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Final Step Sizing+control
Final Step Sizing+control
Process
Equipment
Sizing
1
3.1.
Mixing Tank
2
Vessel Dimension
Volume Tank
How to Estimate?
For safety reason working volume is 80% from
total volume, so wee need to calculate total volume
of the tank (100%).
Tank Height
Total Volume Tank (VT):
Ratio of diameter and height (D:H) is 1:5,
Head and pedestal of ellipsoidal tank with minor
Tank Diameter
axis ratio 2:1,
Diameter and height can calculated using
comparison of height and vessel ratio. Ratio of
diameter and height (D:H) is 1:5. The fermentor tank
will use ellipsoidal head bottom and top.
3
• Pressure Design
Thickness of Cylinder
Corrosion factor (C) (Chuse & Eber, 1954) :
Safety factors for pressure = 20% 0.0420
Allowable working stress (S)
(Brownell&Young,1979): 107,558 kPa
Efficiency of connection (E) (Double welded
butt joint): 85%
• Impeller Design Approximate age of equipment: 15 years
Rule of thumb for impeller design from Wallas, 1988
is:
Da : Dt = 1 : 3, Wa :Da = 1 : 8, C : Dt = 1 : 3 • Thickness of Head
Da : Diameter of agitator
Wa : Width agitator
C : Distance between base and impeller
4
Mixing Molasses Mixing Nutrient
Design Specification Design Specification
Type Cylindrical tank with ellipsoidal Type Cylindrical tank with ellipsoidal
top and bottom top and bottom
Material Carbon Steel A285 Grade A Material Carbon Steel A285 Grade A
Volume 104,99 m3 Volume 8,25 m3
Tank Diameter 4,06 m Tank Diameter 1,74 m
Tank Height 8,12 m Tank Height 4,35 m
Cylinder Height 10,15 m Cylinder Height 3,48 m
Ellipsoidal Height 2,0294 m Ellipsoidal Height 0,869 m
Wall Thickness 4,43 mm Wall Thickness 2,86 mm
Head Thickness 4,43 mm Head Thickness 2,86 mm
Stirrer Design Stirrer Design
Impeller type propeller Impeller type propeller
Impeller diameter 1.35 m Impeller diameter 0,58 m
Impeller to bottom 1.35 m Impeller to bottom 0,58 m
Baffle diameter 0.34 m Baffle diameter 0.14 m
Impeller speed 15 rpm Impeller speed 15 rpm
Utilities Utilities
Power 0,08 kW Power 0,0012 kW
5
3.2.
P&F Filter and
Ion Exchange
Chromatography
6
P&F Filter IEX Chromatography
Equipment Specifications Equipment Specifications
Equipment Name Plate and Frame Filtration Equipment Name Ion Exchange Chromatography
Equipment Code PFF-101 Equipment Code IE-101
Separate bulk impurities from cane
Function Remove metal components from cane
molasses Function
molasses
Number of Unit 1
Type Hydraulic pressure/mechanical pressure Number of Unit 1
Operation Data Type Chromatography
Temperature ≤100oC Operation Data
Pressure 600kPa Temperature ≤100oC
Flow rates 16,742.222 kg/hour Pressure <500 kPa
Construction Data Flow rates < 1 mL/min
Filter Area 400 m2
Construction Data
Length 10,945 mm
Width 1,960 mm Filter Area < 0,8 miuL
Height 2,050 mm Length 500 mm
Total volume of filter cell 6,000 L Width 500 mm
Number of filter plates 103 Height 760 mm
Number of filter cells 104 Eluent Concentration <120 mM
The thickness of filter cake 30
Weight 48 kg
Weight 22,810 kg
Diameter of feed pipe 150 mm
Diameter of feed pipe 150 mm
Diameter of filtrate pipe 90 mm
Diameter of filtrate pipe 90 mm
Motor Power 3 kW Motor Power 150 W
7
3.3.
Heat Sterillizer
8
How to Estimate?
