam Tambah larutan SnCl2
    Dinginkan hingga suhu ruang
    Sampel Terhomogenkan Tambah 10 mL Hgcl2
    Tambah 10 mL H3PO4
    2. Penentuan Hilang Pijar Tambah 3 tetes Indikator BDS
    Titrasi dengan K2Cr2O7
    Sampel
    11 Lembayung (Ungu)
    Larutan berwarna
    Timbang sebanyak 1 gram
    Masukkan kedalam Cawan 4. Penentuan Ferri Oksida dengan Metoda XRF
    Porselen Sampel
    Masukkan kedalam Furnace
    Pijarkan selama 15 menit Timbang sampel sebanyak 0,5 gram
    pada suhu 900 C Tambah Li2B4O7 sebanyak 5 gram
    Pijar dalam Furnace pada suhu 1050 C
    Padatan Hitam selama 5 menit
    Masukkan lelehan kedalam cetakan sampel
    Dinginkan hingga suhu ruang
    Analisis dengan X-ray Flourescence
    Padatan bening kekuningan

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