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  • Gas Chromatography: Perichrom: 1 Alpha M.O.S. - Smell and Taste Analyzing Solutions

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    Manuja Damith
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    This document discusses three types of backflush techniques in gas chromatography: 1) Simple backflush where elution and backflush occur simultaneously with different carrier gas pressures, 2) Backflush directly in the thermal conductivity detector where the sample loop is flushed into the detector, and 3) Backflush directly to the vent where the sample loop is flushed out of the system vent. Diagrams and examples are provided to illustrate how each technique works to remove contaminants from the column.

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    ALPHAMOS GC Backflush

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    This document discusses three types of backflush techniques in gas chromatography: 1) Simple backflush where elution and backflush occur simultaneously with different carrier gas pressures, 2) Backflush directly in the thermal conductivity detector where the sample loop is flushed into the detector, and 3) Backflush directly to the vent where the sample loop is flushed out of the system vent. Diagrams and examples are provided to illustrate how each technique works to remove contaminants from the column.

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    © All Rights Reserved
    Download as PPT, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    27 views12 pages

    Gas Chromatography: Perichrom: 1 Alpha M.O.S. - Smell and Taste Analyzing Solutions

    Uploaded by

    Manuja Damith
    This document discusses three types of backflush techniques in gas chromatography: 1) Simple backflush where elution and backflush occur simultaneously with different carrier gas pressures, 2) Backflush directly in the thermal conductivity detector where the sample loop is flushed into the detector, and 3) Backflush directly to the vent where the sample loop is flushed out of the system vent. Diagrams and examples are provided to illustrate how each technique works to remove contaminants from the column.

    Copyright:

    © All Rights Reserved
    Download as PPT, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    of 12

    Gas chromatography:

    Perichrom

    Julien DELBARY (delbary@alpha-mos.com)

    Alpha M.O.S. - Smell and Taste Analyzing Solutions 1


    Agenda

    3 TYPE OF BACKFLUSH

    I/ Simple “backflush”

    II/ Backflush directly in TCD

    III / Backflush at the vent

    Alpha M.O.S. - Smell and Taste Analyzing Solutions 2


    Simple backflush
    How it works ?

     Basic working  Elution & backflush at the same time


     P carrier 1 > P carrier 2  P carrier 2 > P carrier 1

    Alpha M.O.S. - Smell and Taste Analyzing Solutions 3


    Simple backflush
    Application exemple

    Without backflush

    With backflush

    Alpha M.O.S. - Smell and Taste Analyzing Solutions 4


    Backflush directly in the TCD
    How it works ?

     Step 1 : On line filling of the sample loop

    Alpha M.O.S. - Smell and Taste Analyzing Solutions 5


    Backflush directly in the TCD
    How it works ?

     Step 2 : Injection in the chromatographic system (LOAD to INJECT)

    Alpha M.O.S. - Smell and Taste Analyzing Solutions 6


    Backflush directly in the TCD
    How it works ?

     Step 3 : Backflush position (INJECT to LOAD) All the compounds in the


    backflush are evacuated directly to the TCD

    Alpha M.O.S. - Smell and Taste Analyzing Solutions 7


    Le backflush au TCD
    Application exemple

    Alpha M.O.S. - Smell and Taste Analyzing Solutions 8


    Backflush directly to the vent
    How it works ?

     Step 1 : On line filling of the sample loop

    Alpha M.O.S. - Smell and Taste Analyzing Solutions 9


    Backflush directly to the vent
    How it works ?

     Step 2 : Injection in the chromatographic system (LOAD to INJECT)

    Alpha M.O.S. - Smell and Taste Analyzing Solutions 10


    Backflush directly to the vent
    How it works ?

     Step 3 : Backflush position (INJECT to LOAD) All the compounds in the


    backflush are evacuated directly to the vent

    Alpha M.O.S. - Smell and Taste Analyzing Solutions 11


    Backflush directly to the vent
    Application exemple

    Alpha M.O.S. - Smell and Taste Analyzing Solutions 12

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