◎ Physical
1. properties needed are pressure, temperature, heat capacity
(Cp), conductivity (k), density (ρ) and viscosity (μ).
2. Assume the value of overall heat transfer coefficient for the first
guess
3. Calculate the Log Mean Temperature Different (LMTD)
Δ�1 = (�2−�1)
Δ�2 = (�1−�2)
10
3.4.
Seed Fermenter
and Fermenter
11
Seed Fermenter
Equipment Specifications
Equipment Name Seed Fermenter
Equipment Code SF-101
Cultivating log phase Design Specification
growth of Aspergillus Material Stainless Steel 316
Function Diameter (m) 1.05
niger to ferment and
Height (m) 5.23
produce Citric Acid Shell Thickness (m) 0.03
Equipment Stirrer Head Thickness (m) 0.00086
Amount 2 Agitator
Operation Data Impeller Type Propeller
Mode of Operation Batch Diameter (m) 0.70
Temperature (°C) 30 Agitator Blade Width (m) 0.08
Pressure (bar) 1.013 Distance from Tank 1.74
Flow Rate (m3/h) 0.03
Bottom
Fermentation Time (h) 72
Agitation Speed (rpm) 15
Max Allowable Working
80
Volume (%)
Min Allowable Working
15
Volume (%)
12
Fermenter
Equipment Specifications
Equipment Name Fermenter Design Specification
Equipment Code F-101 Stainless Steel
Ferment Aspergillus Material
16 Cr, 12 Ni, 2 Mo
Function niger fungus to Diameter (m) 2.65
produce Citric Acid Height (m) 13.24
Equipment Stirrer Shell Thickness (m) 0.15
Amount 10 Head Thickness (m) 0.003
Operation Data Agitator
Mode of Operation Batch Impeller Type Propeller
Temperature (°C) 30 Diameter (m) 0.88
Pressure (bar) 1.013 Agitator Blade
Flow Rate (m3/h) 0.499 0.11
Width (m)
Fermentation Time (h) 120 Distance from Tank
Max Allowable 4.41
80 Bottom
Working Volume (%) Agitation Speed
Min Allowable Working 15
15 (rpm)
Volume (%)
13
3.5.
Rotary Vacuum
Filter
14
Equipment Specifications Operation Data
Equipment Name Rotary Vacuum Filter Mode of
Continuous
Removing biomass from Operation
RVF-201 Working
fermentation broth 0.2
Function RVF-202 Calcium Citrate recovery Pressure (bar)
Removing gypsum formed Percent
RVF-203 100%
from reaction Removed
RVF-201 5 Cake Porosity 0.4 v/v
Filter Cloth Cake Wash
RVF-202 8 Water
Size (Mesh) Stream
RVF-203 20
Filtration Area (m2) 30
Drum Diameter (mm) 2640
Drum Length (mm) 3680
Equipment Specifications
Rotating Speed (r/min) 0.1-1.5
Drive Motor (kW) 4
Total Weight (kg) 8420
Outer Dimension (LxWxH) 4800x4380x2940
15
3.6.
Neutralization
Tank
16
1. Neutralization Tank (Precipitation)
Equipment Specifications
Equipment Name Precipitation Tank Design Specification
Equipment Code N-201 Material Stainless Steel 316
Forming Calcium Diameter (m) 1.26
Function Citrate salt using Height (m) 6.71
Shell Thickness (m) 0.052
Lime
Head Thickness (m) 0.002
Equipment Stirrer
Agitator
Amount 3 Impeller Type Propeller
Operation Data Diameter (m) 0.419
Mode of Operation Batch Agitator Blade
Temperature (°C) 30 0.052
Pressure (bar) 1.013 Width (m)
Flow Rate (m3/h) 1.865 Distance from Tank
2.096
Residence Time (h) 3 Bottom
Max Allowable Agitation Speed
15
Working Volume 80 (rpm)
(%)
Min Allowable
Working Volume 15
(%)
17
2. Neutralization Tank (Gypsum Formation)
Equipment Specifications
Gypsum Formation Design Specification
Equipment Name Stainless Steel
Tank Material
Equipment Code N-202 16 Cr, 12 Ni, 2 Mo
Recovery of Citric Diameter (m) 0.998
Acid from Calcium Height (m) 4.99
Function Shell Thickness
Citrate using Sulfuric 0.036
Acid (m)
Equipment Stirrer Head Thickness
0.0019
Amount 2 (m)
Operation Data Agitator
Mode of Operation Batch Impeller Type Propeller
Temperature (°C) 30 Diameter (m) 0.333
Pressure (bar) 1.013 Agitator Blade
0.041
Flow Rate (m3/h) 0.657 Width (m)
Residence Time (h) 3 Distance from Tank
1.663
Max Allowable Bottom
80
Working Volume (%) Agitation Speed
Min Allowable 15
15 (rpm)
Working Volume (%)
18
3.7.
