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The Distillation
Initially an oily water / limonene mixture can be seen condensing on the glassware at a distillation temperature of 98 C. The temperature will rise to 100oC as the distillate composition approaches pure water.
Limonene, an alkene, is extracted into a low density water immiscible solvent (ether). The lower layer is the remaining aqueous distillate
Limonenes structure
Pith Skin
Orange peel cut into small pieces, placed into 100 mL of water
The yield of limonene is about 1% using this outer skin. This is a large yield compared to other essential oil extractions, where yields can range from 1-0.01 % by mass.
Heat
Limonene can be observed as an oily suspension in the final distillate (80 mL).
Essential oils can be steam distilled from flowers, leaves, fruits, barks and woods
Essential oils are found in many household products, ranging from high end cosmetics to basic cleaning materials.
Lavender
Patchouli
Bergamot
Cinnamon