Crystallizer
19
General information
Equipment Name Crystallizer
Equipment Code CR-201
Quantity 1
Function Crystallizing citric acid
Material Stainless Steel
Mode of Operation Continuous
Type of System Closed system
Operation Data
T 40
P 151,950
Density 1236,24
Mass Flowrate
Mass Flowrate 503,149
503,149
Volumetric Flowrate
Volumetric Flowrate 0,407
0,407
Construction Information
Construction Information
Capacity
Capacity 2,79
2,79
Diameter
Diameter 1,124
1,124
Height 2,810
Height 2,810
3.8.
Rotary Dryer
21
General information
Equipment Name Rotary Drier
Equipment Code DR-101
Quantity 1
Function Drying citric acid crystal
Material Stainless Steel
Mode of Operation Continuous
Type of System Closed system
Operation Data
T 110
P 101,3
Mass Flowrate 332,848
Volumetric Flowrate
Volumetric Flowrate 0,334
0,334
Moisture Content Inlet
Moisture Content Inlet 0
0
Moisture Content Outlet
Moisture Content Outlet %
% 3,513
3,513
Construction Information
Construction Information
Volume
Volume 5,072
5,072
Diameter
Diameter 1,089
1,089
Length
Length 5,445
5,445
Drum Area 18,630
Drum Area 18,630
3.9.
Storage Tanks
23
Molasses Storage Raw Water Storage Biomass Storage
25
How to Estimate?
There are several steps to sizing pump.
• Find out physical properties of the stream which will go into
the pump and other information needed in the calculation
(mass flow, pressure inlet, pressure output, vapor pressure,
temperature, density, static head, pipe length after pump).
• By using these formula below, we get the information of
Power, Head, and NPSHa of each pump:
• Assumptions:
Pump efficiency 75%,
The terms of velocity difference neglected due to its
small number
No fitting
• The pump power requirement can be calculated by
equation below.
Efficiency (%) 75 Efficiency (%) 75
Power (kW) 37 Power (kW) 37
28
Equipment Specifications Equipment Specifications
Equipment Name Cartridge Air Filter
Equipment Name Cartridge Air Filter
Equipment Code FL-101
Filtering the air to Equipment Code FL-102
supply sterile aeration
Function Filtering the air to supply
in the fermentation
Function sterile drying source in the
process
rotary drier
Amount 1
Body Material Stainless steel 316L Amount 1
Body Material Stainless steel 316L
Cartridges Length (m) 0.51
Cartridges Length (m) 1.02
Outlet/inlet type Flange
Outlet/inlet type Flange
Filter medium material Microfiber
Filter medium material Microfiber
Filter Porosity 0.2 μm
Filter Porosity 0.2 μm
Operation Data
Operation Data
Inlet Temperature (ºC) 25
Inlet Temperature (ºC) 25
Outlet Temperature Outlet Temperature (ºC) 40
40
(ºC)
Filtration Area (m2) 0.65 m2 per 10 inch
Filtration Area (m2) 0.65 m2 per 10 inch
Maximum Working
Maximum Working 6
6 Pressure (bar)
Pressure (bar)
Power (kW) 18 Power (kW) 18
29
3.11.
Steam Boiler
30
1. Volume of the furnace
The volume is calculated through the value of qv,
from the equation below.
31
2.
Furnace height (Hfu + Hb) and heat transfer 3.
Furnace length and width (a and b)
area (Fgrate)
32
Unit: B-501
Component Value Unit
Heat Release Rate per Unit Volume
ṁc 2 kg/h
ṁc 0.001 kg/s
LHV (for Natural Gas) 47130 kJ/kg
qv 350.00 kW/m3
V 0.1 m3
Heat Release Rate per Unit Cross Sectional Area
ṁc 2 kg/h
ṁc 0.001 kg/s
qf 2130.0 kW/m3
Fgrate 0.014 m2
Hfu+Hb 6.086 m
Heat Release Rate per Unit Wall Area of Burner
qb 1400 kW/m3
b 0.113 m
Hb 0.045 m
Hfu 6.041 m
a 0.125 m
Type of Burner
Power produced 81400.304 kW
Determination of Furnace Size
α 30.000
β 45.000
γ 50.000
E 0.800 m
d 0.011 m
Furnace Material
Inner case material SS-304
Furnace wall Fire brick
33
3.12.
Water Treatment
34
Specifications
Specifications
Name Bag Filter for Water Treatment
Name Bag Filter for Water Treatment
Vendor JCI Technology Co., Ltd. Specifications
Vendor
Place of Origin JCI Technology Co., Ltd.
Shanghasi, Chinna Name Water Tower Storage Tank
Material Stainless Steel Shenzhen Puxin Technology Co.,
Place of Origin Shanghasi, Chinna Vendor
Size 230*225*900 mm Ltd.
Material
Capacity Stainless Steel
316 L Place of Origin Guangdong, China
Filter Accuracy
Size 0.5 m
230*225*900 mm Material Stainless Steel
Applicable Viscosity 1 - 20000 cp Capacity 200000 L
Capacity 316 L Amount 7
Flow Rate 1 – 1000
Filter Accuracy
Pressure 0.6 - 1 Mpa
Applicable Viscosity 1 - 20000 cp
Flow Rate
Pressure 0.6 - 1 Mpa
35
3.13.
Wastewater
Treatment
36
Static Screen Filter
Specifications
Specifications
Name Static Screen
Name Static Screen
Vendor JCI, Shanghai, China
Vendor
Material JCI, Shanghai, China
Stainless Steel Equalization Tank
Material
Dimension Stainless Steel
230*225*900 mm Specifications
Name Equalization Tank
Flowrate
Dimension 1000
230*225*900 mm Shijiazhuang Zhengzhong Technology
Filter Precision 0.5 m Vendor
Flowrate Co., Ltd
Material Double enamel steel sheet
Filter Precision Ph 1 - 14
Coating
0.25 – 0.4 mm
Thickness
Adhesion 3.45 N/cm
Hardness 6 Mohs
37
Dissolved
Dissolved Air
Air Flotation
Flotation Machine
Machine
Specifications
Specifications
Name Flotation Separator
Name
Vendor Flotation Separator
Hongji
Dimension
Vendor 2200*2900*140 mm
Hongji
Voltage 220 V
Dimension
Power 2200*2900*140 mm
30 kW
Tank Capacity
Voltage 8
220 V
Diameter Impeller 760 mm
Power 30 kW
Production Capability 8 /min
Tank Capacity
Rotate Speed of Impeller 191 r/min
Diameter Impeller 760 mm
Production Capability
Rotate Speed of Impeller 191 r/min
Storage Tank
Specifications
Name Water Storage Tank
Vendor Yangzhou Lianhe Chemical Machinery Co., Ltd.
Volume 5000L
Thickness 3 mm
38
4. Process
Control Strategy
39
4.1.
P&ID
40
41
42
43
44
4.2.
Control
Instrumentation
45
Controlled Manipulated
No. Unit Operation Sensor Controller Actuator Mechanism
Variable Variable
The level transmitter will
Digital level Level send an electric signal to
Maintaining Level
indicator controller the level controller;
contents of
Inlet stream which compares the
mixing
Mixing M-101 flow rate (input Diaphragm measured level with its
1 substrate
Tank M-102 from previous valve setpoint and sends
and nutrients
process) Flow signal to the control
for Flowrate Flowmeter
controller valve on each
fermentation
appropriate stream to
adjust the flow rate.
The pressure transmitter
will send an electric
signal to the pressure
Plate and Maintaining Differential controller; which
Inlet stream Pressure Diaphragm
2 Frame PFF-101 Filter Pressure pressure compares the measured
flow rate controller valve
Filter Pressure indicator pressure with its setpoint
and sends signal to
control valve on stream
to adjust the flow rate.
46
Controlled Manipulated
No. Unit Operation Sensor Controller Actuator Mechanism
Variable Variable
The temperature
transmitter will send an
electric signal to the
temperature controller;
Maintaining
Heat E-101 Temperature Inlet stream Temperature Diaphragm which compares the
3 temperature of Temperature
Sterilizer E-102 indicator from utility controller valve measured temperature
Heat Sterilizer
with its setpoint and
sends signal to control
valve on stream to adjust
the flow rate.
The level transmitter will
send an electric signal to
Maintaining Inlet stream the level controller; which
Seed contents of flow rate compares the measured
SF-101 Digital level Level Diaphragm
4 Fermenter fermenter or Level (input from level with its setpoint and
F-101 indicator controller valve
Fermenter seed previous sends signal to the
fermenter process) control valve on each
appropriate streams to
adjust the flow rate.
47
Controlled Manipulated
No. Unit Operation Sensor Controller Actuator Mechanism
Variable Variable
The pressure transmitter
will send an electric signal
RVF-
to the pressure controller;
201
Maintaining Differential which compares the
Rotary RVF- Inlet stream Pressure Diaphragm
5 RVF Pressure pressure measured pressure with
Vacuum Filter 202 flow rate controller valve
Pressure indicator its setpoint and sends
RVF-
signal the control valve on
203
stream 15 to adjust the
flow rate.
The analyzer transmitter
will send an electric signal
to the analyzer controller;
Input flow
Maintaining which compares the
Neutrallization N-201 rate of Diaphragm
6 concentratio Concentration pH meter pH controller measured concentration
Tank N-202 neutrallizing valve
n with its setpoint and
agent(s)
sends signal to the
control valve to adjust the
flow rate
48
Controlled Manipulated
No. Unit Operation Sensor Controller Actuator Mechanism
Variable Variable
Moisture content of the
outlet will make the
Maintaining analyser transmitter
temperature Tempeature Analyser Diaphragm send electrical signal
7 Crystallizer CR-201 Temperature Temperature
crystallizing Indicator controller valve which compare with its
process setpoint and send
signal to raise
operation temperature.
Moisture content of the
outlet air will make the
Maintaining analyser transmitter
temperature Temperature Analyser send electrical signal
8 Rotary Dryer DR-101 Temperature Temperature Alarm
from drying Indicator controller which compare with its
process setpoint and send
signal warn the
operator.
49
Controlled Manipulated
No. Unit Operation Sensor Controller Actuator Mechanism
Variable Variable
Level of the content
will make the level
transmitter send
Molasses Maintaining Level
Digital level Amount of Level electrical signal
9 Storage TK-101 molasses Level indicator
indicator molasses alarm which compare with
Tank content controller
its setpoint and send
signal warn the
operator.
Level of the content
will make the level
transmitter send
Raw Water Maintaining Level
Digital level Amount of Level electrical signal
10 Storage TK-102 raw water Level indicator
indicator water alarm which compare with
Tank content controller
its setpoint and send
signal warn the
operator.
50
Controlled Manipulated
No. Unit Operation Sensor Controller Actuator Mechanism
Variable Variable
Level of the content
will make the level
Maintaining transmitter send
Biomass Level
biomass Digital level Amount of Level electrical signal
11 Storage TK-201 Level indicator
content from indicator biomass alarm which compare with
Tank controller
overflow its setpoint and send
signal warn the
operator.
Level of the content
will make the level
transmitter send
Lime 33% Level
Maintaining Digital level Amount of Level electrical signal
12 Storage TK-202 Level indicator
lime content indicator lime alarm which compare with
Tank controller
its setpoint and send
signal warn the
operator.
51
Controlled Manipulated
No. Unit Operation Sensor Controller Actuator Mechanism
Variable Variable
The analyser
transmitter will send
an electric signal to
Maintaining the analyser
Lime 33%
lime Concentratio Amount of Analyser controller; which
13 Storage TK-202 pH meter Alarm
concentratio n lime controller compares the
Tank
n measured
concentration with its
setpoint and sends a
warning alarm signal.
Level of the content
will make the level
transmitter send
Sulfuric Acid Maintaining Digital Level
Amount of Level electrical signal
14 Storage TK-203 sulfuric acid Level level indicator
sulfuric acid alarm which compare with
Tank content indicator controller
its setpoint and send
signal warn the
operator.
52
Controlled Manipulated
No. Unit Operation Sensor Controller Actuator Mechanism
Variable Variable
The analyser
transmitter will send
an electric signal to
Sulfuric the analyser
Maintaining
Acid Concentratio Amount of Analyser controller; which
15 TK-203 sulfuric acid pH meter Alarm
Storage n sulfuric acid controller compares the
concentration
Tank measured
concentration with its
setpoint and sends a
warning alarm signal.
Level of the content
will make the level
Maintaining
transmitter send
Citric Acid finished citric Digital Level
Amount of Level electrical signal
16 Storage TK-205 acid content Level level indicator
citric acid alarm which compare with
Tank from indicator controller
its setpoint and send
overflowing
signal warn the
operator.
53
Controlled Manipulated
No. Unit Operation Sensor Controller Actuator Mechanism
Variable Variable
The flow transmitter
will send an electric
signal to the flow
Controlling
controller; which
the flow of
Flow Stream inlet Flow Diaphrag compares the
the stream to Flow rate
meter flow rate controller m valve measured flow rate
prevent feed
with its setpoint and
loss in boiler
sends signal the to
the control to adjust
the flow rate.
The temperature
17 Boiler B-501
transmitter will send
Controlling
an electric signal to
the
the temperature
temperature
controller; which
of stream Natural gas Tempreatu
Thermoc Diaphrag compares the
output boiler Temperature stream re
ouple m valve measured
to ensure the temperature controller
temperature with its
boiler output
setpoint and sends
has become
signal the control
steam
valve to adjust the
flow rate
54
Controlled Manipulated
No. Unit Operation Sensor Controller Actuator Mechanism
Variable Variable
Level of the content will make
the level transmitter send
Maintaining Level
Raw Water Digital level Amount of electrical signal which
18 TK-301 raw water Level indicator Level alarm
Storage indicator water compare with its setpoint and
content controller
send signal warn the
operator.
Controlling Analyzer
Amount of The transmitter will send an
outlet flow Flow rate Flow meter indicator
oxygen electric signal to the
rate controller
controller; which compares
C-101 Diaphragm the measured concentration
19 Compressor
C-102 valve with its setpoint and sends
signal the control valve on the
Controlling stream to adjust the air flow
Air Temperature rate.
outlet Temperature Thermocouple
Temperature controller
temperature
55
Controlled Manipulated
No. Unit Operation Sensor Controller Actuator Mechanism
Variable Variable
The level transmitter will
send an electric signal to
Treated Maintaining the level controller; which
Digital Amount of Level
Water storage Diaphragm compares the measured
20 ST-101 Level Level reboiler indicator
Storage tank’s valve level with its setpoint and
Indicator water controller
Tank content sends electric signal to the
controller to open the
valve.
56